Residue-prevention rectifying still for production of ethyl 3-amino-4, 4, 4-trifluorocrotonate
By introducing scraping rings and vibration rings into the stills, the problem of more residues in the existing stills is solved, and more thorough air unloading and manual cleaning are achieved, which improves air unloading rate and working efficiency.
Patent Information
- Application Number
- CN202422525239.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-10-18
- Publication Date
- 2025-08-15
- Estimated Expiration
- 2034-10-18
AI Technical Summary
When the existing 3-amino-4,4,4-trifluorocrinate ethyl ester production kettle is discharged through the discharge pipeline after use, a large amount of material is often left inside, resulting in a poor discharge rate and manual cleaning, which affects work efficiency.
A residual-proof still kettle is designed, which includes a cleaning assembly, including a scraper ring, a rotary rod and a vibration ring. The scraper ring is driven to scrape the inner wall residue through the electric push rod, and the coordinated movement of the rotary rod and the vibration ring can further vibrate and scrape the residue, thereby increasing the air discharge rate.
It effectively reduces residues, improves the air unloading rate, reduces the number of manual cleanings, and improves work efficiency.
Smart Images
Figure CN223220990U_ABST
Abstract
Description
Technical Field
[0001] The utility model belongs to the technical field of rectification kettles, in particular to a rectification kettle for producing ethyl 3-amino-4,4,4-trifluorocrotonate with anti-residue function. Background Art
[0002] The distillation kettle for the production of ethyl 3-amino-4,4,4-trifluorocrotonate is a highly efficient equipment specially used for the purification and separation of ethyl 3-amino-4,4,4-trifluorocrotonate, and is usually distilled in a stirring manner.
[0003] When discharging the existing distillation kettle after use, the material is only discharged through the discharge pipe. A large amount of material usually remains inside, and the unloading rate is poor. This not only affects its reuse, but also requires staff to clean up after discharging, which increases labor. In addition, a lot of time is required to handle it after each discharge, which affects work efficiency. Utility Model Content
[0004] The purpose of the utility model is to provide a distillation kettle for producing ethyl 3-amino-4,4,4-trifluorocrotonate with an anti-residue function. A cleaning component is set, specifically when discharging, the electric push rod is started to drive the connecting block to move downward through the push-pull rod, and the connecting block will drive the scraper ring to move downward, and the scraper ring will scrape off the material remaining on the inner wall of the distillation box, so that the material can be discharged more thoroughly. At the same time, the conical ring can play a role of diversion, and further reduce the residue. At the same time, when the rotating rod rotates, the scraper rod will be driven to rotate through the connecting rod, and the scraper rod will scrape off the material remaining on the surface of the conical ring, thereby improving the unloading rate. This solves the problem that when the existing distillation kettle is discharged after use, the material is only discharged through the discharge pipe, and a large amount of material is usually retained inside, and the unloading rate is poor, which not only affects the reuse, but also requires staff to clean up after discharge, which increases labor.
[0005] In order to solve the above technical problems, the present invention is achieved through the following technical solutions:
[0006] The utility model discloses a distillation kettle for producing ethyl 3-amino-4,4,4-trifluorocrotonate with an anti-residue function, comprising a distillation box, a motor fixedly connected to the top of the distillation box, an electric push rod provided on the back of the motor, a bottom of the electric push rod fixedly connected to the top of the distillation box, a discharge pipe fixedly connected to the bottom of the distillation box, an electric valve provided on the outside of the discharge pipe, and a cleaning component provided inside the distillation box;
[0007] The cleaning assembly includes a scraper ring, the outer side of the scraper ring contacts the inner wall of the distillation box, the back side of the inner wall of the scraper ring is fixedly connected to a connecting block, the top of the connecting block is fixedly connected to a push-pull rod, the top of the push-pull rod is fixedly connected to the bottom output end of the electric push rod, a rotating rod is provided inside the distillation box, and a plurality of connecting rods are fixedly connected to the outer surface of the bottom of the rotating rod, and a plurality of connecting rods are fixedly connected to a scraper rod on the side away from the rotating rod, and a conical ring is fixedly connected to the inner wall of the distillation box.
[0008] Furthermore, the top of the rotating rod is rotatably connected to the distillation box, the top of the rotating rod is fixedly connected to the bottom output end of the motor, the outer surface of the rotating rod is fixedly connected to a pentagonal ring, the outer surface of the pentagonal ring is fixedly connected to several stirring rods, and the scraper rod surface is in contact with the conical ring surface.
[0009] Furthermore, a vibration ring is fixedly connected to the bottom of the rotating rod, a conical fixing block is provided below the vibration ring, a plurality of support frames are fixedly connected to the bottom of the conical fixing block, and the bottom of the support frame is fixedly connected to the bottom of the inner wall of the distillation box.
