Novel rectifying tower for pesticide intermediate production

By introducing automatic cleaning and temperature monitoring systems into the new distillation tower produced by pesticide intermediates, the problem of the adhesion of inner walls affecting distillation is solved, and the cleaning and distillation quality of the distillation tower are improved.

CN222342006UActive Publication Date: 2025-01-14NANTONG WEILIKE CHEM
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Patent Information

Application Number
CN202421061405.1
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-05-16
Publication Date
2025-01-14
Estimated Expiration
2034-05-16

AI Technical Summary

Technical Problem

The existing pesticide intermediate production of new distillation towers is not convenient for automated cleaning of materials attached to the inner wall, which affects the distillation effect and the extraction purity of re-distillation.

Method used

A new distillation tower including a main mechanism and an auxiliary mechanism is designed. The main mechanism automatically cleans the inner wall of the distillation tower through a stirring motor, hydraulic cylinder and cleaning brush. The auxiliary mechanism ensures appropriate temperature through a temperature sensor and heating assembly. And improve the distillation quality through a one-way tube and a condenser.

Benefits of technology

The automatic cleaning of the inner wall of the distillation tower is achieved, the distillation effect and purity are improved, and the real-time temperature control and distillation quality are ensured.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model relates to the technical field of pesticide intermediate production, and discloses a novel rectifying tower for pesticide intermediate production, which comprises a main body mechanism and an auxiliary mechanism, the auxiliary mechanism is positioned on the right side of the main body mechanism, and the main body mechanism comprises a rectifying tower body, a stirring motor, a driving shaft and a first hydraulic cylinder. The stirring motor is fixedly mounted in the middle of the upper end of the rectifying tower body. According to the novel rectifying tower for pesticide intermediate production, by installing the main body mechanism, when the rectifying tower body is used for producing pesticide intermediate materials, a worker can drive a cleaning brush and a scraping plate to rotate at a constant speed through operation, and automatic cleaning of the rectifying tower body is achieved; the situation that materials are attached to the inner wall of the rectifying tower body and consequently rectification is insufficient is avoided, meanwhile, the cleaning effect of the rectifying tower body after use is improved, it is avoided that residues of the materials affect normal operation of secondary rectification operation, and the protective property of the rectifying tower body is improved.
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Description

Technical Field

[0001] The utility model relates to the technical field of pesticide intermediate production, in particular to a novel distillation tower for pesticide intermediate production. Background Art

[0002] A distillation tower is a tower-type vapor-liquid contact device for distillation. It utilizes the different volatilities of the components in the mixture, that is, the different vapor pressures of the components at the same temperature, to transfer the light components (low boiling substances) in the liquid phase to the gas phase, and the heavy components (high boiling substances) in the gas phase to the liquid phase, thereby achieving the purpose of separation. In the production process of pesticide intermediates, distillation towers are usually used to distill materials.

[0003] The existing patent document with technical announcement number CN212090966U provides a new distillation tower for the production of pesticide intermediates. The existing distillation tower cannot control the temperature well. Since different substances require different temperatures, temperature control is a very important step, and a condensing device needs to be connected separately, which makes the operation complicated. The utility model has a reasonable structure and is easy to operate. The baffle can be moved by an electric telescopic rod, so that the size of the through hole can be controlled, which is convenient for controlling the flow of hot gas entering the distillation bin, so that the temperature can be controlled. The steam can be quickly condensed into liquid through the condenser for easy collection.

[0004] However, when the new distillation tower for the existing pesticide intermediate production is used, it is not convenient to automatically clean the materials attached to the inner wall of the distillation tower. When the materials adhere to the inner wall of the distillation tower during the distillation process and cannot be cleaned, it will affect the distillation effect of the distillation tower on the pesticide intermediate materials, and the residual materials inside the distillation tower will affect the extraction purity of the second distillation operation, which is not convenient to meet people's usage needs. Utility Model Content

[0005] 1. Technical issues to be resolved

[0006] The utility model aims to provide a novel distillation tower for producing pesticide intermediates, so as to solve the problem that the novel distillation tower for producing pesticide intermediates proposed in the above background technology is not convenient for automatically cleaning the materials attached to the inner wall of the distillation tower.

