Detection device for cocklebur fruit products

Abstract

The utility model discloses a detection device for cocklebur fruit products, and relates to the technical field of detection, the detection device comprises a raw material processing mechanism and a high performance liquid chromatograph connected with a sample outlet of the raw material processing mechanism, the raw material processing mechanism comprises a crushing device and an ultrasonic treatment device connected with a first feed opening of the crushing device, and the ultrasonic treatment device is connected with a second feed opening of the crushing device. The centrifugal separation device is connected with a second feed opening of the ultrasonic treatment device, the measuring vessel is connected with a third feed opening of the centrifugal separation device, and the measuring vessel is provided with the sample outlet. According to the utility model, the steps of crushing, extracting and filtering for raw material treatment are integrated on one set of device, the time required by extraction is shortened through the ultrasonic treatment device, and the filtering process is accelerated through the centrifugal separation device, so that the steps of raw material treatment are effectively reduced, and the time of raw material treatment is shortened.

Description

TECHNICAL FIELD

[0001] The utility model belongs to the technical field of detection, specifically relates to a detection device for semen xanthii products. BACKGROUND

[0002] Stir-fried semen xanthii is one of semen xanthii products, and the stir-fried semen xanthii is obtained by placing semen xanthii in a stir-frying container, heating the semen xanthii with medium fire until the surface of the semen xanthii is yellow-brown and the thorns are scorched, taking out the semen xanthii, and then grinding off the thorns and sieving the semen xanthii after air cooling. The stir-fried semen xanthii has reduced toxicity and is more conducive to the decoction and exertion of effective components.

[0003] Toxicity content is one of important detection indexes for evaluating the safety of semen xanthii products. Under the current technical background, a high-performance liquid chromatograph is often used to detect toxic components in stir-fried semen xanthii extract. However, the existing high-performance liquid chromatograph is not equipped with a device for pretreating and extracting semen xanthii raw materials, and this step often needs to rely on independent equipment. The use of independent equipment has many raw material processing steps, and the whole processing process is complicated and time-consuming. UTILITY MODEL CONTENT

[0004] In order to overcome the problems in the background art, the utility model provides a detection device for semen xanthii products.

[0005] To achieve the above-mentioned purposes, the utility model is realized through the following technical scheme: a detection device for semen xanthii products, comprising: a raw material processing mechanism, a high-performance liquid chromatograph connected with a sample outlet of the raw material processing mechanism, the raw material processing mechanism comprising: a crushing device, an ultrasonic treatment device connected with a first discharge port of the crushing device, a centrifugal separation device connected with a second discharge port of the ultrasonic treatment device, and a measuring device connected with a third discharge port of the centrifugal separation device, wherein the measuring device is provided with the sample outlet; the centrifugal separation device comprises: a first cylinder connected with the second discharge port, a first motor arranged at the bottom of the first cylinder, and an inner cylinder arranged in the first cylinder and connected with an output shaft of the first motor; a square shaft is arranged on the output shaft of the first motor, a square insertion slot connected with the square shaft is arranged on the bottom surface of the inner cylinder, a second layer of side walls is arranged in the side wall of the inner cylinder, filter paper is arranged between the side wall and the second layer of side walls, and the side wall and the second layer of side walls are both distributed with grid round holes.

[0006] Further, a first sealing cover is arranged at the upper end of the first cylinder, and a first valve connected with the second discharge port is arranged on the first sealing cover.

[0007] Further, a groove is arranged at the bottom of the first cylinder, and the third discharge port is arranged at the bottom of the groove.

[0008] Further, the crushing device comprises a second cylinder body, a second sealing cover threadedly connected to the upper end of the second cylinder body, a second motor arranged on the second sealing cover, a transmission shaft connected with the output shaft of the second motor and entering the second cylinder body, a spiral blade arranged at the bottom end of the transmission shaft, and the first discharge port arranged at the bottom of the second cylinder body, wherein the second valve is arranged on the first discharge port.

