Hesperetin concentrating and refining device

By designing baffle-layered refining tubes and negative pressure components in the hesperidin concentration and refining device, the problems of small evaporation area and uneven heating in traditional equipment are solved, efficient concentration and reuse of alcohol solvents are achieved, and the effect of energy conservation and emission reduction is achieved.

CN223324040UActive Publication Date: 2025-09-12ZHANGJIAJIE GUANGSHEN BIOTECHNOLOGY CO LTD
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Patent Information

Application Number
CN202422791850.X
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-11-15
Publication Date
2025-09-12
Estimated Expiration
2034-11-15

AI Technical Summary

Technical Problem

Traditional hesperetin concentration equipment has a small evaporation area and uneven heating, resulting in low purification efficiency and difficulty in recycling the alcohol solvent.

Method used

A hesperidin concentration and refining device was designed. The device consisted of a refining box divided into two layers by a partition, a refining tube with small holes and wrapped with a heating ring. The alcohol solvent was recovered through a negative pressure component, the dosing component controlled the flow rate, and the heating ring adjusted the heating power, thereby significantly increasing the evaporation area and reusing the alcohol solvent.

Benefits of technology

The concentration efficiency of hesperetin is improved, energy conservation and emission reduction effects are achieved, and the alcohol solvent can be reused.

✦ Generated by Eureka AI based on patent content.

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Abstract

The hesperetin concentrating and refining device comprises a refining box, the interior of the refining box is divided into an upper layer and a lower layer through a partition plate, a plurality of refining pipes are obliquely arranged in an upper-layer evaporation chamber, a plurality of small holes are formed in the upper half pipe body of each refining pipe in the chamber, a heating ring is wound on the pipe body of each refining pipe, and an inlet in the oblique upper end of each refining pipe is connected with a batching assembly. An exhaust port of the evaporation chamber is connected with the lower-layer recovery chamber through a negative pressure assembly; according to the device, an original solution enriched with hesperetin is added into each refining pipe through the batching assembly, and in the process that the original solution downwards flows along the pipe body, an alcohol solvent in the solution is gradually heated and evaporated by the heating ring, so that the evaporation area of the original solution is greatly increased, and the concentration efficiency is improved; and the alcohol solvent is pumped into the recovery chamber through the negative pressure assembly for recycling, so that the device has the characteristics of energy conservation and emission reduction.
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Description

Technical Field

[0001] The utility model relates to the technical field of hesperetin production equipment, in particular to a hesperetin concentration and refining device. Background Art

[0002] Hesperetin is a natural flavonoid compound that is mainly found in the peels of citrus fruits, such as oranges, grapefruits, and lemons. It has strong antioxidant properties, can neutralize free radicals in the body, reduce oxidative damage, and promote cell health. Studies have shown that hesperetin helps reduce inflammation and is helpful in preventing chronic diseases. At the same time, it can also lower blood pressure and improve blood lipid levels, which is beneficial to cardiovascular health. At present, high-purity hesperetin is usually prepared from Citrus aurantium fruits. The preparation process requires multiple extractions with alcohol solvents, and the original solution obtained by extraction needs to be heated and concentrated. Traditional concentration equipment has problems such as small evaporation area and uneven heating, resulting in low purification efficiency and difficulty in recovering the solvent for secondary use. A new type of refining equipment is needed to solve the above problems. Utility Model Content

[0003] In order to solve the above problems, the utility model proposes a hesperidin concentration and refining device, including a refining box, which is divided into an upper and lower layer by a partition. A plurality of refining tubes are arranged obliquely in the upper evaporation chamber. The upper half of the refining tube is provided with a plurality of small holes. The refining tube body is wrapped with a heating ring. The inlet at the oblique upper end of the refining tube is connected to the ingredient assembly. The exhaust port of the evaporation chamber is connected to the lower recovery chamber through a negative pressure assembly.

[0004] Furthermore, the small holes are divided into several small groups and distributed parallel to the axial direction on the refining tube. The heating rings are arranged between adjacent groups. The bottoms of each heating ring are connected by a wiring tube. The positive and negative lines of the heating wire in the heating ring are connected to the distribution box on the outer wall of the refining box through the wiring tube. The power cord of the distribution box is connected to the external power supply. The distribution box can adjust the heating power of each heating ring through the corresponding knob.

[0005] Furthermore, the batching assembly includes a distribution box, the bottom surface of the distribution box is a slope, the top surface of the distribution box is connected to the feed hopper, the bottom outlet of the feed hopper is located above the slope, the lower end of the slope is connected to the upper end of each batching pipe, the batching pipe body is provided with a control valve, and the lower end of the batching pipe is connected to the inclined upper end inlet of the refining pipe.

