Carotenoid microcapsule production mixing device
By designing a mixing device for carotenoid microcapsules, using a combination device of an emulsification tank and a drying tower, combined with mechanical stirring and ultrasonic dispersion technology, the problems of insufficient homogenization and inconvenient equipment cleaning in the existing technology are solved, and efficient and uniform microcapsule preparation and equipment cleaning are achieved.
Patent Information
- Application Number
- CN202421743222.8
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-07-22
- Publication Date
- 2025-06-03
- Estimated Expiration
- 2034-07-22
AI Technical Summary
In the preparation process of carotenoid microcapsules, the core material and wall material are not homogenized sufficiently, the temperature and pressure parameters are inconsistent, the presence of agitation blind spots, waste of raw materials and inconvenient equipment cleaning.
A carotenoid microcapsule production mixing device is designed, including an emulsification tank, a drying tower and an ultrasonic auxiliary stirring device. The emulsification tank is equipped with a mixing motor, a mixing rod, a scraper and an ultrasonic auxiliary stirring device. The full mixing and emulsification of raw materials can be achieved through mechanical stirring and ultrasonic dispersion technology. The drying tower is used for spray granulation and hot air drying to ensure rapid molding of microcapsule granules.
It significantly improves the utilization rate of raw materials and emulsification effect, ensures the consistent quality of microcapsules produced in each batch, reduces material liquid residues and bacterial growth, and improves production efficiency and equipment cleaning efficiency.
Smart Images

Figure CN222930714U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the field of carotenoid microcapsule preparations, and particularly to a mixing device for producing carotenoid microcapsules. Background Art
[0002] The statements herein only provide background art related to the utility model and do not necessarily constitute prior art.
[0003] Carotenoids are important vitamin A source substances, which play an important role in the visual development of the human body and alleviating visual fatigue. They also have the effects of neutralizing free radicals, playing antioxidant, immune regulation, anti-cancer, anti-aging and other functions. However, since the human body cannot synthesize carotenoids de novo, people can only meet the body's needs by ingesting diets containing this substance such as fruits and vegetables. With the development of technology, relevant devices can be used to artificially prepare carotenoid microcapsules to meet people's needs. However, during the preparation process, the inventor found the following prior art problems:
[0004] (1) The utility model patent with the patent number CN221182713 discloses a microcapsule coating device. Although it can reduce the residue of preparation raw materials and the growth of bacteria, the efficient homogenization of the core material and the wall material cannot be achieved only by the rotation of the stirring rod in the processing cylinder, and the parameters such as temperature and pressure in the processing cylinder cannot be ensured to be consistent, which is likely to cause great differences in the microcapsules produced in each batch.
[0005] (2) The utility model patent with the patent number CN220779982U discloses a microcapsule preparation device. Although the stirring efficiency of the mixed liquid is improved by opening turbulence holes on the stirring plate and the reverse rotation of the stirring tank and the stirring shaft, there are still stirring dead corners in the stirring tank, the homogenization efficiency is not significantly improved, and it is easy to cause the residue of the mixed liquid, waste raw materials, and the equipment is inconvenient to clean. Summary of the Utility Model
[0006] The purpose of the utility model is to provide a mixing device for producing carotenoid microcapsules, which includes an emulsifying tank, a drying tower, and an ultrasonic-assisted stirring device. The drying tower is located below the emulsifying tank, and the liquid outlet of the emulsifying tank is communicated with the drying tower; the drying tower and the emulsifying tank are fixedly connected by a first support frame;
[0007] The emulsifying tank includes a stirring motor fixed above the tank body. The output shaft of the stirring motor is connected to one end of a stirring rod. The stirring rod is located inside the tank body, and a first stirring blade is also provided on the stirring rod; the stirring rod is also connected to a stirring frame, and scrapers are fixed on both sides of the stirring frame; the stirring rod passes through the stirring frame, and a second stirring blade is also provided at the end of the stirring rod passing through the stirring frame; a feed inlet is also provided above the emulsifying tank, and a heating device is fixed on the inner wall above the emulsifying tank;
[0008] The ultrasonic-assisted stirring device includes an ultrasonic generator, a transducer, and a horn; the transducer is fixed on the inner walls on both sides of the emulsification tank, and the transducer is connected to the horn; the ultrasonic generator is placed outside the housing and is communicatively connected to the transducer.
[0009] As a further technical solution, the feed inlet is funnel-shaped.
[0010] As a further technical solution, a drain pipe is provided below the inner wall on one side of the emulsification tank, and an exhaust pipe is provided above the inner wall on the other side.
[0011] As a further technical solution, electromagnetic valves for controlling the on / off of the pipeline are provided on both the drain pipe and the exhaust pipe.