[0009] Further, the ultrasonic treatment device comprises a third cylinder body threadedly connected with the first discharge port, an ultrasonic transducer arranged at the bottom surface of the third cylinder body, and at least one solvent bottle arranged on the side wall of the first discharge port.

[0010] Further, the solvent bottle is made of transparent material, the capacity scale is arranged on the side wall of the bottle body, the bottle cap is arranged on the upper end of the bottle body, the flow guide pipe is arranged at the bottom of the bottle body and is communicated with the first discharge port, and the fourth valve is arranged on the flow guide pipe.

[0011] Further, the measuring device is made of transparent material, the third sealing cover is threadedly connected to the upper end of the measuring device, the third sealing cover is connected with the third discharge port, the capacity scale is arranged on the side wall of the measuring device, the sample outlet is arranged at the bottom of the measuring device, and the third valve is arranged on the sample outlet.

[0012] Compared with the prior art, the device has the following beneficial effects:

[0013] The device integrates the steps of crushing, extraction and filtration of raw materials, shortens the extraction time through the ultrasonic treatment device, accelerates the filtration process through the centrifugal separation device, effectively reduces the steps of raw material processing, and shortens the time of raw material processing. BRIEF DESCRIPTION OF DRAWINGS

[0014] Fig. 1 It is a structural schematic view of the detection device for the xanthium product;

[0015] Fig. 2 It is a sectional structural schematic view of the detection device for the xanthium product;

[0016] Fig. 3 It is a structural schematic view of the inner cylinder body.

[0017] In the figure: crushing device 1, first discharge port 2, ultrasonic treatment device 3, second discharge port 4, centrifugal separation device 5, third discharge port 6, measuring device 7, first cylinder 8, first motor 9, inner cylinder 10, square shaft 11, square slot 12, second layer side wall 13, filter paper 14, first sealing cover 15, first valve 16, groove 17, second cylinder 19, second sealing cover 20, second motor 21, transmission shaft 22, spiral blade 23, third cylinder 24, ultrasonic transducer 25, solvent bottle 26, bottle cap 27, flow guide pipe 28, fourth valve 29, third sealing cover 30, sample outlet 31, third valve 32, second valve 33. DETAILED DESCRIPTION

[0018] In order to make the purpose, technical scheme and beneficial effects of the utility model clearer, the preferred embodiments of the utility model will be described in detail below, so as to facilitate the understanding of technicians.

[0019] Please refer to Figs. 1 to 3 (not shown in the figure), the utility model provides a kind of detection device for Xanthium product, it include: raw material processing mechanism, with the raw material processing mechanism sample outlet 31 connection's high performance liquid chromatograph, the raw material processing mechanism includes: crushing device 1, with the first discharge port 2 of crushing device 1 connection's ultrasonic treatment device 3, with the second discharge port 4 of ultrasonic treatment device 3 connection's centrifugal separation device 5, with the third discharge port 6 of centrifugal separation device 5 connection's measuring device 7, the measuring device 7 is equipped with the sample outlet 31.Crushing device 1 is beaten into powder with Xanthium, ultrasonic treatment device 3 cooperates with extraction solvent and extracts the component in Xanthium, extract liquid is filtered in centrifugal separation device 5, and removes impurity in extract liquid.

[0020] The centrifugal separation device 5 includes: a first cylinder 8 connected to the second discharge port 4, a first motor 9 arranged at the bottom of the first cylinder 8, and an inner cylinder 10 arranged in the first cylinder 8 and connected to the output shaft of the first motor 9; a square shaft 11 is arranged on the output shaft of the first motor 9, a square slot 12 connected to the square shaft 11 is arranged on the bottom surface of the inner cylinder 10, a second layer side wall 13 is arranged in the side wall of the inner cylinder 10, a filter paper 14 is arranged between the side wall and the second layer side wall 13, and a plurality of grid round holes are arranged on the side wall and the second layer side wall 13. The first cylinder 8 is fixed, the first motor 9 drives the inner cylinder 10 to rotate, and the filter paper 14 separates the impurities from the extract liquid. The filter paper 14 is supported by the side wall and the second layer side wall 13 and can be replaced; the connection of the square shaft 11 and the square slot 12 allows the inner cylinder 10 to be taken out of the first cylinder 8, facilitating the cleaning of the inner cylinder 10.

