Aminomethylbenzoic acid chlorination catalytic reaction device

Abstract

The utility model discloses an aminomethylbenzoic acid chlorination catalytic reaction device, which relates to the technical field of aminomethylbenzoic acid, and comprises an integral device main body, the integral device main body comprises a base, the base is positioned at the bottom of the integral device main body, a supporting rod is arranged at the top of the periphery of the base, a collecting hopper is mounted at the top of the periphery of the supporting rod, and the collecting hopper is connected with the base. A collecting pipe is installed in the center of the bottom of the periphery of the collecting hopper, an electric control valve is arranged on the outer ring face of the collecting pipe, and a catalysis barrel is arranged on the top of the periphery of the collecting hopper. A catalytic barrel, a connecting ring, a driving motor, a first connecting piece, a connecting pipe, a second connecting piece, a purifying mechanism, a discharging pipe, a recycling barrel, a touch screen, a temperature sensor, an alarm lamp, a stirring rod, a heating mechanism, a first filtering mechanism and a second filtering mechanism are arranged; the problem that a common aminomethylbenzoic acid chlorination catalytic reaction device is poor in alarm function and collection effect is effectively solved.

Description

TECHNICAL FIELD

[0001] The utility model relates to the technical field of aminomethylbenzoic acid, specifically to aminomethylbenzoic acid chlorination catalytic reaction device. BACKGROUND

[0002] Aminomethylbenzoic acid, also known as 4-aminomethylbenzoic acid, is an organic compound with the molecular formula C8H9NO2.

[0003] In the prior art, the alarm function and collection effect of the ordinary aminomethylbenzoic acid chlorination catalytic reaction device are poor. UTILITY MODEL CONTENT

[0004] The utility model provides a kind of aminomethylbenzoic acid chlorination catalytic reaction device to solve the problem in the background art.

[0005] To achieve the above object, the utility model provides the following technical scheme: a kind of aminomethylbenzoic acid chlorination catalytic reaction device, including overall device main body, the overall device main body includes base, wherein base is located at the bottom of overall device main body, the outer periphery top of base is provided with support rod, the outer periphery top of support rod is installed with collecting hopper, the outer periphery bottom center of collecting hopper is installed with collecting pipe, electric control valve is provided on the outer ring surface of collecting pipe, the outer periphery top of collecting hopper is provided with catalytic barrel, the outer ring surface one side of catalytic barrel is provided with touch screen, the outer ring surface one side of catalytic barrel is provided with temperature sensor, the outer ring surface one side of catalytic barrel is provided with alarm lamp, the inside of catalytic barrel is provided with heating mechanism, the outer periphery top of catalytic barrel is provided with connecting ring, the outer periphery top middle of connecting ring is installed with drive motor, the outer periphery bottom output end of drive motor is movably connected with stirring rod, the outer periphery top of connecting ring is provided with first connecting piece near outer edge, the outer periphery top of first connecting piece is provided with connecting pipe;

[0006] The outer periphery end of connecting pipe away from first connecting piece is provided with second connecting piece, the outer periphery bottom of second connecting piece is provided with purification mechanism, the inside of purification mechanism is provided with first filter mechanism, the inside of purification mechanism is provided with second filter mechanism, the outer periphery top of purification mechanism is provided with first pressure gauge, the outer periphery shorter side of purification mechanism is connected with discharge pipe, the outer periphery end of discharge pipe away from purification mechanism is connected with recovery barrel, the outer periphery top of recovery barrel is provided with second pressure gauge.

[0007] Further, the outer periphery top of base is provided with three groups of support rods, and the inside of collecting hopper, catalytic barrel and connecting ring is interconnected.

[0008] Further, the inside of collecting hopper, electric control valve, catalytic barrel and touch screen is electrically connected.

[0009] Further, the heating mechanism arranged in the catalytic barrel is internally provided with a heating lamp, and the catalytic barrel, the touch screen, the heating mechanism, the temperature sensor and the alarm lamp are internally electrically connected.

[0010] Further, the peripheral bottom output end of the driving motor is connected with the stirring rod through the catalytic barrel, and the stirring rod is rotationally connected with the driving shaft on the peripheral bottom output end of the driving motor.

[0011] Further, the first filtering mechanism arranged in the purification mechanism is internally provided with a filter screen, and the second filtering mechanism arranged in the purification mechanism is internally provided with activated carbon.

