Separation equipment for production and preparation of ultra-pure ammonia

Abstract

The utility model belongs to the technical field of separation equipment, and particularly relates to separation equipment for producing and preparing ultrapure ammonia, which comprises an air pump, a connecting pipe is fixedly connected to the top end of the air pump, a jet pipe is fixedly connected to the output end of the air pump, an opening binding pipe is fixedly connected to the inner end of the right side of the jet pipe, and a low-pressure bin is arranged on the inner side of the middle end of the jet pipe. A drainage pipe is fixedly connected to the top end of the low-pressure bin, and a filtering assembly is arranged on the left side of the jet pipe. According to the separation equipment for producing and preparing the ultra-pure ammonia, the mixed ammonia gas is extracted by using the connecting pipe through the air pump and is sprayed out at a high speed through the opening bundling pipe, and the separation medium is extracted by using the drainage pipe through low pressure on the inner side of the opening bundling pipe and is mixed and conveyed out in the jet pipe, so that the dynamic mixing of the gas is realized; the separation efficiency can be improved, the gas-liquid contact is optimized, and the pure ammonia purification effect is promoted. Meanwhile, energy consumption is reduced, liquid accumulation and blockage are prevented, and stable operation of equipment is ensured.

Description

Technical Field

[0001] This utility model belongs to the field of separation equipment technology, specifically a separation equipment for the production and preparation of ultrapure ammonia. Background Technology

[0002] Ultrapure ammonia, as a high-purity chemical, is widely used in high-tech fields such as electronics, semiconductors, and photovoltaics. Its purity and quality requirements are extremely high, needing to reach 99.999% or higher. Traditional preparation methods struggle to meet the stringent control requirements for trace impurities such as moisture, oxides, and metal ions, making efficient separation equipment crucial. Current technologies include adsorption, membrane separation, cryogenic distillation, and composite technologies. These methods achieve efficient separation through specialized adsorbents, polymer membranes, and precise temperature control, while also developing towards highly selective materials, automated intelligent control, and environmental friendliness to improve separation efficiency, reduce energy consumption, and minimize pollution. With the rapid development of 5G, artificial intelligence, and new energy fields, the demand for electronic-grade ultrapure ammonia is increasing. Technological innovation in separation equipment not only helps meet high-purity requirements but also significantly reduces production costs and improves resource utilization, making its development of crucial equipment for the development of high-tech industries.

[0003] However, in actual use of existing solutions, the mixed ammonia gas and the separation medium are directly fed into the separation tower simultaneously for condensation and moisture separation. This may result in low separation efficiency, residual ammonia gas, and increased environmental pollution. Uneven gas-liquid flow within the tower may cause problems such as liquid accumulation and blockage, affecting the stable operation of the equipment. The inefficient condensation process also increases energy consumption, causes corrosion and scaling, reduces equipment lifespan, and increases maintenance costs.

[0004] Therefore, this utility model provides a separation device for the production and preparation of ultrapure ammonia. Utility Model Content

[0005] To overcome the shortcomings of existing technologies and solve the problem that low separation efficiency may result from not dynamically mixing the mixed ammonia gas with the separation medium, this utility model proposes a separation device for the production and preparation of ultrapure ammonia.

[0006] The technical solution adopted by this utility model to solve its technical problem is as follows: The separation equipment for the production and preparation of ultrapure ammonia according to this utility model includes an air pump, a connecting pipe fixedly connected to the top of the air pump, a jet pipe fixedly connected to the output end of the air pump, a bundle tube fixedly connected to the inner right end of the jet pipe, a low-pressure chamber opened on the inner side of the middle end of the jet pipe, a guide pipe fixedly connected to the top of the low-pressure chamber, and a filter assembly arranged on the left side of the jet pipe.

[0007] Furthermore, the filter assembly includes a filter tube, a filter tube is fixedly connected to the left side of the jet tube, a first sealing ring is fixedly connected to the middle of the inner side of the filter tube, a filter screen is fixedly connected to the bottom end of the first sealing ring, a second sealing ring is fixedly connected to the bottom end of the filter screen, a first bolt is fixedly connected to the bottom end of the second sealing ring, and a second bolt is threaded to the inner side of the bottom end of the first bolt.

[0008] Furthermore, a motor is fixedly connected to the inner side of the top of the filter tube, a transmission rod is fixedly connected to the output end of the motor, a cleaning blade is fixedly connected to the bottom end of the transmission rod, a collection cylinder is rotatably connected to the outer side of the bottom end of the cleaning blade, and the collection cylinder is fixedly connected to the filter screen.