[0012] As a further technical solution, a temperature sensor and a pressure sensor are also provided inside the emulsification tank.
[0013] As a further technical solution, an atomizer is provided inside the liquid outlet of the emulsification tank, and the atomizing port of the atomizer is provided at the top of the drying tower, and the positions of the atomizer and the atomizing port correspond to each other.
[0014] As a further technical solution, the atomizer is also communicated with a ventilation duct, and air is supplied through a blower located outside.
[0015] As a further technical solution, an air heater is also provided in the ventilation duct.
[0016] As a further technical solution, the drying tower is funnel-shaped and is fixed to the ground through a second support frame.
[0017] As a further technical solution, a discharge port is provided below the drying tower, and a valve is installed on the discharge port.
[0018] The beneficial effects of the above one or more technical solutions:
[0019] (1) Mechanical stirring by the stirring blades and the scraper can cover the entire inner cavity of the emulsification tank, and an ultrasonic device is added. The mechanical effect and cavitation of ultrasonic waves are used to make the liquid material more dispersed, promote liquid emulsification, significantly improve the raw material utilization rate and emulsification effect, and greatly improve the production efficiency. After the preparation is completed, through the mutual cooperation of the stirring blades, the scraper and the ultrasonic waves, the emulsification tank can be quickly and efficiently cleaned, avoiding pollution such as liquid material residue and bacterial growth.
[0020] (2) The temperature and pressure inside the tank are detected by the pressure sensor and the temperature sensor, and the heating device is used in cooperation with the exhaust pipe and the drain pipe to ensure that the temperature and pressure parameters inside the emulsification tank are consistent.
[0021] (3) An atomizer is also provided in the liquid outlet of the emulsifying tank, and the atomizer is communicated with the ventilation duct. The air heater located in the ventilation duct can heat the air blown by the blower. The high-temperature and high-pressure air enters the atomizer, which can not only maintain the high temperature of the emulsion, but also make the microcapsule particles quickly form through hot air drying, significantly improving the embedding rate and production efficiency. BRIEF DESCRIPTION OF THE DRAWINGS
[0022] The accompanying drawings forming a part of this application are used to provide a further understanding of this application. The schematic embodiments of this application and their descriptions are used to explain this application and do not constitute a limitation to this application.
[0023] Figure 1 It is a schematic diagram of the overall structure of the present utility model.
[0024] Figure 2 It is a schematic diagram of the external structure of the present utility model.
[0025] Figure 3 It is a schematic diagram of the structure of the emulsifying tank in the present utility model.
[0026] In the figure, 1. emulsifying tank; 2. drying tower; 3. feed inlet; 4. stirring motor; 5. stirring rod; 6. first stirring blade; 7. second stirring blade; 8. stirring frame; 9. scraper; 10. heating device; 11. transducer; 12. amplitude transformer; 13. ultrasonic generator; 14. temperature sensor; 15. pressure sensor; 16. drain pipe; 17. exhaust pipe; 18. first support frame; 19. atomizer; 20. atomizing port; 21: ventilation duct; 22. air heater; 23. blower; 24. discharge port; 25. valve; 26. second support frame. DETAILED DESCRIPTION OF THE EMBODIMENTS
[0027] The following will describe the specific implementation manners of this embodiment with reference to the attached Figures 1-3 , explaining the specific implementation manners of this embodiment.
[0028] Carotenoids include one or more of lutein, zeaxanthin, astaxanthin, lycopene, carotene, β-carotene, fucoxanthin, cryptoxanthin, capsanthin. In this embodiment, the preparation of lutein, lutein esters, astaxanthin, and astaxanthin esters is taken as an example, and other types of carotenoids can also be prepared, which does not constitute a limitation to this application.
