Polyaluminum chloride reaction temperature self-adaptive adjusting device

By designing a combination of a three-way ball valve and multiple coils, the steam flow direction can be adjusted according to the temperature inside the reactor, solving the energy waste problem caused by the fixed length of the coils and achieving flexible temperature regulation and efficient heat utilization.

CN223641817UActive Publication Date: 2025-12-09HONGHU YUANTAI TECH CO LTD
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Patent Information

Application Number
CN202423211022.0
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-12-24
Publication Date
2025-12-09
Estimated Expiration
2034-12-24

AI Technical Summary

Technical Problem

In existing technologies, the fixed length of the coil cannot be adjusted according to the amount of polyaluminum chloride reacting with wastewater, resulting in energy waste when the reaction amount is small.

Method used

An adaptive temperature control device for polyaluminum chloride reaction was designed. By using a combination of a three-way ball valve and multiple coils, the steam flow direction is adjusted according to the temperature sensor data inside the reactor, thereby achieving flexible heating of different parts of the reactor.

Benefits of technology

This technology enables flexible adjustment of the coil length based on changes in the reaction volume within the reactor, reducing energy waste and improving heat utilization efficiency.

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Abstract

The utility model provides a polymeric aluminum chloride reaction temperature self-adaptive adjusting device, which relates to the technical field of automatic temperature control, and comprises a reaction kettle, a kettle cover arranged at the top of the reaction kettle, a temperature sensor arranged at the top of the kettle cover, a first coil pipe wound outside the reaction kettle, and a second coil pipe arranged at the top of the first coil pipe, a third coil pipe is arranged at the top of the second coil pipe, and after steam passes through the three-way ball valve at the top end, a part of steam is separated out again and enters the second L-shaped gas conveying pipe at the top end. A part of steam separated from the three-way ball valve at the top end can be conveyed into a third coil pipe through a second L-shaped gas conveying pipe, the bottom end, the middle and the top end of the reaction kettle are heated at the same time through a first coil pipe, a second coil pipe and the third coil pipe, and the steam enters different coil pipes to adapt to different reaction doses in the reaction kettle; the defect that the length of the coil pipe cannot be adjusted according to the reaction amount of polyaluminum chloride and sewage is overcome.
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Description

Technical Field

[0001] This utility model relates to the field of automatic temperature control technology, and in particular to an adaptive temperature adjustment device for polyaluminum chloride reaction. Background Technology

[0002] According to Chinese Publication No. CN219958110U, an automatic temperature control device for a polyaluminum chloride reactor is disclosed, relating to the field of automatic temperature control technology. The device includes a base, a reactor shell on top of the base, a reactor inner liner inside the reactor shell, a reactor lid on top of the reactor inner liner, a sealing gasket between the reactor lid and the reactor inner liner, a drive motor at the top center of the reactor lid, a viewing window on one side of the top of the reactor lid, a charge-coupled device at the top of the viewing window, a power supply box on one side of the top of the base, a control panel on the top of the power supply box, a signal receiver on one side of the control panel, and a thermocouple at the bottom of the inner wall of the reactor inner liner, with a signal transmitter on top of the thermocouple. The device uses thermocouples to sense the internal temperature of the reactor. When the temperature is too high or too low, the temperature is adjusted by increasing or decreasing the steam flow rate at the steam inlet, eliminating the need for manual intervention and reducing workload.

[0003] The reactors described above and in the prior art are mostly connected to steam via a coil, and the internal temperature of the reactor is controlled by the heat transfer of the high-temperature steam. However, the length of the coil in the prior art is fixed at the time of manufacture. However, the amount of polyaluminum chloride reacting with wastewater in the reactor is not fixed during use. When the amount of polyaluminum chloride reacting with wastewater is small, an excessively long coil will cause energy waste. The above-mentioned technologies cannot adjust the length of the coil according to the amount of polyaluminum chloride reacting with wastewater. Utility Model Content

[0004] The purpose of this invention is to address the shortcomings of existing technologies that cannot adjust the length of the coil according to the amount of polyaluminum chloride reacting with wastewater, and to propose an adaptive temperature control device for the polyaluminum chloride reaction.

[0005] To achieve the above objectives, the present invention adopts the following technical solution: a polyaluminum chloride reaction temperature adaptive adjustment device, comprising a reaction vessel, a vessel lid on the top of the reaction vessel, a temperature sensor on the top of the vessel lid, a first coil wound around the outside of the reaction vessel, a second coil on the top of the first coil, a third coil on the top of the second coil, two fixing buckles on both sides of the first, second, and third coils, two three-way ball valves on one side of the reaction vessel, a first connecting pipe between the two three-way ball valves, a first L-shaped gas supply pipe on one side of the first coil, a second L-shaped gas supply pipe on one side of the third coil, a second connecting pipe on the side of the reaction vessel away from the three-way ball valves, and a gas outlet on the surface of the second connecting pipe away from the reaction vessel.

