A germane kettle residue separation device and separation method

By combining the lifting and beating components of the germane residue separation device, the problem of poor grading effect caused by filter clogging was solved, and the residue was thoroughly graded, separated and efficiently collected.

CN120983968BActive Publication Date: 2026-02-10SPECTRUM MATERIALS (FUJIAN) CO LTD +1
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Patent Information

Application Number
CN202511524787.6
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2025-10-24
Publication Date
2026-02-10
Estimated Expiration
2045-10-24

AI Technical Summary

Technical Problem

Existing germane residue separation devices are prone to filter clogging during the separation process, which slows down the speed at which the liquid passes through the filter. When the liquid falls, some residue adheres to the cylinder wall, affecting the classification effect.

Method used

A germane reactor residue separation device is adopted, including connecting pipes, cylinder, filter assembly, lifting assembly, beating assembly and sealing assembly. The lifting assembly drives the cylinder to rise and works in conjunction with the beating assembly to vibrate the inner wall of the cylinder, shaking off the attached residue onto the filter assembly. The vibration of the filter assembly is used to achieve thorough classification and separation of the residue.

Benefits of technology

It effectively solves the problem of filter clogging, improves separation efficiency, ensures thorough classification and collection of residue, and facilitates subsequent processing.

✦ Generated by Eureka AI based on patent content.

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Abstract

The present application relates to germane kettle residue separation technical field, and disclose a kind of germane kettle residue separation device and separation method, the device includes connecting pipe, the outside of the connecting pipe is equipped with cylinder, the inside of the cylinder is equipped with filter assembly, the bottom of the cylinder is threadedly connected with bottom cover, the bottom of the bottom cover is equipped with drain pipe, the bottom cover is connected with the filter assembly by connecting piece, the connecting pipe is equipped with sealing assembly between cylinder. The present application is continuously beaten by beating bar, so that the residue attached to the inner wall of the cylinder is beaten to the filter screen, then cooperate with the vibration of filter screen, so that the residue on the filter screen can pass through the filter screen to be classified and filtered, finally complete the complete classification and separation of residue, facilitate subsequent classification and collection of different size residue, by separating the beating bar from the cylinder, so that the descent of the cylinder is not hindered by the beating bar, speed up the descent speed of the cylinder, to improve the vibration effect of filter screen, and then improve the separation effect.
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Description

Technical Field

[0001] This invention belongs to the field of germane reactor residue separation technology, and specifically relates to a germane reactor residue separation device and separation method. Background Technology

[0002] Germanane reactor residue typically contains a certain amount of germanium, which can be processed for reuse in high-end manufacturing fields such as semiconductor chips and infrared lenses. The germanium-containing raw materials that are not converted into products form granular solids that float in the solution. The first step in achieving recycling is to efficiently separate and recover these reactor residues.

[0003] When collecting germanane reactor residue, it is graded and separated according to particle size for easier subsequent processing. Existing separation devices use multiple layers of filters with different pore sizes inside the cylinder, which is connected to the discharge pipe of the germanane reactor. The liquid is discharged from the germanane reactor and separated by passing through the filters of different pore sizes. However, as separation proceeds, the filters gradually become clogged, causing the liquid to pass through the filters at a slower speed, eventually forming stagnant liquid. After all the liquid in the reactor is discharged, the stagnant liquid drops and is eventually discharged. During this process, some residue adheres to the cylinder wall, preventing it from passing through the filters below for grading, thus affecting the grading effect.

[0004] Therefore, it is necessary to invent a germane residue separation device and separation method to solve the above problems. Summary of the Invention

[0005] To address the aforementioned problems, this invention provides a germanane reactor residue separation device and method to solve the issues raised in the background section.

[0006] To achieve the above objectives, the present invention provides the following technical solution: a germane reactor residue separation device, comprising: a connecting pipe, a cylindrical body sleeved on the outside of the connecting pipe, a filter assembly disposed inside the cylindrical body, a bottom cover threadedly connected to the bottom of the cylindrical body, a drain pipe disposed at the bottom of the bottom cover, the bottom cover and the filter assembly being connected by a connector, a sealing assembly disposed between the connecting pipe and the cylindrical body, and a separation assembly disposed on the outside of the cylindrical body to enable the germane reactor residue inside to be fully classified and collected;

[0007] The separation assembly includes: a sleeve plate, a slide rod, a top plate, a first spring, a lifting assembly for driving the cylinder to rise, and a striking assembly for striking the cylinder;

[0008] The sleeve plate is fixedly sleeved on the outside of the connecting pipe. Multiple sliding rods are provided and slidably installed on the sleeve plate. The top plate is fixedly installed on the top of the sliding rod. The bottom of the sliding rod is fixedly connected to the cylinder. The first spring is sleeved on the outside of the connecting pipe.