[0009] Furthermore, an air inlet pipe is fixedly connected to the left side of the filter pipe, a separation tower is fixedly connected to the outside of the air inlet pipe, a first water inlet pipe is fixedly connected to the bottom of the separation tower, and a first water outlet pipe is fixedly connected to the front side of the top of the separation tower.

[0010] Furthermore, a diversion bowl is fixedly connected to the top of the air inlet pipe, a second water outlet pipe is fixedly connected to the inner left end of the diversion bowl, a collection bowl is fixedly connected to the right side of the second water outlet pipe, a condenser pipe is fixedly connected to the top of the diversion bowl, an air outlet pipe is fixedly connected to the top of the condenser pipe, and the air outlet pipe is fixedly connected to the separation tower.

[0011] Furthermore, a support leg is fixedly connected to the outer side of the bottom end of the separation tower.

[0012] The beneficial effects of this utility model are as follows:

[0013] 1. The separation equipment for the production and preparation of ultrapure ammonia described in this utility model uses a gas pump to extract mixed ammonia gas through a connecting pipe and ejects it at high speed through a jet tube. Meanwhile, a low-pressure system inside the jet tube draws in the separation medium through a guide pipe, where the mixture is mixed within the jet tube before being transported out. This dynamic gas mixing improves separation efficiency, optimizes gas-liquid contact, and promotes the purification of pure ammonia. Simultaneously, it reduces energy consumption, prevents liquid accumulation and blockage, and ensures stable equipment operation.

[0014] 2. The separation equipment for ultrapure ammonia production described in this utility model filters the mixed ammonia gas and separation medium through a filter screen. A motor drives a transmission rod to rotate cleaning blades, pushing the filtered impurities inside the filter screen downwards and collecting them in a collection cylinder. This helps improve the performance of the separation equipment for ultrapure ammonia production. It can increase the purity of ammonia gas, protect the equipment from corrosion, scaling, and clogging, and extend the equipment's service life. Attached Figure Description

[0015] The present invention will be further described below with reference to the accompanying drawings.

[0016] Figure 1 This is a three-dimensional structural diagram of the present invention;

[0017] Figure 2 This is a schematic cross-sectional view of the separation tower in this utility model;

[0018] Figure 3 This is a schematic cross-sectional view of the jet tube in this utility model;

[0019] Figure 4 This is a schematic cross-sectional view of the filter tube in this utility model. Figure 1 ;

[0020] Figure 5 This is a schematic cross-sectional view of the filter tube in this utility model. Figure 2 ;

[0021] In the diagram: 1. Separation tower; 11. First inlet pipe; 12. First outlet pipe; 13. Support leg; 2. Air inlet pipe; 21. Diverter bowl; 22. Collection bowl; 23. Second outlet pipe; 24. Condenser pipe; 25. Air outlet pipe; 3. Filter pipe; 31. First sealing ring; 32. Filter screen; 33. Second sealing ring; 34. First bolt; 35. Second bolt; 36. Motor; 37. Transmission rod; 38. Cleaning blade; 39. Collection cylinder; 4. Jet pipe; 41. Low-pressure chamber; 42. Drain pipe; 43. Bundle pipe; 44. Air pump; 45. Connecting pipe. Detailed Implementation

[0022] To make the technical means, creative features, objectives and effects of this utility model easier to understand, the present utility model will be further described below in conjunction with specific embodiments.

[0023] Example 1:

[0024] like Figures 1 to 5 As shown, the separation equipment for the production and preparation of ultrapure ammonia according to this utility model includes an air pump 44, a connecting pipe 45 fixedly connected to the top of the air pump 44, the connecting pipe 45 being fixed by the air pump 44, a jet pipe 4 fixedly connected to the output end of the air pump 44, the jet pipe 4 being fixed by the air pump 44, a bundled tube 43 fixedly connected to the inner right end of the jet pipe 4, the bundled tube 43 being fixed by the jet pipe 4, and the bundled tube 43 being fixedly connected to the output end of the air pump 44. The mixed ammonia gas drawn by the air pump 44 through the connecting pipe 45 is ejected through the bundled tube 43. A low-pressure chamber 41 is opened on the inner side of the middle end of the jet pipe 4, and a guide pipe 42 is fixedly connected to the top of the low-pressure chamber 41, the guide pipe 42 being supported and fixed by the low-pressure chamber 41. The mixed ammonia gas ejected at high speed through the bundled tube 43 forms a low-pressure zone in the low-pressure chamber 41, and the separation medium is drawn by the guide pipe 42. A filter assembly is provided on the left side of the jet pipe 4.