[0006] Preferably, the vessel cover is installed on the top surface of the reactor and is connected to the reactor flange.

[0007] Preferably, the temperature sensor is installed on the top surface of the vessel lid and is connected to the flange of the vessel lid, with one end of the temperature sensor penetrating into the vessel lid.

[0008] Preferably, the first, second, and third coils are all wound around the outer surface of the reactor, and the first, second, and third coils are all installed on the outer surface of the reactor by four fixing buckles, with the first, second, and third coils being arranged at equal intervals.

[0009] Preferably, the vertical centerlines of the two three-way ball valves are aligned, and both three-way ball valves are connected to the flanges of the first and second serpentine tubes.

[0010] Preferably, both ends of the first connecting pipe are connected to two three-way ball valve flanges, and the second connecting pipe is connected to the flange at the end of the first, second, and third coiled tubes furthest from the three-way ball valves.

[0011] Preferably, the first L-shaped gas supply pipe and the second L-shaped gas supply pipe are mirror-symmetrically arranged with the first connecting pipe as the center, and both the first L-shaped gas supply pipe and the second L-shaped gas supply pipe are connected to the flange of the three-way ball valve.

[0012] Beneficial effects

[0013] In this invention, an external steam source is connected to a first L-shaped gas delivery pipe, and the steam is then delivered through the first L-shaped gas delivery pipe to a three-way ball valve connected to a first coiled tube. Normally, both three-way ball valves will shut off the third gas passage, only opening the gas passage connected to the first and second coiled tubes. This ensures that steam, after passing through the bottom three-way ball valve, is only delivered into the interior of the first coiled tube, heating the bottom of the reactor. When the reaction volume in the reactor is large, the handle of the three-way ball valve is rotated, opening the gas passage connected to the first connecting pipe. This allows some steam to enter the first coiled tube after passing through the bottom three-way ball valve, while the remaining steam is delivered through the first connecting pipe to the top three-way ball valve, and then through the top three-way ball valve into the second coiled tube. Inside the reactor, the bottom and middle sections are heated via the first and second coils. When the reaction volume in the reactor is at its maximum, the handle of the three-way ball valve at the top is turned, allowing steam to pass through the valve and then be partially diverted into the second L-shaped gas delivery pipe at the top. Since the second L-shaped gas delivery pipe is connected to the third coil, a portion of the steam diverted from the three-way ball valve at the top is then transported into the interior of the third coil through the second L-shaped gas delivery pipe. The bottom, middle, and top sections of the reactor are heated simultaneously via the first, second, and third coils. By allowing steam to enter different coils, the reactor's internal reaction volume can be adjusted to accommodate different reaction volumes, thus overcoming the limitation of not being able to adjust the coil length according to the amount of polyaluminum chloride reacting with wastewater. Attached Figure Description

[0014] Figure 1 This is an isometric drawing of the present invention;

[0015] Figure 2 This is a front view of the present invention;

[0016] Figure 3 This is the left view of the present invention;

[0017] Figure 4 For the present utility model Figure 3 Sectional view at point AA.

[0018] Legend:

[0019] 1. Reactor; 2. Reactor lid; 3. First coil; 4. Second coil; 5. Third coil; 6. First L-shaped gas supply pipe; 7. Second L-shaped gas supply pipe; 8. First connecting pipe; 9. Three-way ball valve; 10. Fixing buckle; 11. Second connecting pipe; 12. Gas outlet; 13. Temperature sensor. Detailed Implementation

[0020] To make the technical means, creative features, and achieved objectives and effects of this utility model easier to understand, the present utility model is further described below with reference to specific embodiments and accompanying drawings. However, the following embodiments are merely preferred embodiments of this utility model and not all of them. Other embodiments obtained by those skilled in the art based on the embodiments described in the implementation plan without creative effort are all within the protection scope of this utility model.