[0009] Furthermore, the striking assembly includes: a crossbeam, a striking arm, a second spring, and a pushing assembly for driving the striking arm to move away from the cylinder;

[0010] The crossbeam is fixedly installed around the outside of the connecting pipe at equal intervals, the beater is slidably installed inside the crossbeam, the second spring compresses the beater to fix it to the inner wall of the crossbeam, and the beater abuts against the outer side of the cylinder.

[0011] Furthermore, the pushing component includes: a wedge block, a fixing frame, a base, a vertical plate, a bracket, a rotating shaft, a stop block, and an inclined stop block;

[0012] The wedge-shaped blocks are fixedly connected to the outside of the racket shaft by a fixing bracket. The base is fixedly connected to the bottom of the cylinder. The number of vertical plates corresponds to the number of wedge-shaped blocks. The vertical plates are fixedly installed on the top of the base. The brackets are fixedly installed on the vertical plates at equal intervals from top to bottom. The abutment blocks are rotatably installed inside the brackets via the rotating shaft. The inclined blocks are fixedly installed on the vertical plates at equal intervals. The inclined blocks are located below the abutment blocks and abut against the bottom of the abutment blocks.

[0013] Furthermore, the lifting assembly includes: a first electromagnet and an iron ring;

[0014] The first electromagnet is fixedly installed at the bottom of the sleeve plate, and the iron ring is fixedly installed at the top of the cylinder. When the first electromagnet is energized, the magnetic force generated can attract the iron ring, causing it to lift the cylinder.

[0015] Furthermore, an iron rod is fixedly installed on the side of the racket arm away from the connecting tube, and the end of the iron rod away from the connecting tube extends through the second spring to the outside of the cross frame. The end of the cross frame away from the connecting tube is fixedly installed with a second electromagnet by a positioning bracket.

[0016] Furthermore, the filter assembly includes: a filter frame, a filter screen, a sealing ring, and a connecting rod;

[0017] The filter frames are evenly spaced from top to bottom inside the cylinder. Adjacent filter frames are fixedly connected by connecting rods. The filter screens are located inside the filter frames, and the aperture of the filter screens decreases from top to bottom. The connecting member is a ring magnet, which is fixedly installed on the top of the bottom cover. The filter frames are made of iron and are nickel-plated. The bottommost filter frame is attracted and fixed to the connecting member. The sealing ring is sleeved on the outside of the filter frame and abuts against the inner wall of the cylinder.

[0018] Furthermore, the sealing assembly includes: an annular airbag and a conduit;

[0019] The outer side of the connecting pipe is provided with an annular groove, and the annular airbag is fixedly sleeved in the annular groove. One end of the conduit is connected to the annular airbag, and the other end extends through the inner wall of the connecting pipe to the outside of the connecting pipe. The end of the conduit extending outside the connecting pipe is connected to an air injection device. The inner wall of the junction between the cylinder and the connecting pipe is provided with an annular embedding groove that cooperates with the annular airbag.

[0020] Furthermore, the outer side of the connecting pipe is equidistantly threaded with screws, and the inner wall of the connecting pipe is provided with rubber rings.

[0021] Furthermore, the connecting pipe is symmetrically provided with slots on the outside, and a card plate is provided in the slot. A cover is fixedly installed on the outside of the card plate. A magnetic block is provided on the opposite side of the two covers. The magnetic poles of the opposite magnetic blocks are opposite. The two covers are fixed together by magnetic attraction.

[0022] The method for separating germane residue using the germane residue separation device described above includes the following steps:

[0023] S1. When in use, connect the connecting pipe to the discharge pipe of the germane reactor to perform the liquid discharge operation. After the liquid enters the connecting pipe and the cylinder, it is filtered in stages by the filter assembly to achieve the graded collection of germane reactor residue in the liquid. Finally, the filtered liquid is discharged through the discharge pipe.

[0024] S2. After the liquid has flowed out, the sealing component is removed. The cylinder is driven to rise by the lifting component. During the rise of the cylinder, the outer side of the cylinder is patted by the tapping component. The resulting vibration shakes the slag attached to the inner wall of the cylinder onto the filter component. As the cylinder rises, the sliding rod and top plate move accordingly. At the same time, the cylinder and the sleeve plate compress the first spring.

[0025] S3. When the cylinder rises to the highest position, the lifting component cancels the drive of the cylinder, the first spring quickly resets and carries the cylinder, slide rod and top plate down quickly. The top plate collides with the sleeve plate to generate vibration, which is transmitted to the cylinder, causing the cylinder and the filter components inside to vibrate, and the slag on the filter components to vibrate.

