Reaction kettle for preparing lithium dihydrogen phosphate

By introducing a sealing mechanism and feed box into the reactor, the problem of steam burning operators during the preparation of lithium dihydrogen phosphate is solved, and safe and efficient feeding and sealing effects are achieved, improving operational safety and feeding efficiency.

CN223055602UActive Publication Date: 2025-07-04TONGLING SINCO FINE CHEM CO LTD
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Patent Information

Application Number
CN202422046240.7
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-08-22
Publication Date
2025-07-04
Estimated Expiration
2034-08-22

AI Technical Summary

Technical Problem

During the preparation of lithium dihydrogen phosphate in the existing reactor, the problems of high-temperature hot air drifting and steam burning operators, resulting in low feed efficiency and unsafety.

Method used

A reactor including a sealing mechanism and a feed box is designed. The sealing plate and sealing ring are driven by an electric telescopic rod to achieve reliable sealing of the discharge port, avoid steam dissipation, and ensure that the material enters the kettle body smoothly through the inclined plate guide.

Benefits of technology

Improve operational safety, ensure that the steam does not burn the staff, improve feeding efficiency and sealing effect, and facilitate cleaning and assembly.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model is suitable for the technical field of reaction kettles, and provides a reaction kettle for preparing lithium dihydrogen phosphate, which comprises a kettle body and a feeding pipe arranged on the kettle body, the connecting pipe is arranged on the feeding pipe; the feeding box is fixedly mounted on the connecting pipe; the group of connecting plates are arranged in the connecting pipe; the group of discharging openings are respectively formed in the group of connecting plates; and the sealing mechanism is arranged on the group of connecting plates and is used for sealing the discharge port. The reaction kettle for preparing lithium dihydrogen phosphate provided by the scheme has the advantage that materials can be safely added into the kettle body, so that steam in the kettle body cannot scald workers.
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Description

Technical Field

[0001] The utility model belongs to the technical field of reaction kettles, and particularly relates to a reaction kettle for preparing lithium dihydrogen phosphate. Background Technique

[0002] A reaction kettle is a reaction vessel for physical or chemical reactions, with excellent chemical stability and high structural strength. Through the structural design and parameter configuration of the container, heating, evaporation, cooling, and mixing functions at low and high speeds required by the process are achieved, and it is widely used in the production of petroleum, chemical industry, rubber, pesticides, medicine, food, coatings, paints, etc. In the preparation of lithium dihydrogen phosphate, lithium dihydrogen phosphate needs to be put into the reaction kettle for reaction.

[0003] Since the preparation of lithium dihydrogen phosphate requires a relatively high temperature, when the high-temperature hot gas generated during the preparation of lithium dihydrogen phosphate drifts through the feed hopper, it is easy to cause a relatively high temperature near the feed hopper. At the same time, when adding materials to the feed hopper, the steam in the kettle body is also easy to scald people, which is not convenient for the staff to feed materials into the reaction kettle through the feed hopper, not convenient for the normal operation of the staff, and reduces the feeding efficiency during the preparation of lithium dihydrogen phosphate. Content of the Utility Model

[0004] The utility model provides a reaction kettle for preparing lithium dihydrogen phosphate, aiming to solve the problem that it is inconvenient to add materials to the feed hopper during the operation of the currently used reaction kettle proposed in the above background technique.

[0005] To solve the above problems, the utility model is realized as follows. A reaction kettle for preparing lithium dihydrogen phosphate includes: a kettle body and a feed pipe installed on the kettle body; a connecting pipe provided on the feed pipe; a feed box fixedly installed on the connecting pipe and having an open top; two spaced-apart connecting plates installed radially in the connecting pipe; two discharge ports respectively opened in the centers of the two connecting plates; and a sealing mechanism provided on the connecting plate for sealing the discharge ports.

[0006] Preferably, the sealing mechanism includes: two sealing plates rotatably installed on the inner wall of the discharge port, and the two sealing plates are adapted to the discharge port when closed; connecting rods respectively hinged on the upper and lower corresponding sealing plates; two first electric telescopic rods hinged at the bottom of the upper connecting plate and on both sides of the discharge port, and the output rods of the two first electric telescopic rods are respectively hinged to the middle parts of the two connecting rods, and the two ends of the two connecting rods are respectively connected to the upper and lower corresponding sealing plates; and an auxiliary sealing mechanism provided in the feed box for assisting in sealing the discharge port.

