Heating furnace tube partition structure of double-tube vertical thermogravimetric atmosphere furnace

Abstract

The utility model discloses a heating furnace tube partition structure of a double-tube vertical thermogravimetric atmosphere furnace, relates to the technical field of experimental atmosphere furnaces, and aims to solve the problem that the heating environment cannot be adjusted according to the reaction condition of materials when the conventional experimental atmosphere furnace is used. The first inner cavity is formed in the lower portion of the interior of the double-tube vertical atmosphere furnace, a feeding vertical rod is arranged on one side of the interior of the first inner cavity, a connecting bottom plate is arranged at the upper end of the feeding vertical rod, the connecting bottom plate is in threaded connection with the upper end of the feeding vertical rod, and a mounting base is arranged above the connecting bottom plate; a supporting rod body is arranged in the middle of the upper end face of the feeding vertical rod, the supporting rod body penetrates through the connecting bottom plate and extends to one side of the outer portion of the upper mounting base, a temperature monitoring mechanism is arranged between the connecting bottom plate and the outer wall of the supporting rod body, and the second inner cavity is formed in the upper portion of the interior of the double-pipe furnace body. And a ceramic inner tube is arranged in the second inner cavity.

Description

Technical Field

[0001] This utility model relates to the field of experimental atmosphere furnace technology, specifically a partitioned structure for the heating tubes of a dual-tube vertical thermogravimetric atmosphere furnace. Background Technology

[0002] During the use of experimental atmosphere furnaces, the heated materials usually undergo physicochemical reactions at high temperatures, releasing fumes and gases that are harmful to humans and the environment. Experimental atmosphere furnaces can perform high-temperature heat treatment on materials under the protection of inert gases such as nitrogen and argon, avoiding oxidation of the materials and preparing high-purity samples. Therefore, they have become commonly used heat treatment experimental equipment in the fields of chemistry, chemical engineering, and materials science.

[0003] For example, the Chinese patent with publication number CN213668324U, entitled "(An Experimental Atmosphere Furnace Flue Gas Treatment Device)," includes: a cylindrical body, a filter assembly, and an exhaust assembly. The cylindrical body is equipped with a flue gas inlet pipe, and the cylindrical body contains a lower first limiting block and an upper second limiting block. The filter assembly is located within the cylindrical body above the flue gas inlet pipe, and includes a first filter structure and a second filter structure. This invention effectively purifies the flue gas generated by the experimental atmosphere furnace, preventing direct emission of the flue gas into the external environment and avoiding significant harm to experimental personnel and the environment. It employs a dual purification process using graphene carbon blocks and activated carbon blocks to ensure the cleanliness of the treated flue gas. Furthermore, the inclusion of a second stainless steel mesh inside the cylindrical body facilitates the replacement of the activated carbon blocks and graphene carbon blocks.

[0004] However, existing experimental atmosphere furnaces cannot adjust the heating environment according to the reaction status of the materials during use; therefore, they do not meet the current requirements. To address this, we propose a dual-tube vertical thermogravimetric atmosphere furnace with partitioned heating tube structure. Utility Model Content

[0005] The purpose of this invention is to provide a dual-tube vertical thermogravimetric atmosphere furnace heating tube partition structure to solve the problem mentioned in the background art that existing experimental atmosphere furnaces cannot adjust the heating environment according to the reaction status of the materials during use.

[0006] To achieve the above objectives, the present invention provides the following technical solution: a partitioned structure for the heating tubes of a double-tube vertical thermogravimetric atmosphere furnace, comprising: a double-tube vertical atmosphere furnace, wherein double-tube furnace bodies are provided inside both ends of the double-tube vertical atmosphere furnace, and two double-tube furnace bodies are provided.

[0007] Also includes:

[0008] The first inner cavity is installed below the interior of the dual-tube vertical atmosphere furnace. A feeding rod is provided on one side of the first inner cavity. A connecting base plate is provided at the upper end of the feeding rod, and the connecting base plate is threadedly connected to the upper end of the feeding rod. An installation base is provided above the connecting base plate. A support rod is provided at the middle position of the upper end face of the feeding rod, and the support rod passes through the connecting base plate and extends to the outside of the upper installation base. A temperature monitoring mechanism is provided between the connecting base plate and the outer wall of the support rod.

[0009] The second inner cavity is installed above the interior of the dual-tube furnace body. The interior of the second inner cavity is provided with a ceramic inner tube. Several ceramic inner tubes are provided, and several ceramic inner tubes are detachable and installable. A heating tube is provided around the outer wall of several ceramic inner tubes.

[0010] Preferably, a lifting moving rod mechanism is provided on one side of the feeding upright, and a horizontal moving rod mechanism is provided on the rear side of the lifting moving rod mechanism. A connecting bracket is provided between the lifting moving rod mechanism and the feeding upright, and both sides of the connecting bracket are threadedly connected to the feeding upright and the horizontal moving rod mechanism.

[0011] Preferably, a ceramic bowl is provided on the upper end surface of the support rod.

[0012] Preferably, the two double-tube furnace bodies are provided with an outer protective cover, and the outer protective cover is fixedly connected to the double-tube vertical atmosphere furnace.