[0026] S4. Repeat the above operation to shake the slag attached to the inner wall of the cylinder onto the filter assembly. Then, rely on the vibration of the filter assembly itself to shake the slag, so that the slag on the filter assembly can pass through the filter assembly and be filtered in stages. Finally, the slag is completely separated and graded, which is convenient for subsequent collection of slag of different sizes.

[0027] The technical effects and advantages of this invention are as follows:

[0028] 1. This invention uses a beater to continuously beat the slag attached to the inner wall of the cylinder onto the filter screen. Combined with the vibration of the filter screen, the slag on the filter screen can pass through the filter screen and be filtered in stages, thus completing the thorough separation of the slag and facilitating the subsequent collection of slag of different sizes.

[0029] 2. By separating the beater from the cylinder, the descent of the cylinder is not hindered by the beater, thus accelerating the descent speed of the cylinder, thereby improving the vibration effect of the filter screen and improving the separation effect. Attached Figure Description

[0030] Figure 1 A schematic diagram of the germanane reactor residue separation device according to an embodiment of the present invention is shown. Figure 1 ;

[0031] Figure 2 A schematic diagram of the internal structure of the germane residue separation device according to an embodiment of the present invention is shown;

[0032] Figure 3 A cross-sectional structural schematic diagram of the germanane reactor residue separation device according to an embodiment of the present invention is shown;

[0033] Figure 4 An embodiment of the present invention is shown. Figure 3 Enlarged structural diagram at point A in the middle;

[0034] Figure 5 An embodiment of the present invention is shown. Figure 3 Enlarged structural diagram at point B;

[0035] Figure 6 A schematic diagram of the structure of the filtering component according to an embodiment of the present invention is shown;

[0036] Figure 7 A schematic diagram of the germanane reactor residue separation device according to an embodiment of the present invention is shown. Figure 2 ;

[0037] Figure 8 A schematic diagram of a portion of the structure of an embodiment of the present invention is shown;

[0038] Figure 9 A physical diagram of the present invention is shown;

[0039] In the diagram: 1. Connecting pipe; 2. Cylinder; 3. Filter frame; 4. Filter screen; 5. Bottom cover; 6. Pipeline; 7. Sleeve plate; 8. Sliding rod; 9. Top plate; 10. First spring; 11. First electromagnet; 12. Iron ring; 13. Horizontal frame; 14. Paddle rod; 15. Second spring; 16. Wedge block; 17. Base; 18. Vertical plate; 19. Abutment block; 20. Slanted stop block; 21. Iron rod; 22. Positioning frame; 23. Second electromagnet; 24. Connecting rod; 25. Connector; 26. Annular airbag; 27. Guide tube; 28. Cover; 29. ​​Rubber ring. Detailed Implementation

[0040] To make the objectives, technical solutions, and advantages of the embodiments of the present invention clearer, the technical solutions of the present invention will be clearly and completely described below in conjunction with the embodiments.

[0041] This invention provides a germanane reactor residue separation device, such as... Figures 1 to 8 As shown, it includes: a connecting pipe 1, a cylindrical body 2 sleeved on the outside of the connecting pipe 1, the cylindrical body 2 being a transparent cylindrical component made of PP material, a filter assembly inside the cylindrical body 2, a bottom cover 5 threaded to the bottom of the cylindrical body 2, a drain pipe 6 at the bottom of the bottom cover 5, the bottom cover 5 being connected to the filter assembly via a connector 25, a sealing assembly between the connecting pipe 1 and the cylindrical body 2, and a separation assembly on the outside of the cylindrical body 2 that enables the germane residue inside to be fully classified and collected.

[0042] The separation assembly includes: a sleeve plate 7, a slide bar 8, a top plate 9, a first spring 10, a lifting assembly for driving the cylinder 2 to rise, and a striking assembly for striking the cylinder 2;

[0043] The sleeve 7 is fixedly sleeved on the outside of the connecting pipe 1. Multiple sliding rods 8 are provided and slidably installed on the sleeve 7. The top plate 9 is fixedly installed on the top of the sliding rod 8. The bottom of the sliding rod 8 is fixedly connected to the cylinder 2. The first spring 10 is sleeved on the outside of the connecting pipe 1.

