Novel yellow phosphorus burning acid spraying device

By improving the structure of the spray device and using high-temperature and corrosion-resistant materials and designs, the problem of easy melting of the graphite spray tower nozzle was solved, the temperature was reduced and the output was increased, the nozzle had a uniform condensation effect, and the service life of the spray gun was extended.

CN223351915UActive Publication Date: 2025-09-19HUBEI XINGFA CHEM GRP CO LTD
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Patent Information

Application Number
CN202422691481.7
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-11-05
Publication Date
2025-09-19
Estimated Expiration
2034-11-05

AI Technical Summary

Technical Problem

The nozzles of traditional graphite spray towers are easy to melt, resulting in poor absorption effect and high exhaust gas temperature, which affects the subsequent absorption process. In addition, the nozzles are not resistant to high temperatures, which limits the increase in production.

Method used

A graphite spray tower and a spray water pipe are connected to the spray gun. The spray gun consists of a spray pipe, a spray flange, a connecting flange and a nozzle. The nozzle is equipped with an asymmetric inclined baffle. The spray gun and sleeve are made of 904L material, and the nozzle is a nickel-based high-temperature alloy to enhance temperature and corrosion resistance.

Benefits of technology

The temperature of the spray tower is reduced by 25℃, and the output is increased by 30%. The nozzles are evenly distributed to condense the high-temperature gas, extending the life of the spray gun. The spray gun is resistant to high temperature and corrosion, and its service life is extended.

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Abstract

The utility model discloses a novel yellow phosphorus burning acid spraying device, which adopts the technical scheme that the novel yellow phosphorus burning acid spraying device comprises a graphite spraying tower, a spraying water pipe is arranged above the graphite spraying tower, the spraying water pipe is connected with a spraying gun, the spraying gun is connected with the graphite spraying tower, the spraying gun comprises a spraying pipe, a spraying flange, a connecting flange and a spraying head, one end of the spraying pipe is provided with the connecting flange, and the other end of the spraying pipe is provided with the spraying head. A spraying flange and a connecting flange are arranged at the upper part of the spraying pipe; the device has the beneficial effects that (1) the device is used for spraying, the temperature in the graphite spraying tower is reduced by about 25 DEG C on the original basis, and the yield is increased by about 30%; (2) the spray head adopts two baffles which are inclined in different directions, so that the spray area can be increased, spray water is uniformly distributed, and high-temperature gas is condensed more quickly; (3) the spray gun is wrapped by the graphite sleeve, corrosion of a pipe body is reduced, and the service life of the spray gun is further prolonged; and (4) the whole spray gun is made of a 904L material, so that the service life of the spray gun is longer than that of a plastic spray gun adopted before.
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Description

Technical Field

[0001] The utility model belongs to the technical field of yellow phosphorus acid production, in particular to a novel yellow phosphorus acid spraying device. Background Art

[0002] The current process for producing acid from yellow phosphorus involves spontaneous combustion of phosphorus sludge in a furnace to produce phosphorus pentoxide, which is then absorbed with water to produce phosphoric acid. The temperature difference between the lean and rich phosphorus sludge production processes is significant. Traditional graphite spray tower nozzles are made of spiral plastic, and the high-temperature phosphorus pentoxide vapor easily melts the nozzles. This results in poor absorption efficiency and high exhaust temperatures, severely impacting subsequent absorption processes. The subsequent plastic PP tower is not heat-resistant, creating limitations and hindering production increases. Summary of the Invention

[0003] In response to the problems in the above-mentioned prior art, the utility model provides a new yellow phosphating acid spraying device, whose technical solution is: it includes a graphite spray tower, a spray water pipe is arranged above the graphite spray tower, the spray water pipe is connected to the spray gun, the spray gun is connected to the graphite spray tower, the spray gun includes a spray pipe, a spray flange, a connecting flange and a nozzle, a connecting flange is arranged at one end of the spray pipe, a spray flange and a connecting flange are arranged on the upper part, and the other end of the spray pipe is connected to the nozzle.

