High-flux preparation device for synthesizing electrode material precursor based on solution method
By designing a high-throughput preparation device based on solution method, the problems of long experimental cycles and high trial and error costs in the synthesis of traditional electrode materials are solved, and efficient and automated preparation of electrode material precursors is realized, which significantly shortens the development cycle and R&D costs.
Patent Information
- Application Number
- CN202421249247.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-05-31
- Publication Date
- 2025-02-11
- Estimated Expiration
- 2034-05-31
AI Technical Summary
Traditional synthetic electrode materials have long experimental cycles and high trial and error costs, making it difficult to efficiently prepare electrode material precursors.
A high-throughput preparation device based on the solution method is designed, including a first pipetting assembly, a second pipetting assembly, a flow distribution assembly and a heating oscillation platform, and the electrode material precursor is realized through an automated solution spraying and mixing process. Efficient preparation.
The device can automatically prepare electrode material precursors, simplify process flow, significantly shorten development cycles and R&D costs, and achieve a large number of experimental results in one run.
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Figure CN222446361U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of high-throughput material preparation devices, in particular to a high-throughput preparation device for synthesizing electrode material precursors based on a solution method. Background Art
[0002] At present, high-throughput preparation technologies represented by magnetron sputtering, diffusion multi-node method, and combined material thin film preparation method are limited to the preparation of alloy materials and oxide materials, and there is little research on the application of high-throughput technology to the preparation of electrode materials.
[0003] In the traditional electrode material synthesis process, artificial synthesis is mostly used, which has many problems. For example, the traditional artificial synthesis experimental method has the disadvantages of long experimental cycle and high trial and error cost. Utility Model Content
[0004] The utility model aims to provide a high-throughput preparation device for synthesizing electrode material precursors based on a solution method, so as to alleviate the technical problems of long experimental cycle and high trial and error cost in the traditional artificial synthesis experimental method in the prior art.
[0005] The utility model provides a high-throughput preparation device for synthesizing electrode material precursors based on a solution method, comprising: a first liquid transfer component, a second liquid transfer component, a flow distribution component and a heating and shaking platform;
[0006] The first pipetting component extends along a first direction, the second pipetting component extends along a second direction, the second pipetting component is slidably connected to the first pipetting component, and the first direction is perpendicular to the second direction;
[0007] The heating and shaking platform is arranged below the second liquid transfer component, and a plurality of sample slots arranged in an array are arranged on the heating and shaking platform;
[0008] The flow distribution component is slidably connected to the second pipetting component. The flow distribution component includes a liquid storage component and a nozzle. The nozzle is connected to the liquid storage component. The liquid storage component is used to store multiple solutions. The solutions in the liquid storage component can enter the sample tank through the nozzle.
[0009] In an alternative embodiment,
[0010] The first pipetting assembly includes a first lead screw and a first slide rail, and the second pipetting assembly includes a first connecting member;
[0011] The first slide rail is arranged parallel to the first lead screw;
[0012] The first connecting member is threadedly connected to the first lead screw and is slidably connected to the first slide rail;
[0013] The first lead screw can rotate around its own axis to drive the first connecting member to move along the first direction.
[0014] In an alternative embodiment,
[0015] The first pipetting assembly also includes a first driving member and a first supporting base;
[0016] The first driving member is connected to the first supporting base, and the output end is connected to the first lead screw;
[0017] The first supporting base is connected below the first slide rail.
[0018] In an alternative embodiment,
[0019] The second liquid transfer assembly includes a second lead screw and a second slide rail, and the flow distribution assembly includes a second connecting member;
[0020] The second slide rail is arranged in parallel with the second lead screw, and the second slide rail is connected to the first connecting member;
[0021] The second connecting member is threadedly connected to the second lead screw and is slidably connected to the second slide rail;
[0022] The second lead screw can rotate around its own axis to drive the second connecting member to move along the second direction.
[0023] In an alternative embodiment,
[0024] The second pipetting assembly also includes a second driving member and a second supporting base;
[0025] The second driving member is connected to the second supporting base, and the output end is connected to the second lead screw;
[0026] The second supporting base is connected below the second slide rail.