[0025] The filter assembly includes a filter tube 3. The filter tube 3 is fixedly connected to the left side of the jet tube 4. A first sealing ring 31 is fixedly connected to the middle of the inner side of the filter tube 3, and the filter tube 3 fixes the first sealing ring 31. A filter screen 32 is fixedly connected to the bottom of the first sealing ring 31, and the filter screen 32 is fixedly fixed by the first sealing ring 31, which also seals the filter tube 3 and the filter screen 32. A second sealing ring 33 is fixedly connected to the bottom of the filter screen 32, and the filter screen 32 fixes the second sealing ring 33. A first bolt 34 is fixedly connected to the bottom of the second sealing ring 33, and the second sealing ring 33 fixes the first bolt 34, which also seals the filter screen 32 and the first bolt 34. A second bolt 35 is threadedly connected to the inner side of the bottom of the first bolt 34, and the second bolt 35 seals the inner bottom of the first bolt 34.

[0026] A motor 36 is fixedly connected to the inner side of the top of the filter tube 3, supporting and fixing the motor 36 through the filter tube 3. A transmission rod 37 is fixedly connected to the output end of the motor 36, fixing the transmission rod 37 through the motor 36 and driving the transmission rod 37 to rotate. A cleaning blade 38 is fixedly connected to the bottom end of the transmission rod 37, fixing the cleaning blade 38 through the transmission rod 37 and driving the cleaning blade 38 to rotate through the transmission rod 37. A collection cylinder 39 is rotatably connected to the outer side of the bottom end of the cleaning blade 38. The collection cylinder 39 is fixedly connected to the filter screen 32, fixing the collection cylinder 39 through the filter screen 32. At the same time, the cleaning blade 38 rotates inside the filter screen 32 and the collection cylinder 39, thereby cleaning the inner wall of the filter screen 32 and pushing the cleaned impurities into the collection cylinder 39 for storage. After the collection cylinder 39 stores a certain amount, the second bolt 35 can be removed to clean the inside of the collection cylinder 39.

[0027] An air inlet pipe 2 is fixedly connected to the left side of the filter pipe 3. The air inlet pipe 2 is fixedly connected to the filter pipe 3. A separation tower 1 is fixedly connected to the outside of the air inlet pipe 2. The air inlet pipe 2 is fixedly connected to the separation tower 1. A first water inlet pipe 11 is fixedly connected to the bottom end of the separation tower 1. A first water outlet pipe 12 is fixedly connected to the front side of the top end of the separation tower 1. The first water inlet pipe 11 and the first water outlet pipe 12 are fixedly connected to the separation tower 1. Liquid nitrogen is delivered into the separation tower 1 through the first water inlet pipe 11 and output through the first water outlet pipe 12.

[0028] A diversion bowl 21 is fixedly connected to the top of the inlet pipe 2, and the diversion bowl 21 is supported and fixed by the inlet pipe 2. A second water outlet pipe 23 is fixedly connected to the inner left side of the diversion bowl 21, and the second water outlet pipe 23 is supported and fixed by the diversion bowl 21. A collection bowl 22 is fixedly connected to the right side of the second water outlet pipe 23, and the collection bowl 22 is supported and fixed by the second water outlet pipe 23. A condenser pipe 24 is fixedly connected to the top of the diversion bowl 21, and the bottom of the condenser pipe 24 is fixed by the diversion bowl 21. The mixed ammonia gas and separation medium after mixing and filtration are diverted into the condenser pipe 24 through the inlet pipe 2. The mixed ammonia gas and separation medium inside the condenser pipe 24 are condensed by the liquid nitrogen on the outside, thereby separating the water in the mixed ammonia gas and separation medium. An outlet pipe 25 is fixedly connected to the top of the condenser pipe 24, and the outlet pipe 25 is fixedly connected to the separation tower 1, and the outlet pipe 25 is fixed by the separation tower 1.

[0029] A support leg 13 is fixedly connected to the outer side of the bottom end of the separation tower 1, and the separation tower 1 is supported and fixed by the support leg 13.