[0013] Preferably, a conveying mechanism is provided on the upper end face of the two double-tube furnace bodies, a discharge pipe is provided on one side above the conveying mechanism, and a conveying pipeline is provided between the discharge pipe and the conveying mechanism.

[0014] Preferably, the front end face of the outer protective cover is provided with a flip-up baffle, and the flip-up baffle is rotatably connected to the outer protective cover.

[0015] Compared with the prior art, the beneficial effects of this utility model are:

[0016] 1. This utility model, through the setting of a feeding upright, a lifting moving rod mechanism, and a horizontal moving rod mechanism, as well as a ceramic bowl and a temperature monitoring mechanism set on the feeding upright, allows the material to be placed inside the ceramic bowl. The lifting moving rod mechanism is then reset and lowered, and the horizontal moving rod mechanism is moved to drive the lifting moving rod mechanism, so that the upper end of the feeding upright is directly below the ceramic inner tube. During the reaction operation, the heating tube is turned on to heat the ceramic inner tube. Simultaneously, an external reaction atmosphere is added into the ceramic inner tube to support the material's reaction. The required temperature varies depending on the material's state. The temperature monitoring mechanism monitors the temperature in real time, allowing the feeding upright to move up and down as needed. When a higher temperature is required, the feeding upright is moved upwards; when a higher temperature is not needed, it is moved downwards. This effectively avoids the problem of existing experimental atmosphere furnaces being unable to adjust the heating environment according to the material's reaction status. Attached Figure Description

[0017] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0018] Figure 2 This is a schematic diagram of the internal structure of the double-tube vertical atmosphere furnace of this utility model.

[0019] Figure 3 This is a schematic diagram of the internal structure at point A of this utility model;

[0020] In the diagram: 100, Double-tube vertical atmosphere furnace; 101, Outer protective cover; 10101, Tilting baffle; 102, First inner cavity; 103, Lifting moving rod mechanism; 104, Feeding upright; 10401, Ceramic bowl; 10402, Support rod; 10403, Mounting base; 10404, Connecting base plate; 10405, Temperature monitoring mechanism; 105, Connecting bracket; 106, Horizontal moving rod mechanism; 200, Double-tube furnace body; 201, Conveying mechanism; 202, Conveying pipe; 203, Discharge pipe; 204, Second inner cavity; 205, Ceramic inner tube; 206, Heating tube. Detailed Implementation

[0021] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments of the present utility model. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments.

[0022] Example 1

[0023] Please see Figure 1-3The present invention provides an embodiment of a dual-tube vertical thermogravimetric atmosphere furnace heating tube partition structure, comprising: a dual-tube vertical atmosphere furnace 100, wherein dual-tube furnace bodies 200 are provided inside both ends of the dual-tube vertical atmosphere furnace 100, and two dual-tube furnace bodies 200 are provided.

[0024] Also includes:

[0025] The first inner cavity 102 is installed below the interior of the double-tube vertical atmosphere furnace 100. A feeding rod 104 is provided on one side of the first inner cavity 102. A connecting base plate 10404 is provided at the upper end of the feeding rod 104, and the connecting base plate 10404 is threadedly connected to the upper end of the feeding rod 104. An mounting base 10403 is provided above the connecting base plate 10404. A support rod 10402 is provided at the middle position of the upper end face of the feeding rod 104. The support rod 10402 passes through the connecting base plate 10404 and extends to the outside of the mounting base 10403. A temperature monitoring mechanism 10405 is provided between the connecting base plate 10404 and the outer wall of the support rod 10402.

[0026] The second inner cavity 204 is installed above the inside of the double-tube furnace body 200. The second inner cavity 204 is provided with a ceramic inner tube 205. Several ceramic inner tubes 205 are provided. Several ceramic inner tubes 205 can be detached and installed. A heating tube 206 is provided around the outer wall of several ceramic inner tubes 205.

[0027] The feeding upright 104 and the vertical ceramic inner tube 205 are configured such that the feeding upright 104 can be moved up and down as needed for the material. When a high temperature is required, the feeding upright 104 is moved upward, and when a high temperature is not required, the feeding upright 104 is moved downward.

[0028] Example 2

[0029] Please see Figure 2 A lifting moving rod mechanism 103 is provided on one side of the feeding upright 104, and a horizontal moving rod mechanism 106 is provided on the rear side of the lifting moving rod mechanism 103. A connecting bracket 105 is provided between the lifting moving rod mechanism 103 and the feeding upright 104. Both sides of the connecting bracket 105 are threadedly connected to the feeding upright 104 and the horizontal moving rod mechanism 106. A ceramic bowl 10401 is provided on the upper end face of the support rod 10402.

[0030] The ceramic bowl 10401 is designed to effectively provide a reaction space cavity for materials that need to react.