[0010] Furthermore, a plurality of protrusions are fixedly connected to the outer surface of the conical fixing block, a plurality of movable grooves are opened on the inner wall of the vibration ring, and a collision block is slidably connected to the inner wall of the movable groove.
[0011] Furthermore, a sliding rod is fixedly connected to the top of the collision block, the sliding rod passes through the vibration ring and extends to the outside, the sliding rod is slidably connected to the vibration ring, a spring is sleeved on the outside of the sliding rod, the top of the spring is fixedly connected to the top of the inner wall of the movable groove, and the bottom of the spring is fixedly connected to the top of the collision block.
[0012] Furthermore, the vibration ring and the conical fixing block are both conical, the side of the convex block close to the vibration ring is an arc surface, and the side of the collision block close to the conical fixing block is an arc surface.
[0013] The utility model has the following beneficial effects:
[0014] 1. The utility model is provided with a cleaning component. Specifically, when discharging, the electric push rod is started to drive the connecting block to move downward through the push-pull rod, and the connecting block will drive the scraper ring to move downward. The scraper ring will scrape off the residual material on the inner wall of the distillation box, so that the material can be discharged more thoroughly. At the same time, the conical ring can play a role in diversion, and further reduce the residue. At the same time, when the rotating rod rotates, it will drive the scraper rod to rotate through the connecting rod, and the scraper rod will scrape off the residual material on the surface of the conical ring, thereby improving the unloading rate.
[0015] 2. The utility model sets a vibration ring. Specifically, when the rotating rod rotates, the vibration ring will rotate along with it, and the vibration ring will drive the collision block to rotate together. When the collision block contacts the protrusion, a collision effect will occur. Such a reciprocating effect will continue to produce a vibration effect, and the residual materials on the vibration ring, rotating rod, pentagonal ring and stirring rod will be vibrated off, thereby further improving the unloading effect. The staff does not need to clean it many times, which reduces labor.
[0016] Of course, any product implementing the present invention does not necessarily need to achieve all of the advantages described above at the same time. BRIEF DESCRIPTION OF THE DRAWINGS
[0017] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following is a brief introduction to the drawings required for describing the embodiments. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying any creative work.
[0018] Figure 1 This is a schematic diagram of the overall structure of the utility model;
[0019] Figure 2 This is a schematic diagram of the internal structure of the distillation box of the utility model;
[0020] Figure 3 This is a schematic diagram of the overall structure of the scraper ring of the utility model;
[0021] Figure 4 This is a schematic diagram of the overall structure of the rotating rod of the utility model;
[0022] Figure 5 This is a schematic diagram of the front cross-sectional structure of the vibration ring of the utility model.
[0023] In the accompanying drawings, the components represented by the reference numerals are as follows:
[0024] 1. Distillation box; 11. Cleaning assembly; 111. Scraper ring; 112. Connecting block; 113. Push-pull rod; 12. Rotating rod; 121. Five-sided ring; 122. Stirring rod; 123. Connecting rod; 124. Scraper rod; 13. Conical ring; 14. Vibrating ring; 141. Conical fixing block; 142. Support frame; 143. Bump; 144. Movable groove; 441. Collision block; 442. Sliding rod; 443. Spring; 2. Motor; 3. Electric push rod; 4. Discharge pipe; 41. Electric valve. DETAILED DESCRIPTION
[0025] The following will be combined with the accompanying drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the embodiments described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.
[0026] See also Figure 1-5 As shown, the utility model is a distillation kettle for producing ethyl 3-amino-4,4,4-trifluorocrotonate with an anti-residue function, comprising a distillation box 1, a motor 2 is fixedly connected to the top of the distillation box 1, an electric push rod 3 is provided on the back of the motor 2, the bottom of the electric push rod 3 is fixedly connected to the top of the distillation box 1, a discharge pipe 4 is fixedly connected to the bottom of the distillation box 1, an electric valve 41 is provided on the outside of the discharge pipe 4, and a cleaning component 11 is provided inside the distillation box 1;
[0027] The cleaning assembly 11 includes a scraper ring 111, the outer side of the scraper ring 111 contacts the inner wall of the distillation box 1, the back of the inner wall of the scraper ring 111 is fixedly connected to a connecting block 112, the top of the connecting block 112 is fixedly connected to a push-pull rod 113, the top of the push-pull rod 113 is fixedly connected to the bottom output end of the electric push rod 3, a rotating rod 12 is provided inside the distillation box 1, and a plurality of connecting rods 123 are fixedly connected to the outer surface of the bottom of the rotating rod 12, and a plurality of connecting rods 123 are fixedly connected to a scraper 124 on the side away from the rotating rod 12, and a conical ring is fixedly connected to the inner wall of the distillation box 1 13. By setting up the cleaning component 11, specifically when discharging, the electric push rod 3 is started to drive the connecting block 112 to move downward through the push-pull rod 113, and the connecting block 112 will drive the scraper ring 111 to move downward, and the scraper ring 111 will scrape off the material remaining on the inner wall of the distillation box 1, so that the material can be discharged more thoroughly. At the same time, the conical ring 13 can play a role in diversion, and further reduce the residue. At the same time, when the rotating rod 12 rotates, it will drive the scraper rod 124 to rotate through the connecting rod 123, and the scraper rod 124 will scrape off the material remaining on the surface of the conical ring 13, thereby improving the unloading rate.