[0044] In use, the connecting pipe 1 is connected to the discharge pipe of the germane reactor to perform the liquid discharge operation. After the liquid enters the connecting pipe 1 and the cylinder 2, it is filtered through the filter assembly to achieve graded filtration, thereby achieving graded collection of germane reactor residue in the liquid. Finally, the filtered liquid is discharged through the discharge pipe 6. As filtration proceeds, more and more material accumulates on the filter assembly, causing the liquid to be unable to flow out quickly through the filter assembly, resulting in liquid accumulation. The accumulated liquid fills the interior of the cylinder 2. The presence of the sealing assembly prevents the liquid from flowing out through the gap between the connecting pipe 1 and the cylinder 2. Finally, when all the liquid in the germane reactor is discharged, as the accumulated liquid slowly descends, it is eventually discharged through the filter assembly and the discharge pipe 6. However, as the accumulated liquid slowly descends, some residue will remain on the inner wall of the cylinder 2, resulting in stagnation. This stagnant residue cannot pass through the filter assembly below for graded filtration, affecting subsequent collection.

[0045] Therefore, after the liquid has flowed out, the sealing component is removed, and the cylinder 2 is driven to rise by the lifting component. During the rise of the cylinder 2, the outer side of the cylinder 2 is patted by the tapping component. The resulting vibration shakes the slag attached to the inner wall of the cylinder 2 onto the filter component. As the cylinder 2 rises, the sliding rod 8 and the top plate 9 move accordingly. At the same time, the cylinder 2 compresses the first spring 10 with the sleeve plate 7. When the cylinder 2 rises to the highest position, the lifting component cancels the drive of the cylinder 2, and the first spring 10 quickly returns to its original position, causing the cylinder 2, sliding rod 8, and top plate 9 to descend rapidly. The top plate 9 collides with the sleeve plate 7 to generate vibration, which is transmitted to the cylinder 2, causing the cylinder 2 and the filter component inside to vibrate. This vibrates the slag on the filter component. The above operation is repeated to shake the slag attached to the inner wall of the cylinder 2 onto the filter component first. Then, relying on the vibration of the filter component itself, the slag is shaken, allowing the slag on the filter component to pass through the filter component for graded filtration. Finally, the slag is completely graded and separated, which facilitates the subsequent graded collection of slag of different sizes.

[0046] After collection is complete, the forward rotation of the drain pipe 6 causes the bottom cover 5 to rotate and leave the cylinder 2. At this time, the filter assembly also leaves, and the slag collected in the filter assembly can be taken out and collected later.

[0047] like Figures 2 to 8 As shown, the striking assembly includes: a crossbar 13, a striking bar 14, a second spring 15, and a pushing assembly for driving the striking bar 14 to move away from the cylinder 2;

[0048] The crossbeam 13 is fixedly installed around the outside of the connecting tube 1 at equal intervals, and the paddle 14 is slidably installed inside the crossbeam 13. The second spring 15 presses the paddle 14 to fix it to the inner wall of the crossbeam 13, and the paddle 14 abuts against the outer side of the cylinder 2.

[0049] As the cylinder 2 rises, the push assembly moves the flapper 14 away from the cylinder 2, compressing the second spring 15 and causing it to deform and generate force. Then, the push assembly releases the push on the flapper 14, and the second spring 15 quickly returns the flapper 14 to its original position, causing the flapper 14 to strike the outside of the cylinder 2. Subsequently, the push assembly intermittently pushes the flapper 14, which, together with the second spring 15, enables the flapper 14 to continuously strike the cylinder 2, shaking the slag attached to the inner wall of the cylinder 2 onto the filter assembly.

[0050] like Figure 3 and Figure 5 As shown, the pushing assembly includes: wedge block 16, fixed frame, base 17, vertical plate 18, bracket, rotating shaft, stop block 19, and inclined stop block 20;

[0051] The wedge block 16 is fixedly connected to the outside of the racket shaft 14 by a fixing bracket. The base 17 is fixedly connected to the bottom of the cylinder 2. The vertical plate 18 corresponds to the number of wedge blocks 16. The vertical plate 18 is fixedly installed on the top of the base 17. The bracket is fixedly installed on the vertical plate 18 at equal intervals from top to bottom. The abutment block 19 is rotatably installed inside the bracket through a rotating shaft. The inclined block 20 is fixedly installed on the vertical plate 18 at equal intervals. The inclined block 20 is located below the abutment block 19 and abuts against the bottom of the abutment block 19.

[0052] The inclined stop 20 prevents the stop block 19 from rotating downwards, but allows the stop block 19 to rotate upwards by 60 degrees.

