Purification synthesis equipment with detection function
By designing a purified and synthetic equipment with detection functions, the motor -driven mixing rod and the automatic feeding mechanism are used to mix and add the reactor. Combined with heating rods and inner barrels for material heating and storage The problem has achieved more efficient purification and safer operating environment of more efficient oxide powder.
Patent Information
- Application Number
- CN202323629759.X
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2023-12-29
- Publication Date
- 2025-01-28
- Estimated Expiration
- 2033-12-29
AI Technical Summary
Existing purification and synthesis equipment is prone to artificial errors when adding reaction agents, resulting in incomplete reaction or damage to the yttrium oxide powder, and complex operation increases work tasks and scald risks.
Design a purifying synthetic equipment with detection functions. The mixing and mixing of rare earth oxides and reactive agents is used to drive the rare earth and reactives through the motor. operate.
A fuller integration of rare earth oxide raw materials and reactions, improved the purity of oxide powder, reduced artificial operation tasks, reduced the risk of burns, and improved the efficiency of equipment.
Smart Images
Figure CN222401438U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of purification and synthesis equipment, in particular to a purification and synthesis equipment with a detection function. Background Art
[0002] Spherical yttrium oxide powder for spraying is a functional material. Its application in the fields of aviation, aerospace, atomic energy and high-tech ceramics has shown its superior performance. In recent years, yttrium oxide powder has been more widely used in the electronics industry and semiconductor industry, especially as a coating material for semiconductor etcher to prevent plasma corrosion. The purity of yttrium oxide powder directly affects the quality of its downstream products.
[0003] Yttrium oxide powder is generally purified by acid decomposition, purification and impurity removal, multi-stage fractionation extraction, oxalic acid precipitation and calcination and other steps. Different reaction reagents need to be added according to needs during the purification process. The existing purification and synthesis equipment requires a dryer to open the sealing cover and then add various reaction reagents inside for stirring reaction. The manual addition of reagents is prone to errors, resulting in incomplete reaction of the yttrium oxide powder or excessive addition of reagents, resulting in damage to the yttrium oxide powder and unusable, which also increases the workload of the operator.
[0004] Therefore, the utility model provides a purification and synthesis device with a detection function to solve the problems raised in the above background technology. Utility Model Content
[0005] The purpose of the utility model is to solve the shortcomings of the prior art, and to propose a purification and synthesis equipment with a detection function. The motor at the upper middle end of the sealing mechanism can drive the stirring rod at the lower end to rotate. The rare earth oxide raw material and various reaction reagents can be stirred and mixed by rotating the stirring rod. The stirring blade can be used to make the materials more evenly mixed, and the rare earth oxide raw material and the reactant can be more fully integrated, thereby increasing the purity of the yttrium oxide powder. At the same time, the cylinder at the upper end of the fixed frame can drive the sealing mechanism to move up and down, which is convenient for the staff to clean the inside of the mixing mechanism. At the same time, the cylinder does not need to be operated. The operator manually punches in or closes the sealing mechanism to avoid burns to the operator due to excessive gas temperature inside the mixing mechanism. The materials can be stored and mixed through the inner barrel inside the mixing mechanism, which is heated by the heating rod inside the protective shell and then transferred to the internal materials in conjunction with the inner barrel. The unloading mechanism at the upper end is used in conjunction with the feeding pump at the rear end to automatically add reagents to the mixing mechanism for reaction. The operator does not need to frequently open the sealing mechanism for feeding, which effectively reduces the operator's work tasks and the probability of burns to the operator, while also improving the utilization efficiency of the purification and synthesis equipment.
[0006] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a purification and synthesis device with a detection function, comprising a fixed frame, cylinders are fixedly arranged on both sides of the upper end of the fixed frame, sealing mechanisms are fixedly arranged on the upper ends of the two cylinders, a protective shell is fixedly arranged inside the upper end of the fixed frame, a mixing mechanism is fixedly arranged inside the protective shell, and a heating rod is fixedly arranged inside the protective shell;
[0007] A detection box is fixedly arranged on one side of the upper end of the fixing frame, a feeding mechanism is fixedly arranged on one side of the upper end of the sealing mechanism, the feeding mechanism includes a storage box, the mixing mechanism includes an inner barrel, and the sealing mechanism includes a fixing plate;
[0008] Through the above technical scheme, the purity of the material can be detected through the detection box, different reaction reagents can be added to the mixing mechanism in proportion for reaction through the feeding mechanism, a variety of reagents can be stored through the storage box, the material can be conveniently stored and purified through the inner barrel, and the feeding mechanism, stirring rod and sealing cover can be fixed through the fixing plate.