[0029] The embodiment of this application provides a mixing device for producing carotenoid microcapsules. Refer to Figures 1-3, a carotenoid microcapsule production mixing device, including an emulsification tank 1, a drying tower 2 and an ultrasonic assisted stirring device, wherein the drying tower 2 and the emulsification tank 1 are fixedly connected by a first support frame 18, the drying tower 2 is located below the emulsification tank 1, and the drying tower 2 is fixed to the ground by a second support frame 26. The emulsification tank 1 includes a stirring motor 4 fixed above the tank body, the output shaft of the stirring motor 4 is connected to one end of a stirring rod 5, the stirring rod 5 is located inside the tank body, and the stirring rod 5 is also provided with a first stirring blade 6. In this embodiment, the number of the first stirring blade 6 can be set according to specific circumstances. In addition, the stirring rod 5 is also connected to a stirring frame 8, the stirring frame 8 is rectangular, and scrapers 9 are fixed on both sides of the stirring frame 8; the outer side of the scraper 9 is in contact with the inner wall of the emulsification tank 1, and the scraper 9 is used to scrape the inner wall, which can prevent the raw materials for preparing lutein, lutein ester or astaxanthin, astaxanthin ester from sticking to the inner wall of the emulsification tank during the reaction, and can also use the scraper 9 to mix the above-mentioned raw materials more evenly. In addition, after the preparation is completed, the scraper 9 can be used to quickly and effectively clean the inner wall of the emulsification tank 1. One end of the stirring rod 5 is arranged through the stirring frame 8, and a second stirring blade 7 is also arranged on the end of the stirring rod 5 passing through the stirring frame 8; the second stirring blade 7 is located close to the bottom of the emulsification tank 1, and the volume of the second stirring blade 7 is slightly smaller than the first stirring blade 6, but the thickness of the second stirring blade 7 is wider, which is convenient for fully mixing the preparation materials of lutein or astaxanthin deposited at the bottom.
[0030] A feed port 3 is also provided above the emulsification tank 1. The feed port 3 is funnel-shaped, which is convenient for quickly adding lutein, lutein esters or astaxanthin, astaxanthin ester preparation raw materials during the preparation process. Since a certain temperature is required during the preparation process, a heating device 10 is also fixed on the inner wall above the emulsification tank 1 to adjust the temperature inside the emulsification tank 1.
[0031] In this embodiment, an ultrasonic auxiliary stirring device is also provided. Since ultrasonic waves have mechanical effects and cavitation effects, during the preparation process, the use of ultrasonic auxiliary stirring devices can effectively promote the mixing of the raw materials to be prepared more fully, promote liquid emulsification, and thus improve the utilization rate and emulsification effect of the raw materials, greatly improving the production efficiency. After the preparation is completed, the ultrasonic waves generated by the ultrasonic auxiliary stirring device can also be used to quickly and efficiently clean the inside of the emulsification tank 1, effectively avoiding contamination such as residual liquid and bacterial growth. The ultrasonic auxiliary stirring device includes an ultrasonic generator 13, a transducer 11 and a horn 12; wherein the horn 12 is connected to the transducer 11 and is embedded on both sides of the inner wall of the emulsification tank 1, and establishes a communication connection with the ultrasonic generator 13, and the ultrasonic generator 13 is used to control the generation time and frequency of the ultrasonic wave, and control the transducer 11 and the horn 12 to emit ultrasonic waves of a specific frequency. The above-mentioned ultrasonic wave generation process belongs to the existing technical means, and will not be described in detail here.
[0032] In order to monitor the preparation process in real time, a temperature sensor 14 and a pressure sensor 15 are also provided on the inner wall of the emulsifying tank 1, which are used to observe the temperature and pressure parameters in the emulsifying tank 1 in real time, and upload the above data to the terminal. If the monitored temperature and pressure values exceed the appropriate range, an alarm will be automatically issued for reminder. A drain pipe 16 is provided below the inner wall on one side of the emulsifying tank 1, and an exhaust pipe 17 is provided above the inner wall on the other side. Solenoid valves for controlling the on-off of the pipeline are provided on both the drain pipe 16 and the exhaust pipe 17. When the terminal issues an alarm, the air pressure inside the emulsifying tank 1 can be adjusted by opening the solenoid valves located on the drain pipe 16 and the exhaust pipe 17.
[0033] When the preparation raw materials are fully mixed and emulsified, they flow into the drying tower 2 through the liquid outlet of the emulsifying tank 1 for spray granulation. In this embodiment, an atomizer 19 is installed in the liquid outlet of the emulsifying tank 1, and the atomizing port 20 of the atomizer 19 is located at the top of the drying tower 2, and the positions of the atomizer 19 and the atomizing port 20 correspond to each other. In order to further improve the effect of spray granulation, the atomizer 19 in the liquid outlet of the emulsifying tank 1 is also communicated with a ventilation duct 21, and an air heater 22 is provided in the ventilation duct 21, which can heat the air sent by the air blower 23, so that the high-temperature and high-pressure air enters the atomizer 19. This can not only maintain the temperature of the emulsion, but also use the heated air to quickly form microcapsule particles, significantly improving the embedding rate and production efficiency. After the preparation liquid is atomized and dried to form microcapsule particles, they enter the drying tower 2, are quickly cooled and fixed in shape in the drying tower 2, and finally are collected in the collection box through the discharge port 24 below the drying tower 2. A valve 25 for controlling the on-off of the discharge port is provided on the discharge port, and a new collection box can be replaced at any time after the collection box is full.
