Electrolytic bath for realizing mutual deflection electric field of two deposition electric fields

By designing an electrolytic groove with a reinforcement device, the deflection of the two sedimentary electric fields is realized, and the problem of the existing electrolytic groove is difficult to prepare the problem of aluminum composite film with saturation and gradient structure. The preparation of magnetic aluminum film is prepared and improved the connection stability of the electrolytic groove.

CN222411908UActive Publication Date: 2025-01-28HEBEI NORMAL UNIV FOR NATTIES
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Patent Information

Application Number
CN202420852289.9
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-04-23
Publication Date
2025-01-28
Estimated Expiration
2034-04-23

AI Technical Summary

Technical Problem

It is difficult for existing electrolytic cells to obtain a saturated, gradient structure-colored alumina composite film through a one-time preparation process, and at the same time, the outer side of the bottom connection mounting base is lacking reinforcement.

Method used

A electrolytic groove that realizes the two types of sedimentary electric fields as a deformed electric field. By fixed the installation seat at the bottom of the electrolyte body, and a reinforcement device is set on the outer side, the structure of the variable diameter copper electrode, circular aluminum foil and firming spirality is combined. Implement electricity deposition and reinforcement.

Benefits of technology

This electrolyte can prepare two micro -structures that are exactly the same and structured and magnetic in the process of electrical deposition.

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Abstract

The utility model relates to the technical field of electrolytic baths, and discloses an electrolytic bath capable of realizing mutual deflection electric fields of two deposition electric fields, and the electrolytic bath can be used for preparing two aluminum oxide composite films with the same microstructure and the same iridescent strip-shaped structural color macroscopically by a one-time deposition process; comprising an electrolytic bath body, a mounting base is fixed to the bottom of the electrolytic bath body, a reinforcing device is arranged on the outer side of the electrolytic bath body, and a connecting device is mounted at the top of the mounting base; the device is provided with the reinforcing device, so that the movable connecting sleeve and the mounting fixing pad can be conveniently fixed, the connecting stability of the electrolytic bath main body and the mounting seat is improved, and the placement stability is facilitated; the device is provided with the connecting device, and after the electrolytic bath main body and the mounting seat are fixedly connected, the positioning connecting block at one end of the movable connecting pad is movably inserted into the preset groove of the corresponding electrolytic bath main body, so that the connection part between the mounting seat and the electrolytic bath main body is reinforced, and the connection stability is improved.
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Description

Technical Field

[0001] The utility model relates to the technical field of electrolytic cells, in particular to an electrolytic cell which realizes two deposition electric fields as mutually deflecting electric fields. Background Art

[0002] Since aluminum oxide films with nanopores are wide-bandgap metal oxide semiconductor materials with thermal stability, corrosion resistance, chemical stability and high dielectric constant, they have been widely used in the synthesis of ordered nanostructures. With the deepening of photonic crystal research, there have also been some studies on the structural color of aluminum oxide films. Since 1969, Diggle et al. reported that in the visible light range, aluminum oxide films supported by aluminum substrates will produce bright colors due to light interference when the thickness is less than 1μm. Many scientific researchers are committed to preparing aluminum oxide films with uniform structural colors, and continuously improve the preparation process during the preparation process. However, only one aluminum oxide film can be prepared at a time, and the film presents a single structural color.

[0003] However, in the use of the existing electrolytic cell, it is not easy to obtain an aluminum oxide composite film with a saturated and gradient structural color through a one-time preparation process, and the outer side of the bottom connection mounting seat lacks reinforcement. Therefore, those skilled in the art provide an electrolytic cell that realizes two deposition electric fields as mutually deflecting electric fields to solve the problems raised in the above background technology. Utility Model Content

[0004] The purpose of the utility model is to provide an electrolytic cell which realizes two deposition electric fields as mutually deflecting electric fields, so as to solve the problems raised in the above background technology.

