Chlorobenzene collecting device for aminomethylbenzoic acid production
The gas generated by heating the chlorobenzene solution was cooled multiple times through the liquid collection mechanism, which solved the problem of chlorobenzene solution not being recovered in time, and achieved efficient condensation and pollution-reducing chlorobenzene recovery.
Patent Information
- Application Number
- CN202422474119.4
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-10-14
- Publication Date
- 2025-08-05
- Estimated Expiration
- 2034-10-14
AI Technical Summary
During the existing toluene acid production process, the excess chlorobenzene solution is not recycled in time, resulting in waste and pollution, and gas is prone to flow out during the condensation process, affecting the recycling efficiency.
The gas generated when the chlorobenzene solution is heated is cooled by a liquid collection mechanism, and the purified chlorobenzene solution is formed through multiple cooling of the first and second liquid collection plates to prevent the gas from flowing out.
It improves the condensation effect, achieves efficient recycling of chlorobenzene solution and reduces pollution, and avoids waste of resources.
Smart Images

Figure CN223184081U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of auxiliary equipment for the production of aminomethylbenzoic acid, in particular to a chlorobenzene collecting device for the production of aminomethylbenzoic acid. Background Art
[0002] During the production and processing of aminomethylbenzoic acid, chlorobenzene solution needs to be added. However, if the excess chlorobenzene solution is not recovered in time during the production process, the chlorobenzene solution will cause a certain degree of waste. However, the existing chlorobenzene solution collection method is direct collection. During the collection process, the chlorobenzene solution will cause a certain degree of pollution, resulting in the chlorobenzene solution being unable to be reused, which is also a waste of resources.
[0003] Existing chlorobenzene recovery kettles for aminomethylbenzoic acid production, such as the one disclosed in Publication (Announcement) No. CN213761798U, generate a large amount of gas when heating the chlorobenzene solution. The gas is recovered as liquid through condensation, but the condensation takes a certain amount of time and the gas easily flows out of the drain port. Utility Model Content
[0004] In order to overcome the deficiencies in the background technology, the utility model discloses a chlorobenzene collection device for the production of aminomethylbenzoic acid. The utility model cools the gas generated when the chlorobenzene solution is heated through a liquid collecting mechanism to form a purified chlorobenzene solution. The chlorobenzene gas is cooled secondary to improve the condensation effect and prevent the chlorobenzene gas from flowing out of the cylinder.
[0005] In order to achieve the purpose of the utility model, the utility model adopts the following technical solutions:
[0006] A chlorobenzene collection device for aminomethylbenzoic acid production comprises a cylinder, wherein a liquid supply pipe is installed in the liquid inlet of the cylinder, a liquid collecting mechanism and a flow guiding mechanism are installed in the cylinder, the liquid collecting mechanism is located on the upper side of the flow guiding mechanism, and the exhaust end of the flow guiding mechanism corresponds to the receiving end of the liquid collecting mechanism.
[0007] The liquid collecting mechanism includes a first liquid collecting plate, a second liquid collecting plate, a liquid collecting rack and a water supply pipe. The first liquid collecting plate and the second liquid collecting plate are both located in the cylinder and fixedly connected, and the contact end and the exhaust end of the second liquid collecting plate respectively correspond to the exhaust end of the guide mechanism and the second liquid collecting plate. There are two liquid collecting racks, and the two liquid collecting racks respectively correspond to the discharge ends of the first liquid collecting plate and the second liquid collecting plate. The liquid inlets of the first liquid collecting plate and the second liquid collecting plate are respectively connected to the water supply pipe.
[0008] The first liquid collecting plate and the second liquid collecting plate are both conical hollow plates, and the first liquid collecting plate and the second liquid collecting plate are arranged up and down.
[0009] The second liquid collecting plate is provided with equidistantly arranged exhaust holes, and the exhaust holes are not connected to the hollow cavity in the second liquid collecting plate.
[0010] The liquid inlet of the cavity in the second liquid collecting plate is connected to the liquid outlet of the cavity in the first liquid collecting plate through a water supply pipe, and the liquid inlet of the cavity in the first liquid collecting plate is also connected to the liquid inlet of the cylinder through a water supply pipe.