[0006] Furthermore, the negative pressure component includes a transfer box, each input pipe on the top of the transfer box is connected to the exhaust port on the side wall of the evaporation chamber, the bottom outlet of the transfer box is connected to the recovery chamber through a negative pressure pump, the output pipe of the negative pressure pump is inserted below the liquid level of the recovery chamber, and a discharge pipe with a regulating valve is provided at the bottom of the recovery chamber.

[0007] Furthermore, the outlet at the oblique lower end of the refining tube passes through the outside of the evaporation chamber, and a collecting tank is provided below the outlet of the refining tube.

[0008] The beneficial effects of the utility model are as follows: the utility model adds a raw solution enriched with hesperidin into each refining tube through the ingredient component, the flow rate of each refining tube is adjusted by a control valve, and the raw solution is heated step by step by the heating ring to evaporate the alcohol solvent in the solution during the process of flowing downward along the tube body. The heating power of each heating ring is adjusted by the distribution box, which greatly increases the evaporation area of ​​the raw solution and improves the concentration efficiency. The alcohol solvent is drawn into the recovery room through the negative pressure component for reuse, so that the device has the characteristics of energy saving and emission reduction. BRIEF DESCRIPTION OF THE DRAWINGS

[0009] Figure 1 This is a front view structural cross-sectional view of the utility model;

[0010] Figure 2 It is a side structural schematic diagram of the utility model.

[0011] The description of the accompanying numbers is as follows: 1. Refining box; 101. Partition; 102. Evaporation chamber; 103. Exhaust port; 104. Recovery chamber; 105. Discharge pipe; 2. Refining pipe; 201. Small hole; 3. Heating ring; 301. Wiring pipe; 302. Distribution box; 303. Knob; 4. Distribution box; 401. Slope; 5. Feed hopper; 6. Dosing pipe; 601. Control valve; 7. Transfer box; 701. Input pipe; 8. Negative pressure pump; 9. Collection tank. DETAILED DESCRIPTION

[0012] In the description of this utility model, it should be noted that the terms "center," "upper," "lower," "left," "right," "vertical," "horizontal," "inner," and "outer," etc., indicating directions or positional relationships, are based on the directions or positional relationships shown in the accompanying drawings and are intended solely to facilitate the description of this utility model and simplify the description. They do not indicate or imply that the devices or components referred to must have a specific direction, be constructed, or operate in a specific direction. Therefore, they should not be construed as limitations on this utility model. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and should not be construed as indicating or implying relative importance.

[0013] In the description of this utility model, it should be noted that, unless otherwise expressly specified or limited, the terms "mounted," "connected," and "connected" should be understood in a broad sense. For example, they can refer to fixed connections, detachable connections, or integral connections; mechanical connections, electrical connections; direct connections, indirect connections through an intermediate medium, and internal communication between two components. Those skilled in the art will understand the specific meanings of the above terms in this utility model based on the specific circumstances.

[0014] The present invention will be further described below with reference to the accompanying drawings:

[0015] like Figure 1 and Figure 2 As shown, the hesperetin concentration and refining device includes a refining box 1, which is divided into an upper and lower layer by a partition 101. A plurality of refining tubes 2 are obliquely arranged in the upper evaporation chamber 102. The upper half of the refining tube 2 in the chamber is provided with a plurality of groups of small holes 201 distributed parallel to the axial direction. The refining tube 2 is wrapped around the tube body of the refining tube 2. The heating ring 3 is arranged between adjacent groups. The bottom of each heating ring 3 is connected by a wiring tube 301. The positive and negative lines of the heating wire in the heating ring 3 are connected to the distribution box 302 on the outer wall of the refining box 1 through the wiring tube 301. The power line of the distribution box 302 is connected to the external power supply. The distribution box 302 can adjust the heating power of each heating ring 3 through the corresponding knob 303.

[0016] In this embodiment, each refining tube 2 distributes the flow through a dosing assembly, which includes a distribution box 4. The bottom surface of the distribution box 4 is a slope 401. The top surface of the distribution box 4 is connected to the feed hopper 5. The bottom outlet of the feed hopper 5 is located above the slope 401. The bottom of the slope 401 is connected to the upper end of each dosing tube 6. The tube body of the dosing tube 6 is provided with a control valve 601. The lower end of the dosing tube 6 is connected to the oblique upper end inlet of the refining tube 2. The oblique lower end outlet of the refining tube 2 passes through the outside of the evaporation chamber 102. A collecting tank 9 is provided below the outlet of the refining tube 2.