[0009] Furthermore, a material discharge plate is hingedly provided inside the lower end of the inner barrel, and two filter screens are fixedly provided inside the lower end of the inner barrel;
[0010] Through the above technical solution, the reacted materials can be conveniently discharged through the discharge plate, and the reacted materials can be filtered through the filter net to avoid incomplete reaction of the materials and impurities inside that affect their use.
[0011] Furthermore, a fixing screw is rotatably arranged inside the lower end of one side of the inner barrel, and a sealing plate is threadedly sleeved on the outer surface of the fixing screw;
[0012] Through the above technical solution, the sealing plate can be fixed by the fixing screw, and it is also convenient to adjust the position of the sealing plate later. The through hole on one side of the inner barrel can be sealed by the sealing plate, and it is also convenient to transport the material to the inside of the detection box for use.
[0013] Furthermore, a rotating motor is fixedly arranged on one side of the lower end of the inner barrel, and a sealing cover is fixedly arranged around the lower end of the fixing plate;
[0014] Through the above technical solution, the fixed screw can be driven to rotate by the rotating motor, and the gap at the connection between the mixing mechanism and the sealing mechanism can be sealed by the sealing cover.
[0015] Furthermore, a stirring rod is fixedly arranged in the middle of the lower end of the fixed plate, and a plurality of stirring blades are fixedly arranged on the outer surface of the stirring rod;
[0016] Through the above technical solution, the internal materials can be mixed and stirred more evenly by using a stirring rod in conjunction with a plurality of stirring blades, thereby avoiding uneven mixing of materials and incomplete reaction of materials.
[0017] Furthermore, a plurality of feeding ports are provided at the upper end of the storage box, and a plurality of feeding pumps are fixedly provided at the upper end of the storage box;
[0018] Through the above technical solution, different medicines can be conveniently added to the interior of the storage box through the feeding port, and different medicines can be adjusted to the interior of the mixing mechanism through multiple feeding pumps.
[0019] The utility model has the following beneficial effects:
[0020] 1. The utility model proposes a purification and synthesis equipment with a detection function. The motor at the middle upper end of the sealing mechanism can drive the stirring rod at the lower end to rotate. The rare earth oxide raw material and various reaction reagents can be stirred and mixed by rotating the stirring rod. The stirring blade can be used to make the materials mixed more evenly, and the rare earth oxide raw material and the reactant can be more fully integrated, thereby increasing the purity of the yttrium oxide powder. At the same time, the cylinder at the upper end of the fixed frame can drive the sealing mechanism to move up and down, which is convenient for the staff to clean the inside of the mixing mechanism. At the same time, the cylinder does not require the staff to manually punch in or close the sealing mechanism, which can avoid the excessive temperature of the gas inside the mixing mechanism causing burns to the staff.
[0021] 2. The utility model proposes a purification and synthesis equipment with a detection function. Materials can be stored and mixed through an inner barrel inside a mixing mechanism. The materials can be heated by a heating rod inside a protective shell, and then the heat can be transferred to the materials inside in cooperation with the inner barrel to heat the materials or gases inside for reaction. This can prevent the materials from directly contacting the heating rod, causing damage to the heating rod and making it unusable. The unloading mechanism at the upper end can be used in cooperation with the feeding pump at the rear end to automatically add reagents to the mixing mechanism for reaction. The staff does not need to frequently open the sealing mechanism for feeding, which effectively reduces the staff's work tasks and the probability of scalding the staff, while also improving the use efficiency of the purification and synthesis equipment. BRIEF DESCRIPTION OF THE DRAWINGS
[0022] Figure 1 It is an axonometric schematic diagram of the utility model;
[0023] Figure 2 It is a schematic diagram of the expansion of the utility model;
[0024] Figure 3 It is a cross-sectional schematic diagram of the mixing mechanism of the utility model;
[0025] Figure 4It is a cross-sectional schematic diagram of the protective shell of the utility model.