[0007] Preferably, the auxiliary sealing mechanism includes: a fixing plate fixedly installed in the feeding box, the fixing plate being located above the discharging port; a second electric telescopic rod fixedly installed at the bottom of the fixing plate; a connecting plate installed on the output rod of the second electric telescopic rod, the connecting plate being in contact with the uppermost connecting plate; and a sealing ring installed at the bottom of the connecting plate.

[0008] Preferably, a cover plate is hinged to the top of the feeding box, a limiting block is fixedly installed on one side of the cover plate, an arc-shaped frame is fixedly installed on one side of the feeding box, and the output rod of the arc-shaped frame is rotatably connected to the limiting block.

[0009] Preferably, an inclined plate is installed at the bottom of the inner wall of the feeding box, the tops of the fixing plate and the connecting plate are both arc-shaped, rectangular frames are fixedly sleeved on both the feeding pipe and the connecting pipe near the butt joint surface of the feeding pipe and the connecting pipe, and the two rectangular frames are close to each other.

[0010] Preferably, a connecting piece is detachably arranged on the two rectangular frames, a sealing gasket is fixedly installed in the connecting piece, and the sealing gasket is in close contact with the two rectangular frames.

[0011] Preferably, the connecting piece is composed of two arc-shaped frames, two mounting plates, a positioning rod and a positioning block. The two arc-shaped frames are hinged, the two mounting plates are respectively installed on the two arc-shaped frames, the positioning rod is slidably installed on the two mounting plates, a mounting groove is opened at the top of the positioning rod, a return spring is fixedly installed in the mounting groove, the positioning block is fixedly installed at the top end of the return spring and is in sliding contact with the inner wall of the mounting groove, and the positioning block is in sliding contact with any one of the mounting plates.

[0012] Compared with the related art, the reaction kettle for preparing lithium dihydrogen phosphate provided by the utility model has the following beneficial effects:

[0013] 1. Through the combined use of the sealing mechanism and the feeding box, it can ensure that when adding materials to the kettle body, the staff will not contact water vapor, thereby improving the operation safety. The first electric telescopic rod drives the connecting rod to move, so that the connecting rod drives the sealing plate to move to open and close the sealing plate, which is beneficial to the subsequent discharging operation of the materials. Through the sealing ring and the connecting plate in contact with the connecting plate, the discharging port is sealed for the second time to ensure that the water vapor will not escape, and the sealing effect is good;

[0014] 2. The cover plate is fixed by the arc-shaped frame to ensure that the cover plate will not move randomly, and the fixing is relatively fast. Through the setting of the inclined plate, it can ensure that the materials in the feeding box are smoothly discharged into the kettle body, and the material guiding effect is good;

[0015] 3. The provision of detachable connectors facilitates the disassembly of the connecting pipe, thereby facilitating the removal of the feed box for cleaning. The two arc-shaped frames are fixed by positioning rods, thus enabling the rapid assembly of the connectors with relatively high assembly efficiency.

[0016] Compared with the prior art, the reactor for preparing lithium dihydrogen phosphate provided by this solution can add materials to the reactor body relatively safely, thereby ensuring the advantage that the steam in the reactor body will not scald the staff. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 is the front view structural schematic diagram of a reactor for preparing lithium dihydrogen phosphate provided by the present utility model;

[0018] Figure 2 is the front view cross-sectional structural schematic diagram of the feed box and the connecting pipe in the present utility model;

[0019] Figure 3 is the front view structural schematic diagram of the feed box and the connecting pipe in the present utility model;

[0020] Figure 4 is the side view cross-sectional structural schematic diagram of the feed box and the connecting pipe in the present utility model;

[0021] Figure 5 is Figure 2 the enlarged structural schematic diagram of part A shown in;

[0022] Figure 6 is Figure 2 the enlarged structural schematic diagram of part B shown in;

[0023] Figure 7 is Figure 3 the enlarged structural schematic diagram of part C shown in.