[0007] (II) Technical solution

[0008] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a new distillation tower for the production of pesticide intermediates, comprising a main mechanism and an auxiliary mechanism, wherein the auxiliary mechanism is located on the right side of the main mechanism, and the main mechanism comprises a distillation tower body, a stirring motor, a driving shaft and a first hydraulic cylinder, wherein the stirring motor is fixedly mounted at the middle of the upper end of the distillation tower body, the transmission end of the lower end of the stirring motor extends to the interior of the distillation tower body, the driving shaft is fixedly mounted at the transmission end of the lower end of the stirring motor, and the first hydraulic cylinder is fixedly mounted at the left and right ends of the driving shaft;

[0009] The main mechanism also includes a first adjusting rod, a second hydraulic cylinder, a second adjusting rod, a cleaning brush and a scraper. The first adjusting rod is fixedly mounted on the transmission end of the outer end of the first hydraulic cylinder, the second hydraulic cylinder is fixedly mounted on the lower end of the first adjusting rod, the second adjusting rod is fixedly mounted on the transmission end of the lower end of the second hydraulic cylinder, the cleaning brush is fixedly mounted on the outer end of the second adjusting rod, the cleaning brush is movably connected to the distillation tower body, and the scraper is fixedly mounted on the lower end of the outer end of the drive shaft.

[0010] Preferably, the auxiliary mechanism includes a feed pipe, a control panel, a heating assembly, a movable seat, a temperature sensor, a stirring blade, a one-way tube, a condenser, a first collecting tube and a second collecting tube. The feed pipe is fixedly installed at the left end of the distillation tower body. The design of the feed pipe facilitates the feeding of the pesticide intermediate material.

[0011] Preferably, the control panel is fixedly mounted on the left end of the distillation tower body, the heating component is fixedly mounted inside the distillation tower body, the heating component is electrically connected to the control panel, and the design of the heating component facilitates heating of the distillation tower body.

[0012] Preferably, the movable seat is fixedly mounted at the lower end inside the distillation tower body, the lower end of the drive shaft is rotatably connected to the movable seat, the temperature sensor is fixedly mounted at the front end of the drive shaft, the temperature sensor is electrically connected to the control panel, and the design of the movable seat provides a supporting effect for the drive shaft.

[0013] Preferably, the stirring blade is fixedly mounted on the outer end of the driving shaft, the one-way tube is fixedly mounted on the right end of the distillation tower body, and the condenser is fixedly mounted on the right end of the one-way tube. The design of the one-way tube facilitates the transportation of gaseous pesticide intermediate materials to the interior of the condenser, and a filter screen is arranged inside the one-way tube.

[0014] Preferably, the first collecting tube is fixedly installed at the lower end of the condenser, and the second collecting tube is fixedly installed at the lower end of the distillation tower body. The design of the first collecting tube is convenient for collecting the liquid pesticide intermediate material inside the condenser, and the design of the second collecting tube is convenient for collecting the liquid pesticide intermediate material after processing inside the distillation tower body.

[0015] Compared with the prior art, the beneficial effects of the utility model are:

[0016] 1. The new distillation tower for the production of pesticide intermediates is equipped with a main body mechanism, so that when the distillation tower body is used for the production of pesticide intermediate materials, the staff can drive the cleaning brush and the scraper to rotate at a uniform speed through operation, so as to realize the automatic cleaning of the distillation tower body, avoid the material adhering to the inner wall of the distillation tower body and cause the distillation to be insufficient, and at the same time improve the cleaning effect of the distillation tower body after use, avoid the residual material affecting the normal distillation operation again, and improve the protection of the distillation tower body;

[0017] 2. The new distillation tower for the production of pesticide intermediates is equipped with auxiliary mechanisms, so that when the distillation tower body is performing the distillation operation of the pesticide intermediate material, the temperature sensor is designed to monitor the internal temperature of the distillation tower body in real time, which is convenient for the staff to control the working state of the heating component, provide a good distillation temperature for the pesticide intermediate material, and improve the practicality of the distillation tower body;

[0018] 3. The new distillation tower for the production of pesticide intermediates is equipped with a one-way pipe, so that when the distillation tower body is in use, the design of the one-way pipe allows the gaseous pesticide intermediate materials generated during the distillation process to enter the condenser for condensation treatment, and the one-way pipe can filter the gaseous pesticide intermediate materials to improve the distillation accuracy of the pesticide intermediate materials, thereby improving the distillation quality of the pesticide intermediate materials by the distillation tower body. BRIEF DESCRIPTION OF THE DRAWINGS

[0019] Figure 1 It is a schematic diagram of the three-dimensional structure of the utility model;

[0020] Figure 2 This is a schematic diagram of the three-dimensional structure of the distillation tower body of the utility model;

[0021] Figure 3 This is a schematic diagram of the three-dimensional structure of the main mechanism of the utility model;

[0022] Figure 4 It is a schematic diagram of the enlarged structure of the local details of the heating component of the utility model.