[0031] Please see Figure 1The two double-tube furnace bodies 200 are provided with an outer protective cover 101, and the outer protective cover 101 is fixedly connected to the double-tube vertical atmosphere furnace 100. The upper end face of the two double-tube furnace bodies 200 is provided with a conveying mechanism 201. A discharge pipe 203 is provided on one side above the conveying mechanism 201. A conveying pipe 202 is provided between the discharge pipe 203 and the conveying mechanism 201. The front end face of the outer wall of the outer protective cover 101 is provided with a flip baffle 10101, and the flip baffle 10101 is rotatably connected to the outer protective cover 101.

[0032] The flip-over baffle 10101 allows external materials to be effectively conveyed into the sealed cavity space.

[0033] Working principle: The flip-up baffle 10101 is flipped open, and the material to be reacted is placed inside the ceramic bowl 10401. The rising moving rod mechanism 103 is reset and lowered, and then the horizontal moving rod mechanism 106 is moved to drive the rising moving rod mechanism 103, so that the upper end of the feeding rod 104 is directly below the ceramic inner tube 205. During the reaction operation, the heating tube 206 is turned on to heat the ceramic inner tube 205. At the same time, the external reaction atmosphere is added into the ceramic inner tube 205 to support the reaction operation of the material. The required temperature varies depending on the state of the material. The temperature varies depending on the depth of the ceramic inner tube 205. The temperature increases from bottom to top according to the depth of the ceramic inner tube 205. The temperature monitoring mechanism 10405 monitors in real time and can move the feeding rod 104 up and down as needed by the material. When a high temperature is needed, the feeding rod 104 is moved upward, and when a high temperature is not needed, the feeding rod 104 is moved downward. Because the ceramic inner tube 205 is vertical, the temperature of the internal cavity is concentrated at the top, while the temperature at the bottom is relatively low.

[0034] It will be apparent to those skilled in the art that this invention is not limited to the details of the exemplary embodiments described above, and that it can be implemented in other specific forms without departing from the spirit or essential characteristics of this invention. Therefore, the embodiments should be considered illustrative and non-limiting in all respects, and the scope of this invention is defined by the appended claims rather than the foregoing description. Thus, it is intended that all variations falling within the meaning and scope of equivalents of the claims be included within this invention. No reference numerals in the claims should be construed as limiting the scope of the claims.

Claims

1. A partitioned structure for heating furnace tubes of a dual-tube vertical thermogravimetric atmosphere furnace, comprising a dual-tube vertical atmosphere furnace (100), wherein dual-tube furnace bodies (200) are provided inside both ends of the dual-tube vertical atmosphere furnace (100), and two dual-tube furnace bodies (200) are provided; Its features are: Also includes: The first inner cavity (102) is installed below the interior of the double-tube vertical atmosphere furnace (100). A feeding rod (104) is provided on one side of the first inner cavity (102). A connecting base plate (10404) is provided at the upper end of the feeding rod (104), and the connecting base plate (10404) is threadedly connected to the upper end of the feeding rod (104). An mounting base (10403) is provided above the connecting base plate (10404). A support rod (10402) is provided at the middle position of the upper end face of the feeding rod (104), and the support rod (10402) passes through the connecting base plate (10404) and extends to the outside of the mounting base (10403). A temperature monitoring mechanism (10405) is provided between the outer walls of the connecting base plate (10404) and the support rod (10402). The second inner cavity (204) is installed above the inside of the double-tube furnace body (200). The second inner cavity (204) is provided with a ceramic inner tube (205). There are several ceramic inner tubes (205). Several ceramic inner tubes (205) can be detached and installed. A heating tube (206) is provided around the outer wall of several ceramic inner tubes (205).

2. The partitioned structure of the heating tubes in a dual-tube vertical hot gravity atmosphere furnace according to claim 1, characterized in that: A lifting moving rod mechanism (103) is provided on one side of the feeding upright (104), and a horizontal moving rod mechanism (106) is provided on the rear side of the lifting moving rod mechanism (103). A connecting bracket (105) is provided between the lifting moving rod mechanism (103) and the feeding upright (104), and both sides of the connecting bracket (105) are threadedly connected to the feeding upright (104) and the horizontal moving rod mechanism (106).

3. The partitioned structure of the heating tubes in a dual-tube vertical hot gravity atmosphere furnace according to claim 1, characterized in that: A ceramic bowl (10401) is provided on the upper end surface of the support rod (10402).

4. The partitioned structure of the heating tubes in a dual-tube vertical hot gravity atmosphere furnace according to claim 1, characterized in that: The two double-tube furnace bodies (200) are provided with an outer protective cover (101), and the outer protective cover (101) is fixedly connected to the double-tube vertical atmosphere furnace (100).

5. The partitioned structure of the heating tubes in a dual-tube vertical hot gravity atmosphere furnace according to claim 1, characterized in that: The upper end face of the two double-tube furnace bodies (200) is provided with a conveying mechanism (201), and a discharge pipe (203) is provided on one side above the conveying mechanism (201). A conveying pipe (202) is provided between the discharge pipe (203) and the conveying mechanism (201).

6. The partitioned structure of the heating tubes in a dual-tube vertical hot gravity atmosphere furnace according to claim 4, characterized in that: The front end face of the outer wall of the outer protective cover (101) is provided with a flip baffle (10101), and the flip baffle (10101) is rotatably connected to the outer protective cover (101).

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