[0005] In order to achieve the above purpose, the utility model provides the following technical solutions:

[0006] An electrolytic cell for realizing two mutually deflecting electric fields of deposition, comprising an electrolytic cell body, a mounting seat fixed at the bottom of the electrolytic cell body, a reinforcement device arranged at the outside of the electrolytic cell body, a connecting device installed at the top of the mounting seat, a variable diameter copper electrode extending to the outside arranged inside the electrolytic cell body, a circular aluminum foil connected to one end of the variable diameter copper electrode, a fastening screw connected to one side of the circular aluminum foil, and an annular silicone pad arranged at the outside of the variable diameter copper electrode;

[0007] The reinforcement device includes a guide plate, the outer side of the guide plate is slidably connected to a sliding block through a sliding groove, the outer side of the sliding block is fixed with a movable connecting sleeve, the outer side of the movable connecting sleeve is installed with a plastic rod, the top of the mounting seat is fixed with a mounting fixing pad, the top of the mounting fixing pad is provided with a positioning sleeve, the top of the mounting fixing pad is fixed with a connecting threaded rod, and the outer side of the connecting threaded rod is threadedly connected to a connecting threaded column.

[0008] As a further solution of the utility model: the connecting device includes a fixed shell, a support spring is provided on the inner wall of one side of the fixed shell, one end of the support spring is connected to a movable connecting pad, one side of the movable connecting pad is fixed with a movable limiting rod passing through the other side thereof, one end of the movable limiting rod is fixed with a plastic plate, and one end of the movable limiting rod is provided with a positioning connecting block.

[0009] As a further solution of the utility model: the fixed shell and the mounting seat are fixedly connected, and the outer side of the plastic plate is provided with anti-slip grooves.

[0010] As a further solution of the utility model: a groove is provided inside the electrolytic cell body, and the size of the groove is adapted to the size of the positioning connection block.

[0011] As a further solution of the utility model: the guide plate is fixedly connected to the electrolytic cell body, and a groove matching the size of the connecting threaded rod is provided on the outer side of the movable connecting sleeve.

[0012] As a further solution of the utility model: a through hole is provided inside the positioning sleeve, and the size of the through hole is adapted to the size of the mobile connecting sleeve.

[0013] Compared with the prior art, the beneficial effects of the utility model are:

[0014] 1. The device is provided with a reinforcement device. Before electrodeposition, the carbon rod is placed at the diagonal positions of the two electrode holes and a suitable deflection electric field is applied at the same time to conduct an electrodeposition experiment. Two "twin" AAO composite films with completely identical microstructures and two completely identical structural colors and magnetic properties are prepared at the same time, i.e., highly saturated strip iridescent structural color magnetic alumina films. At the same time, after the electrolytic cell body and the mounting seat are fixedly connected, the mobile connection sleeve and the mounting fixing pad can be easily fixed, thereby improving the connection stability between the electrolytic cell body and the mounting seat, which is conducive to stable placement;

[0015] 2. The device is provided with a connecting device. When the electrolytic cell body and the mounting seat are fixedly connected, the positioning connecting block at one end of the movable connecting pad is movably inserted into the preset groove of the corresponding electrolytic cell body, thereby completing the reinforcement of the connection part between the mounting seat and the electrolytic cell body and improving the connection stability. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] Figure 1 A three-dimensional diagram of an electrolytic cell that realizes two deposition electric fields as mutually deflecting electric fields;

[0017] Figure 2 A schematic diagram of partial structural decomposition of an electrolytic cell for realizing two deposition electric fields as mutually deflecting electric fields;

[0018] Figure 3 A structural schematic diagram of a reinforcement device in an electrolytic cell for realizing two deposition electric fields as mutually deflecting electric fields;

[0019] Figure 4 The present invention is a structural schematic diagram of a connecting device in an electrolytic cell for realizing two deposition electric fields as mutually deflecting electric fields.

[0020] In the figure: 1. electrolytic cell body; 2. mounting seat; 3. reinforcement device; 31. guide plate; 32. sliding block; 33. movable connecting sleeve; 34. plastic rod; 35. mounting fixing pad; 36. positioning sleeve; 37. connecting threaded rod; 38. connecting threaded column; 4. connecting device; 41. fixed shell; 42. supporting spring; 43. movable connecting pad; 44. movable limiting rod; 45. plastic plate; 46. positioning connecting block; 5. variable diameter copper electrode; 6. round aluminum foil; 7. fastening screw; 8. annular silicone pad. DETAILED DESCRIPTION

[0021] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0022] See also Figure 1-3 In an embodiment of the utility model, an electrolytic cell for realizing two mutually deflecting electric fields of deposition electric fields comprises an electrolytic cell body 1, a mounting seat 2 is fixed at the bottom of the electrolytic cell body 1, a reinforcing device 3 is arranged on the outside of the electrolytic cell body 1, a connecting device 4 is installed on the top of the mounting seat 2, a variable diameter copper electrode 5 extending to the outside is arranged inside the electrolytic cell body 1, a circular aluminum foil 6 is connected to one end of the variable diameter copper electrode 5, a fastening screw 7 is connected to one side of the circular aluminum foil 6, and an annular silicone pad 8 is arranged on the outside of the variable diameter copper electrode 5;