[0026] Legend:
[0027] 1. Fixed frame; 2. Protective shell; 3. Cylinder; 4. Detection box; 5. Mixing mechanism; 501. Inner barrel; 502. Unloading plate; 503. Filter screen; 504. Rotating motor; 505. Fixed screw; 506. Sealing plate; 6. Sealing mechanism; 601. Fixed plate; 602. Sealing cover; 603. Stirring rod; 604. Stirring blade; 7. Unloading mechanism; 701. Storage box; 702. Feeding port; 703. Feeding pump; 8. Heating rod. DETAILED DESCRIPTION
[0028] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.
[0029] Reference Figure 1-4 The utility model provides an embodiment: a purification and synthesis device with a detection function, comprising a fixed frame 1, cylinders 3 are fixedly arranged on both sides of the upper end of the fixed frame 1, sealing mechanisms 6 are fixedly arranged on the upper ends of the two cylinders 3, a protective shell 2 is fixedly arranged inside the upper end of the fixed frame 1, a mixing mechanism 5 is fixedly arranged inside the protective shell 2, and a heating rod 8 is fixedly arranged inside the protective shell 2. A detection box 4 is fixedly arranged on one side of the upper end of the fixed frame 1, and a feeding mechanism 7 is fixedly arranged on one side of the upper end of the sealing mechanism 6.
[0030] The fixing frame 1 can support and fix the purification and synthesis equipment, the position of the sealing mechanism 6 can be adjusted through the cylinder 3, and the sealing mechanism 6 can be driven to move up and down, the protective shell 2 can protect the outer surface of the mixing mechanism 5, the purity of the material can be detected through the detection box 4, and different reaction reagents can be added to the mixing mechanism 5 in proportion through the feeding mechanism 7 for reaction, the upper end of the mixing mechanism 5 can be sealed through the sealing mechanism 6, and the material inside the inner barrel 501 can also be stirred and mixed, and the material can be stored through the mixing mechanism 5, and the heating rod 8 can cooperate with the inner barrel 501 to transfer heat to the internal material, so as to heat the internal material or gas for reaction.
[0031] Reference Figure 3The mixing mechanism 5 includes an inner barrel 501, a material discharge plate 502 is hingedly provided inside the lower end of the inner barrel 501, two filter screens 503 are fixedly provided inside the lower end of the inner barrel 501, a fixed screw 505 is rotatably provided inside the lower end of one side of the inner barrel 501, a sealing plate 506 is threadedly sleeved on the outer surface of the fixed screw 505, and a rotating motor 504 is fixedly provided on one side of the lower end of the inner barrel 501.
[0032] The inner barrel 501 is convenient for storing and purifying materials, the discharge plate 502 is convenient for discharging reacted materials, the filter net 503 can filter the reacted materials to avoid incomplete reaction of materials and impurities affecting their use, the discharge plate 502 is convenient for discharging reacted materials, the filter net 503 can filter the reacted materials to avoid incomplete reaction of materials and impurities affecting their use, the sealing plate 506 can be fixed by the fixing screw 505, and it is also convenient to adjust the position of the sealing plate 506 later, the through hole on one side of the inner barrel 501 can be sealed by the sealing plate 506, and it is also convenient to transport the materials to the inside of the detection box 4 for use, and the fixing screw 505 can be driven to rotate by the rotating motor 504.
[0033] Reference Figure 2 The sealing mechanism 6 includes a fixed plate 601 , a sealing cover 602 is fixedly arranged around the lower end of the fixed plate 601 , a stirring rod 603 is fixedly arranged in the middle of the lower end of the fixed plate 601 , and a plurality of stirring blades 604 are fixedly arranged on the outer surface of the stirring rod 603 .
[0034] The gap at the connection between the mixing mechanism 5 and the sealing mechanism 6 can be sealed by the sealing cover 602, and the internal materials can be mixed and stirred more evenly by using the stirring rod 603 in conjunction with the multiple stirring blades 604, thereby avoiding uneven mixing of materials and incomplete reaction of materials.