[0053] The cylinder 2, along with the base 17, vertical plate 18, bracket, rotating shaft, and abutment 19, rises. After the abutment 19 contacts the inclined surface of the wedge block 16, the abutment 19 pushes the wedge block 16, causing it to move away from the cylinder 2 along with the fixing frame and the beater 14. When the abutment 19 leaves the wedge block 16, the wedge block 16 is located in the gap between adjacent abutments 19. At this time, the second spring 15 quickly resets the beater 14, causing the beater 14 to strike the cylinder 2. When the cylinder 2 descends, the abutment 19 contacts the wedge block 16. At this time, the abutment 19 rotates upward to avoid the wedge block 16, allowing the abutment 19 to descend smoothly. When the abutment 19 leaves the wedge block 16, under the action of gravity, the abutment 19 rotates and resets to contact the inclined stop 20, allowing the cylinder 2 to return to its original position smoothly.

[0054] When the cylinder 2 descends, the lever 14 contacts the outside of the cylinder 2, and the elastic force of the first spring 10 is sufficient to push the cylinder 2 to descend rapidly.

[0055] like Figure 4 As shown, the lifting assembly includes: a first electromagnet 11 and an iron ring 12;

[0056] The first electromagnet 11 is fixedly installed at the bottom of the sleeve plate 7, and the iron ring 12 is fixedly installed at the top of the cylinder 2. When the first electromagnet 11 is energized, the magnetic force generated can attract the iron ring 12, causing it to lift the cylinder 2.

[0057] When the first electromagnet 11 is energized, it becomes magnetic, causing the iron ring 12 to rise with the cylinder 2. When the first electromagnet 11 is de-energized, the drive on the iron ring 12 and the cylinder 2 is canceled.

[0058] like Figure 4 As shown, an iron rod 21 is fixedly installed on the side of the racket 14 away from the connecting tube 1. The end of the iron rod 21 away from the connecting tube 1 extends through the second spring 15 to the outside of the cross frame 13. The end of the cross frame 13 away from the connecting tube 1 is fixedly installed with a second electromagnet 23 through a positioning bracket 22.

[0059] The sleeve 7 is equipped with a controller (not shown in the figure), which is used to control the energization and de-energization of the first electromagnet 11 and the second electromagnet 23.

[0060] During the descent of the cylinder 2, the beater 14 is in contact with the cylinder 2 throughout the entire process, which causes friction between the beater 14 and the cylinder 2, hindering the rapid descent of the cylinder 2 and affecting the vibration effect.

[0061] Therefore, after the first electromagnet 11 is energized for a period of time, the cylinder 2 rises to its highest position. At this time, the second electromagnet 23 is energized and becomes magnetic, thereby attracting the iron rod 21 and the flapping rod 14 to move away from the cylinder 2, causing the flapping rod 14 to leave the cylinder 2. Then the first electromagnet 11 is de-energized, and the cylinder 2 descends. During the descent of the cylinder 2, it does not come into contact with the flapping rod 14. Therefore, the cylinder 2 will not be subjected to friction from the flapping rod 14 when it descends, making the cylinder 2 fall faster and the vibration effect better. After the second electromagnet 23 is energized for a period of time, the cylinder 2 descends to its reset position, and the second electromagnet 23 is de-energized.

[0062] When the second electromagnet 23 is energized, the batter 14 moves with the iron rod 21 until it stops, at which point the batter 14 does not contact the vertical plate 18.

[0063] like Figure 3 and Figure 6 As shown, the filter assembly includes: filter frame 3, filter screen 4, sealing ring, and connecting rod 24;

[0064] The filter screen frames 3 are evenly spaced from top to bottom inside the cylinder 2. Adjacent filter screen frames 3 are fixedly connected by connecting rods 24. The filter screen 4 is placed inside the filter screen frame 3. The aperture of the filter screen 4 decreases from top to bottom. The connecting piece 25 is a ring magnet. The connecting piece 25 is fixedly installed on the top of the bottom cover 5. The filter screen frame 3 is made of iron and is nickel-plated. The bottom filter screen frame 3 is attracted and fixed to the connecting piece 25. The sealing ring is sleeved on the outside of the filter screen frame 3 and abuts against the inner wall of the cylinder 2.

[0065] The slag passes through multiple filters 4 in sequence and is graded. Different sizes of slag remain on different filters 4. After the bottom cover 5 is removed, the connector 25 takes the filter frame 3 out with it. The filter frame 3 can be separated from the connector 25 later to collect the slag on the filter frame 3 and clean the bottom cover 5.