[0011] The guide mechanism includes a collecting rack and a guide pipe. The collecting rack is located in the cylinder and is fixedly connected. The collecting rack is located on the upper side of the liquid inlet of the cylinder. The exhaust port of the collecting rack is fixedly connected with the guide pipe, and the exhaust port of the guide pipe corresponds to the second liquid collecting plate.
[0012] Due to the adoption of the above technical solution, the utility model has the following beneficial effects:
[0013] The utility model discloses a chlorobenzene collecting device for producing aminomethylbenzoic acid. The device cools the gas generated when the chlorobenzene solution is heated by a liquid collecting mechanism to form a purified chlorobenzene solution. The device further performs secondary cooling on the chlorobenzene gas to improve the condensation effect and prevent the chlorobenzene gas from flowing out of the cylinder. BRIEF DESCRIPTION OF THE DRAWINGS
[0014] Figure 1 It is a schematic diagram of the three-dimensional structure of the utility model;
[0015] Figure 2 It is a cross-sectional view of the utility model;
[0016] Figure 3 This is a schematic structural diagram of the first liquid collecting plate and the second liquid collecting plate of the utility model;
[0017] 1. Cylinder; 2. Liquid collecting mechanism; 201. First liquid collecting plate; 202. Second liquid collecting plate; 203. Liquid collecting rack; 204. Water supply pipe; 3. Liquid supply pipe; 4. Flow diversion mechanism. DETAILED DESCRIPTION
[0018] The present invention will be explained in detail through the following embodiments. The purpose of disclosing the present invention is to protect all technical improvements within the scope of the present invention.
[0019] Combined with attachment Figures 1-3 The chlorobenzene collection device for the production of aminomethylbenzoic acid includes a cylinder 1, and a liquid supply pipe 3 is installed in the liquid inlet of the cylinder 1. A liquid collecting mechanism 2 and a flow guiding mechanism 4 are installed in the cylinder 1. The liquid collecting mechanism 2 is located on the upper side of the flow guiding mechanism 4, and the exhaust end of the flow guiding mechanism 4 corresponds to the receiving end of the liquid collecting mechanism 2.
[0020] The liquid collecting mechanism 2 includes a first liquid collecting plate 201, a second liquid collecting plate 202, a liquid collecting frame 203 and a water supply pipe 204. The first liquid collecting plate 201 and the second liquid collecting plate 202 are both located in the cylinder 1 and fixedly connected, and the contact end and the exhaust end of the second liquid collecting plate 202 respectively correspond to the exhaust end of the guide mechanism 4 and the second liquid collecting plate 202. There are two liquid collecting frames 203, and the two liquid collecting frames 203 respectively correspond to the discharge ends of the first liquid collecting plate 201 and the second liquid collecting plate 202. The liquid inlets of the first liquid collecting plate 201 and the second liquid collecting plate 202 are respectively connected to the water supply pipe 204, and a confluence pipe is connected between the drainage outlets of the two liquid collecting frames 203 to facilitate the collection of condensed chlorobenzene by the staff.
[0021] The first liquid collecting plate 201 and the second liquid collecting plate 202 are both conical hollow plates, and the first liquid collecting plate 201 and the second liquid collecting plate 202 are arranged vertically, and the liquid collecting frame 203 is located on one side of the bottom end of the inclined surface of the first liquid collecting plate 201 and the second liquid collecting plate 202.
[0022] The second liquid collecting plate 202 is provided with equidistantly arranged exhaust holes, and the exhaust holes are not connected to the hollow cavity in the second liquid collecting plate 202 .
[0023] The liquid inlet of the hollow cavity in the second liquid collecting plate 202 is connected to the liquid discharge port of the hollow cavity in the first liquid collecting plate 201 through the water supply pipe 204, and the liquid inlet of the hollow cavity in the first liquid collecting plate 201 is also connected to the liquid inlet of the cylinder 1 through the water supply pipe 204. An electric heating tube is provided at the bottom of the cylinder 1 to heat the chlorobenzene solution.
[0024] The guide mechanism 4 includes a collection rack and a guide pipe. The collection rack is located in the cylinder 1 and is fixedly connected. The collection rack is located on the upper side of the liquid inlet of the cylinder 1. The exhaust port of the collection rack is fixedly connected with the guide pipe, and the exhaust port of the guide pipe corresponds to the second liquid collecting plate 202.