[0035] Reference Figure 2 The unloading mechanism 7 includes a storage box 701 , a plurality of feeding ports 702 are opened at the upper end of the storage box 701 , and a plurality of feeding pumps 703 are fixedly arranged at the upper end of the storage box 701 .
[0036] The unloading mechanism 7, the stirring rod 603 and the sealing cover 602 can be fixed by the fixing plate 601, a variety of medicines can be stored by the storage box 701, different medicines can be conveniently added to the interior of the storage box 701 through the feeding port 702, and different medicines can be adjusted to the interior of the mixing mechanism 5 through multiple feeding pumps 703.
[0037] Working principle: Various reaction reagents are added to the storage box 701 from the multiple feeding ports 702 at the front end of the feeding mechanism 7 for storage, and then the cylinders 3 on both sides of the fixed frame 1 are started to move the sealing mechanism 6 upward to open the sealing cover 602, and then the rare earth oxide raw materials are adjusted to the mixing mechanism 5 for storage, and at the same time, the motor at the upper end drives the stirring rod 603 to rotate, and then the corresponding feeding pump 703 is started according to the reaction requirements to add the reagents in the inner barrel 501 in a suitable proportion, and then the stirring rod 603 cooperates with the stirring blade 604 to stir the rare earth oxide raw materials in the inner barrel 501. The rare earth oxide raw material and the reaction reagent are stirred and mixed. At the same time, the heating rod 8 can be started according to the reaction requirements to heat the rare earth oxide raw material inside. At the same time, the detection box 4 is started, and then the rotating motor 504 is started to drive the fixed screw 505 to rotate, and the sealing plate 506 at the upper end is moved. The material is transported to the inside of the detection box 4 for testing in conjunction with the conveying pipeline. After the test is qualified, the unloading plate 502 at the lower end of the inner barrel 501 is opened to allow the material to be filtered through the filter screen 503 at the lower end, and then the reacted material is filtered and discharged.
[0038] Finally, it should be noted that the above are only preferred embodiments of the present invention and are not intended to limit the present invention. Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art can still modify the technical solutions described in the aforementioned embodiments or make equivalent substitutions for some of the technical features therein. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.
Claims
1. A purification and synthesis device with a detection function, comprising a fixed frame (1), characterized in that: Cylinders (3) are fixedly arranged on both sides of the upper end of the fixing frame (1), sealing mechanisms (6) are fixedly arranged on the upper ends of the two cylinders (3), a protective shell (2) is fixedly arranged inside the upper end of the fixing frame (1), a mixing mechanism (5) is fixedly arranged inside the protective shell (2), and a heating rod (8) is fixedly arranged inside the protective shell (2); A detection box (4) is fixedly arranged on one side of the upper end of the fixing frame (1), a feeding mechanism (7) is fixedly arranged on one side of the upper end of the sealing mechanism (6), the feeding mechanism (7) comprises a storage box (701), the mixing mechanism (5) comprises an inner barrel (501), and the sealing mechanism (6) comprises a fixing plate (601).
2. The purification and synthesis equipment with detection function according to claim 1, characterized in that: A material discharge plate (502) is hingedly arranged inside the lower end of the inner barrel (501), and two filter screens (503) are fixedly arranged inside the lower end of the inner barrel (501).
3. The purification and synthesis equipment with detection function according to claim 1, characterized in that: A fixing screw (505) is rotatably arranged inside the lower end of one side of the inner barrel (501), and a sealing plate (506) is threadedly sleeved on the outer surface of the fixing screw (505).
4. The purification and synthesis equipment with detection function according to claim 1, characterized in that: A rotating motor (504) is fixedly arranged on one side of the lower end of the inner barrel (501), and a sealing cover (602) is fixedly arranged around the lower end of the fixing plate (601).
5. The purification and synthesis equipment with detection function according to claim 1, characterized in that: A stirring rod (603) is fixedly arranged in the middle of the lower end of the fixed plate (601), and a plurality of stirring blades (604) are fixedly arranged on the outer surface of the stirring rod (603).
6. The purification and synthesis equipment with detection function according to claim 1, characterized in that: The upper end of the storage box (701) is provided with a plurality of feeding ports (702), and the upper end of the storage box (701) is fixedly provided with a plurality of feeding pumps (703).