Colloid palladium solution water bath heating device

By designing a water bath heating device for colloidal palladium solution, the synergistic effect of mobile components and extractor components is used to solve the problem of uneven heating of colloidal palladium solution, uniform heating and stirring are achieved, and reaction efficiency and material utilization are improved.

CN223263807UActive Publication Date: 2025-08-26ZHEJIANG ENSEN CHEM TECH CO LTD
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Patent Information

Application Number
CN202422529233.2
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-10-19
Publication Date
2025-08-26
Estimated Expiration
2034-10-19

AI Technical Summary

Technical Problem

In the prior art, the colloidal palladium solution is heated unevenly, resulting in unsatisfactory catalytic effect of the reaction solution and local high temperatures are prone to occur, resulting in solution consumption.

Method used

A colloidal palladium solution water bath heating device is adopted to achieve flow heating and stirring of the water inside the heating box through the coordination of the moving component and the extraction component, ensuring that the material is heated evenly and avoiding condensation.

Benefits of technology

The uniform heating of colloidal palladium solution is achieved, the reaction efficiency is improved, the material coagulation is reduced, and the use effect is improved.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a colloid palladium solution water bath heating device which comprises a heating box, a control panel is fixedly connected to the side wall of the heating box, a liquid discharge pipe is fixedly connected to the surface of the heating box, a liquid discharge valve is connected to the side wall of the liquid discharge pipe, a waterproof shell is arranged in the heating box, and a water outlet valve is arranged in the waterproof shell. The outer side wall of the waterproof shell is fixedly sleeved with an assembly frame, an assembly branch pipe is arranged on the front face of the heating box, and the outer side wall of the assembly branch pipe is fixedly sleeved with a heater. According to the device, the driving block, the driving motor and the driving worm can be matched through the adjusting assembly, so that the driving motor drives the adjusting worm gear on the driving worm to rotate, then the adjusting worm gear drives the adjusting mixing pipe to rotate, and a plurality of stirring pipes on the adjusting mixing pipe stir and heat materials; and therefore, the condensation effect of the material is reduced, the material is fully and uniformly heated, and the using effect is improved.
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Description

Technical Field

[0001] The utility model relates to the technical field of colloidal palladium production, in particular to a device for heating a colloidal palladium solution in a water bath. Background Art

[0002] The colloidal catalyst is the most widely used colloidal palladium in industry. It is prepared by the reaction of PdC12 and SnC12 in an acidic solution. The core of the colloidal catalyst is palladium, and the outer layer is hydrated divalent and tetravalent tin ions. Excessive Sn2+ plays a key role in the stability of the catalyst liquid. Modern colloidal catalysts also contain a large amount of acid or salt. The colloidal palladium process is a colloid that provides a catalyst solution for the metallization reaction on the surface of plastic parts. This colloid is easily decomposed when exposed to high temperature and water. Generally, the heating tube is mostly installed inside the sub-tank and the heating is uneven. At the same time, the catalyst solution in the sub-tank is prone to local high temperature, which makes the catalytic effect of the reaction solution unsatisfactory and causes the consumption of the solution, thereby reducing the use effect. Utility Model Content

[0003] The purpose of the utility model is to solve the shortcomings of the prior art and to propose a device for heating a colloidal palladium solution in a water bath.

[0004] In order to achieve the above-mentioned purpose, the present invention adopts the following technical scheme: a device for heating a colloidal palladium solution in a water bath, comprising a heating box, a control panel fixedly connected to the side wall of the heating box, a drain pipe fixedly connected to the surface of the heating box, a drain valve connected to the side wall of the drain pipe, a water-proof shell provided inside the heating box, an assembly frame fixedly sleeved on the outer wall of the water-proof shell, an assembly branch pipe provided on the front of the heating box, a heater fixedly sleeved on the outer wall of the assembly branch pipe, an assembly serpentine pipe rotatably connected between the two sides of the inner wall of the heating box, one end of the assembly serpentine pipe passes through the heating box and is rotatably connected to the assembly branch pipe, an assembly gear fixedly sleeved on the outer wall of the assembly serpentine pipe, and a moving component for adjusting the rotation of the assembly gear is connected to the surface of the heating box;

[0005] A heating pipe is fixedly connected between the two sides of the inner wall of the heating box, an adjustment bracket is fixedly connected to the top of the water-proof shell, and a material extraction component is connected to the top of the adjustment bracket.

