Soaking solution filling and proportioning device

Abstract

The utility model discloses a soak solution filling and proportioning device, which belongs to the technical field of bone gelatin preparation and comprises a reaction component, a circulation component connected with the reaction component and a filling component connected with the circulation component. Wherein the reaction assembly is a reaction container used for accommodating a soaking object for soaking, and comprises a reaction tank, a stirring device and a stirring device, the circulation assembly is used for keeping circulation of soaking liquid and comprises a four-way pipe and first electromagnetic valves arranged on the four-way pipe, and the first electromagnetic valves are used for adjusting the communication state of all connectors of the four-way pipe; one connector of the four-way pipe is connected with the bottom of the reaction assembly, and the circulating assembly further comprises a pump body connected with the four-way pipe and a filtering channel connected with the pump body; and one interface of the four-way pipe is connected with the pump body. The flow speed of the circulating liquid is adjusted to mix the supplementary soaking liquid with the circulating soaking liquid, and the technical effect of adjusting the pH value of the soaking liquid is achieved through the supplementary soaking liquid.

Description

TECHNICAL FIELD

[0001] The utility model discloses bone gelatin preparation technical field, specifically relates to a soaking liquid filling proportioning device. BACKGROUND

[0002] The pickling process is an important link in the bone gelatin preparation process, which is used to remove inorganic minerals such as tricalcium phosphate (Ca3(PO4)2) and calcium carbonate (CaCO3) from the bone material, thereby improving the quality and yield of gelatin. The pickling process mainly uses hydrochloric acid as the acid source, and through chemical reaction, the inorganic substances in the bone material are converted into soluble salts, thereby realizing the separation from collagen.

[0003] However, too high pH value in the pickling process may reduce the acid leaching efficiency, because the acid leaching process usually relies on an acidic environment to dissolve the minerals such as calcium and phosphorus in the bone; on the other hand, the increase of pH value may cause some metal ions to form insoluble hydroxide precipitates, such as Fe 3+ Fe(OH)3precipitate, which will wrap some valuable components such as vanadium in the bone, causing them to be unable to be effectively leached out, thereby increasing the loss rate, therefore, it is necessary to adjust the pH value of the soaking liquid in real time during the pickling process, and add fresh soaking liquid to adjust the pH value of the soaking liquid when the pH value changes. CONTENT OF THE UTILITY MODEL

[0004] To solve the above problems, the utility model provides a kind of soaking liquid filling proportioning device, comprising: reaction component, with the circulation component being connected with the reaction component, and with the filling component being connected with the circulation component;

[0005] Wherein, the reaction component is the reaction container for accommodating soaking material to soak, comprising: reaction tank;

[0006] The circulation component is used to keep the soaking liquid circulating, comprising: four-way pipe, first solenoid valve respectively arranged on the four-way pipe, and the first solenoid valve is used to adjust the communication state of each interface of four-way pipe;

[0007] One of the interfaces of the four-way pipe is connected with the bottom of the reaction component, and the circulation component further comprises a pump body connected with the four-way pipe, and a filter channel connected with the pump body;

[0008] One of the interfaces of the four-way pipe is connected with the pump body.

[0009] In some embodiments, the reaction component further comprises a first supplementary tank, a first supplementary pipe connected with the first supplementary tank, a second supplementary tank, and a second supplementary pipe connected with the second supplementary tank;

[0010] The circulation component further comprises:

[0011] a filter box arranged on the filter channel;

[0012] a first connecting pipe connected with the filter channel, a storage chamber connected with the first connecting pipe, and a backflushing channel connected with the filter box.

[0013] In some embodiments, the first connecting pipe is connected with the filter channel, and a second electromagnetic valve is arranged on the first connecting pipe, which is used to adjust the passing state of the first connecting pipe.

[0014] The backflushing channel is connected with the filter box, and by opening the second electromagnetic valve, the filtered impurities in the filter box are backflushed into the storage chamber.

[0015] In some embodiments, the circulating assembly further comprises a first storage chamber and a second storage chamber, wherein the first storage chamber and the second storage chamber are respectively connected with two interfaces of the four-way pipe.

[0016] In some embodiments, the filling assembly is used to add the soaking liquid during the soaking liquid circulation process, comprising:

[0017] a three-way flow guide member, a retaining frame arranged in the three-way flow guide member, a main shaft movably connected with the retaining frame, and a flow guide fin arranged on the main shaft.