[0004] As a preferred solution, the spray water pipe is fixedly connected to the connecting flange through the spray water pipe flange at the pipe mouth.

[0005] As a preferred solution, the spray gun is fixedly connected to the compressed graphite sleeve flange on the graphite spray tower through a spray flange.

[0006] As a preferred solution, the surface of the spray pipe is sheathed with a graphite sleeve.

[0007] As a preferred solution, a graphite sleeve flange is provided on the graphite sleeve, and the graphite sleeve flange is fixedly connected to the spray flange and the pressed graphite sleeve flange.

[0008] As a preferred solution, the other end of the spray pipe is provided with an external thread, the inner wall of the spray head is provided with an internal thread matching the external thread, and the spray pipe is threadedly connected to the spray head.

[0009] As a preferred solution, a first baffle and a second baffle are fixedly provided on the inner wall of the nozzle, the first baffle is inclined to the left, and the second baffle is inclined to the right.

[0010] As a preferred solution, the inclination angle of the first baffle and the second baffle is 45-120°.

[0011] As a preferred solution, the spray gun as a whole, the pressed graphite sleeve flange, the spray water pipe flange and the graphite sleeve flange are all made of 904L material, which is resistant to high temperature and corrosion.

[0012] As a preferred solution, the nozzle is made of nickel-based high-temperature alloy.

[0013] Beneficial effects of the utility model:

[0014] (1) By spraying with this device, the temperature in the graphite spray tower drops by about 25°C compared with the original level, and the output increases by about 30%;

[0015] (2) The nozzle uses two baffles tilted in opposite directions, which can increase the spraying area, distribute the spray water evenly, and condense the high-temperature gas more quickly;

[0016] (3) The graphite sleeve wraps the spray gun to reduce the corrosion of the tube body and further extend the service life of the spray gun;

[0017] (4) The spray gun is made of 904L material. Compared with the plastic spray gun used before, 904L is more resistant to high temperature and corrosion, and the service life of the spray gun is longer. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] Figure 1 It is a schematic diagram of the overall structure of the utility model.

[0019] Figure 2 This is a structural diagram of the nozzle in the utility model.

[0020] In the figure: 1. Graphite spray tower; 101. Pressed graphite casing flange; 2. Spray gun; 201. Spray pipe; 202. Spray flange; 203. Connecting flange; 204. Spray head; 2041. First baffle; 2042. Second baffle; 3. Spray water pipe; 301. Spray water pipe flange; 4. Graphite casing; 401. Graphite casing flange. DETAILED DESCRIPTION

[0021] The present invention will be described in further detail below based on the accompanying drawings and specific embodiments.

[0022] Example 1

[0023] like Figure 1-2 The figure shows a novel yellow phosphating acid spraying device, comprising a graphite spray tower 1, a spray water pipe 3 is arranged above the graphite spray tower 1, the spray water pipe 3 is connected to the spray gun 2, the spray gun 2 is connected to the graphite spray tower 1, the spray gun 2 comprises a spray pipe 201, a spray flange 202, a connecting flange 203 and a spray head 204, a connecting flange 203 is provided at one end of the spray pipe 201, a spray flange 202 and a connecting flange 203 are provided at the upper part, and the other end of the spray pipe 201 is connected to the spray head 204.

[0024] Furthermore, the spray water pipe 3 is fixedly connected to the connecting flange 203 through the spray water pipe flange 301 at the pipe mouth.

[0025] Furthermore, the spray gun 2 is fixedly connected to the compressed graphite sleeve flange 101 on the graphite spray tower 1 through the spray flange 202.

[0026] Furthermore, a graphite sleeve 4 is sleeved on the surface of the spray pipe 201 , and the graphite sleeve 4 is used to isolate the spray pipe 201 , reduce corrosion of the pipe body, and extend the service life of the spray gun 2 .