[0024] Reference numerals: 1, reactor body; 2, feed pipe; 3, connecting pipe; 4, feed box; 5, connecting plate; 6, discharge port; 7, sealing plate; 8, connecting rod; 9, first electric telescopic rod; 10, fixing plate; 11, second electric telescopic rod; 12, connecting plate; 13, sealing ring; 14, cover plate; 15, limiting block; 16, arc-shaped frame; 17, inclined plate; 18, rectangular frame; 19, connector; 20, sealing gasket; 21, mounting plate; 22, positioning rod; 23, positioning block. DETAILED DESCRIPTION OF THE EMBODIMENTS

[0025] Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the technical field to which this application belongs; the terms used in the specification of this application are only for the purpose of describing specific embodiments and are not intended to limit this application; the terms "including" and "having" and any variations thereof in the specification and claims of this application and the above drawings are intended to cover non-exclusive inclusion. The terms "first", "second", etc. in the specification and claims of this application or the above drawings are used to distinguish different objects and not to describe a specific order; the orientation or positional relationship indicated by the terms "inside", "outside", "left", "right" is based on the orientation or positional relationship shown in the drawings, and is only for the convenience of describing the present utility model and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus cannot be construed as a limitation on the present utility model.

[0026] Reference to "embodiments" herein means that a particular feature, structure, or characteristic described in connection with the embodiments can be included in at least one embodiment of the present application. The phrase appears in various places in the specification and does not necessarily refer to the same embodiment, nor is it an independent or alternative embodiment mutually exclusive with other embodiments. Those skilled in the art will explicitly and implicitly understand that the embodiments described herein can be combined with other embodiments.

[0027] An embodiment of the present utility model provides a reaction kettle for preparing lithium dihydrogen phosphate, as Figure 1-7 shown, the reaction kettle for preparing lithium dihydrogen phosphate includes: a kettle body 1 and a feed pipe 2 installed on the kettle body 1; a connecting pipe 3 provided on the feed pipe 2; a feed box 4 fixedly installed on the connecting pipe 3 and having an open top; two spaced-apart connecting plates 5 installed radially in the connecting pipe 3; two discharge ports 6 respectively opened in the centers of the two connecting plates 5; and a sealing mechanism provided on the connecting plates 5 for sealing the discharge ports 6.

[0028] In this embodiment, when it is necessary to add materials into the kettle body 1, first pour the materials into the feed box 4, then close the cover plate 14, and the sealing plate 7 of the sealing mechanism rotates along the discharge port 6, so that the discharge port 6 is exposed, and then the materials in the feed box 4 can be discharged into the kettle body 1 through the discharge port 6. At the same time, during discharging, it can also ensure that water vapor will not be directly discharged, avoiding accidental injury to the staff. When it is necessary to perform another feeding operation, the sealing mechanism seals the discharge port 6 to ensure that the hot air will not escape, and then materials can be added into the feed box 4 again. The operation safety is relatively high. By using the sealing mechanism and the feed box 4 in combination, it can be ensured that when adding materials into the kettle body 1, the staff will not come into contact with water vapor, thereby improving the operation safety.

[0029] In a further preferred embodiment of the present utility model, the sealing mechanism includes: two sealing plates 7 rotatably installed on the inner wall of the discharge port 6, and when the two sealing plates 7 are closed, they are adapted to the discharge port 6; connecting rods 8 respectively hinged on the upper and lower corresponding sealing plates 7; two first electric telescopic rods 9 hinged at the bottom of the upper connecting plate 5 and located on both sides of the discharge port, and the output rods of the two first electric telescopic rods 9 are respectively hinged to the middle parts of the two connecting rods 8, and the two ends of the two connecting rods are respectively connected to the upper and lower corresponding sealing plates; an auxiliary sealing mechanism arranged in the feed box 4 for assisting in sealing the discharge port 6.

[0030] In this embodiment, when discharging materials, first start the two first electric telescopic rods 9, so that the two first electric telescopic rods 9 drive the two connecting rods 8 to move. Each connecting rod 8 simultaneously drives the upper and lower corresponding sealing plates 7 to move. The two connecting rods drive the four sealing plates to move, so that the sealing plates 7 rotate around the discharge port 6, so that the sealing plates 7 are misaligned with the discharge port 6, and the upper and lower two discharge ports 6 are exposed. Then the materials in the feed box 4 can be discharged. The discharging is relatively fast. The first electric telescopic rod 9 drives the connecting rod 8 to move, so that the connecting rod 8 drives the sealing plate 7 to move, and the opening and closing operation of the sealing plate 7 is carried out, which is beneficial to the subsequent discharging operation of the materials.