[0018] The three-way flow guide member comprises two groups of flow guide covers, and a containing pipe connected between the two groups of flow guide covers, and the containing pipe is perpendicular to the two groups of flow guide covers.

[0019] In some embodiments, the containing pipe is a hollow structure, and two sides of the containing pipe are respectively connected with the flow guide covers, and the retaining frame divides the hollow structure of the containing pipe into a flow guide compartment and a mixing compartment, wherein the flow guide compartment is in communication with the flow guide cover.

[0020] The flow guide fin is arranged on the main shaft and located in the flow guide compartment, and when the soaking liquid flows through the flow guide compartment, the main shaft is driven to rotate by the flow guide fin.

[0021] In some embodiments, the filling assembly further comprises a liquid injection compartment, an arc-shaped pipe connected with the liquid injection compartment, a shaft sleeve connected with the main shaft, an inner rotating piston matched with the shaft sleeve, and a booster fan blade arranged on the shaft sleeve.

[0022] The inner rotating piston is matched with the arc-shaped pipe, which is used to adjust the communication state of the arc-shaped pipe, and the booster fan blade is arranged in the liquid injection compartment.

[0023] In some embodiments, the liquid injection compartment is respectively connected with the first supplementary pipe and the second supplementary pipe, which is used to supplement the soaking liquid into the filling assembly.

[0024] When the soaking liquid is in a circulating state, the inner rotary piston abuts against one end of the arc-shaped tube away from the liquid filling bin to block the arc-shaped tube, and the circulating flow of the soaking liquid in the three-way flow guide piece is a first circulating flow;

[0025] The shaft sleeve is movably connected with the main shaft through a spline;

[0026] The end of the inner rotary piston away from the shaft sleeve is provided with a spring, and when the soaking liquid is in a circulating supplement state, the circulating flow of the soaking liquid in the three-way flow guide piece is a second circulating flow;

[0027] The second circulating flow is greater than the first circulating flow;

[0028] The high-pressure fan blade rotates to push the shaft sleeve to compress the spring through the inner rotary piston, and the inner rotary piston is separated from the arc-shaped tube to make the soaking liquid in the arc-shaped tube enter the mixing bin;

[0029] The retainer is provided with a through hole to make the mixing bin and the flow guide bin in a communicating state.

[0030] In some embodiments, the reaction assembly further comprises a ring pipe and a branch pipe connected with the ring pipe, wherein the ring pipe is connected with the filling assembly, and the branch pipe is connected with the reaction tank in a distributed manner.

[0031] By adopting the above technical scheme, the utility model mainly has the following technical effects:

[0032] The flow rate of the circulating liquid is adjusted to mix the supplement soaking liquid and the circulating soaking liquid, and the supplement soaking liquid is used to realize the technical effect of adjusting the pH value of the soaking liquid. BRIEF DESCRIPTION OF DRAWINGS

[0033] Figure 1 It is a structural schematic view of the soaking liquid filling and proportioning device of the utility model;

[0034] Figure 2 It is a structural schematic view of the soaking liquid filling and proportioning device of the utility model;

[0035] Figure 3 It is a structural schematic view of the soaking liquid filling and proportioning device (another view) of the utility model;

[0036] Figure 4 It is a structural schematic view of the soaking liquid filling and proportioning device (another view) of the utility model;

[0037] Figure 5 It is a structural schematic view of the circulating assembly in the soaking liquid filling and proportioning device of the utility model;

[0038] Figure 6The utility model relates to a kind of structure schematic diagram of filling assembly of infusion liquid filling proportioning device.

[0039] Figure 7 The utility model relates to a kind of structure schematic diagram of filling assembly (another view) of infusion liquid filling proportioning device.