[0066] like Figure 3 and Figure 4 As shown, the sealing assembly includes: an annular airbag 26 and a conduit 27;

[0067] The outer side of the connecting pipe 1 is provided with an annular groove, and the annular airbag 26 is fixedly sleeved in the annular groove. One end of the conduit 27 is connected to the annular airbag 26, and the other end extends through the inner wall of the connecting pipe 1 to the outside of the connecting pipe 1. The end of the conduit 27 extending outside the connecting pipe 1 is connected to an air injection device (not shown in the figure). The inner wall of the junction between the cylinder 2 and the connecting pipe 1 is provided with an annular embedding groove that cooperates with the annular airbag 26.

[0068] Air is injected into the conduit 27 through the air injection component. After the air enters the annular airbag 26, the annular airbag 26 expands and embeds itself into the annular embedding groove, thereby sealing the gap between the connecting pipe 1 and the cylinder 2. The air injection component works in the opposite direction, which can draw out the air in the annular airbag 26 and make it deflate, so that the annular airbag 26 does not contact the cylinder 2, canceling the seal, so that the cylinder 2 will not be obstructed by the annular airbag 26 when it moves vertically.

[0069] like Figure 3 As shown, the outer side of the connecting pipe 1 is equidistantly threaded with screws, and the inner wall of the connecting pipe 1 is provided with rubber rings 29.

[0070] The connecting pipe 1 is placed outside the discharge pipe of the germane reactor, and the outer side of the discharge pipe of the germane reactor abuts against the rubber ring 29, which improves the airtightness of the connection between the connecting pipe 1 and the discharge pipe of the germane reactor. The screw is rotated so that the screw abuts against the discharge pipe of the germane reactor, thus connecting the connecting pipe 1 and the discharge pipe of the germane reactor.

[0071] like Figure 1 As shown, the outer side of the connecting pipe 1 is symmetrically provided with slots, and a card plate is provided in the slot. A cover 28 is fixedly installed on the outside of the card plate. A magnetic block is provided on the opposite side of the two covers 28. The magnetic poles of the opposite magnetic blocks are opposite. The two covers 28 are fixed together by magnetic attraction.

[0072] The cover 28 can shield the structure below the connecting pipe 1, preventing the user from accidentally hitting the structure below the connecting pipe 1 and thus protecting the structure below the connecting pipe 1. Pulling a pair of covers 28 to separate them makes it easier to observe the situation inside the cylinder 2.

[0073] Working principle: During use, the connecting pipe 1 is connected to the discharge pipe of the germane reactor to perform the liquid discharge operation. After the liquid enters the connecting pipe 1 and the cylinder 2, it is filtered through the various filter screens 4 on the filter assembly to achieve graded collection of germane reactor residue in the liquid. Finally, the filtered liquid is discharged through the discharge pipe 6. As filtration proceeds, more and more material accumulates on the filter screens 4 inside the filter assembly, which prevents the liquid from flowing out quickly through the filter screens 4, resulting in liquid accumulation. The accumulated liquid fills the inside of the cylinder 2. The presence of the sealing component prevents the liquid from flowing out through the gap between the connecting pipe 1 and the cylinder 2. Finally, when all the liquid in the germane reactor is discharged, as the accumulated liquid slowly descends, it is eventually discharged through multiple filter screens 4 and the discharge pipe 6. However, as the accumulated liquid slowly descends, some residue will remain on the inner wall of the cylinder 2, resulting in stagnation. This stagnant residue cannot pass through the filter screens 4 below it for graded filtration, affecting subsequent collection.

[0074] Therefore, after the liquid has flowed out, the sealing assembly is removed, and the first electromagnet 11 is energized to make it magnetic. This causes the attracting iron ring 12 to lift the cylinder 2, which in turn lifts the base 17, vertical plate 18, bracket, rotating shaft, and abutment 19. After the abutment 19 contacts the inclined surface of the wedge block 16, it pushes the wedge block 16, causing it to move away from the cylinder 2 along with the fixing frame and the lever 14. This compresses the second spring 15. When the abutment 19 leaves the wedge block 16, the wedge... The wedge 16 is located in the gap between adjacent abutment blocks 19. At this time, the second spring 15 quickly resets the flapping rod 14, causing the flapping rod 14 to strike the cylinder 2. Subsequently, as multiple abutment blocks 19 continuously contact and separate from the wedge 16, the cylinder 2 is continuously struck. The resulting vibration shakes the slag attached to the inner wall of the cylinder 2 onto the filter screen 4. As the cylinder 2 rises, it causes the sliding rod 8 and the top plate 9 to move accordingly. At the same time, the cylinder 2, in conjunction with the sleeve plate 7, compresses the first spring 10. When the cylinder... After body 2 rises to its highest position, the first electromagnet 11 is de-energized, which in turn cancels the drive to the iron ring 12 and cylinder 2. The first spring 10 quickly resets, causing cylinder 2, slide rod 8, and top plate 9 to descend rapidly. When cylinder 2 descends, the stop block 19 contacts the wedge block 16. At this time, the stop block 19 rotates upward to avoid the wedge block 16, allowing the stop block 19 to descend smoothly. After the stop block 19 leaves the wedge block 16, under the action of gravity, the stop block 19 rotates back to its original position and contacts the inclined stop block 20, causing... Once the cylinder 2 can be successfully reset, the top plate 9 and the sleeve plate 7 collide and generate vibration. The vibration is transmitted to the cylinder 2, causing the cylinder 2 and the filter screen 4 inside to vibrate. This vibrates the slag on the filter screen 4. The above operation is repeated so that the slag attached to the inner wall of the cylinder 2 can be shaken off onto the filter screen 4. Then, relying on the vibration of the filter screen 4 itself, the slag can be shaken off, allowing the slag on the filter screen 4 to pass through the filter screen 4 for graded filtration. Finally, the slag is completely graded and separated, which facilitates the subsequent graded collection of slag of different sizes.