[0031] In a further preferred embodiment of the present utility model, the auxiliary sealing mechanism includes: a fixing plate 10 fixedly installed in the feed box 4, and the fixing plate 10 is located above the discharge port 6; a second electric telescopic rod 11 fixedly installed at the bottom of the fixing plate 10; an adapter plate 12 installed on the output rod of the second electric telescopic rod 11, and the adapter plate 12 is in contact with the uppermost connecting plate 5; a sealing ring 13 installed at the bottom of the adapter plate 12.

[0032] In this embodiment, when sealing the discharge port 6, first seal the discharge port 6 with the sealing plate 7, and then start the second electric telescopic rod 11, so that the output rod of the second electric telescopic rod 11 drives the adapter plate 12 to slide, so that the adapter plate 12 drives the sealing ring 13 to slide, so that the sealing ring 13 slides down and tightly contacts the uppermost connecting plate 5, so as to perform a secondary sealing operation on the discharge port 6, ensuring that water vapor will not escape, and the sealing effect is better. The sealing ring 13 and the adapter plate 12 are in contact with the connecting plate 5, so as to perform a secondary sealing operation on the discharge port 6, ensuring that water vapor will not escape, and the sealing effect is better.

[0033] In a further preferred embodiment of the present utility model, a cover plate 14 is hinged to the top of the feed box 4, a limiting block 15 is fixedly installed on one side of the cover plate 14, an arc-shaped frame 16 is fixedly installed on one side of the feed box 4, and the output rod of the arc-shaped frame 16 is rotatably connected to the limiting block 15.

[0034] In this embodiment, when it is necessary to add materials into the kettle body 1, first rotate the arc-shaped frame 16 to make the output rod of the arc-shaped frame 16 rotate away from the limit block 15. Then, the cover plate 14 can be opened to add materials into the feeding box 4. The cover plate 14 is fixed by the arc-shaped frame 16 to ensure that the cover plate 14 will not move randomly, and the fixing is relatively fast.

[0035] In a further preferred embodiment of the present utility model, a sloping plate 17 is installed at the bottom of the inner wall of the feeding box 4. The tops of the fixing plate 10 and the connecting plate 12 are both arc-shaped. Rectangular frames 18 are fixedly sleeved on both sides of the feeding pipe 2 and the connecting pipe 3 near the butt joint surface of the feeding pipe and the connecting pipe.

[0036] In this embodiment, through the arrangement of the sloping plate 17, it can ensure that the materials in the feeding box 4 are smoothly discharged into the kettle body 1, and the material guiding effect is better.

[0037] In a further preferred embodiment of the present utility model, a connecting member 19 is detachably arranged on the two rectangular frames 18. A sealing gasket 20 is fixedly installed in the connecting member 19, and the sealing gasket 20 is in close contact with the two rectangular frames 18.

[0038] In this embodiment, through the arrangement of the detachable connecting member 19, it is convenient to disassemble the connecting pipe 3, so as to facilitate the removal of the feeding box 4 for cleaning operation.

[0039] In a further preferred embodiment of the present utility model, the connecting member 19 is composed of two arc-shaped frames, two mounting plates 21, a positioning rod 22 and a positioning block 23. The two arc-shaped frames are hinged. The two mounting plates 21 are respectively installed on the two arc-shaped frames. The positioning rod 22 is slidably installed on the two mounting plates 21. An installation groove is formed at the top of the positioning rod 22. A return spring is fixedly installed in the installation groove. The positioning block 22 is fixedly installed at the top end of the return spring and is in sliding contact with the inner wall of the installation groove. The positioning block 23 is in sliding contact with any one of the mounting plates 21.

[0040] In this embodiment, when it is necessary to remove the feeding box 4 from the feeding pipe 2, first press the positioning block 22 to make the positioning block 22 slide down into the installation groove. At the same time, the return spring contracts. Then, the positioning rod 22 can be removed from the mounting plate 21. After the positioning rod 22 is removed, the two arc-shaped frames can be opened and removed from the rectangular frame 18. The two arc-shaped frames are fixed by the positioning rod 22, so as to realize the rapid assembly operation of the connecting member 19, and the assembly efficiency is relatively high.