[0006] As a further description of the above technical solution:

[0007] The moving component includes a moving groove opened on the surface of the heating box, a moving slider is slidably connected inside the moving groove, a moving rack is fixedly connected to the surface of the moving slider, multiple assembly gears are meshed with the moving rack, a moving circular plate is fixedly connected to the bottom of the moving rack, and a moving L-shaped support plate is fixedly connected to the surface of the heating box.

[0008] As a further description of the above technical solution:

[0009] The surface of the movable L-shaped support plate is fixedly connected to a movable motor, the output shaft of the movable motor passes through the movable L-shaped support plate and is fixedly connected to a movable disk, the back side of the movable disk is rotatably connected to a movable shaft, and the movable shaft is slidably connected to the inside of the movable circular plate.

[0010] As a further description of the above technical solution:

[0011] The pumping assembly includes a regulating pump fixedly connected to the top of the regulating bracket, and the water inlet and outlet of the regulating pump are respectively fixedly connected to the first regulating branch pipe and the second regulating branch pipe. The end of the first regulating branch pipe passes through the waterproof shell and extends to the inside of the heating box.

[0012] As a further description of the above technical solution:

[0013] The other end of the second regulating branch pipe is rotatably connected to an regulating mixing tube, the end of the regulating mixing tube passes through the regulating bracket and the water-proof shell and extends to the inside of the heating box, the outer wall of the regulating mixing tube is fixedly sleeved with an regulating worm gear, and multiple stirring tubes are fixedly connected on both sides of the outer wall of the regulating mixing tube, and the top of the regulating bracket is connected to an regulating component for adjusting the rotation of the regulating worm gear.

[0014] As a further description of the above technical solution:

[0015] The adjustment assembly includes two driving blocks fixedly connected to the top of the adjustment bracket, wherein the side wall of one of the driving blocks is fixedly connected to a driving motor, the output end of the driving motor is fixedly connected to a driving worm, the end of the driving worm passes through one of the driving blocks and is rotatably connected to the other driving block, and the driving worm is engaged with the adjusting worm gear.

[0016] The utility model has the following beneficial effects:

[0017] The moving assembly can be used to make the moving slider, moving rack, moving circular plate, moving L-shaped support plate, moving motor, moving disk and moving shaft cooperate, so that the moving shaft on the moving disk can be driven to rotate by the moving motor, and then the moving shaft slides inside the moving circular plate, so as to push the moving rack on the moving circular plate to move and rotate the multiple assembly gears, and at the same time the assembly gears also drive the serpentine tube to rotate, so as to flow and heat the water inside the heating box, thereby fully conducting the heating effect on the material inside the waterproof shell, and the pumping assembly can be used to make the adjusting bracket, adjusting pump, first adjusting branch pipe, second adjusting branch pipe and adjusting mixing pipe, and adjusting worm gear cooperate, so as to The regulating pump drives the first regulating branch pipe to extract the heated water inside the heating box, so that the heated water is discharged into the second regulating branch pipe, and then the hot water is discharged into the regulating mixing tube, followed by the hot water on the regulating mixing tube being discharged into multiple stirring tubes, so as to facilitate the stirring and heating of the material. The regulating assembly can be used to cooperate with the driving block, the driving motor and the driving worm, so that the driving motor drives the regulating worm gear on the driving worm to rotate, and then the regulating worm gear also drives the regulating mixing tube to rotate, so that the multiple stirring tubes on the regulating mixing tube stir and heat the material, thereby reducing the condensation of the material and making the material fully and evenly heated, thereby improving the use effect. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] Figure 1 This is a schematic diagram of the overall structure of a device for heating a colloidal palladium solution in a water bath proposed by the present invention;