[0075] During the descent of the cylinder 2, the beater 14 is in contact with the cylinder 2 throughout the entire process, which causes friction between the beater 14 and the cylinder 2, hindering the rapid descent of the cylinder 2 and affecting the vibration effect.

[0076] Therefore, after the first electromagnet 11 is energized for a period of time, the cylinder 2 rises to its highest position. At this time, the second electromagnet 23 is energized and becomes magnetic, thereby attracting the iron rod 21 and the flapping rod 14 to move away from the cylinder 2, causing the flapping rod 14 to leave the cylinder 2. Then the first electromagnet 11 is de-energized, and the cylinder 2 descends. During the descent of the cylinder 2, it does not come into contact with the flapping rod 14. Therefore, the cylinder 2 will not be subjected to friction from the flapping rod 14 when it descends, making the cylinder 2 fall faster and the vibration effect better. After the second electromagnet 23 is energized for a period of time, the cylinder 2 descends to its reset position. The second electromagnet 23 is de-energized, and the flapping rod 14 returns to its reset position under the push of the second spring 15 and comes into contact with the cylinder 2.

[0077] The above embodiments are only used to illustrate the technical solutions of the present invention, and are not intended to limit it.

Claims

1. A germanane reactor residue separation device, characterized in that, include: Connecting pipe (1), the outside of the connecting pipe (1) is fitted with a cylinder (2), the inside of the cylinder (2) is fitted with a filter assembly, the bottom of the cylinder (2) is threaded with a bottom cover (5), the bottom of the bottom cover (5) is fitted with a drain pipe (6), the bottom cover (5) and the filter assembly are connected by a connector (25), a sealing assembly is provided between the connecting pipe (1) and the cylinder (2), and the outside of the cylinder (2) is fitted with a separation assembly that can fully classify and collect the germane residue inside; The separation assembly includes: a sleeve plate (7), a slide bar (8), a top plate (9), a first spring (10), a lifting assembly for driving the cylinder (2) to rise, and a striking assembly for striking the cylinder (2); The sleeve (7) is fixedly sleeved on the outside of the connecting pipe (1), the slide rod (8) is configured as multiple and slidably installed on the sleeve (7), the top plate (9) is fixedly installed on the top of the slide rod (8), the bottom of the slide rod (8) is fixedly connected to the cylinder (2), and the first spring (10) is sleeved on the outside of the connecting pipe (1). The striking assembly includes: a crossbar (13), a striking rod (14), a second spring (15), and a pushing assembly for driving the striking rod (14) to move away from the cylinder (2); The crossbar (13) is fixedly installed around the outside of the connecting pipe (1) at equal intervals, and the drumstick (14) is slidably installed inside the crossbar (13). The second spring (15) squeezes the drumstick (14), and the drumstick (14) abuts against the outside of the cylinder (2). The pushing assembly includes: a wedge block (16), a fixing frame, a base (17), a vertical plate (18), a bracket, a rotating shaft, a stop block (19), and an inclined stop block (20). The wedge block (16) is fixedly connected to the outside of the racket arm (14) by a fixing bracket. The base (17) is fixedly connected to the bottom of the cylinder (2). The vertical plate (18) corresponds to the number of the wedge block (16). The vertical plate (18) is fixedly installed on the top of the base (17). The bracket is fixedly installed on the vertical plate (18) at equal intervals from top to bottom. The abutment block (19) is rotatably installed inside the bracket through the rotating shaft. The inclined block (20) is fixedly installed on the vertical plate (18) at equal intervals. The inclined block (20) is located below the abutment block (19) and abuts against the bottom of the abutment block (19). An iron rod (21) is fixedly installed on the side of the racket (14) away from the connecting tube (1). The end of the iron rod (21) away from the connecting tube (1) extends through the second spring (15) to the outside of the cross frame (13). The end of the cross frame (13) away from the connecting tube (1) is fixedly installed with a second electromagnet (23) through a positioning frame (22).