[0021] The upper end of the first cylinder 8 is provided with a first sealing cover 15, and the first sealing cover 15 is provided with a first valve 16 connected with the second discharge port 4. The first sealing cover 15 allows the first cylinder 8 to be detachably connected with the second discharge port 4, so as to facilitate the cleaning of the inside; and the first valve 16 prevents the extract from entering the first cylinder 8 in advance.

[0022] The bottom of the first cylinder 8 is provided with a groove 17, and the bottom of the groove 17 is provided with the third discharge port 6. The extract after removing impurities is concentrated in the groove 17 and can be discharged from the third discharge port 6.

[0023] The crushing device 1 comprises a second cylinder 19, a second sealing cover 20 threadedly connected to the upper end of the second cylinder 19, a second motor 21 provided on the second sealing cover 20, a transmission shaft 22 connected with the output shaft of the second motor 21 and entering the second cylinder 19, a spiral blade 23 provided at the bottom end of the transmission shaft 22, the first discharge port 2 provided at the bottom of the second cylinder 19, and a second valve 33 provided on the first discharge port 2. The second motor 21 drives the spiral blade 23 to rotate to crush the xanthium fruit into powder.

[0024] The ultrasonic treatment device 3 comprises a third cylinder 24 threadedly connected with the first discharge port 2, an ultrasonic transducer 25 provided on the bottom surface of the third cylinder 24, and at least one solvent bottle 26 provided on the side wall of the first discharge port 2. The ultrasonic transducer 25 is a prior art, and the ultrasonic transducer 25 (also known as “ultrasonic wave converter” and “piezoelectric transducer”) is an electromechanical element that converts electrical energy from an ultrasonic generator into mechanical energy in the form of ultrasonic vibrations. These mechanical vibrations are then amplified by the tool head and delivered to the treated liquid. When the high-frequency electrical energy generated by the ultrasonic generator acts on the ultrasonic transducer 25, the transducer converts the electrical energy into mechanical energy in the form of ultrasonic vibrations, which are amplified by the tool head and transmitted to the liquid, causing the molecules of the liquid to vibrate violently and collide with each other, rapidly destroying the cell walls of the plant, allowing the active ingredients in the xanthium fruit to be released efficiently and improving the extraction efficiency. The ultrasonic transducer 25 also contains the necessary control circuit.

[0025] The bottle body of the solvent bottle 26 is made of transparent material, and the side wall of the bottle body is provided with a capacity scale. The upper end of the bottle body is provided with a bottle cap 27, and the bottom of the bottle body is provided with a flow guide pipe 28 in communication with the first discharge port 2. The flow guide pipe 28 is provided with a fourth valve 29. In this embodiment, one solvent bottle 26 is used, and ethanol is added to the solvent bottle 26. The amount of ethanol added is controlled by the fourth valve 29 and the capacity scale.

[0026] The measurer 7 is made of transparent material, a third sealing cover 30 is threadedly connected to the upper end of the measurer 7, the third sealing cover 30 is connected with the third discharging port 6, a capacity scale is arranged on the side wall of the measurer 7, a sample outlet 31 is arranged at the bottom of the measurer 7, and a third valve 32 is arranged on the sample outlet 31.

[0027] The embodiment also comprises a support for supporting the raw material processing mechanism.

[0028] The detection device for the xanthium fruit products is used as follows:

[0029] The second sealing cover 20 is opened, the fried xanthium fruit products are put into the second cylinder 19, the second motor 21 is started to beat the xanthium fruit products into powder, then the second valve 33 is opened, the xanthium fruit powder machine enters the third cylinder 24, and the second valve 33 is closed; the solvent in the solvent bottle 26 is put into the third cylinder 24, the ultrasonic transducer 25 is started, after a period of time, the first valve 16 is opened to let the extracting solution enter the inner cylinder 10, the first motor 9 is started to rapidly filter out impurities in the extracting solution, the extracting solution enters the measurer 7, and the amount of the extracting solution entering the high-performance liquid chromatograph is controlled through the third valve 32 and the capacity scale.