[0041] In summary, compared with the related technology, this device can add materials into the kettle body 1 more safely, so as to ensure the advantage that the steam in the kettle body 1 will not scald the staff.

[0042] In several embodiments provided by the present application, it should be understood that the disclosed device can be implemented in other ways.

[0043] The above embodiments are only used to illustrate the technical solutions of the present invention, rather than limiting the protection scope of the invention. Obviously, the described embodiments are only some embodiments of the present invention, rather than all embodiments. Based on these embodiments, all other embodiments obtained by those of ordinary skill in the art without making creative efforts belong to the scope of protection of the present invention. Although the present invention has been described in detail with reference to the above embodiments, those of ordinary skill in the art can still, without conflict, make combinations, additions, deletions or other adjustments to the features in the embodiments of the present invention according to the situation without making creative efforts, so as to obtain different technical solutions that essentially do not deviate from the concept of the present invention, and these technical solutions also belong to the scope of protection of the present invention.

Claims

1. A reactor for preparing lithium dihydrogen phosphate, characterized in that, Comprising: A kettle body and a feed pipe installed on the kettle body; A connecting pipe provided on the feed pipe; A feed box fixedly installed on the connecting pipe and having an open top; Two spaced-apart connecting plates radially installed in the connecting pipe; two discharge ports respectively opened in the centers of the two connecting plates; a sealing mechanism provided on the connecting plates for sealing the discharge ports.

2. The reactor for preparing lithium dihydrogen phosphate according to claim 1, wherein, The sealing mechanism includes: two sealing plates rotatably installed on the inner wall of the discharge port, and when the two sealing plates are closed, they are adapted to the discharge port; connecting rods respectively hinged to the upper and lower corresponding sealing plates; two first electric telescopic rods hinged to the bottom of the upper connecting plate and located on both sides of the discharge port, and the output rods of the two first electric telescopic rods are respectively hinged to the middle parts of the two connecting rods, and the two ends of the two connecting rods are respectively connected to the upper and lower corresponding sealing plates; an auxiliary sealing mechanism provided in the feed box for assisting in sealing the discharge port.

3. The reactor for preparing lithium dihydrogen phosphate according to claim 2, characterized in that, The auxiliary sealing mechanism includes: a fixing plate fixedly installed in the feed box, and the fixing plate is located above the discharge port; a second electric telescopic rod fixedly installed at the bottom of the fixing plate; an adapter plate installed on the output rod of the second electric telescopic rod, and the adapter plate is in contact with the uppermost connecting plate; a sealing ring installed at the bottom of the adapter plate.

4. The reactor for preparing lithium dihydrogen phosphate according to claim 1, wherein A cover plate is hinged to the top of the feed box, a limiting block is fixedly installed on one side of the cover plate, an arc-shaped frame is fixedly installed on one side of the feed box, and the output rod of the arc-shaped frame is rotatably connected to the limiting block.

5. The reactor for preparing lithium dihydrogen phosphate according to claim 3, characterized in that, An inclined plate is installed at the bottom of the inner wall of the feed box, the tops of the fixing plate and the adapter plate are both arc-shaped, and rectangular frames are fixedly sleeved on the feed pipe and the connecting pipe near the docking surface of the feed pipe and the connecting pipe, and the two rectangular frames are close to each other.

6. The reactor for preparing lithium dihydrogen phosphate according to claim 5, characterized in that, A connecting member is detachably provided on the two rectangular frames, a sealing gasket is fixedly installed in the connecting member, and the sealing gasket is in close contact with the two rectangular frames.

7. The reactor for preparing lithium dihydrogen phosphate according to claim 6, characterized in that, The connecting member is composed of two arc-shaped frames, two mounting plates, a positioning rod and a positioning block. The two arc-shaped frames are hinged, the two mounting plates are respectively installed on the two arc-shaped frames, the positioning rod is slidably installed on the two mounting plates, an installation groove is opened at the top of the positioning rod, a return spring is fixedly installed in the installation groove, the positioning block is fixedly installed at the top end of the return spring and is in sliding contact with the inner wall of the installation groove, and the positioning block is in sliding contact with any one of the mounting plates.