[0021] The specific embodiments of this utility model are described below with reference to the accompanying drawings. Specific Implementation Example 1:

[0023] Reference Figure 1-4 An adaptive temperature control device for polyaluminum chloride reaction includes a reactor 1, a reactor lid 2 on top of the reactor 1, a temperature sensor 13 on top of the reactor lid 2, a first coiled tube 3 wound around the outside of the reactor 1, a second coiled tube 4 on top of the first coiled tube 3, and a third coiled tube 5 on top of the second coiled tube 4. Two fixing buckles 10 are provided on both sides of the first coiled tube 3, the second coiled tube 4, and the third coiled tube 5. Two three-way ball valves 9 are provided on one side of the reactor 1, with a first connecting pipe 8 between the two three-way ball valves 9. A first L-shaped gas supply pipe 6 is provided on one side of the first coiled tube 3, and a second L-shaped gas supply pipe 7 is provided on one side of the third coiled tube 5. A second connecting pipe 11 is provided on the side of the reactor 1 away from the three-way ball valves 9, with a gas outlet 12 on the surface of the second connecting pipe 1 away from the reactor 1. The reactor lid 2 is installed on the top surface of the reactor 1 and is connected to the flange of the reactor 1. The temperature sensor 13 is installed on the reactor lid 2. The top surface is covered, and the temperature sensor 13 is connected to the flange of the vessel cover 2. One end of the temperature sensor 13 penetrates into the vessel cover 2. The first coil 3, the second coil 4, and the third coil 5 are all wrapped around the outer surface of the reactor 1. The first coil 3, the second coil 4, and the third coil 5 are all installed on the outer surface of the reactor 1 by four fixing buckles 10. The first coil 3, the second coil 4, and the third coil 5 are set at equal intervals. The vertical central axis of the two three-way ball valves 9 is consistent. The two three-way ball valves 9 are connected to the flanges of the first coil 3 and the second coil 4. Both ends of the first connecting pipe 8 are connected to the flanges of the two three-way ball valves 9. The second connecting pipe 11 is connected to the flange of the end of the first coil 3, the second coil 4, and the third coil 5 away from the three-way ball valves 9. The first L-shaped gas supply pipe 6 and the second L-shaped gas supply pipe 7 are set up symmetrically in mirror with the first connecting pipe 8 as the center. The first L-shaped gas supply pipe 6 and the second L-shaped gas supply pipe 7 are both connected to the flanges of the three-way ball valves 9.

[0024] A lid 2 is installed on the top surface of the reactor 1, covering the top of the reactor 1 and sealing the internal space of the reactor 1. A temperature sensor 13 is installed on the top surface of the lid 2. The temperature sensor 13 penetrates into the internal space of the reactor 1 to monitor the internal temperature. When the internal temperature of the reactor 1 is low, the temperature sensor 13 processes the collected data through an internal control chip, digitizes it, and transmits it to the display screen on top of the temperature sensor 13, displaying the internal temperature of the reactor 1. The operator uses the temperature displayed by the temperature sensor 13 to determine whether the internal temperature of the reactor 1 needs to be heated. (First coil...) 3. The second coil 4 and the third coil 5 are both wound around the outer surface of the reactor 1, and the top and bottom ends of the first coil 3, the second coil 4, and the third coil 5 are fixed to the outer surface of the reactor 1 by two fixing buckles 10. High-temperature steam is supplied to the first coil 3, the second coil 4, and the third coil 5 to heat them. When the first coil 3, the second coil 4, and the third coil 5 are heated, because they are attached to the outer surface of the reactor 1, the heated first coil 3, the second coil 4, and the third coil 5 heat the reactor 1, thereby increasing the internal temperature of the reactor 1. Since the two coils are perpendicular to each other... The three-way ball valve 9 is connected to the flanges of the first serpentine pipe 3 and the second serpentine pipe 4. Both ends of the first connecting pipe 8 are connected to the flanges of the two three-way ball valves 9, allowing the two three-way ball valves 9 to communicate. This enables the bottom three-way ball valve 9 to deliver steam through the interior of the first connecting pipe 8 into the interior of the top three-way ball valve 9. The top surface of the first L-shaped gas pipe 6 is connected to the bottom flange of the bottom three-way ball valve 9, and the bottom surface of the second L-shaped gas pipe 7 is connected to the top flange of the top three-way ball valve 9. The top surface of the second L-shaped gas pipe 7 is also connected to the flange of the third serpentine pipe 5. This ensures that when steam enters the first L-shaped gas pipe 6, it is first delivered to the bottom three-way ball valve 9. The opening and closing of the third gas passage of the bottom three-way ball valve 9 controls whether steam can pass through the first serpentine pipe 5. A connecting pipe 8 enters the interior of the three-way ball valve 9 at the top, thereby controlling whether steam enters the interior of the second coil 4. When steam enters the three-way ball valve 9 at the top, the opening and closing of the third air passage of the three-way ball valve 9 at the top determines whether steam can enter the second L-shaped gas supply pipe 7, thereby controlling whether steam enters the interior of the third coil 5 connected to the second L-shaped gas supply pipe 7. The second connecting pipe 11 is connected to the flange at the end of the first coil 3, the second coil 4, and the third coil 5 away from the three-way ball valve 9. The steam delivered into the interior of the first coil 3, the second coil 4, and the third coil 5 is heated and then delivered into the interior of the second connecting pipe 11, and is discharged from the second connecting pipe 11 through the air outlet 12 on the surface of the second connecting pipe 11.