[0027] In an alternative embodiment,
[0028] A plurality of evenly arranged liquid storage tubes are arranged in the liquid storage component.
[0029] In an alternative embodiment,
[0030] The flow distribution assembly also includes a high-precision flow controller;
[0031] The input end of the high-precision flow controller is connected to the liquid storage component, and the output end is connected to the nozzle. The high-precision flow controller is used to control the liquid inlet flow of solutions of different components in the liquid storage tube.
[0032] In an alternative embodiment,
[0033] The flow distribution assembly also includes a detachable connector;
[0034] The detachable connector is arranged between the liquid storage component and the high-precision flow controller, the input end is communicated with the liquid storage component, and the output end is communicated with the high-precision flow controller.
[0035] In an alternative embodiment,
[0036] It also includes a central control platform and sensors for positioning;
[0037] The central control platform is electrically connected to the first pipetting component, the second pipetting component, the flow distribution component and the heating and shaking platform;
[0038] The sensor is connected to the second pipetting component.
[0039] In an alternative embodiment,
[0040] A resistance wire heating base is also arranged in the heating and oscillating platform, and the resistance wire heating base is arranged at the bottom of the sample tank.
[0041] The utility model provides a high-throughput preparation device for synthesizing electrode material precursors based on a solution method. By setting a first pipetting component, a second pipetting component and a flow distribution component can be moved along a first direction. By setting a second pipetting component, the flow distribution component can be moved along a second direction. Since the first direction is perpendicular to the second direction, the solution in the liquid storage component can be sprayed into each sample slot on the heating and oscillating platform through a nozzle. The device can realize automatic preparation of electrode material precursors. The entire preparation process is simple, and a large number of experimental results can be obtained in one operation, which greatly shortens the development cycle and R&D cost of electrode materials. BRIEF DESCRIPTION OF THE DRAWINGS
[0042] In order to more clearly illustrate the specific implementation methods of the utility model or the technical solutions in the prior art, the drawings required for use in the specific implementation methods or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are some implementation methods of the utility model. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative work.
[0043] Figure 1 A front view of a high-throughput preparation device for synthesizing electrode material precursors based on a solution method provided in an embodiment of the utility model;
[0044] Figure 2 It is a structural schematic diagram of a liquid storage component;
[0045] Figure 3 Schematic diagram of the structure of the heating and oscillating platform.
[0046] Icons: 100-first pipetting assembly; 110-first lead screw; 120-first slide rail; 130-first driving member; 140-first supporting base; 200-second pipetting assembly; 210-first connecting member; 220-second lead screw; 230-second slide rail; 240-second driving member; 250-second supporting base; 300-flow distribution assembly; 310-liquid storage member; 311-liquid storage tube; 320-nozzle; 330-second connecting member; 340-high-precision flow controller; 350-detachable connector; 400-heating and oscillating platform; 410-sample slot; 420-resistance wire heating base; 500-central control platform; 600-sensor. DETAILED DESCRIPTION
[0047] The technical solution of the utility model will be described clearly and completely below in conjunction with the accompanying drawings. Obviously, the described embodiments are part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments of the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.
[0048] In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", etc., indicating the orientation or positional relationship, are based on the orientation or positional relationship shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as limiting the present invention. In addition, the terms "first", "second", and "third" are used for descriptive purposes only, and cannot be understood as indicating or implying relative importance.
[0049] In the description of the present invention, it should be noted that, unless otherwise clearly specified and limited, the terms "installation", "connection" and "connection" should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection, or it can be indirectly connected through an intermediate medium, or it can be the internal communication of two components. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.
[0050] The specific implementation of the present invention is described in detail below in conjunction with the accompanying drawings. It should be understood that the specific implementation described here is only used to illustrate and explain the present invention, and is not used to limit the present invention.