[0019] Figure 2 This is a schematic diagram of the internal structure of a heating box for a device for heating a colloidal palladium solution in a water bath proposed by the present invention;

[0020] Figure 3 for Figure 1 A schematic diagram of the structure enlarged in the middle;

[0021] Figure 4 for Figure 1 Schematic diagram of the structure enlarged at point B.

[0022] Legend:

[0023] 1. Heating box; 2. Control panel; 3. Waterproof shell; 4. Assembly frame; 5. Assembly serpentine pipe; 6. Assembly gear; 7. Assembly branch pipe; 8. Heater; 9. Moving slider; 10. Moving rack; 11. Moving circular plate; 12. Moving L-shaped support plate; 13. Moving motor; 14. Moving disk; 15. Moving shaft; 16. Heating duct; 17. Adjustment bracket; 18. Adjustment pump; 19. First adjustment branch pipe; 20. Second adjustment branch pipe; 21. Adjustment mixing pipe; 22. Adjustment worm gear; 23. Drive block; 24. Drive motor; 25. Drive worm. DETAILED DESCRIPTION

[0024] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the embodiments described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.

[0025] Reference Figure 1-4 The utility model provides a device for heating a colloidal palladium solution in a water bath, comprising a heating box 1, a control panel 2 fixedly connected to the side wall of the heating box 1, a drain pipe fixedly connected to the surface of the heating box 1, a drain valve connected to the side wall of the drain pipe, a water-proof shell 3 provided inside the heating box 1, an assembly frame 4 fixedly sleeved on the outer wall of the water-proof shell 3, an assembly branch pipe 7 provided on the front of the heating box 1, a heater 8 fixedly sleeved on the outer wall of the assembly branch pipe 7, an assembly serpentine pipe 5 rotatably connected between the two sides of the inner wall of the heating box 1, one end of the assembly serpentine pipe 5 passes through the heating box 1 and is rotatably connected to the assembly branch pipe 7, an assembly gear 6 fixedly sleeved on the outer wall of the assembly serpentine pipe 5, a moving component for adjusting the rotation of the assembly gear 6 is connected to the surface of the heating box 1, and the adjustment is achieved through the moving component. The assembly gear 6 has the function of rotating, and the moving component includes a moving groove opened on the surface of the heating box 1, and a moving slider 9 is slidably connected inside the moving groove, and a moving rack 10 is fixedly connected to the surface of the moving slider 9, and multiple assembly gears 6 are meshed with the moving rack 10. The bottom of the moving rack 10 is fixedly connected to a moving circular plate 11, and a moving L-shaped support plate 12 is fixedly connected to the surface of the heating box 1. The surface of the moving L-shaped support plate 12 is fixedly connected to a moving motor 13, and the output shaft of the moving motor 13 passes through the moving L-shaped support plate 12 and is fixedly connected to a moving disk 14. The back of the moving disk 14 is rotatably connected to a moving shaft 15, and the moving shaft 15 is slidably connected to the inside of the moving circular plate 11, and drives the moving disk 14 to rotate through the moving motor 13.