[0025] When in use, an external steam source is connected to the first L-shaped gas supply pipe 6, and the steam is delivered through the first L-shaped gas supply pipe 6 to the three-way ball valve 9 connected to the first coiled tube 3. Normally, both three-way ball valves 9 will cut off the third gas passage, only opening the gas passage connected to the first coiled tube 3 and the second coiled tube 4. This allows steam to enter the bottom three-way ball valve 9 and only be delivered into the interior of the first coiled tube 3, heating the bottom of the reactor 1 through the first coiled tube 3. When the reaction volume in the reactor 1 is large, the handle of the three-way ball valve 9 is turned, opening the gas passage connected to the first connecting pipe 8. This allows some steam to enter the first coiled tube 3 after passing through the bottom three-way ball valve 9, while the other part is delivered to the top three-way ball valve 9 through the first connecting pipe 8. Since the top three-way ball valve 9 is connected to the second coiled tube 4, the steam entering the top three-way ball valve 9 is also delivered into the interior of the second coiled tube 4. The steam then passes through the first coiled tube 3 and the second coiled tube 4 to heat the bottom of the reactor 1. The bottom and middle parts of the reactor 1 are heated. When the reaction volume in the reactor 1 is at its maximum, the handle 9 of the three-way ball valve at the top is turned to open the gas passage connected to the second L-shaped gas supply pipe 7. Steam enters the three-way ball valve at the top and then a portion of the steam is diverted into the second L-shaped gas supply pipe 7 at the top. The steam is then transported into the interior of the third coil 5 through the second L-shaped gas supply pipe 7. The bottom, middle and top parts of the reactor 1 are heated simultaneously through the first coil 3, the second coil 4 and the third coil 5. The steam enters different coils to adapt to different reaction volumes inside the reactor 1, which solves the problem of not being able to adjust the length of the coil according to the amount of polyaluminum chloride reacting with wastewater. When the steam enters the first coil 3, the second coil 4 and the third coil 5 and completes the heat transfer, it is discharged through the outlet 12 of the second connecting pipe 11 connected to the right end of the first coil 3, the second coil 4 and the third coil 5. Specific Implementation Example 2:

[0027] Reference Figure 1-4 A polyaluminum chloride reaction temperature adaptive adjustment device, further based on the basic structure in Specific Embodiment 1, can have threaded grooves opened on the surface of the reaction vessel 1 where the first coil 3, the second coil 4, and the third coil 5 are attached. The opened threaded grooves correspond one-to-one with the first coil 3, the second coil 4, and the third coil 5. By embedding the first coil 3, the second coil 4, and the third coil 5 into the opened threaded grooves, the contact area between the first coil 3, the second coil 4, and the third coil 5 and the reaction vessel 1 is increased, thereby increasing the heat transfer effect and reducing heat waste.

[0028] In summary:

[0029] 1. An external steam source is connected to the first L-shaped gas supply pipe 6, and the steam is delivered through the first L-shaped gas supply pipe 6 to the three-way ball valve 9 connected to the first serpentine tube 3. Normally, both three-way ball valves 9 will shut off the third gas passage, only opening the gas passage connected to the first serpentine tube 3 and the second serpentine tube 4. This ensures that steam, after passing through the bottom three-way ball valve 9, is only delivered into the interior of the first serpentine tube 3, heating the bottom of the reactor 1 through the first serpentine tube 3. When the reaction volume in the reactor 1 is large, the handle of the three-way ball valve 9 is turned, opening the gas passage connected to the first connecting pipe 8. This allows some steam to enter the first serpentine tube 3 after passing through the bottom three-way ball valve 9, while the other part is delivered through the first connecting pipe 8 to the top three-way ball valve 9, and then through the top three-way ball valve 9 to the second serpentine tube 4. Inside, the bottom and middle of the reactor 1 are heated by the first coil 3 and the second coil 4. When the reaction volume in the reactor 1 is at its maximum, the handle 9 of the three-way ball valve at the top is turned so that steam passes through the three-way ball valve at the top and then a portion of the steam is diverted into the second L-shaped gas supply pipe 7 at the top. Since the second L-shaped gas supply pipe 7 is connected to the third coil 5, a portion of the steam diverted by the three-way ball valve 9 at the top is transported into the interior of the third coil 5 through the second L-shaped gas supply pipe 7. The bottom, middle and top of the reactor 1 are heated simultaneously by the first coil 3, the second coil 4 and the third coil 5. The steam enters different coils to adapt to different reaction volumes inside the reactor 1, which solves the problem of not being able to adjust the length of the coils according to the amount of polyaluminum chloride reacting with wastewater.