[0023] The reinforcement device 3 includes a guide plate 31, the outer side of the guide plate 31 is slidably connected with a sliding block 32 through a slide groove, the outer side of the sliding block 32 is fixed with a movable connecting sleeve 33, the outer side of the movable connecting sleeve 33 is installed with a plastic rod 34, the top of the mounting seat 2 is fixed with a mounting fixing pad 35, the top of the mounting fixing pad 35 is provided with a positioning sleeve 36, the interior of the positioning sleeve 36 is provided with a through hole, and the size of the through hole is adapted to the size of the movable connecting sleeve 33, the top of the mounting fixing pad 35 is fixed with a connecting threaded rod 37, the outer side of the connecting threaded rod 37 is threadedly connected with a connecting threaded column 38, the guide plate 31 and the electrolytic cell body 1 are fixedly connected, the outer side of the movable connecting sleeve 33 is provided with a groove adapted to the size of the connecting threaded rod 37, firstly, the annular silicone pad 8 is installed, then the circular aluminum foil 6 is installed, and then the variable diameter copper electrode 5 is installed, and then the fastening screw 7 can be installed, and finally the outer screw buckle is installed, and the outer screw buckle and the corresponding inner screw buckle are threadedly connected. The variable diameter copper electrode 5, the circular aluminum foil 6, the fastening screw 7 and the annular silicone pad 8 can be conveniently completed, and the leakage can be prevented. Before the electrodeposition, the carbon rod is placed at the diagonal positions of the two electrode holes, and a suitable deflection electric field is applied at the same time to carry out the electrodeposition experiment. At the same time, two "twin" AAO composite films with exactly the same microstructure and two structural colors and magnetic properties are prepared, that is, a highly saturated strip iridescent structural color magnetic alumina film. At the same time, after the fixed connection between the electrolytic cell body 1 and the mounting seat 2, the plastic rod 34 can be moved to drive the sliding block 32 to move, so that the movable connecting sleeve 33 outside the sliding block 32 can be moved, so that the movable connecting sleeve 33 can be movably sleeved on the outside of the connecting threaded rod 37. Finally, the connecting threaded column 38 is threadedly connected to the connecting threaded rod 37, so that the fixing between the movable connecting sleeve 33 and the mounting fixed pad 35 can be conveniently completed, and the connection stability between the electrolytic cell body 1 and the mounting seat 2 is improved, which is conducive to stable placement.

[0024] As an embodiment of the utility model, the connecting device 4 includes a fixed shell 41, and a support spring 42 is provided on the inner wall of one side of the fixed shell 41, and one end of the support spring 42 is connected to a movable connecting pad 43, and one side of the movable connecting pad 43 is fixed with a movable limit rod 44 running through the other side thereof, and one end of the movable limit rod 44 is fixed with a plastic plate 45, and one end of the movable limit rod 44 is provided with a positioning connecting block 46, the fixed shell 41 and the mounting seat 2 are fixedly connected, and the outer side of the plastic plate 45 is provided with anti-slip grooves, and a groove is opened inside the electrolytic cell body 1, and the size of the groove is adapted to the size of the positioning connecting block 46.