[0028] The top of the rotating rod 12 is rotatably connected to the distillation box 1, and the top of the rotating rod 12 is fixedly connected to the bottom output end of the motor 2. The outer surface of the rotating rod 12 is fixedly connected to a pentagonal ring 121, and the outer surface of the pentagonal ring 121 is fixedly connected to a plurality of stirring rods 122. The surface of the scraper rod 124 contacts the surface of the conical ring 13. When the motor 2 is started to drive the rotating rod 12 to rotate, the rotating rod 12 drives the plurality of stirring rods 122 to rotate through the pentagonal ring 121 to stir and distill the material inside the distillation box 1.
[0029] The bottom of the rotating rod 12 is fixedly connected to a vibration ring 14, and a conical fixing block 141 is provided below the vibration ring 14. The bottom of the conical fixing block 141 is fixedly connected to a plurality of support frames 142. The bottom of the support frame 142 is fixedly connected to the bottom of the inner wall of the distillation box 1. The support frame 142 is used to support the conical fixing block 141, and openings are formed between the plurality of support frames 142 for discharging.
[0030] A plurality of protrusions 143 are fixedly connected to the outer surface of the conical fixed block 141, and a plurality of movable grooves 144 are opened on the inner wall of the vibration ring 14. The inner wall of the movable groove 144 is slidably connected with a collision block 441. By setting the vibration ring 14, specifically when the rotating rod 12 rotates, the vibration ring 14 will follow the rotation, and the vibration ring 14 will drive the collision block 441 to rotate together. When the collision block 441 contacts the protrusion 143, a collision effect will occur, and the reciprocating effect will continue to produce a vibration effect, which will vibrate the residual materials on the vibration ring 14, the rotating rod 12, the five-sided ring 121 and the stirring rod 122, thereby improving the unloading effect again. There is no need for the staff to clean it many times, reducing labor.
[0031] The top of the collision block 441 is fixedly connected to a sliding rod 442, which passes through the vibration ring 14 and extends to the outside. The sliding rod 442 is slidably connected to the vibration ring 14, and a spring 443 is sleeved on the outside of the sliding rod 442. The top of the spring 443 is fixedly connected to the top of the inner wall of the movable groove 144, and the bottom of the spring 443 is fixedly connected to the top of the collision block 441. When the collision block 441 passes through the protrusion 143, the collision block 441 is reset under the elastic action of the spring 443.
[0032] The vibration ring 14 and the conical fixing block 141 are both conically set, the side of the protrusion 143 close to the vibration ring 14 is set as an arc surface, and the side of the collision block 441 close to the conical fixing block 141 is set as an arc surface. Since the sides of the protrusion 143 and the collision block 441 close to each other are both set as arc surfaces, the protrusion 143 can smoothly push the collision block 441.
[0033] A specific application of this embodiment is:
[0034] After scraping, the electric push rod 3 drives the connecting block 112 to move upward through the push-pull rod 113 to reset the scraper ring 111. At the same time, when the rotating rod 12 rotates, it drives the scraper rod 124 to rotate through the connecting rod 123. The scraper rod 124 is driven to rotate. The material remaining on the surface of the conical ring 13 is scraped off, thereby improving the unloading rate. When the rotating rod 12 rotates, the vibrating ring 14 will rotate accordingly, and the vibrating ring 14 will drive the collision block 441 to rotate together. When the collision block 441 contacts the protrusion 143, a collision effect will occur, thereby generating vibration, and at the same time, the collision block 441 will be pushed into the movable groove 144. At the same time, the sliding rod 442 slides on the vibrating ring 14 and squeezes the spring 443, so that the collision block 441 can pass through the protrusion 143 smoothly. Then the collision block 441 is reset under the elastic action of the spring 443, and the vibrating ring 14 and the conical fixed block 141 will continue to produce a vibration effect, vibrating the residual material on the vibrating ring 14, the rotating rod 12, the pentagonal ring 121 and the stirring rod 122, thereby improving the unloading effect again. There is no need for staff to clean it many times, reducing labor.