[0027] Furthermore, a graphite sleeve flange 401 is provided on the graphite sleeve 4 , and the graphite sleeve flange 401 is fixedly connected to the spray flange 202 and the pressed graphite sleeve flange 101 .

[0028] Furthermore, the other end of the spray pipe 201 is provided with an external thread, the inner wall of the spray head 204 is provided with an internal thread matching the external thread, and the spray pipe 201 is threadedly connected to the spray head 204.

[0029] Furthermore, a first baffle 2041 and a second baffle 2042 are fixedly provided on the inner wall of the nozzle 204 . The first baffle 2041 is inclined to the left, and the second baffle 2042 is inclined to the right.

[0030] Furthermore, the inclination angles of the first baffle 2041 and the second baffle 2042 are 45-120 degrees. This design enables the nozzle to increase the spraying area, distribute the spray water evenly, and condense the high-temperature gas more quickly.

[0031] Furthermore, the entire spray gun 2, the pressed graphite sleeve flange 101, the spray water pipe flange 301 and the graphite sleeve flange 401 are all made of 904L material, which is resistant to high temperature and corrosion.

[0032] Furthermore, the nozzle 204 is made of nickel-based high-temperature alloy, making the nozzle 204 more durable.

[0033] The above-mentioned device is used in the following process: the spray gun 2 is assembled with the graphite sleeve 4, and then inserted into the compressed graphite sleeve flange 101 of the graphite spray tower 1, the spray flange 202, the graphite sleeve flange 401 and the compressed graphite sleeve flange 101 are fixedly connected with bolts, and the spray water pipe flange 301 on the spray water pipe 3 is fixedly connected with the connecting flange 203 with bolts, the installation of the spray gun 2 is completed, and the spray water pipe is opened to spray acid.

Claims

1. A novel yellow phosphating acid spraying device, comprising a graphite spray tower (1), a spray water pipe (3) being arranged above the graphite spray tower (1), characterized in that: The spray water pipe (3) is connected to the spray gun (2), and the spray gun (2) is connected to the graphite spray tower (1). The spray gun (2) includes a spray pipe (201), a spray flange (202), a connecting flange (203) and a spray head (204). The connecting flange (203) is provided at one end of the spray pipe (201), and the spray flange (202) and the connecting flange (203) are provided at the upper part. The other end of the spray pipe (201) is connected to the spray head (204).

2. A novel yellow phosphating acid spraying device according to claim 1, characterized in that, The spray water pipe (3) is fixedly connected to the connecting flange (203) via the spray water pipe flange (301) at the pipe opening.

3. A novel yellow phosphating acid spraying device according to claim 1, characterized in that, The spray gun (2) is fixedly connected to the compressed graphite sleeve flange (101) on the graphite spray tower (1) via the spray flange (202).

4. A novel yellow phosphating acid spraying device according to claim 1, characterized in that, The surface of the spray pipe (201) is sheathed with a graphite sleeve (4).

5. A novel yellow phosphating acid spraying device according to claim 4, characterized in that, A graphite sleeve flange (401) is provided on the graphite sleeve (4), and the graphite sleeve flange (401) is fixedly connected to the spray flange (202) and the pressed graphite sleeve flange (101).

6. A novel yellow phosphating acid spraying device according to claim 1, characterized in that, The other end of the spray pipe (201) is provided with an external thread, the inner wall of the spray head (204) is provided with an internal thread that matches the external thread, and the spray pipe (201) and the spray head (204) are threadedly connected.

7. A novel yellow phosphating acid spraying device according to claim 1, characterized in that, A first baffle (2041) and a second baffle (2042) are fixedly provided on the inner wall of the nozzle (204), wherein the first baffle (2041) is inclined to the left, and the second baffle (2042) is inclined to the right.

8. A novel yellow phosphating acid spraying device according to claim 7, characterized in that: The inclination angles of the first baffle (2041) and the second baffle (2042) are 45-120°.