[0040] Wherein, the meaning of the reference sign is as follows:

[0041] 1, reaction component;11, reaction tank;12, metal net rack;13, first supplementary tank;14, first supplementary pipe;15, second supplementary tank;16, second supplementary pipe;17, ring pipe;18, branch pipe;

[0042] 2, circulating component;21, four-way pipe;22, first electromagnetic valve;23, pump body;24, filter passage;25, filter box;251, first filter screen;252, second filter screen;26, first connecting pipe;261, stockpiling chamber;262, second electromagnetic valve;27, backflushing passage;28, first storage chamber;29, second storage chamber;

[0043] 3, filling assembly;31, three-way flow guide piece;311, flow guide cover;312, containing pipe;313, flow guide bin;314, mixing bin;32, retainer;321, through hole;33, main shaft;34, flow guide fin;35, liquid injection bin;36, arc pipe;37, shaft sleeve;38, inner rotary piston;381, spring;39, booster fan blade. DETAILED DESCRIPTION

[0044] In order to make the personnel in the art better understand the utility model scheme, the technical scheme in the embodiment of the utility model will be described clearly and completely in conjunction with the drawings of the specification of the utility model below, obviously, the described embodiment is only a part of the embodiment of the utility model, not all the embodiments. Based on the embodiment in the utility model, all other embodiments obtained by the person skilled in the art without making creative labor belong to the scope of the utility model protection.

[0045] In this paper, "embodiment" means that the specific features, structures or characteristics described in conjunction with the embodiment can be contained in at least one embodiment of the utility model. The phrase appears in the specification does not necessarily refer to the same embodiment, nor is it an independent or alternative embodiment that is not mutually exclusive with other embodiments. The person skilled in the art explicitly and implicitly understands that the embodiments described in this paper can be combined with other embodiments.

[0046] Please refer to Figures 1-7The utility model provides a kind of soaking liquid filling proportioning device, comprising: reaction component 1, the circulation component 2 connected with the reaction component 1 and the filling component 3 connected with the circulation component 2.

[0047] In some embodiments, the reaction component 1 is a reaction container for accommodating the soaking material for soaking. Specifically, the reaction component 1 comprises a reaction tank 11 and a metal mesh frame 12 arranged in the reaction tank 11. In some embodiments, the reaction tank 11 is used to accommodate the soaking material and the soaking liquid, so as to realize the soaking process of the soaking material. In some embodiments, the metal mesh frame 12 is horizontally arranged in the reaction tank 11. The metal mesh frame 12 is used to support the soaking material and can also assist in salvaging the soaking material.

[0048] In some embodiments, the reaction component 1 further comprises a first supplementary tank 13, a first supplementary pipe 14 connected with the first supplementary tank 13, a second supplementary tank 15 and a second supplementary pipe 16 connected with the second supplementary tank 15. In some embodiments, the first supplementary tank 13 and the second supplementary tank 15 are used to accommodate the soaking liquid. For example, the first supplementary tank 13 and the second supplementary tank 15 can contain at least one of acidic soaking liquid, alkaline soaking liquid and deionized water. The first supplementary pipe 14 and the second supplementary pipe 16 are also connected with the filling component 3, and are used to supplement the soaking liquid to the filling component 3.

[0049] Further, the bottom of the reaction tank 11 is connected with the circulation component 2, and the bottom of the reaction tank 11 is in a funnel shape with the upper part being wide and the lower part being narrow, so as to facilitate the soaking liquid to enter the circulation component 2, thereby realizing the circulation of the soaking liquid.

[0050] In some embodiments, the circulation component 2 is used to keep the soaking liquid circulating. By keeping the soaking liquid in the reaction tank 11 circulating, the soaking liquid in the reaction tank 11 is mixed uniformly, so as to keep the pH value of the soaking liquid uniform and keep the interlayer temperature uniform.

[0051] Further, the circulation component 2 comprises a four-way pipe 21 and a first electromagnetic valve 22 arranged on the four-way pipe 21. The four-way pipe 21 is a connecting pipe with four independent interfaces, and the first electromagnetic valve 22 is arranged on each interface of the four-way pipe 21. The first electromagnetic valve 22 is used to adjust the communication state of each interface of the four-way pipe 21.

[0052] In some embodiments, one of the interfaces of the four-way pipe 21 is connected with the bottom of the reaction component 1. Further, the circulation component 2 further comprises a pump body 23 connected with the four-way pipe 21, a filter channel 24 connected with the pump body 23 and a filter box 25 arranged on the filter channel 24.

[0053] Further, one of the interfaces of the four-way pipe 21 is connected with the pump body 23, when the first electromagnetic valve 22 on the two interfaces of the four-way pipe 21 connected with the pump body 23 and the reaction assembly 1 is in the communication state, the soaking liquid in the reaction assembly 1 can be extracted through the pump body 23, so as to realize the circulation of the soaking liquid. In some embodiments, the pump body 23 can be a magnetic pump, which can use magnetic coupling technology to transmit power, so as to realize the pumping without shaft seal or mechanical seal, effectively avoiding the leakage problem that may occur when the conventional pump is used to transport toxic, harmful or corrosive medium.

