A method for determining the fisher particle size of refractory metal powders with a managed test loop

By using the same material sample for instrument status verification and omitting the degassing step, the Fisher particle size determination method solves the problems of instrument drift and low efficiency in the determination of refractory metal powders, and achieves efficient and accurate particle size determination.

CN122409438APending Publication Date: 2026-07-17JINDUICHENG MOLYBDENUM CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
JINDUICHENG MOLYBDENUM CO LTD
Filing Date
2026-06-04
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing Fisher particle size determination methods lack an instrument condition verification mechanism consistent with the characteristics of the powder being tested in the determination of refractory metal powders, which leads to the measurement results deviating from the true value, and the degassing step takes too long and is inefficient.

Method used

Routine verification is performed using management samples of the same material and with high stability. A Fisher particle size determination process without degassing is established. By comparing the measured values ​​of the management samples with the standard values, instrument drift can be detected in a timely manner. The degassing step is omitted in the preset test procedure to improve efficiency.

Benefits of technology

It enables real-time monitoring of instrument status and accuracy of measurement results, shortens measurement time, improves detection efficiency, and ensures batch consistency and accuracy.

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Abstract

本发明公开了一种含管理样测试环节的难熔金属粉末费氏粒度测定方法及垫板组件,属于粉末材料检测技术领域。该方法利用难熔金属粉末高度稳定、表面气体吸附极微的特性,选用标准值绝对偏差不超过±0.2μm且一年内粒度相对变化≤3%的同材质难熔金属粉末标准样品作为管理样;每日按照包括称量、装样、压力控制和数据采集但不包括脱气处理的预设测试规程对管理样进行费氏粒度测定;将管理样实测值与标准值比对,若偏差在±3%以内则进行样品测试,否则停机检修;样品测试按相同规程执行。本发明以同材质的稳定管理样作为日常基准,及时发现仪器微小漂移,同时省去脱气冗余操作,显著提升效率,确保测定结果长期准确可靠。
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