Crystalline flake graphite pickling tank

By setting multiple liquid inlet pipes and nozzles at the bottom of the pickling tank and combining the overflow port to discharge the acid, the problem of low pickling efficiency is solved, and the pickling efficiency is improved and impurities are effectively treated.

CN223417862UActive Publication Date: 2025-10-10HUBEI LONGSHENG NEW MATERIALS CO LTD
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Patent Information

Application Number
CN202422663140.9
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-10-31
Publication Date
2025-10-10
Estimated Expiration
2034-10-31

AI Technical Summary

Technical Problem

The pickling efficiency of flake graphite pickling in the prior art is low, mainly because the flow efficiency of the acid solution is limited by the flow rate of the liquid inlet pipe, and increasing the flow rate may cause the acid solution to overflow.

Method used

A plurality of liquid inlet pipes are arranged in parallel at the bottom of the pickling tank body. A plurality of nozzles are installed on each liquid inlet pipe. The acid is sprayed upward through the nozzle and discharged through the overflow port to increase the acid flow rate. The loading tank is stabilized by a supporting structure, and a slag discharge device is set to handle impurities.

Benefits of technology

The pickling efficiency is improved, the acid flow rate is increased, the problem of low pickling efficiency is solved, and at the same time, the stable discharge of acid and the timely removal of impurities are ensured.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model provides a crystalline flake graphite pickling tank which comprises a pickling tank body, a plurality of liquid inlet pipes which are transversely arranged side by side are arranged at the bottom in the pickling tank body, a plurality of spray heads are respectively arranged on each liquid inlet pipe, the spray heads on each liquid inlet pipe are distributed in the axial direction, and outlets of the spray heads face upwards. An overflow port is further formed in the side wall of the upper end of the pickling tank body; the loading tank comprises a surrounding frame and a partition plate for separating the bottom of the surrounding frame, a plurality of through holes are formed in the surrounding frame and the partition plate, supporting plates are fixedly connected to the two ends of the bottom of the surrounding frame respectively, and notches for containing the liquid inlet pipes are formed in the supporting plates so that the supporting plates can abut against the inner bottom face of the pickling tank body. According to the utility model, the problem that the pickling efficiency is maintained at a lower level in the prior art is solved.
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Description

Technical Field

[0001] The utility model relates to the technical field of flake graphite processing equipment, in particular to a flake graphite pickling tank. Background Art

[0002] During the processing of expandable graphite, the flake graphite used as the raw material requires pickling. In existing technology, the raw material (flake graphite) is typically placed in a pickling tank, where acid is then introduced for soaking and rinsing. Wastewater generated during this process is continuously discharged and then filtered and processed before being returned for recycling. During the pickling process, the acid is typically introduced into the tank via an inlet pipe, typically located at a higher position, and then discharged through a drain pipe at the bottom. During this process, the acid soaks and rinses the material. However, the acid flow efficiency depends on the inlet flow rate, which is typically low. Furthermore, increasing the flow rate could cause the acid to overflow the tank, resulting in a relatively low overall pickling efficiency. Utility Model Content

[0003] In view of the deficiencies in the prior art, the utility model provides a flake graphite pickling tank, which solves the problem in the prior art that the pickling efficiency is maintained at a low level.

[0004] According to an embodiment of the present utility model, a flake graphite pickling tank comprises: a pickling tank body, a plurality of liquid inlet pipes arranged side by side in a transverse manner are installed at the bottom of the pickling tank body, a plurality of nozzles are installed on each liquid inlet pipe, the nozzles on each liquid inlet pipe are distributed along the axial direction and the outlet is arranged upward, and an overflow port is also provided on the upper end side wall of the pickling tank body; a loading tank, the loading tank comprises a surrounding frame and a partition separating the bottom of the surrounding frame, a plurality of through holes are provided on the surrounding frame and the partition, support plates are respectively fixedly connected to the two ends of the bottom of the surrounding frame, and notches are also provided on the support plates for accommodating each liquid inlet pipe so that the support plates can be against the inner bottom surface of the pickling tank body.