[0026] A heating tube 16 is fixedly connected between the two sides of the inner wall of the heating box 1, an adjusting bracket 17 is fixedly connected to the top of the watertight outer shell 3, and a pumping assembly is connected to the top of the adjusting bracket 17. The pumping assembly includes a regulating pump 18 fixedly connected to the top of the regulating bracket 17, and the water inlet and outlet of the regulating pump 18 are respectively fixedly connected to the first regulating branch pipe 19 and the second regulating branch pipe 20. The end of the first regulating branch pipe 19 passes through the watertight outer shell 3 and extends to the interior of the heating box 1. The other end of the second regulating branch pipe 20 is rotatably connected to the regulating mixing pipe 21. The end of the regulating mixing pipe 21 passes through the adjusting bracket 17 and the watertight outer shell 3 and extends to the interior of the heating box 1. An adjusting worm gear 22 is fixedly sleeved on the outer wall of the regulating mixing pipe 21. A plurality of stirring pipes are fixedly connected on both sides of the outer wall of the regulating mixing pipe 21. The regulating pump 18 drives the first regulating branch pipe 19 to extract the heated water inside the heating box 1, so that the water passes through the second regulating branch pipe 20 and is discharged into the interior of the regulating mixing pipe 21.

[0027] The top of the adjusting bracket 17 is connected to an adjusting component for rotating the adjusting worm gear 22. The adjusting component includes two driving blocks 23 fixedly connected to the top of the adjusting bracket 17. The side wall of one of the driving blocks 23 is fixedly connected to a driving motor 24. The output end of the driving motor 24 is fixedly connected to a driving worm 25. The end of the driving worm 25 passes through one of the driving blocks 23 and is rotatably connected to the other driving block 23. The driving worm 25 is engaged with the adjusting worm gear 22, and the driving motor 24 drives the driving worm 25 to rotate.

[0028] Working principle: When in use, first add water to the inside of the heating box 1, then fit the watertight shell 3 on the assembly frame 4 with the heating box 1, then pour the material to be heated into the bottom of the watertight shell 3, then install the assembly branch pipe 7 and the external water pump, then start the water pump to discharge the water into the assembly branch pipe 7, then start the heater 8 on the assembly branch pipe 7 to heat the water, so that the heated water passes through the assembly branch pipe 7 and is discharged into the assembly serpentine pipe 5, then the assembly branch pipe 7 conducts heating to the water inside the heating box 1, followed by starting the heating conduit 16, so that the heating conduit 16 heats the water inside the heating box 1, so that the heated water passes through the watertight shell 3 for conduction heating, so that the material inside the watertight shell 3 is heated in a water bath to ensure the conduction heating effect.

[0029] At the same time, the moving motor 13 is started, and the moving shaft 15 on the moving disk 14 is driven to rotate by the moving motor 13. Then the moving shaft 15 slides inside the moving circular plate 11, so as to push the moving rack 10 on the moving circular plate 11 to move. Then the moving slider 9 on the moving rack 10 slides and guides along the inside of the moving groove, so that the moving rack 10 moves back and forth. Then the moving rack 10 also drives multiple assembly gears 6 to rotate. At the same time, the assembly gear 6 also drives the serpentine tube 5 to rotate, thereby flowing and heating the water inside the heating box 1, thereby fully conducting and heating the material inside the watertight shell 3, ensuring the adjustment of the conduction heating effect.

[0030] Then start the regulating pump 18, and drive the first regulating branch 19 to extract the heated water inside the heating box 1 through the regulating pump 18, so that the heated water is discharged into the second regulating branch 20, and then the hot water is discharged into the regulating mixing tube 21, followed by the hot water on the regulating mixing tube 21 being discharged into multiple stirring tubes, so that the material is stirred and heated, and at the same time, the heated water is discharged from the regulating mixing tube 21 into the interior of the heating box 1, so as to continuously stir and heat the material, and then start the driving motor 24, and drive the regulating worm gear 22 on the driving worm 25 to rotate through the driving motor 24, and then the regulating worm gear 22 also drives the regulating mixing tube 21 to rotate, so that the multiple stirring tubes on the regulating mixing tube 21 stir the material, thereby reducing the condensation of the material and ensuring the active stirring and heating effect.

[0031] Finally, it should be noted that the above is only a preferred embodiment of the present invention and is not intended to limit the present invention. Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art can still modify the technical solutions described in the aforementioned embodiments or make equivalent replacements for some of the technical features therein. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present invention should be included in the scope of protection of the present invention.