2. The germanane reactor residue separation device according to claim 1, characterized in that: The lifting assembly includes: a first electromagnet (11) and an iron ring (12). The first electromagnet (11) is fixedly installed at the bottom of the sleeve plate (7), and the iron ring (12) is fixedly installed at the top of the cylinder (2). When the first electromagnet (11) is energized, the magnetic force generated can attract the iron ring (12) and make it lift the cylinder (2) up.

3. The germanane reactor residue separation device according to claim 2, characterized in that: The filter assembly includes: a filter frame (3), a filter (4), a sealing ring, and a connecting rod (24). The filter frames (3) are arranged at equal intervals from top to bottom inside the cylinder (2). Adjacent filter frames (3) are fixedly connected by connecting rods (24). The filter screen (4) is arranged inside the filter frame (3). The aperture of the filter screen (4) decreases from top to bottom. The connector (25) is set as a ring magnet. The connector (25) is fixedly installed on the top of the bottom cover (5). The filter frame (3) is made of iron. The filter frame (3) is nickel-plated. The bottom filter frame (3) is attracted and fixed to the connector (25). The sealing ring is sleeved on the outside of the filter frame (3). The sealing ring abuts against the inner wall of the cylinder (2).

4. The germanane reactor residue separation device according to claim 3, characterized in that: The sealing assembly includes: an annular airbag (26) and a conduit (27); The outer side of the connecting pipe (1) is provided with an annular groove, and the annular airbag (26) is fixedly sleeved in the annular groove. One end of the conduit (27) is connected to the annular airbag (26), and the other end extends through the inner wall of the connecting pipe (1) to the outside of the connecting pipe (1). One end of the conduit (27) extending to the outside of the connecting pipe (1) is connected to an air injection device. The inner wall of the junction between the cylinder (2) and the connecting pipe (1) is provided with an annular embedding groove that cooperates with the annular airbag (26).

5. The germanane reactor residue separation device according to claim 4, characterized in that: The outer side of the connecting pipe (1) is equidistantly threaded with a screw rod, and the inner wall of the connecting pipe (1) is provided with a rubber ring (29).

6. The germanane reactor residue separation device according to claim 5, characterized in that: The connecting pipe (1) has symmetrical slots on its outside. The slots are equipped with card plates. Covers (28) are fixedly installed on the outside of the card plates. Magnetic blocks are provided on opposite sides of the two covers (28). The magnetic poles of the opposite magnetic blocks are opposite. The two covers (28) are fixed together by magnetic attraction.

7. A method for separating germanane residue using the germanane reactor residue separation device as described in claim 6, characterized in that, Includes the following steps: S1. When in use, connect the connecting pipe (1) to the discharge pipe of the germane reactor and perform the liquid discharge operation. After the liquid enters the connecting pipe (1) and the cylinder (2), it is filtered by the filter assembly to achieve graded collection of germane reactor residue in the liquid. Finally, the filtered liquid is discharged through the discharge pipe (6). S2. After the liquid has flowed out, the sealing component is removed and the cylinder (2) is driven to rise by the lifting component. During the rise of the cylinder (2), the outer side of the cylinder (2) is patted by the patting component. The resulting vibration shakes the slag attached to the inner wall of the cylinder (2) onto the filter component. As the cylinder (2) rises, the sliding rod (8) and the top plate (9) move accordingly. At the same time, the cylinder (2) compresses the first spring (10) in conjunction with the sleeve plate (7). S3. When the cylinder (2) rises to the highest position, the lifting component cancels the drive of the cylinder (2), the first spring (10) quickly resets and carries the cylinder (2), slide rod (8), and top plate (9) down quickly. The top plate (9) collides with the sleeve plate (7) to generate vibration, and the vibration is transmitted to the cylinder (2), causing the cylinder (2) and the filter components inside to vibrate, which in turn vibrates the slag on the filter components. S4. Repeat the above operation to shake the slag attached to the inner wall of the cylinder (2) onto the filter assembly. Then, rely on the vibration of the filter assembly itself to shake the slag, so that the slag on the filter assembly can pass through the filter assembly and be graded and filtered. Finally, the slag is completely graded and separated, which is convenient for subsequent graded collection of slag of different sizes.

Citation Information

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