[0034] The working principle of a carotenoid microcapsule production mixing device provided in this embodiment is as follows:
[0035] First, start the switches of the stirring motor 4, the heating device 10 and the ultrasonic assisted stirring device. Add the preparation raw materials of lutein, lutein ester or astaxanthin, astaxanthin ester into the emulsifying tank 1 through the feed port 3. Drive the first stirring blade 6, the second stirring blade 7, the stirring frame 8 and the scraper 9 to rotate through the stirring motor 4, and cooperate with the ultrasonic waves generated by the ultrasonic assisted stirring device to fully mix and emulsify the preparation raw materials. The fully mixed and emulsified liquid flows through the atomizer 19 for spray granulation. During the spray granulation process, the air blown by the air blower 23 is heated by the air heater 22 and then introduced into the atomizer 19 to spray granulate the fully mixed and emulsified liquid to form microcapsule particles. The microcapsule particles are quickly cooled and fixed in shape in the drying tower 2, and finally are collected in the collection box through the discharge port 24 below the drying tower 2.
[0036] After preparation, cleaning liquid is added through the feed inlet 3. By the mutual cooperation of the first stirring blade 6, the second stirring blade 7, the scraper 9 and ultrasonic waves, the material residues in the device are quickly cleaned through stirring and ultrasonic assistance, avoiding the pollution of materials in the next use, realizing the rapid and efficient cleaning of the emulsifying tank 1, avoiding pollution such as liquid residue and bacterial growth, and improving production efficiency.
[0037] Although the specific implementation manners of the present invention have been described above in conjunction with the accompanying drawings, it is not a limitation on the protection scope of the present invention. Those skilled in the art should understand that based on the technical solutions of the present invention, various modifications or deformations that can be made by those skilled in the art without creative efforts are still within the protection scope of the present invention.
Claims
1. A carotenoid microcapsule production mixing device, characterized in that: include: An emulsification tank, a drying tower and an ultrasonic auxiliary stirring device, wherein the drying tower is located below the emulsification tank, and the liquid outlet of the emulsification tank is connected to the drying tower; the drying tower and the emulsification tank are fixedly connected by a first support frame; The emulsification tank comprises a stirring motor fixed on the top of the tank body, the output shaft of the stirring motor is connected to one end of a stirring rod, the stirring rod is located inside the tank body, and a first stirring blade is provided on the stirring rod; the stirring rod is also connected to a stirring frame, and scrapers are fixed on both sides of the stirring frame; the stirring rod is arranged through the stirring frame, and a second stirring blade is also provided on one end of the stirring rod passing through the stirring frame; a feed port is also provided on the top of the emulsification tank, and a heating device is also fixed on the inner wall above the emulsification tank; The ultrasonic auxiliary stirring device comprises an ultrasonic generator, a transducer and an amplitude transformer; the transducer is fixed on the inner walls of both sides of the emulsification tank, and the transducer is connected to the amplitude transformer; the ultrasonic generator is placed outside the shell and is communicatively connected to the transducer.
2. A carotenoid microcapsule production mixing device as claimed in claim 1, characterized in that: The feed inlet is funnel-shaped.
3. A carotenoid microcapsule production mixing device as claimed in claim 1, characterized in that: A liquid discharge pipe is arranged below the inner wall of one side of the emulsification tank, and an exhaust pipe is arranged above the inner wall of the other side.
4. A carotenoid microcapsule production mixing device as claimed in claim 3, characterized in that: The liquid discharge pipe and the exhaust pipe are both provided with electromagnetic valves for controlling the on-off of the pipelines.
5. A carotenoid microcapsule production mixing device as claimed in claim 1, characterized in that: A temperature sensor and a pressure sensor are also arranged inside the emulsification tank.
6. A carotenoid microcapsule production mixing device as claimed in claim 1, characterized in that: An atomizer is arranged in the liquid outlet of the emulsification tank, and the atomization port of the atomizer is arranged at the top of the drying tower, and the positions of the atomizer and the atomization port correspond to each other.
7. A carotenoid microcapsule production mixing device as claimed in claim 6, characterized in that: The atomizer is also communicated with a ventilation duct, and air is supplied by an external blower.
8. A carotenoid microcapsule production mixing device as claimed in claim 7, characterized in that: An air heater is also provided in the ventilation duct.
9. A carotenoid microcapsule production mixing device as claimed in claim 1, characterized in that: The drying tower is funnel-shaped and is fixed to the ground via a second supporting frame.
10. A carotenoid microcapsule production mixing device as claimed in claim 1, characterized in that: A discharge port is provided below the drying tower, and a valve is installed on the discharge port.
Citation Information
Patent Citations
Plant omega-3 water-soluble microcapsule preparation device
CN220779982U