[0005] In the above embodiment, more liquid inlet pipes are provided at the bottom of the pickling tank body, and more acid is introduced into the pickling tank body through the nozzle, and then the raw materials in the loading tank are flushed upward and discharged through the overflow port provided at a higher position. In this way, the flow rate of the acid can be increased, thereby improving the pickling efficiency accordingly, solving the problem of the pickling efficiency being maintained at a low level in the prior art.

[0006] Furthermore, support bars are fixedly connected to the two end walls facing each other in the pickling tank body, and ears that can overlap with the two support bars are fixedly connected to the loading tank, and the two ears are fixedly connected to lifting ears that extend above the pickling tank body.

[0007] Furthermore, the overflow port is located above the support bar.

[0008] Furthermore, the ear includes a horizontal plate and a vertical plate fixedly connected thereto, the horizontal plate is fixedly connected to the outer wall of the upper end of the loading slot, the vertical plate is abutted against the support bar, and all the through holes are located below the horizontal plate.

[0009] Furthermore, a plurality of reinforcing bars are fixedly connected to the frame and are located below the partition and fixedly connected to the partition.

[0010] Furthermore, both ends of the liquid inlet pipe are fixedly passed through the outside of the pickling tank body and are respectively installed with valves.

[0011] Furthermore, the bottom of the pickling tank body is fixedly connected to a slag discharge bucket communicated therewith.

[0012] Furthermore, a slag discharge pipe is fixedly connected to the lower end of the slag discharge bucket. The slag discharge pipe is arranged horizontally and a drive motor is installed on the outside of one end. A conveying screw is coaxially rotated in the slag discharge pipe and one end of the conveying screw is connected to the drive motor. An opening is provided at the end of the slag discharge pipe away from the drive motor.

[0013] Furthermore, a guide groove connected to the overflow port is fixedly connected to the outer wall of the pickling tank body.

[0014] Furthermore, support legs are fixedly connected to the four corners of the bottom of the pickling tank body.

[0015] Compared with the prior art, the present invention has the following beneficial effects:

[0016] By arranging the liquid inlet pipe in the pickling tank body and introducing more acid liquid by spraying acid liquid upward through the nozzle, the flow rate of the acid liquid during the pickling process is increased, thereby improving the pickling efficiency accordingly, solving the problem of the pickling efficiency being maintained at a low level in the prior art. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 This is a schematic diagram of the overall structure of an embodiment of the present utility model;

[0018] Figure 2 This is a schematic diagram of the side structure of the loading tank according to an embodiment of the present utility model;

[0019] Figure 3 for Figure 1 A magnified schematic diagram of the local structure at center A;

[0020] In the above drawings:

[0021] Pickling tank body 1, liquid inlet pipe 2, nozzle 3, overflow port 4, loading tank 5, frame 6, partition 7, support plate 8, notch 9, slag discharge bucket 10, slag discharge pipe 11, drive motor 12, reinforcement bar 13, guide groove 14, support foot 15, support bar 16, support ear 17, lifting ear 18. DETAILED DESCRIPTION

[0022] The technical solution of the present invention is further described below with reference to the accompanying drawings and embodiments.

[0023] In the description of the present invention, it should be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "up", "down", "front", "back", "left", "right", "vertical", "horizontal", "top", "bottom", "inside", "outside", "clockwise", "counterclockwise", "axial", "radial", "circumferential" and the like to indicate orientations or positional relationships based on the orientations or positional relationships shown in the accompanying drawings, and are only for the convenience of describing the present invention and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore should not be understood as a limitation to the present invention.