[0030] In this invention, unless otherwise explicitly specified and limited, "above" or "below" the second feature can include direct contact between the first and second features, or contact between the first and second features through another feature between them. Furthermore, "above," "over," and "on top" of the second feature includes the first feature directly above or diagonally above the second feature, or simply indicates that the first feature is at a higher horizontal level than the second feature. "Below," "below," and "under" the second feature includes the first feature directly below or diagonally below the second feature, or simply indicates that the first feature is at a lower horizontal level than the second feature.

[0031] The foregoing has shown and described the basic principles, main features, and advantages of this utility model. Those skilled in the art should understand that this utility model is not limited to the above embodiments. The embodiments and descriptions in the specification are merely preferred examples and are not intended to limit the utility model. Various changes and modifications can be made to this utility model without departing from its spirit and scope, and all such changes and modifications fall within the scope of the claimed utility model. The scope of protection of this utility model is defined by the appended claims and their equivalents.

Claims

1. A device for adaptive temperature control of polyaluminum chloride reaction, comprising a reaction vessel (1), characterized in that: The reactor (1) is provided with a lid (2) on top, and a temperature sensor (13) is provided on the top of the lid (2). A first coil (3) is wound around the outside of the reactor (1). A second coil (4) is provided on the top of the first coil (3). A third coil (5) is provided on the top of the second coil (4). Two fixing buckles (10) are provided on both sides of the first coil (3), the second coil (4) and the third coil (5). Two three-way ball valves (9) are provided on one side of the reactor (1). A first connecting pipe (8) is provided between the two three-way ball valves (9). A first L-shaped gas supply pipe (6) is provided on one side of the first coil (3). A second L-shaped gas supply pipe (7) is provided on one side of the third coil (5). A second connecting pipe (11) is provided on the side of the reactor (1) away from the three-way ball valves (9). An outlet (12) is provided on the surface of the second connecting pipe (11) away from the reactor (1).

2. The adaptive temperature control device for polyaluminum chloride reaction according to claim 1, characterized in that: The lid (2) is installed on the top surface of the reactor (1) and is connected to the flange of the reactor (1).

3. The adaptive temperature control device for polyaluminum chloride reaction according to claim 1, characterized in that: The temperature sensor (13) is installed on the top surface of the lid (2) and is connected to the flange of the lid (2). One end of the temperature sensor (13) penetrates into the lid (2).

4. The adaptive temperature control device for polyaluminum chloride reaction according to claim 1, characterized in that: The first snake tube (3), the second snake tube (4) and the third snake tube (5) are all wrapped around the outer surface of the reactor (1), and the first snake tube (3), the second snake tube (4) and the third snake tube (5) are all installed on the outer surface of the reactor (1) by four fixing buckles (10). The first snake tube (3), the second snake tube (4) and the third snake tube (5) are set at equal intervals.

5. The adaptive temperature control device for polyaluminum chloride reaction according to claim 1, characterized in that: The vertical centerlines of the two three-way ball valves (9) are aligned, and both three-way ball valves (9) are connected to the flanges of the first serpentine tube (3) and the second serpentine tube (4).

6. The adaptive temperature control device for polyaluminum chloride reaction according to claim 1, characterized in that: Both ends of the first connecting pipe (8) are connected to the flanges of two three-way ball valves (9), and the second connecting pipe (11) is connected to the flanges of the first coil (3), the second coil (4) and the third coil (5) away from the three-way ball valves (9).

7. The adaptive temperature control device for polyaluminum chloride reaction according to claim 1, characterized in that: The first L-shaped gas pipe (6) and the second L-shaped gas pipe (7) are mirror-symmetrically arranged with the first connecting pipe (8) as the center, and both the first L-shaped gas pipe (6) and the second L-shaped gas pipe (7) are connected to the flange of the three-way ball valve (9).

Citation Information

Patent Citations

  • Device for automatically controlling reaction temperature in polyaluminum chloride reactor

    CN219958110U