[0025] The chlorobenzene collection device for aminomethylbenzoic acid production is described. When in use, chlorobenzene solution is added to the cylinder 1 through the liquid supply pipe 3, and the chlorobenzene solution is heated by the electric heating pipe in the cylinder 1. The hot gas generated by the heating of the chlorobenzene solution is guided through the collection rack and the guide pipe. During the heating process of the chlorobenzene solution, condensed water is injected into the first liquid collecting plate 201 and the second liquid collecting plate 202 respectively through the water supply pipe 204. The hot gas is first condensed after passing through the second liquid collecting plate 202. The hot gas that cannot be condensed will contact the first liquid collecting plate 201 through the exhaust hole of the second liquid collecting plate 202 and condense again. The chlorobenzene generated by the condensation is collected by the liquid collecting rack 203, and the condensed chlorobenzene is discharged through the confluence pipe, which is convenient for staff to collect.
[0026] The parts of the present invention that are not described in detail are prior art. Although the present invention is specifically demonstrated and introduced in conjunction with the preferred implementation scheme, there are many methods and ways to implement the technical solution. The above is only a preferred implementation scheme of the present invention. However, technical personnel in the relevant field should understand that various changes can be made to the form and details of the present invention without departing from the spirit and scope of the present invention as defined by the attached claims, and all of them are within the scope of protection of the present invention.
Claims
1. A chlorobenzene collecting device for producing aminomethylbenzoic acid, comprising a cylinder (1), wherein a liquid supply pipe (3) is installed in the liquid inlet of the cylinder (1), and the device is characterized by: A liquid collecting mechanism (2) and a flow guiding mechanism (4) are installed in the cylinder (1); the liquid collecting mechanism (2) is located on the upper side of the flow guiding mechanism (4), and the exhaust end of the flow guiding mechanism (4) corresponds to the receiving end of the liquid collecting mechanism (2).
2. Chlorobenzene collecting device for producing aminomethylbenzoic acid according to claim 1, is characterized in that: The liquid collecting mechanism (2) comprises a first liquid collecting plate (201), a second liquid collecting plate (202), a liquid collecting frame (203) and a water supply pipe (204); the first liquid collecting plate (201) and the second liquid collecting plate (202) are both located in the cylinder (1) and fixedly connected; the contact end and the exhaust end of the second liquid collecting plate (202) respectively correspond to the exhaust end of the flow guide mechanism (4) and the second liquid collecting plate (202); there are two liquid collecting frames (203), the two liquid collecting frames (203) respectively correspond to the discharge ends of the first liquid collecting plate (201) and the second liquid collecting plate (202); the liquid inlets of the first liquid collecting plate (201) and the second liquid collecting plate (202) are respectively connected to the water supply pipe (204).
3. Chlorobenzene collecting device for producing aminomethylbenzoic acid according to claim 2, is characterized in that: The first liquid collecting plate (201) and the second liquid collecting plate (202) are both conical hollow plates, and the first liquid collecting plate (201) and the second liquid collecting plate (202) are arranged in an upper and lower manner.
4. Chlorobenzene collecting device for producing aminomethylbenzoic acid according to claim 2, is characterized in that: The second liquid collecting plate (202) is provided with equidistantly arranged exhaust holes, and the exhaust holes are not connected to the hollow cavity in the second liquid collecting plate (202).
5. Chlorobenzene collecting device for producing aminomethylbenzoic acid according to claim 2, characterized in that: The liquid inlet of the hollow cavity of the second liquid collecting plate (202) is connected to the liquid outlet of the hollow cavity of the first liquid collecting plate (201) via the water supply pipe (204), and the liquid inlet of the hollow cavity of the first liquid collecting plate (201) is also connected to the liquid inlet of the cylinder (1) via the water supply pipe (204).
6. Chlorobenzene collecting device for producing aminomethylbenzoic acid according to claim 1, characterized in that: The flow guiding mechanism (4) comprises a collecting rack and a flow guiding pipe, the collecting rack is located in the cylinder (1) and is fixedly connected, and the collecting rack is located on the upper side of the liquid inlet of the cylinder (1), the flow guiding pipe is fixedly connected in the exhaust port of the collecting rack, and the exhaust port of the flow guiding pipe corresponds to the second liquid collecting plate (202).
Citation Information
Patent Citations
Chlorobenzene recovery kettle for aminomethylbenzoic acid production
CN213761798U