[0024] In an exemplary embodiment, Figure 1 、 2 As shown, this embodiment provides a flake graphite pickling tank, which includes: a pickling tank body 1, a plurality of liquid inlet pipes 2 arranged side by side in a transverse manner are installed at the bottom of the pickling tank body 1, and both ends of the liquid inlet pipes 2 are fixedly extended to the outside of the pickling tank body 1, both of which can be used as inlet ends for acid to enter, and are respectively installed with valves for controlling the opening and closing states, a plurality of nozzles 3 are respectively installed on each liquid inlet pipe 2, and the nozzles 3 on each liquid inlet pipe 2 are distributed along the axial direction and the outlet is arranged upward, and an overflow port 4 is also provided on the upper end side wall of the pickling tank body 1, the acid is introduced through the liquid inlet pipe 2, sprayed upward through the nozzle 3, and then the acid gradually rises and finally is discharged in an overflow manner through the overflow port 4 arranged at a higher position, so that the flow rate of the acid can be appropriately improved; a valve for loading the original A loading tank 5 for raw materials (i.e., flake graphite) is provided. The loading tank 5 includes a frame 6 and a partition 7 separating the bottom of the frame 6. A plurality of through holes are provided on the frame 6 and the partition 7. The raw materials are loaded into the frame 6 of the loading tank 5, and the bottom is supported by the partition 7. The through holes on the periphery, i.e., the bottom, allow the acid to pass through normally, so that pickling can be smoothly achieved. Support plates 8 are fixedly connected to both ends of the bottom of the frame 6, and notches 9 are provided on the support plates 8 for accommodating each liquid inlet pipe 2 so that the support plates 8 can be against the inner bottom surface of the pickling tank body 1. The notch 9 is an inverted U-shaped structure, so that the loading tank 5 can be smoothly placed in the pickling tank body 1 without contacting or colliding with the provided liquid inlet pipe 2 and the nozzle 3 (the nozzle 3 is located below the partition 7 and is separated by a distance).

[0025] In the above embodiment, more liquid inlet pipes 2 are provided at the bottom of the pickling tank body 1, and more acid liquid is introduced into the pickling tank body 1 through the nozzles 3, and then the raw materials in the loading tank 5 are washed upward (the raw materials are also soaked), and are discharged through the overflow port 4 provided at a higher position. The overflow port 4 provided can be of a larger size (wider, higher), so that the acid liquid introduced through multiple liquid inlet pipes 2 can be discharged smoothly, so that the flow rate of the acid liquid can be increased, thereby improving the pickling efficiency accordingly, solving the problem of the pickling efficiency being maintained at a low level in the prior art; in more detail, all the nozzles 3 provided can be located directly below the enclosure 6; further, during operation, pickling may cause some impurities to fall, and heavier ones may settle downward, so a nozzle 3 connected to it is also provided at the bottom of the pickling tank body 1. The slag discharge hopper 10 is connected, and a slag discharge pipe 11 is fixedly connected to the lower end of the slag discharge hopper 10. The slag discharge pipe 11 is arranged horizontally and a drive motor 12 is installed on the outside of one end. A conveying screw is coaxially rotated in the slag discharge pipe 11 and one end of the conveying screw is connected to the drive motor 12. An opening is provided at the end of the slag discharge pipe 11 away from the drive motor 12, and the opening is the outlet. A valve is installed at the outlet (or a valve can be installed on the lower end of the slag discharge hopper 10). After a period of time, the valve can be opened, and the drive motor 12 can be started to drive the conveying screw to discharge the impurities at the bottom (together with the acid remaining in the pickling tank body 1). After the acid is discharged, the loading tank 5 can be taken out and the bottom can be cleaned through the opening above the pickling tank body 1. In this solution, each structure can be made of a material resistant to acid corrosion to ensure long-term normal operation.

[0026] like Figure 1 、 3 As shown, in order to improve the overall structural stability of the loading slot 5, a number of reinforcing bars 13 located below the partition 7 and fixedly connected to the partition 7 are fixedly connected in the frame 6. The reinforcing bars 13 provide upward support for the partition 7, thereby making it more stable.

[0027] In a further exemplary embodiment, Figure 1 、 3 As shown, the overflow port 4 can be a square frame-shaped structure, and a guide groove 14 connected to the overflow port 4 is fixedly connected to the outer wall of the pickling tank body 1 for receiving the overflowing acid liquid. Similar to the prior art, this part of the acid liquid can be filtered and processed, and then returned for reuse; furthermore, support legs 15 are fixedly connected at the four corners of the bottom of the pickling tank body 1, so that the bottom is raised and a height space is left for the smooth arrangement of structures such as the slag discharge bucket 10 and the slag discharge pipe 11.