[0025] The working principle of the utility model is as follows: the device is provided with a reinforcement device 3, firstly, the annular silicone pad 8 is installed, then the circular aluminum foil 6 is installed, and then the variable diameter copper electrode 5 is installed, and then the fastening screw 7 can be installed, and finally the outer screw buckle is installed. Through the threaded connection between the outer screw buckle and the corresponding inner screw buckle, the variable diameter copper electrode 5, the circular aluminum foil 6, the fastening screw 7 and the annular silicone pad 8 can be easily completed, and the function of preventing liquid leakage is played. Before electrodeposition, the carbon rod is placed at the diagonal position of the two electrode holes, and a suitable deflection electric field is applied at the same time, and the electrodeposition experiment can be carried out, and two "twin" AAO composite films with exactly the same microstructure and two identical structural colors and magnetic properties are prepared at the same time, that is, a highly saturated strip iridescent structural color magnetic alumina film, and after being fixedly connected between the electrolytic cell main body 1 and the mounting seat 2, the plastic rod 34 can be moved to drive the sliding block 32 to move, Move the movable connecting sleeve 33 on the outside of the sliding block 32 so that the movable connecting sleeve 33 is movably sleeved on the outside of the connecting threaded rod 37, and finally use the connecting threaded column 38 and the connecting threaded rod 37 to threadably connect, so as to conveniently complete the fixation between the movable connecting sleeve 33 and the mounting fixing pad 35, thereby improving the connection stability between the electrolytic cell body 1 and the mounting seat 2, and facilitating stable placement; the device is provided with a connecting device 4, and when the electrolytic cell body 1 and the mounting seat 2 are fixedly connected, the supporting spring 42 in the fixed shell 41 can provide elastic force to push the movable connecting pad 43, so that the movable connecting pad 43 drives the movable limiting rod 44 and the plastic plate 45 to move, and the positioning connecting block 46 at one end of the movable connecting pad 43 is movably inserted into the preset groove of the corresponding electrolytic cell body 1, thereby completing the reinforcement of the connection part between the mounting seat 2 and the electrolytic cell body 1 and improving the connection stability.

[0026] The above are only preferred specific implementation methods of the utility model, but the protection scope of the utility model is not limited to this. Any technician familiar with the technical field within the technical scope disclosed by the utility model, who makes equivalent replacements or changes based on the technical scheme and utility model concept of the utility model, should be covered by the protection scope of the utility model.

Claims

1. An electrolytic cell for realizing two deposition electric fields as mutually deflecting electric fields, comprising an electrolytic cell body (1), characterized in that: A mounting seat (2) is fixed at the bottom of the electrolytic cell body (1), a reinforcing device (3) is arranged on the outside of the electrolytic cell body (1), a connecting device (4) is installed on the top of the mounting seat (2), a variable diameter copper electrode (5) extending to the outside is arranged inside the electrolytic cell body (1), one end of the variable diameter copper electrode (5) is connected to a circular aluminum foil (6), one side of the circular aluminum foil (6) is connected to a fastening screw (7), and an annular silicone pad (8) is arranged on the outside of the variable diameter copper electrode (5); The reinforcing device (3) comprises a guide plate (31), the outer side of the guide plate (31) is slidably connected to a sliding block (32) via a sliding groove, the outer side of the sliding block (32) is fixed with a movable connecting sleeve (33), the outer side of the movable connecting sleeve (33) is installed with a plastic rod (34), the top of the mounting seat (2) is fixed with a mounting fixing pad (35), the top of the mounting fixing pad (35) is provided with a positioning sleeve (36), the top of the mounting fixing pad (35) is fixed with a connecting threaded rod (37), and the outer side of the connecting threaded rod (37) is threadedly connected with a connecting threaded column (38).

2. The electrolytic cell for realizing two deposition electric fields as mutually deflecting electric fields according to claim 1, characterized in that: The connecting device (4) comprises a fixed shell (41), a support spring (42) is arranged on an inner wall of one side of the fixed shell (41), one end of the support spring (42) is connected to a movable connection pad (43), one side of the movable connection pad (43) is fixed with a movable limit rod (44) passing through the other side thereof, one end of the movable limit rod (44) is fixed with a plastic plate (45), and one end of the movable limit rod (44) is provided with a positioning connection block (46).

3. The electrolytic cell for realizing two deposition electric fields as mutually deflecting electric fields according to claim 2, characterized in that: The fixed housing (41) and the mounting seat (2) are fixedly connected, and the outer side of the plastic plate (45) is provided with anti-slip grooves.

4. The electrolytic cell for realizing two deposition electric fields as mutually deflecting electric fields according to claim 2, characterized in that: A groove is provided inside the electrolytic cell body (1), and the size of the groove matches the size of the positioning connection block (46).

5. The electrolytic cell for realizing two deposition electric fields as mutually deflecting electric fields according to claim 1, characterized in that: The guide plate (31) and the electrolytic cell body (1) are fixedly connected, and a groove matching the size of the connecting threaded rod (37) is provided on the outer side of the movable connecting sleeve (33).

6. The electrolytic cell for realizing two deposition electric fields as mutually deflecting electric fields according to claim 1, characterized in that: A through hole is provided inside the positioning sleeve (36), and the size of the through hole matches the size of the movable connection sleeve (33).