[0054] In some embodiments, the filter box 25 is arranged in the filter channel 24, for filtering the soaking liquid passing through the filter channel 24, further, the filter box 25 is provided with a first filter screen 251 and a second filter screen 252, in some embodiments, the diameters of the filter eyes of the first filter screen 251 and the second filter screen 252 are different, for example, the diameter of the filter eye of the first filter screen 251 can be larger than that of the second filter screen 252, so as to filter the soaking liquid for multiple times, to improve the filtering effect.

[0055] Further, the circulation assembly 2 further comprises a first connecting pipe 26 connected with the filter channel 24, a storage chamber 261 connected with the first connecting pipe 26, and a backflushing channel 27 connected with the filter box 25. Wherein, the first connecting pipe 26 is connected with the filter channel 24, in some embodiments, the second electromagnetic valve 262 is arranged on the first connecting pipe 26, and the second electromagnetic valve 262 is used to adjust the passing state of the first connecting pipe 26. Further, the backflushing channel 27 is connected with the filter box 25, when the operator cleans the filter box 25, the second electromagnetic valve 262 can be opened to inject high-pressure water flow or high-pressure gas flow into the filter box 25, so as to backflush the impurities filtered in the filter box 25 to the storage chamber 261, so as to realize the cleaning process of the filter box 25. Of course, the circulation process of the soaking liquid can also be realized by closing the second electromagnetic valve 262 and the backflushing channel 27. In some embodiments, the storage chamber 261 is a box-shaped container with a certain volume, which can accommodate multiple impurities for cleaning and then be treated, so as to avoid the operator to treat multiple times during use, reduce the labor intensity of the operator and enhance the practicability.

[0056] In some embodiments, the circulating assembly 2 further comprises a first storage chamber 28 and a second storage chamber 29, wherein the first storage chamber 28 and the second storage chamber 29 are respectively connected with two interfaces of the four-way pipe 21, for example, when the first electromagnetic valve 22 on the interface where the four-way pipe 21 is connected with the reaction assembly 1 and the first storage chamber 28 and / or the second storage chamber 29 is in a communication state, the soaking liquid can be guided into the first storage chamber 28 and / or the second storage chamber 29, and then the soaking liquid is added into the reaction tank 11 to realize the soaking liquid replacement process.

[0057] Further, the filling assembly 3 is used to add the soaking liquid during the soaking liquid circulation process, and in some embodiments, the soaking liquid entering the filling assembly 3 is soaking liquid that has not been soaked, for example, fresh acidic soaking liquid or deionized water can be added to adjust the pH value of the soaking liquid during the circulation process.

[0058] In some embodiments, the filling assembly 3 comprises a three-way flow guide 31, a holder 32 arranged in the three-way flow guide 31, a main shaft 33 movably connected with the holder 32, and a flow guide fin 34 arranged on the main shaft 33, and in some embodiments, the three-way flow guide 31 is a connecting pipe with three flow guide ports, wherein the three-way flow guide 31 comprises two groups of flow guide covers 311 and a containing pipe 312 connected between the two groups of flow guide covers 311, and the containing pipe 312 is perpendicular to the two groups of flow guide covers 311.

[0059] In some embodiments, the flow guide cover 311 is a funnel-shaped structure to facilitate the guiding of the soaking liquid into the containing pipe 312 or the discharge of the soaking liquid from the containing pipe 312. The containing pipe 312 is a hollow structure, and its two sides are respectively connected with the flow guide covers 311. By arranging the holder 32 in the containing pipe 312, the holder 32 divides the hollow structure of the containing pipe 312 into a flow guide compartment 313 and a mixing compartment 314, wherein the flow guide compartment 313 is in communication with the flow guide cover 311.

[0060] In some embodiments, the flow guide fin 34 is arranged on the main shaft 33 and located in the flow guide compartment 313. When the soaking liquid flows through the flow guide compartment 313, the flow guide fin 34 drives the main shaft 33 to rotate.