[0028] like Figure 1-3As shown, the loading tank 5 is supported in the pickling tank body 1 by the support plate 8 at the bottom. In order to further improve its stability in the pickling tank body 1, support bars 16 are fixedly connected to the two end walls facing each other in the pickling tank body 1. The loading tank 5 is fixedly connected with ears 17 that can overlap with the two support bars 16. The two ears 17 are fixedly connected with lifting ears 18 extending to the top of the pickling tank body 1. At the same time, the loading tank 5 can be lifted out by lifting through the lifting ears 18 to facilitate the placement of raw materials. In and out, in more detail, the overflow port 4 is located above the support bar 16, and the upper edge of the overflow port 4 can also be located above all the through holes; in further detail, the ear 17 includes a horizontal plate and a vertical plate fixedly connected thereto, the horizontal plate is fixedly connected to the outer wall of the upper end of the loading slot 5, the vertical plate is against the support bar 16, all the through holes are located below the horizontal plate, the horizontal plate and the vertical plate are enclosed to form a "7", and the vertical plate is against the corresponding support bar 16, and cooperates with the support plate 8 at the bottom to stabilize the loading slot 5.

[0029] Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the utility model and are not limiting. Although the utility model is described in detail with reference to the preferred embodiments, ordinary technicians in this field should understand that the technical solution of the utility model can be modified or replaced by equivalents without departing from the purpose and scope of the technical solution of the utility model, which should be included in the scope of the claims of the utility model.

Claims

1. A flake graphite pickling tank, characterized in that: include: A pickling tank body, wherein a plurality of liquid inlet pipes are installed in parallel at the bottom of the pickling tank body, each of which is respectively installed with a plurality of nozzles, the nozzles on each of the liquid inlet pipes are distributed along the axial direction and the outlet is arranged upward, and an overflow port is also provided on the upper end side wall of the pickling tank body; The loading tank includes a frame and a partition separating the bottom of the frame. The frame and the partition are both provided with a plurality of through holes. The two ends of the bottom of the frame are also fixedly connected with support plates, and the support plates are also provided with notches for accommodating each of the liquid inlet pipes so that the support plates can be against the inner bottom surface of the pickling tank body.

2. The flake graphite pickling tank according to claim 1, characterized in that: Support bars are fixedly connected to the two end walls facing each other in the pickling tank body, and ears that can overlap with the two support bars are fixedly connected to the loading tank. The two ears are fixedly connected to lifting ears extending above the pickling tank body.

3. The flake graphite pickling tank according to claim 2, characterized in that: The overflow port is located above the support bar.

4. The flake graphite pickling tank according to claim 2, characterized in that: The support ear includes a horizontal plate and a vertical plate fixedly connected thereto, the horizontal plate is fixedly connected to the outer wall of the upper end of the loading slot, the vertical plate is against the support bar, and all the through holes are located below the horizontal plate.

5. The flake graphite pickling tank according to claim 1, characterized in that: A plurality of reinforcing bars are also fixedly connected in the enclosure frame and are located below the partition and fixedly connected to the partition.

6. The flake graphite pickling tank according to claim 1, characterized in that: Both ends of the liquid inlet pipe are respectively fixed to penetrate the outside of the pickling tank body and are respectively equipped with valves.

7. The flake graphite pickling tank according to claim 1, characterized in that: The bottom of the pickling tank body is also fixedly connected to a slag discharge bucket communicated therewith.

8. The flake graphite pickling tank according to claim 7, characterized in that: The lower end of the slag discharge hopper is also fixedly connected to a slag discharge pipe, which is arranged horizontally and has a drive motor installed on the outside of one end. A conveying screw is coaxially rotated in the slag discharge pipe and one end of the conveying screw is connected to the drive motor. An opening is provided at the end of the slag discharge pipe away from the drive motor.

9. The flake graphite pickling tank according to claim 1, characterized in that: A guide groove connected to the overflow port is also fixedly connected to the outer wall of the pickling tank body.

10. The flake graphite pickling tank according to any one of claims 1 to 9, characterized in that: Support legs are fixedly connected to the four corners of the bottom of the pickling tank body.