[0030] Working Principle: During operation of the separation equipment for ultrapure ammonia production, mixed ammonia gas is first drawn from the gas pump 44 via the connecting pipe 45 and ejected at high speed through the nozzle 43. This high-speed ejection of the mixed ammonia gas creates a low-pressure zone within the low-pressure chamber 41. The separation medium is then drawn from the outlet pipe 42, thus mixing the mixed ammonia gas and the separation medium. The mixture is then conveyed into the filter pipe 3. After entering the filter screen 32, the mixed ammonia gas and the separation medium are filtered, removing impurities. Simultaneously, the motor 36 drives the cleaning blades 38 to rotate via the transmission rod 37, thereby clearing impurities. The cleaning blades 38 clean the impurities filtered from the inner wall of the filter screen 32 and push the impurities into the collection cylinder 39. The collection cylinder 39 collects the impurities. After a certain amount of impurities are collected, the second bolt 35 is removed to clean the impurities in the collection cylinder 39. Then, the filtered mixed ammonia and separation medium are transported into the diversion bowl 21 through the air inlet pipe 2 and diverted into the condenser pipe 24 through the diversion bowl 21. At the same time, liquid nitrogen is introduced into the separation tower 1 through the first water inlet pipe 11 to cool the condenser pipe 24. The water in the mixed ammonia and separation medium can be condensed through the condenser pipe 24, and the liquid nitrogen is discharged through the first water outlet pipe 12.

[0031] The terms "front," "back," "left," "right," "top," and "bottom" all refer to the figures in the accompanying drawings. Figure 1 Based on the perspective of the observer, the side of the device facing the observer is defined as the front, the left side of the observer is defined as the left, and so on.

[0032] In the description of this utility model, it should be understood that the terms "center", "longitudinal", "lateral", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings. They are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limiting the scope of protection of this utility model.

[0033] The foregoing has shown and described the basic principles, main features, and advantages of this utility model. Those skilled in the art should understand that this utility model is not limited to the above embodiments. The embodiments and descriptions in the specification are merely illustrative of the principles of this utility model. Various changes and modifications can be made to this utility model without departing from its spirit and scope, and all such changes and modifications fall within the scope of the claimed utility model. The scope of protection of this utility model is defined by the appended claims and their equivalents.

Claims

1. A separation device for the production and preparation of ultrapure ammonia, characterized in that, Includes an air pump (44), the top of which is fixedly connected to a connecting pipe (45), the output end of which is fixedly connected to a jet pipe (4), the inner right end of which is fixedly connected to a constriction tube (43), a low-pressure chamber (41) is provided on the inner side of the middle end of the jet pipe (4), the top of which is fixedly connected to a drainage pipe (42), and a filter assembly is provided on the left side of the jet pipe (4).

2. The separation equipment for the production and preparation of ultrapure ammonia according to claim 1, characterized in that, The filter assembly includes a filter tube (3), the filter tube (3) is fixedly connected to the left side of the jet tube (4), a first sealing ring (31) is fixedly connected to the middle of the inner side of the filter tube (3), a filter screen (32) is fixedly connected to the bottom of the first sealing ring (31), a second sealing ring (33) is fixedly connected to the bottom of the filter screen (32), a first bolt (34) is fixedly connected to the bottom of the second sealing ring (33), and a second bolt (35) is threadedly connected to the inner side of the bottom of the first bolt (34).

3. The separation equipment for the production and preparation of ultrapure ammonia according to claim 2, characterized in that, A motor (36) is fixedly connected to the inner side of the top of the filter tube (3). A transmission rod (37) is fixedly connected to the output end of the motor (36). A cleaning blade (38) is fixedly connected to the bottom end of the transmission rod (37). A collection cylinder (39) is rotatably connected to the outer side of the bottom end of the cleaning blade (38). The collection cylinder (39) is fixedly connected to the filter screen (32).

4. The separation equipment for the production and preparation of ultrapure ammonia according to claim 3, characterized in that, The filter tube (3) is fixedly connected to the left side of the air inlet pipe (2), the air inlet pipe (2) is fixedly connected to the outside of the separation tower (1), the bottom of the separation tower (1) is fixedly connected to the first water inlet pipe (11), and the top front of the separation tower (1) is fixedly connected to the first water outlet pipe (12).

5. The separation equipment for the production and preparation of ultrapure ammonia according to claim 4, characterized in that, The top end of the air inlet pipe (2) is fixedly connected to a diversion bowl (21), the inner left end of the diversion bowl (21) is fixedly connected to a second water outlet pipe (23), the right side of the second water outlet pipe (23) is fixedly connected to a collection bowl (22), the top end of the diversion bowl (21) is fixedly connected to a condenser pipe (24), the top end of the condenser pipe (24) is fixedly connected to an air outlet pipe (25), and the air outlet pipe (25) is fixedly connected to the separation tower (1).

6. The separation equipment for the production and preparation of ultrapure ammonia according to claim 5, characterized in that, The bottom outer side of the separation tower (1) is fixedly connected to a support leg (13).

Images