[0017] In this embodiment, the evaporation chamber 102 is connected to the lower recovery chamber 104 through a negative pressure component. The negative pressure component includes a transfer box 7. Each input pipe 701 on the top of the transfer box 7 is connected to the exhaust port 103 on the side wall of the evaporation chamber 102. The bottom outlet of the transfer box 7 is connected to the recovery chamber 104 through a negative pressure pump 8. The output pipe 801 of the negative pressure pump 8 is inserted below the liquid level of the recovery chamber 104. The alcohol gas drawn into the chamber is directly dissolved in the alcohol solution. A discharge pipe 105 with a regulating valve is provided at the bottom of the recovery chamber 104. The alcohol solution is discharged from the recovery chamber 104 through the discharge pipe 105 for secondary utilization.

[0018] The working principle of this utility model is as follows:

[0019] A raw solution enriched with hesperetin is injected from the feed hopper 5 into the distribution box 4. The control valves 601 are adjusted to ensure a laminar flow of the raw solution into the refining tube 2 at a specified flow rate. The heating power of the front, middle, and rear heating rings 3 is adjusted using knobs 303 to gradually evaporate the alcohol solvent in the raw solution and allow it to enter the evaporation chamber 102 through the aperture 201, while also preventing overheating of the raw solution. During the concentration process, the negative pressure pump 8 is activated to evacuate the evaporation chamber 102, drawing the alcohol vapor into the recovery chamber 104 for subsurface dissolution. The regulating valve on the discharge pipe 105 is then opened to transfer the alcohol solution for secondary use. After evaporation and alcohol removal, the hesperetin concentrate flows into the collection tank 9 for collection. The collected concentrate can then be reinjected into the feed hopper 5 for secondary refining.

[0020] The utility model adds a raw solution enriched with hesperetin into each refining tube 2 through a dosing assembly. As the raw solution flows downward along the tube body, it is gradually heated by the heating ring 3 to evaporate the alcohol solvent in the solution, thereby significantly increasing the evaporation area of ​​the raw solution and improving the concentration efficiency. The alcohol solvent is drawn into the recovery chamber 104 through the negative pressure assembly for reuse, thereby achieving the characteristics of energy conservation and emission reduction.

[0021] The above shows and describes the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited to the above embodiments. The above embodiments and descriptions are merely illustrative of the principles of the present invention. Various changes and improvements may be made to the present invention without departing from the spirit and scope of the present invention, and such changes and improvements shall fall within the scope of the present invention as claimed.

Claims

1. A hesperidin concentration and refining device, comprising a refining box (1), characterized in that: The refining box (1) is divided into an upper layer and a lower layer by a partition (101). A plurality of refining tubes (2) are obliquely arranged in the upper evaporation chamber (102). The upper half of the refining tube (2) in the chamber is provided with a plurality of small holes (201). The refining tube (2) is wound around a heating ring (3). The inlet at the oblique upper end of the refining tube (2) is connected to a batching assembly. The exhaust port (103) of the evaporation chamber (102) is connected to a lower recovery chamber (104) via a negative pressure assembly.

2. The hesperetin concentration and refining device according to claim 1, characterized in that: The small holes (201) are divided into a plurality of small groups and are distributed in parallel along the axial direction on the refining tube (2). The heating rings (3) are arranged between adjacent small groups. The bottoms of the heating rings (3) are connected through a wiring tube (301). The positive and negative lines of the heating wires in the heating rings (3) are connected to the distribution box (302) on the outer wall of the refining box (1) through the wiring tube (301). The power line of the distribution box (302) is connected to an external power supply. The distribution box (302) can adjust the heating power of each heating ring (3) through a corresponding knob (303).

3. The hesperetin concentration and refining device according to claim 1, characterized in that: The batching assembly comprises a distribution box (4), the bottom surface of the distribution box (4) is a slope (401), the top surface of the distribution box (4) is connected to the feed hopper (5), the bottom outlet of the feed hopper (5) is located above the slope (401), the bottom of the slope (401) is connected to the upper end of each batching pipe (6), the pipe body of the batching pipe (6) is provided with a control valve (601), and the lower end of the batching pipe (6) is connected to the upper inlet of the oblique end of the refining pipe (2).

4. The hesperetin concentration and refining device according to claim 1, characterized in that: The negative pressure assembly comprises a transfer box (7), wherein each input pipe (701) at the top of the transfer box (7) is connected to an exhaust port (103) on the side wall of the evaporation chamber (102), and the bottom outlet of the transfer box (7) is connected to the recovery chamber (104) via a negative pressure pump (8), wherein the output pipe (801) of the negative pressure pump (8) is inserted below the liquid level of the recovery chamber (104), and a discharge pipe (105) with a regulating valve is provided at the bottom of the recovery chamber (104).

5. The hesperetin concentration and refining device according to claim 1, characterized in that: The outlet at the oblique lower end of the refining tube (2) passes out of the evaporation chamber (102), and a collecting tank (9) is provided below the outlet of the refining tube (2).