[0051] like Figure 1 , Figure 2 and Figure 3 As shown, this embodiment provides a high-throughput preparation device for synthesizing electrode material precursors based on a solution method, including: a first pipetting component 100, a second pipetting component 200, a flow distribution component 300 and a heating and shaking platform 400; the first pipetting component 100 extends along a first direction, the second pipetting component 200 extends along a second direction, the second pipetting component 200 is slidably connected to the first pipetting component 100, and the first direction and the second direction are vertically arranged; the heating and shaking platform 400 is arranged below the second pipetting component 200, and a plurality of sample slots 410 arranged in an array are arranged on the heating and shaking platform 400; the flow distribution component 300 is slidably connected to the second pipetting component 200, and the flow distribution component 300 includes a liquid storage component 310 and a nozzle 320, the nozzle 320 is connected to the liquid storage component 310, the liquid storage component 310 is used to store a variety of solutions, and the solution in the liquid storage component 310 can enter the sample slot 410 through the nozzle 320.
[0052] The high-throughput preparation device for synthesizing electrode material precursors based on the solution method provided in this embodiment enables the second pipetting component 200 and the flow distribution component 300 to move in a first direction by setting the first pipetting component 100, and enables the flow distribution component 300 to move in a second direction by setting the second pipetting component 200. Since the first direction is perpendicular to the second direction, the solution in the liquid storage component 310 can be sprayed into each sample slot 410 on the heating and oscillating platform 400 through the nozzle 320. The device can realize automatic preparation of electrode material precursors. The entire preparation process is simple and a large number of experimental results can be obtained in one operation, which greatly shortens the development cycle and R&D cost of electrode materials.
[0053] Regarding the shape and structure of the first pipetting component 100, in detail:
[0054] like Figure 1 As shown, the first moving component includes a first lead screw 110 and a first slide rail 120, both of which extend along the first direction, and the first slide rail 120 is arranged below the first lead screw 110 and parallel to the first lead screw 110; the second pipetting component 200 includes a first connecting member 210, which is threadedly connected to the first lead screw 110 and slidably connected to the first slide rail 120; the first lead screw 110 can rotate around its own axis to drive the first connecting member 210 to move along the first direction.
[0055] Specifically, the first connecting member 210 is sleeved on the first lead screw 110 and is threadedly connected to the first lead screw 110. The bottom of the first connecting member 210 extends into the first slide rail 120 and is slidably connected to the first slide rail 120. The first slide rail 120 plays a role of limiting and guiding. When the first lead screw 110 rotates around its own axis, due to the limitation of the first slide rail 120, the first connecting member 210 can move along the length direction (i.e., the first direction) of the first lead screw 110. The first connecting member 210 can be specifically configured as a slider, and the slider has a through hole, and the inner wall of the through hole is provided with a thread. The slider is sleeved on the first lead screw 110, and the internal thread of the slider matches the external thread of the first lead screw 110. The slider is threadedly connected to the first lead screw 110. Since the structure of the slider is an existing structure, it is not repeated here.
[0056] In an optional embodiment, in order to enable the first screw 110 to rotate, the first moving assembly is also provided with a first driving member 130. The first driving member 130 can be specifically configured as a stepping motor. The output end of the first driving member 130 is connected to the first screw 110, and the first driving member 130 drives the first screw 110 to rotate around its own axis.
[0057] In an optional embodiment, the first moving assembly is further provided with a first support base 140 , the first driving member 130 is connected to the first support base 140 , and the first support base 140 is connected below the first slide rail 120 .
[0058] Specifically, a plurality of first support bases 140 may be provided, the first driving member 130 may be fixedly connected to the first support base 140 near the first driving member 130 through a connecting plate, a support frame is provided on the first support base 140, one end of the first lead screw 110 passes through the support frame and is connected to the output shaft of the motor, and the end of the first lead screw 110 is rotatably connected to the support frame, and the other end of the first lead screw 110 is rotatably connected to a support frame provided on another first support base 140. Preferably, in order to make the first lead screw 110 rotate smoothly, the first lead screw 110 and the support frame may be connected through a bearing. The remaining first support bases 140 may be evenly distributed at the bottom of the first slide rail 120 to play a supporting role.