[0023] In the figure: 1. Main mechanism; 101. Distillation tower body; 102. Stirring motor; 103. Driving shaft; 104. First hydraulic cylinder; 105. First adjusting rod; 106. Second hydraulic cylinder; 107. Second adjusting rod; 108. Cleaning brush; 109. Scraper; 2. Auxiliary mechanism; 201. Feed pipe; 202. Control panel; 203. Heating assembly; 204. Movable seat; 205. Temperature sensor; 206. Stirring blade; 207. One-way pipe; 208. Condenser; 209. First collecting pipe; 210. Second collecting pipe. DETAILED DESCRIPTION

[0024] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0025] See also Figure 1 - Figure 4 The utility model provides a technical solution: a new distillation tower for the production of pesticide intermediates, comprising a main mechanism 1 and an auxiliary mechanism 2, the auxiliary mechanism 2 is located on the right side of the main mechanism 1, the main mechanism 1 comprises a distillation tower body 101, a stirring motor 102, a drive shaft 103 and a first hydraulic cylinder 104, the stirring motor 102 is fixedly installed in the middle of the upper end of the distillation tower body 101, the transmission end of the lower end of the stirring motor 102 extends to the inside of the distillation tower body 101, the drive shaft 103 is fixedly installed at the transmission end of the lower end of the stirring motor 102, and the first hydraulic cylinder 104 is fixedly installed at the left and right ends of the drive shaft 103;

[0026] The main mechanism 1 also includes a first adjusting rod 105, a second hydraulic cylinder 106, a second adjusting rod 107, a cleaning brush 108 and a scraper 109. The first adjusting rod 105 is fixedly mounted on the transmission end of the outer end of the first hydraulic cylinder 104, the second hydraulic cylinder 106 is fixedly mounted on the lower end of the first adjusting rod 105, the second adjusting rod 107 is fixedly mounted on the transmission end of the lower end of the second hydraulic cylinder 106, the cleaning brush 108 is fixedly mounted on the outer end of the second adjusting rod 107, the cleaning brush 108 is movably connected to the distillation tower body 101, and the scraper 109 is fixedly mounted on the drive shaft. At the lower end of the outer end 103, the staff adds clean water into the distillation tower body 101, and then starts the first hydraulic cylinder 104 to make the cleaning brush 108 fully contact with the inner wall of the distillation tower body 101, and driven by the stirring motor 102, the two groups of cleaning brushes 108 and the scraper 109 rotate at a uniform speed to clean the residual materials in the inner cavity of the distillation tower body 101. By adjusting the second hydraulic cylinder 106, the positions of the two groups of cleaning brushes 108 are appropriately adjusted to achieve full cleaning of the inner wall of the distillation tower body 101, so as to prepare for the distillation operation to be carried out again.

[0027] The auxiliary mechanism 2 includes a feed pipe 201, a control panel 202, a heating component 203, a movable seat 204, a temperature sensor 205, a stirring blade 206, a one-way pipe 207, a condenser 208, a first collecting pipe 209 and a second collecting pipe 210. The feed pipe 201 is fixedly installed at the left end of the distillation tower body 101, the control panel 202 is fixedly installed at the left end of the distillation tower body 101, the heating component 203 is fixedly installed inside the distillation tower body 101, and the heating component 203 is electrically connected to the control panel 202. The movable seat 204 is fixedly mounted on the lower end of the distillation tower body 101, the lower end of the drive shaft 103 is rotatably connected to the movable seat 204, the temperature sensor 205 is fixedly mounted on the front end of the drive shaft 103, the temperature sensor 205 is electrically connected to the control panel 202, the stirring blade 206 is fixedly mounted on the outer end of the drive shaft 103, the one-way pipe 207 is fixedly mounted on the right end of the distillation tower body 101, the condenser 208 is fixedly mounted on the right end of the one-way pipe 207, and the first collecting pipe 209 is fixedly mounted on the condenser 20 8, the second collecting pipe 210 is fixedly installed at the lower end of the distillation tower body 101. When the distillation tower body 101 is used to perform the distillation operation of the pesticide intermediate material, the staff transports the pesticide intermediate material to the inside of the distillation tower body 101 through the feed pipe 201, and operates the control panel 202 to make the heating component 203 work to heat the inner cavity of the distillation tower body 101. The stirring motor 102 works to drive the driving shaft 103 to rotate at a uniform speed, and the driving shaft 103 drives the stirring blade 206 to rotate at a uniform speed. , so that the pesticide intermediate material is heated more evenly and fully, the temperature sensor 205 monitors the internal temperature of the distillation tower body 101 and uploads the data to the control panel 202, and under the operation of the heating component 203, the material with a lower boiling point is turned into steam, which enters the interior of the condenser 208 through the one-way pipe 207, and is condensed into a liquid pesticide intermediate material and discharged through the first collecting pipe 209. The liquid pesticide intermediate material after distillation in the distillation tower body 101 is discharged through the second collecting pipe 210 for collection.