[0035] Throughout this specification, references to terms such as "one embodiment," "example," or "specific example" indicate that a specific feature, structure, material, or characteristic described in conjunction with that embodiment or example is included in at least one embodiment or example of the present invention. In this specification, schematic representations of these terms do not necessarily refer to the same embodiment or example. Furthermore, the specific features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
[0036] The preferred embodiments of the present invention disclosed above are intended only to help illustrate the present invention. These preferred embodiments do not exhaustively describe all details, nor do they limit the present invention to the specific embodiments described. Obviously, many modifications and variations are possible based on the contents of this specification. These embodiments are selected and described in detail in this specification to better explain the principles and practical applications of the present invention, thereby enabling those skilled in the art to better understand and utilize the present invention. The present invention is limited only by the claims and their full scope and equivalents.
Claims
1. A distillation kettle for producing ethyl 3-amino-4,4,4-trifluorocrotonate with an anti-residue function, comprising a distillation box (1), a motor (2) fixedly connected to the top of the distillation box (1), an electric push rod (3) provided on the back of the motor (2), the bottom of the electric push rod (3) fixedly connected to the top of the distillation box (1), a discharge pipe (4) fixedly connected to the bottom of the distillation box (1), an electric valve (41) provided on the outside of the discharge pipe (4), and a cleaning component (11) provided inside the distillation box (1), characterized in that ； The cleaning assembly (11) comprises a scraper ring (111), the outer side of the scraper ring (111) contacts the inner wall of the distillation box (1), the back side of the inner wall of the scraper ring (111) is fixedly connected to a connecting block (112), the top of the connecting block (112) is fixedly connected to a push-pull rod (113), the top of the push-pull rod (113) is fixedly connected to the bottom output end of the electric push rod (3), a rotating rod (12) is provided inside the distillation box (1), the outer surface of the bottom of the rotating rod (12) is fixedly connected to a plurality of connecting rods (123), the side of the plurality of connecting rods (123) away from the rotating rod (12) is fixedly connected to a scraper rod (124), and the inner wall of the distillation box (1) is fixedly connected to a conical ring (13).
2. The method for producing ethyl 3-amino-4,4,4-trifluorocrotonate with an anti-residue property according to claim 1, wherein: The top of the rotating rod (12) is rotatably connected to the distillation box (1), and the top of the rotating rod (12) is fixedly connected to the bottom output end of the motor (2). The outer surface of the rotating rod (12) is fixedly connected to a pentagonal ring (121), and the outer surface of the pentagonal ring (121) is fixedly connected to a plurality of stirring rods (122). The surface of the scraper rod (124) contacts the surface of the conical ring (13).
3. The anti-residue 3-amino-4,4,4-trifluorocrotonate production distillation kettle according to claim 2, characterized in that: The bottom of the rotating rod (12) is fixedly connected to a vibration ring (14), a conical fixing block (141) is provided below the vibration ring (14), the bottom of the conical fixing block (141) is fixedly connected to a plurality of support frames (142), and the bottom of the support frames (142) is fixedly connected to the bottom of the inner wall of the distillation box (1).
4. The anti-residue 3-amino-4,4,4-trifluorocrotonate production distillation kettle according to claim 3, characterized in that: The outer surface of the conical fixed block (141) is fixedly connected with a plurality of protrusions (143); the inner wall of the vibration ring (14) is provided with a plurality of movable grooves (144); and the inner wall of the movable groove (144) is slidably connected with a collision block (441).
5. The anti-residue 3-amino-4,4,4-trifluorocrotonate production distillation kettle according to claim 4, characterized in that: A sliding rod (442) is fixedly connected to the top of the collision block (441), the sliding rod (442) passes through the vibration ring (14) and extends to the outside, and the sliding rod (442) is slidably connected to the vibration ring (14).
6. The residual-proof distillation kettle for producing ethyl 3-amino-4,4,4-trifluorocrotonate according to claim 5, characterized in that: A spring (443) is sleeved on the outside of the slide bar (442), the top of the spring (443) is fixedly connected to the top of the inner wall of the movable groove (144), and the bottom of the spring (443) is fixedly connected to the top of the collision block (441).
7. The residual-proof distillation kettle for producing ethyl 3-amino-4,4,4-trifluorocrotonate according to claim 4, characterized in that: The vibration ring (14) and the conical fixing block (141) are both conically arranged, the side of the convex block (143) close to the vibration ring (14) is arranged as an arc surface, and the side of the collision block (441) close to the conical fixing block (141) is arranged as an arc surface.