[0059] Regarding the shape and structure of the second pipetting component 200, in detail:
[0060] like Figure 1As shown, the second pipetting assembly 200 includes a second lead screw 220 and a second slide rail 230, both of which extend in the second direction, and the second slide rail 230 is arranged below the second lead screw 220, and the second slide rail 230 is arranged in parallel with the second lead screw 220; the second slide rail 230 is connected to the top of the first connecting member 210, and in order to make the movement of the second slide rail 230 more stable, the number of the first connecting members 210 is set to two, and the two first connecting members 210 are respectively connected to the bottom ends of the second slide rail 230, and correspondingly, the first pipetting assembly 100 is also provided with two groups, and the two groups of first pipetting assemblies 100 are arranged in parallel, and the two first connecting members 210 are respectively slidably connected with the two first lead screws 110. The flow distribution assembly 300 includes a second connecting member 330, which is threadedly connected to the second lead screw 220 and slidably connected to the second slide rail 230, and the second lead screw 220 can rotate around its own axis to drive the second connecting member 330 to move in the second direction.
[0061] Specifically, the second connecting member 330 is sleeved on the first lead screw 110 and is threadedly connected to the second lead screw 220. The bottom of the second connecting member 330 extends into the second slide rail 230 and is slidably connected to the second slide rail 230. The second slide rail 230 plays a role of limiting and guiding. When the second lead screw 220 rotates around its own axis, due to the limitation of the second slide rail 230, the second connecting member 330 can move along the length direction (i.e., the second direction) of the second lead screw 220. The second connecting member 330 can be specifically configured as a slider, the slider has a through hole, and the inner wall of the through hole is provided with a thread. The slider is sleeved on the second lead screw 220, the internal thread of the slider matches the external thread of the second lead screw 220, and the slider is threadedly connected to the second lead screw 220. Since the structure of the slider is an existing structure, it is not repeated here.
[0062] In an optional embodiment, in order to enable the second lead screw 220 to rotate, the second moving assembly is further provided with a second driving member 240. The second driving member 240 can be specifically configured as a stepping motor. The output end of the second driving member 240 is connected to the second lead screw 220. The second driving member 240 drives the second lead screw 220 to rotate around its own axis.
[0063] In an optional embodiment, the second moving assembly is further provided with a second support base 250 , the second driving member 240 is connected to the second support base 250 , and the second support base 250 is connected below the second slide rail 230 .
[0064] Specifically, the second support base 250 is connected to the bottom of the second slide rail 230 and to the top of the first connection member 210. The second support base 250 plays a role of supporting and strengthening stability. At least two second support bases 250 may be provided. The second driving member 240 may be fixedly connected to the second support base 250 near the second driving member 240 through a connecting plate. A support frame is provided on the second support base 250. One end of the second lead screw 220 passes through the support frame and is connected to the output shaft of the motor. One end of the second lead screw 220 is rotatably connected to the support frame, and the other end of the second lead screw 220 is rotatably connected to the support frame provided on another second support base 250. Preferably, in order to make the second lead screw 220 rotate smoothly, the second lead screw 220 and the support frame may be connected through a bearing.
[0065] Preferably, the traversal speeds of the first pipetting component 100 and the second pipetting component 200 can be divided into three speeds of high, medium and low speeds with an adjustment speed range of 0-3m / s, wherein the maximum speed does not exceed 3m / s because too high a speed will cause the stepper motor to slip and lose the transmission effect.
[0066] Regarding the shape and structure of the heating and shaking platform 400, in detail:
[0067] like Figure 3 As shown, the heating and shaking platform 400 is disposed below the second pipetting component 200 , and a plurality of sample slots 410 arranged in an array are disposed on the heating and shaking platform 400 .