[0030] Finally, it should be pointed out that the above preferred embodiments are only used for describing the technical scheme of the utility model and not for limiting, although the utility model has been described in detail through the above preferred embodiments, those skilled in the art should understand that various changes can be made to the utility model in form and details without departing from the range defined by the claims of the utility model.

Claims

1. A device for detecting a product of Fructus Xanthii, comprising: The utility model relates to a raw material processing mechanism, high performance liquid chromatograph connected with sample outlet (31) of raw material processing mechanism, it is characterized by: the raw material processing mechanism includes: the smashing device (1), the ultrasonic treatment device (3) connected with the first discharge port (2) of smashing device (1), the centrifugal separation device (5) connected with the second discharge port (4) of ultrasonic treatment device (3), the measure (7) connected with the third discharge port (6) of centrifugal separation device (5), and the measure (7) is equipped with sample outlet (31);The centrifugal separation device (5) includes: the first cylinder (8) connected with the second discharge port (4), the first motor (9) arranged at the bottom of the first cylinder (8), the inner cylinder (10) arranged in the first cylinder (8) and connected with the output shaft of the first motor (9);Square shaft (11) is arranged on the output shaft of the first motor (9), the bottom surface of the inner cylinder (10) is provided with square slot (12) connected with the square shaft (11), the second layer of side wall (13) is arranged in the side wall of the inner cylinder (10), the filter paper (14) is arranged between the side wall and the second layer of side wall (13), and the side wall and the second layer of side wall (13) are evenly distributed with grid round hole.

2. The device for detecting Xanthium product according to claim 1, wherein, The upper end of the first cylinder (8) is provided with a first sealing cover (15), and the first valve (16) is arranged on the first sealing cover (15) and connected with the second discharge port (4).

3. The device for detecting Xanthium product according to claim 2, wherein, The bottom of the first cylinder (8) is provided with a groove (17), and the third discharge port (6) is arranged at the bottom of the groove (17).

4. The device for detecting Xanthium product according to claim 1, wherein, The smashing device (1) includes: the second cylinder (19), the second sealing cover (20) threadedly connected to the upper end of the second cylinder (19), the second motor (21) arranged on the second sealing cover (20), the transmission shaft (22) connected with the output shaft of the second motor (21) and entering the second cylinder (19), the spiral blade (23) arranged at the bottom end of the transmission shaft (22), the first discharge port (2) arranged at the bottom of the second cylinder (19), and the second valve (33) arranged on the first discharge port (2).

5. The device for detecting Xanthium product according to claim 4, wherein, The ultrasonic treatment device (3) includes the third cylinder (24) threadedly connected with the first discharge port (2), the ultrasonic transducer (25) arranged on the bottom surface of the third cylinder (24), and at least one solvent bottle (26) arranged on the side wall of the first discharge port (2).

6. The device for detecting Xanthium product according to claim 5, wherein, The bottle body of the solvent bottle (26) is made of transparent material, the capacity scale is arranged on the side wall of the bottle body, the bottle cap (27) is arranged on the upper end of the bottle body, the flow guide pipe (28) is arranged at the bottom of the bottle body and communicated with the first discharge port (2), and the fourth valve (29) is arranged on the flow guide pipe (28).

7. The device for detecting Xanthium product according to claim 3, wherein, The said measurer (7) is of transparent material, the upper end of the measurer (7) is threadedly connected with a third sealing cover (30), the third sealing cover (30) is connected with the third blanking port (6), a capacity scale is arranged on the lateral wall of the measurer (7), and the bottom of the measurer (7) is provided with the sample outlet (31), and the sample outlet (31) is provided with a third valve (32).

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