[0061] In some embodiments, the filling assembly 3 further comprises a liquid injection compartment 35, an arc-shaped pipe 36 connected with the liquid injection compartment 35, a shaft sleeve 37 connected with the main shaft 33, an inner rotating piston 38 matched with the shaft sleeve 37, and a booster fan blade 39 arranged on the shaft sleeve 37, wherein the inner rotating piston 38 is matched with the arc-shaped pipe 36 to adjust the communication state of the arc-shaped pipe 36, and the booster fan blade 39 is arranged in the liquid injection compartment 35.

[0062] In some embodiments, the liquid injection tank 35 is connected to the first and second replenishment pipes 14 and 16 respectively, when the soaking liquid is replenished into the filling assembly 3, the soaking liquid first enters the liquid injection tank 35, and then enters the arc-shaped pipe 36, when the soaking liquid circulates, the inner rotating piston 38 abuts against one end of the arc-shaped pipe 36 away from the liquid injection tank 35 to block the arc-shaped pipe 36, so as to prevent the soaking liquid in the arc-shaped pipe 36 from entering the mixing tank 314.

[0063] Further, the shaft sleeve 37 is movably connected to the main shaft 33 by means of the spline, in some embodiments, when the main shaft 33 rotates, the shaft sleeve 37 is driven to rotate along with the main shaft 33, thereby driving the booster fan blade 39 to rotate, when the booster fan blade 39 rotates, the blade pushes the soaking liquid to flow backward, and the pressure difference between the leading edge (suction surface) and the trailing edge (pressure surface) of the blade makes the soaking liquid speed up at the trailing edge of the blade, thereby generating a forward thrust to push the shaft sleeve 37 to move towards the inner rotating piston 38, and further push the inner rotating piston 38 to move, so that the inner rotating piston 38 is separated from the arc-shaped pipe 36.

[0064] In some embodiments, a spring 381 is arranged at one end of the inner rotating piston 38 away from the shaft sleeve 37, when the soaking liquid is in a circulating state, the circulating flow rate of the soaking liquid in the three-way flow guide 31 is a first circulating flow rate, under the limiting action of the spring 381, the inner rotating piston 38 is in a state of blocking the arc-shaped pipe 36; when the soaking liquid is in a circulating and replenishing state, the circulating flow rate of the soaking liquid in the three-way flow guide 31 is a second circulating flow rate, wherein the second circulating flow rate is greater than the first circulating flow rate, by increasing the circulating flow rate of the soaking liquid, the rotating speed of the main shaft 33 is accelerated under the action of the flow guide fin 34, the thrust generated by the booster fan blade 39 is greater, thereby compressing the spring 381, so that the inner rotating piston 38 is separated from one end of the arc-shaped pipe 36, thereby enabling the soaking liquid in the arc-shaped pipe 36 to enter the mixing tank 314.

[0065] In some embodiments, a through hole 321 is arranged on the retainer 32, so that the mixing tank 314 and the flow guide tank 313 are in a communicating state, so that the replenished soaking liquid can enter the three-way flow guide 31 to mix with the circulating soaking liquid, thereby adjusting the flow rate of the circulating liquid to mix the replenished soaking liquid with the circulating soaking liquid, and adjusting the pH value of the soaking liquid by the replenished soaking liquid.

[0066] Further, the reaction assembly 1 further comprises a ring pipe 17 and branch pipes 18 connected with the ring pipe 17, wherein the ring pipe 17 is connected with the filling assembly 3 and used for receiving the circulating soaking liquid or the circulating soaking liquid after liquid injection; the branch pipes 18 are connected with the reaction tank 11 in a distributed manner and used for injecting the circulating soaking liquid or the circulating soaking liquid after liquid injection into the reaction tank 11 in a distributed manner, so that the soaking liquid in the reaction tank 11 is evenly distributed.

[0067] Finally, it should be noted that: the embodiments of the utility model only for the preferred embodiment of the utility model, only for the description of the technical scheme of the utility model, but not to limit it; although the utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art should understand; it still can modify the technical scheme recorded in the foregoing embodiments, or make equivalent replacement to part of the technical features; and these modifications or replacements do not make the essence of the corresponding technical scheme deviate from the spirit and scope of the technical scheme of the embodiments of the utility model.