[0068] Specifically, the two groups of first pipetting components 100 are symmetrically arranged on both sides of the heating and oscillating platform 400. The heating and oscillating platform 400 in this embodiment is a multi-channel heating and oscillating platform 400. The slot group of the multi-channel heating and oscillating platform 400 is arranged on the platform in a 7×7 array. A resistance wire heating base 420 is provided at the bottom of each sample slot 410. The resistance wire heating base 420 is a heating function realized by the resistance wire provided at the bottom of the sample slot 410.
[0069] In an optional embodiment, the heating oscillation platform 400 can achieve an oscillation frequency of 0-50 Hz, and the resistance wire heating base 420 can control the temperature of the solution medium in the sample tank 410 to be between 70-100°C.
[0070] In an optional embodiment, the capacity of the sample tank 410 may be set between 50-200 mL. The reason is that a capacity exceeding 200 mL may cause the solution to spill out of the sample tank 410 during the shaking process, while a capacity that is too low may result in insufficient mixing of the solution.
[0071] Regarding the shape and structure of the flow distribution component 300, in detail:
[0072] like Figure 2 As shown, the flow distribution component 300 in this embodiment is a multi-channel flow distribution component 300, and the flow distribution component 300 includes a liquid storage component 310 and a nozzle 320. The nozzle 320 is connected to the liquid storage component 310. The liquid storage component 310 is used to store a variety of solutions. The solution in the liquid storage component 310 can enter the sample tank 410 through the nozzle 320. A plurality of uniformly arranged liquid storage tubes 311 are provided in the liquid storage component 310.
[0073] In an optional embodiment, the flow distribution assembly 300 further includes a high-precision flow controller 340; the input end of the high-precision flow controller 340 is connected to the liquid storage component 310, and the output end is connected to the nozzle 320. The high-precision flow controller 340 is used to control the liquid inlet flow of different component solutions in the liquid storage tube 311. The high-precision flow controller 340 can independently control the flow of each channel.
[0074] Specifically, the liquid storage component 310 is a multi-channel liquid storage tank, which is composed of 8 independent liquid storage tubes 311. Through the high-precision flow controller 340, the liquid inlet flow rate of different component solutions in the liquid storage tube 311 can be independently controlled, and finally added to the sample tank 410 through the nozzle 320.
[0075] In an optional embodiment, in order to facilitate cleaning and replacement of the multi-channel liquid storage tank, it is connected to the flow controller via a detachable connector. The detachable connector 350 is arranged between the liquid storage component 310 and the high-precision flow controller 340, and the input end is connected to the liquid storage component 310, and the output end is connected to the high-precision flow controller 340.
[0076] In order to achieve automation and precise control, the present embodiment is also provided with a central control platform 500 and a sensor 600 for positioning. The central control platform 500 is electrically connected to the first pipetting component 100, the second pipetting component 200, the flow distribution component 300 and the heating and shaking platform 400; the sensor 600 is connected to the second pipetting component 200.
[0077] Specifically, the first pipetting component 100, the second pipetting component 200, the flow distribution component 300 and the heating and shaking platform 400 are all connected to the central control platform 500 through control lines. The first pipetting component 100 and the second pipetting component 200 control the motor and the screw rod through the preset program of the central control platform 500 to allow the connecting component to adjust the position of the flow distribution component 300, wherein the role of the sensor 600 is mainly to play a positioning role. With the cooperation of the first pipetting component 100 and the second pipetting component 200, the flow distribution component 300 can be controlled to traverse each sample slot 410 according to the preset program.
[0078] In view of the many problems existing in the traditional electrode material synthesis process, such as long experimental cycle, high cost, and complicated steps, this embodiment provides a high-throughput preparation device. The high-throughput preparation device utilizes a high-throughput, automated solution to automatically prepare electrode material precursors with various doping ratios. The entire preparation process is simple and a large number of experimental results can be obtained in one run, which greatly shortens the development cycle and R&D cost of electrode materials.
[0079] The following specifically lists examples of high-throughput preparation of multi-element doped sodium superionic conductor-type electrode material precursors.