Claims

1. A device for heating a colloidal palladium solution in a water bath, comprising a heating box (1), characterized in that: The side wall of the heating box (1) is fixedly connected with a control panel (2), the surface of the heating box (1) is fixedly connected with a drain pipe, the side wall of the drain pipe is connected with a drain valve, a water-proof shell (3) is provided inside the heating box (1), the outer wall of the water-proof shell (3) is fixedly sleeved with an assembly frame (4), the front of the heating box (1) is provided with an assembly branch pipe (7), the outer wall of the assembly branch pipe (7) is fixedly sleeved with a heater (8), an assembly serpentine pipe (5) is rotatably connected between the two sides of the inner wall of the heating box (1), one end of the assembly serpentine pipe (5) passes through the heating box (1) and is rotatably connected to the assembly branch pipe (7), the outer wall of the assembly serpentine pipe (5) is fixedly sleeved with an assembly gear (6), and the surface of the heating box (1) is connected with a moving component for adjusting the rotation of the assembly gear (6); A heating conduit (16) is fixedly connected between the two sides of the inner wall of the heating box (1), an adjustment bracket (17) is fixedly connected to the top of the water-proof shell (3), and a material extraction component is connected to the top of the adjustment bracket (17).

2. The device for heating a colloidal palladium solution in a water bath according to claim 1, characterized in that: The movable assembly comprises a movable groove provided on the surface of the heating box (1); a movable slider (9) is slidably connected inside the movable groove; a movable rack (10) is fixedly connected to the surface of the movable slider (9); a plurality of assembly gears (6) are all meshed and connected to the movable rack (10); a movable circular plate (11) is fixedly connected to the bottom of the movable rack (10); and a movable L-shaped support plate (12) is fixedly connected to the surface of the heating box (1).

3. The device for heating a colloidal palladium solution in a water bath according to claim 2, wherein: The surface of the movable L-shaped support plate (12) is fixedly connected to a movable motor (13); the output shaft of the movable motor (13) passes through the movable L-shaped support plate (12) and is fixedly connected to a movable disk (14); the back of the movable disk (14) is rotatably connected to a movable rotating shaft (15); and the movable rotating shaft (15) is slidably connected to the inside of the movable circular plate (11).

4. The device for heating a colloidal palladium solution in a water bath according to claim 1, wherein: The pumping assembly includes a regulating pump (18) fixedly connected to the top of the regulating bracket (17), and the water inlet and water outlet of the regulating pump (18) are respectively fixedly connected to a first regulating branch pipe (19) and a second regulating branch pipe (20), and the end of the first regulating branch pipe (19) passes through the waterproof shell (3) and extends to the interior of the heating box (1).

5. The device for heating a colloidal palladium solution in a water bath according to claim 4, characterized in that: The other end of the second regulating branch pipe (20) is rotatably connected to an regulating mixing pipe (21), the end of the regulating mixing pipe (21) passes through the regulating bracket (17) and the water-proof shell (3) and extends to the interior of the heating box (1), the outer wall of the regulating mixing pipe (21) is fixedly sleeved with an regulating worm gear (22), and a plurality of stirring pipes are fixedly connected on both sides of the outer wall of the regulating mixing pipe (21), and the top of the regulating bracket (17) is connected to an regulating component for adjusting the rotation of the regulating worm gear (22).

6. The device for heating a colloidal palladium solution in a water bath according to claim 5, characterized in that: The adjustment assembly comprises two driving blocks (23) fixedly connected to the top of the adjustment bracket (17), wherein a driving motor (24) is fixedly connected to the side wall of one of the driving blocks (23), and a driving worm (25) is fixedly connected to the output end of the driving motor (24), and the end of the driving worm (25) passes through one of the driving blocks (23) and is rotationally connected to the other driving block (23), and the driving worm (25) is engaged with the adjustment worm wheel (22).