[0028] Working principle: When the distillation tower body 101 is used to perform distillation of pesticide intermediate materials, the staff transports the pesticide intermediate materials to the interior of the distillation tower body 101 through the feed pipe 201, and operates the control panel 202 to operate the heating component 203 to heat the inner cavity of the distillation tower body 101. The stirring motor 102 drives the drive shaft 103 to rotate at a constant speed, and the drive shaft 103 drives the stirring blade 206 to rotate at a constant speed, so that the pesticide intermediate materials are heated more evenly and fully. The temperature sensor 205 monitors the internal temperature of the distillation tower body 101 and uploads the data to the control panel 202. Under the operation of the heating component 203, the material with a lower boiling point is turned into steam and enters the condenser through the one-way pipe 207. The inside of 208 is condensed and turned into liquid pesticide intermediate material, which is discharged through the first collecting pipe 209. The liquid pesticide intermediate material after distillation in the distillation tower body 101 is discharged through the second collecting pipe 210 for collection. The staff adds clean water into the inside of the distillation tower body 101, and then starts the first hydraulic cylinder 104 to make the cleaning brush 108 fully contact with the inner wall of the distillation tower body 101. Under the drive of the stirring motor 102, the two groups of cleaning brushes 108 and the scraper 109 are driven to rotate at a uniform speed to clean the residual materials in the inner cavity of the distillation tower body 101. By adjusting the second hydraulic cylinder 106, the positions of the two groups of cleaning brushes 108 are appropriately adjusted to achieve full cleaning of the inner wall of the distillation tower body 101, so as to prepare for the distillation operation to be carried out again.

[0029] Finally, it should be noted that the above content is only used to illustrate the technical solution of the utility model, rather than to limit the protection scope of the utility model. Simple modifications or equivalent substitutions of the technical solution of the utility model by ordinary technicians in this field do not deviate from the essence and scope of the technical solution of the utility model.

Claims

1. A novel distillation tower for producing pesticide intermediates, comprising a main mechanism (1) and an auxiliary mechanism (2), characterized in that: The auxiliary mechanism (2) is located on the right side of the main mechanism (1); the main mechanism (1) comprises a distillation tower body (101), a stirring motor (102), a drive shaft (103) and a first hydraulic cylinder (104); the stirring motor (102) is fixedly mounted at the middle of the upper end of the distillation tower body (101); the transmission end of the lower end of the stirring motor (102) extends into the interior of the distillation tower body (101); the drive shaft (103) is fixedly mounted at the transmission end of the lower end of the stirring motor (102); and the first hydraulic cylinder (104) is fixedly mounted at the left and right ends of the drive shaft (103); The main body mechanism (1) further comprises a first adjusting rod (105), a second hydraulic cylinder (106), a second adjusting rod (107), a cleaning brush (108) and a scraper (109); the first adjusting rod (105) is fixedly mounted on the transmission end of the outer end of the first hydraulic cylinder (104); the second hydraulic cylinder (106) is fixedly mounted on the lower end of the first adjusting rod (105); the second adjusting rod (107) is fixedly mounted on the transmission end of the lower end of the second hydraulic cylinder (106); the cleaning brush (108) is fixedly mounted on the outer end of the second adjusting rod (107); the cleaning brush (108) is movably connected to the distillation tower body (101); and the scraper (109) is fixedly mounted on the lower end of the outer end of the driving shaft (103).

2. The novel distillation tower for producing pesticide intermediates according to claim 1, characterized in that: The auxiliary mechanism (2) comprises a feed pipe (201), a control panel (202), a heating component (203), a movable seat (204), a temperature sensor (205), a stirring blade (206), a one-way pipe (207), a condenser (208), a first collecting pipe (209) and a second collecting pipe (210); the feed pipe (201) is fixedly installed at the left end of the distillation tower body (101).

3. The novel distillation tower for producing a pesticide intermediate according to claim 2, characterized in that: The control panel (202) is fixedly installed at the left end of the distillation tower body (101), the heating component (203) is fixedly installed inside the distillation tower body (101), and the heating component (203) is electrically connected to the control panel (202).

4. The novel distillation tower for producing pesticide intermediates according to claim 3, characterized in that: The movable seat (204) is fixedly mounted at the lower end of the distillation tower body (101); the lower end of the driving shaft (103) is rotatably connected to the movable seat (204); the temperature sensor (205) is fixedly mounted at the front end of the driving shaft (103); and the temperature sensor (205) is electrically connected to the control panel (202).

5. The novel distillation tower for producing pesticide intermediates according to claim 4, characterized in that: The stirring blade (206) is fixedly mounted on the outer end of the driving shaft (103), the one-way tube (207) is fixedly mounted on the right end of the distillation tower body (101), and the condenser (208) is fixedly mounted on the right end of the one-way tube (207).

6. The novel distillation tower for producing pesticide intermediates according to claim 5, characterized in that: The first collecting tube (209) is fixedly installed at the lower end of the condenser (208), and the second collecting tube (210) is fixedly installed at the lower end of the distillation tower body (101).

Citation Information

Patent Citations

  • Novel rectifying tower for pesticide intermediate production

    CN212090966U