[0080] Example 1
[0081] Sodium salts (including but not limited to sodium acetate, sodium oxalate, sodium carbonate), iron salts (including but not limited to ferrous acetate, ferrous oxalate, ferrous acetylacetonate), vanadium salts (including but not limited to ammonium metavanadate, vanadium acetylacetonate), phosphates (ammonium dihydrogen phosphate or phosphoric acid) and citric acid are configured into solutions of different concentrations according to different molar ratios and added into the liquid storage tube 311. Then, the first pipetting component 100 and the second pipetting component 200 will control the flow distribution component 300 to traverse the sample slot 410 array according to the set program. Finally, the solution is evenly mixed in the heating and shaking platform 400 and the corresponding precursor can be obtained after the solution is evaporated. In one embodiment, different proportions of iron can replace vanadium to synthesize the precursor of sodium iron vanadium phosphate.
[0082] Example 2
[0083] Sodium salts (including but not limited to sodium acetate, sodium oxalate, sodium carbonate), manganese salts (including but not limited to manganese acetate, manganese oxalate, manganese acetylacetonate), vanadium salts (including but not limited to ammonium metavanadate, vanadium acetylacetonate), phosphates (ammonium dihydrogen phosphate or phosphoric acid) and citric acid are configured into solutions of different concentrations according to different molar ratios and added into the liquid storage tube 311. Then, the first pipetting component 100 and the second pipetting component 200 will control the flow distribution component 300 to traverse the sample slot 410 array according to the set program. Finally, the solution is evenly mixed in the heating and shaking platform 400 and the solution is evaporated to obtain the corresponding precursor. In one embodiment, manganese can be substituted for vanadium in different proportions to synthesize the precursor of sodium manganese vanadium phosphate.
[0084] Example 3
[0085] Sodium salts (including but not limited to sodium acetate, sodium oxalate, sodium carbonate), titanium salts (including but not limited to titanium trichloride, ethanol titanium salts), vanadium salts (including but not limited to ammonium metavanadate, vanadium acetylacetonate), phosphates (ammonium dihydrogen phosphate or phosphoric acid) and citric acid are configured into solutions of different concentrations in different molar ratios and added into the liquid storage tube 311. Then, the first pipetting component 100 and the second pipetting component 200 will control the flow distribution component 300 to traverse the sample slot 410 array according to the set program. In one embodiment, different proportions of titanium can replace vanadium to synthesize the precursor of sodium titanium vanadium phosphate.
[0086] Example 4
[0087] Sodium salts (including but not limited to sodium acetate, sodium oxalate, sodium carbonate), iron salts (including but not limited to ferrous acetate, ferrous oxalate, ferrous acetylacetonate), manganese salts (including but not limited to manganese acetate, manganese oxalate, manganese acetylacetonate), titanium salts (including but not limited to titanium trichloride, titanium ethanolate), vanadium salts (including but not limited to ammonium metavanadate, vanadium acetylacetonate), phosphates (ammonium dihydrogen phosphate or phosphoric acid) and citric acid are configured into solutions of different concentrations in different molar ratios and added into the liquid storage tube 311, and then the first pipetting component 100 and the second pipetting component 200 will control the flow distribution component 300 to traverse the sample slot 410 array according to the set program. In one embodiment, different proportions of iron, manganese and titanium can replace vanadium to synthesize the precursor of sodium titanium iron manganese vanadium phosphate.
[0088] Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the utility model, rather than to limit it. Although the utility model has been described in detail with reference to the aforementioned embodiments, ordinary technicians in this field should understand that they can still modify the technical solutions recorded in the aforementioned embodiments, or replace some or all of the technical features therein with equivalents. However, these modifications or replacements do not make the essence of the corresponding technical solution deviate from the scope of the technical solution of the embodiments of the utility model.