Claims

1. An infusion liquid filling ratio device characterized by comprising: The application relates to a reaction device for a liquid infusion machine. The reaction device comprises a reaction assembly, a circulating assembly connected to the reaction assembly, and a filling assembly connected to the circulating assembly. The reaction assembly is a reaction container for accommodating infusion materials for infusion, and comprises a reaction tank. The circulating assembly is used for keeping infusion liquid circulating, and comprises a four-way pipe, a first electromagnetic valve arranged on the four-way pipe, and used for adjusting the communication state of each interface of the four-way pipe. One of the interfaces of the four-way pipe is connected to the bottom of the reaction assembly. The circulating assembly further comprises a pump body connected to the four-way pipe, and a filtering channel connected to the pump body.

2. The infusion fluid priming device of claim 1, wherein, One of the interfaces of the four-way pipe is connected to the pump body. The reaction assembly further comprises a first supplementary tank, a first supplementary pipe connected to the first supplementary tank, a second supplementary tank, and a second supplementary pipe connected to the second supplementary tank. The circulating assembly further comprises: a filtering box arranged on the filtering channel; 3. The device according to claim 2, wherein a first connecting pipe connected to the filtering channel, a storage chamber connected to the first connecting pipe, and a backflushing channel connected to the filtering box. The first connecting pipe is connected to the filtering channel, and a second electromagnetic valve is arranged on the first connecting pipe and used for adjusting the passing state of the first connecting pipe.

4. The device according to claim 3, wherein The backflushing channel is connected to the filtering box, and when the second electromagnetic valve is opened, the filtered impurities in the filtering box are backflushed into the storage chamber.

5. The device of claim 3, wherein the device is a device for adding a liquid to a container. The circulating assembly further comprises a first storage chamber and a second storage chamber, wherein the first storage chamber and the second storage chamber are respectively connected to two interfaces of the four-way pipe. The filling assembly is used for adding infusion liquid during the circulation of the infusion liquid, and comprises: a three-way flow guide piece, a retaining frame arranged in the three-way flow guide piece, a main shaft movably connected to the retaining frame, and flow guide fins arranged on the main shaft.

6. The device according to claim 5, wherein The three-way flow guide piece comprises two groups of flow guide covers, and a containing pipe connected between the two groups of flow guide covers, and the containing pipe is perpendicular to the two groups of flow guide covers. The containing pipe is a hollow structure, and two sides of the containing pipe are respectively connected to the flow guide covers.

7. The device according to claim 6, wherein The retaining frame divides the hollow structure of the containing pipe into a flow guide chamber and a mixing chamber, wherein the flow guide chamber is connected to the flow guide covers. The flow guide fins are arranged on the main shaft and located in the flow guide chamber, and when the infusion liquid flows through the flow guide chamber, the flow guide fins drive the main shaft to rotate.

8. The device according to claim 7, wherein The filling assembly further comprises a liquid injection chamber, an arc-shaped pipe connected to the liquid injection chamber, a shaft sleeve connected to the main shaft, an inner rotary piston matched with the shaft sleeve, and a booster fan blade arranged on the shaft sleeve. The inner rotary piston is matched with the arc-shaped pipe and used for adjusting the communication state of the arc-shaped pipe, and the booster fan blade is arranged in the liquid injection chamber. The liquid injection chamber is respectively connected to the first supplementary pipe and the second supplementary pipe, and used for supplementing infusion liquid to the filling assembly. When the infusion liquid is in a circulating state, the inner rotary piston abuts against one end of the arc-shaped pipe away from the liquid injection chamber to block the arc-shaped pipe, and the circulating flow of the infusion liquid in the three-way flow guide piece is a first circulating flow. The shaft sleeve and the main shaft are movably connected through a spline. The inner rotary piston is provided with a spring at one end away from the sleeve, when the soaking liquid is in a circulating replenishment state, the circulating flow of the soaking liquid in the three-way flow guide is a second circulating flow; The second circulating flow is greater than the first circulating flow; The rotation of the booster fan blade pushes the sleeve to compress the spring through the inner rotary piston, and the soaking liquid in the arc-shaped tube is separated from the inner rotary piston to enter the mixing bin; The retainer is provided with a through hole to make the mixing bin and the flow guide bin in a communication state.

9. The device of claim 2, wherein, The reaction assembly further comprises a ring tube and a branch tube connected with the ring tube, wherein the ring tube is connected with the filling assembly, and the branch tube is connected with the reaction tank in a distributed manner.

Images