Claims
1. A high-throughput preparation device for synthesizing electrode material precursors based on a solution method, characterized in that: include: A first pipetting component (100), a second pipetting component (200), a flow distribution component (300) and a heating and shaking platform (400); The first pipetting component (100) extends along a first direction, the second pipetting component (200) extends along a second direction, the second pipetting component (200) is slidably connected to the first pipetting component (100), and the first direction is perpendicular to the second direction; The heating and shaking platform (400) is arranged below the second liquid transfer component (200), and a plurality of sample slots (410) arranged in an array are arranged on the heating and shaking platform (400); The flow distribution component (300) is slidably connected to the second pipetting component (200), and the flow distribution component (300) includes a liquid storage component (310) and a nozzle (320). The nozzle (320) is connected to the liquid storage component (310), and the liquid storage component (310) is used to store a variety of solutions. The solution in the liquid storage component (310) can enter the sample tank (410) through the nozzle (320).
2. The high-throughput preparation device for synthesizing electrode material precursors based on a solution method according to claim 1, characterized in that: The first pipetting assembly (100) comprises a first lead screw (110) and a first slide rail (120), and the second pipetting assembly (200) comprises a first connecting member (210); The first slide rail (120) is arranged in parallel with the first lead screw (110); The first connecting member (210) is threadedly connected to the first lead screw (110) and is slidably connected to the first slide rail (120); The first lead screw (110) is capable of rotating around its own axis to drive the first connecting member (210) to move along the first direction.
3. The high-throughput preparation device for synthesizing electrode material precursors based on a solution method according to claim 2, characterized in that: The first pipetting assembly (100) further comprises a first driving member (130) and a first supporting base (140); The first driving member (130) is connected to the first supporting base (140), and the output end is connected to the first lead screw (110); The first supporting base (140) is connected below the first slide rail (120).
4. The high-throughput preparation device for synthesizing electrode material precursors based on a solution method according to claim 2, characterized in that: The second liquid transfer assembly (200) comprises a second lead screw (220) and a second slide rail (230), and the flow distribution assembly (300) comprises a second connecting member (330); The second slide rail (230) is arranged in parallel with the second lead screw (220), and the second slide rail (230) is connected to the first connecting member (210); The second connecting member (330) is threadedly connected to the second lead screw (220) and is slidably connected to the second slide rail (230); The second lead screw (220) is capable of rotating around its own axis to drive the second connecting member (330) to move along the second direction.
5. The high-throughput preparation device for synthesizing electrode material precursors based on a solution method according to claim 4, characterized in that: The second pipetting assembly (200) further comprises a second driving member (240) and a second supporting base (250); The second driving member (240) is connected to the second supporting base (250), and the output end is connected to the second lead screw (220); The second supporting base (250) is connected below the second slide rail (230).
6. The high-throughput preparation device for synthesizing electrode material precursors based on a solution method according to claim 2, characterized in that: A plurality of evenly arranged liquid storage tubes (311) are provided in the liquid storage component (310).
7. The high-throughput preparation device for synthesizing electrode material precursors based on a solution method according to claim 6, characterized in that: The flow distribution component (300) further includes a high-precision flow controller (340); The input end of the high-precision flow controller (340) is connected to the liquid storage component (310), and the output end is connected to the nozzle (320). The high-precision flow controller (340) is used to control the liquid inlet flow of solutions of different components in the liquid storage tube (311).
8. The high-throughput preparation device for synthesizing electrode material precursors based on a solution method according to claim 7, characterized in that: The flow distribution assembly (300) further comprises a detachable connector (350); The detachable connector (350) is disposed between the liquid storage component (310) and the high-precision flow controller (340), with an input end being connected to the liquid storage component (310) and an output end being connected to the high-precision flow controller (340).
9. The high-throughput preparation device for synthesizing electrode material precursors based on a solution method according to claim 1, characterized in that: It also includes a central control platform (500) and a sensor (600) for positioning; The central control platform (500) is electrically connected to the first pipetting component (100), the second pipetting component (200), the flow distribution component (300) and the heating and shaking platform (400); The sensor (600) is connected to the second pipetting component (200).
10. The high-throughput preparation device for synthesizing electrode material precursors based on a solution method according to claim 1, characterized in that: A resistance wire heating base (420) is also provided in the heating and oscillating platform (400), and the resistance wire heating base (420) is provided at the bottom of the sample tank (410).