[0012] Compared with the prior art, the utility model provides a kind of p-toluene sulfonic acid chlorination catalytic reaction device, with following beneficial effects:

[0013] 1、The catalytic reaction device of p-toluene sulfonic acid chlorination, by setting catalytic barrel, connecting ring, driving motor, first connecting piece, connecting pipe, second connecting piece, purification mechanism, discharge pipe, recovery barrel, touch screen, temperature sensor, alarm lamp, stirring rod, heating mechanism, first filtering mechanism and second filtering mechanism, the heating mechanism 22 arranged in the catalytic barrel 5 is internally provided with heating lamp, and the catalytic barrel 5, touch screen 16, heating mechanism 22, temperature sensor 19 and alarm lamp 20 are internally electrically connected, so that staff controls heating mechanism 22 inside heating lamp to start by motor touch screen 16, carries out heating treatment to catalytic barrel 5 inside, improves catalytic efficiency, at the same time, when temperature sensor 19 senses that catalytic barrel 5 inside temperature is too high, alarm lamp 20 sends out sound to remind staff, prevents temperature from being too high to influence catalytic result, ensures that reaction is carried out in optimum temperature range, the first filtering mechanism 23 arranged in the purification mechanism 11 is internally provided with filter screen, and the second filtering mechanism 24 arranged in the purification mechanism 11 is internally provided with activated carbon, so that in chlorination reaction process, unreacted chlorine is passed through purification mechanism 11, the first filtering mechanism 23 in the purification mechanism 11 carries out first heavy impurity filtration to unreacted chlorine, then the second filtering mechanism 24 in the purification mechanism 11 carries out second heavy impurity filtration to unreacted chlorine, and finally, unreacted chlorine after filtration is collected into recovery barrel 14, effectively solve the problem of poor alarm function and collection effect of ordinary p-toluene sulfonic acid chlorination catalytic reaction device. ACCURACY OF DRAWINGS

[0014] Figure 1 It is the whole structure schematic diagram of the utility model;

[0015] Figure 2 It is the catalytic barrel part structure schematic diagram of the utility model;

[0016] Figure 3 It is the inside amplification structure schematic view of the catalytic barrel of the utility model;

[0017] Figure 4 It is the inside amplification structure schematic view of the purifying mechanism of the utility model.

[0018] In the figure: 1, overall device main body; 2, base; 3, support rod; 4, collection hopper; 5, catalytic barrel; 6, connecting ring; 7, drive motor; 8, first connecting piece; 9, connecting pipe; 10, second connecting piece; 11, purifying mechanism; 12, first pressure gauge; 13, discharge pipe; 14, recovery barrel; 15, second pressure gauge; 16, touch screen; 17, collection pipe; 18, electric control valve; 19, temperature sensor; 20, alarm lamp; 21, stirring rod; 22, heating mechanism; 23, first filtering mechanism; 24, second filtering mechanism. DETAILED DESCRIPTION

[0019] The technical solutions in the embodiments of the utility model will be clearly and completely described below with reference to the drawings in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by those skilled in the art without creative labor belong to the scope of protection of the utility model.

[0020] Please refer to Figures 1-4 The utility model discloses a p-aminophenylalanine chlorination catalytic reaction device,

[0021] Specifically, a p-aminophenylalanine chlorination catalytic reaction device, including overall device main body 1, overall device main body 1 including base 2, wherein base 2 is located at the bottom of overall device main body 1, and the outer periphery top of base 2 is provided with support rod 3, the outer periphery top of support rod 3 is installed with collection hopper 4, the outer periphery bottom center of collection hopper 4 is installed with collection pipe 17, and the outer ring surface of collection pipe 17 is provided with electric control valve 18, the outer periphery top of collection hopper 4 is provided with catalytic barrel 5, one side of the outer ring surface of catalytic barrel 5 is provided with touch screen 16, one side of the outer ring surface of catalytic barrel 5 is provided with temperature sensor 19, one side of the outer ring surface of catalytic barrel 5 is provided with alarm lamp 20, the inside of catalytic barrel 5 is provided with heating mechanism 22, the outer periphery top of catalytic barrel 5 is provided with connecting ring 6, the outer periphery top middle of connecting ring 6 is installed with drive motor 7, and the outer periphery bottom output end of drive motor 7 is movably connected with stirring rod 21, and the outer periphery top of connecting ring 6 is provided with first connecting piece 8 near the outer edge, and the outer periphery top of first connecting piece 8 is provided with connecting pipe 9;

[0022] The second connecting piece 10 is arranged at the outer periphery of the one end of the connecting pipe 9 away from the first connecting piece 8, the bottom of the outer periphery of the second connecting piece 10 is provided with a purification mechanism 11, the inside of the purification mechanism 11 is provided with a first filtering mechanism 23, the inside of the purification mechanism 11 is provided with a second filtering mechanism 24, the top of the outer periphery of the purification mechanism 11 is provided with a first pressure gauge 12, the shorter side of the outer periphery of the purification mechanism 11 is connected with a discharge pipe 13, the one end of the outer periphery of the discharge pipe 13 away from the purification mechanism 11 is connected with a recovery bucket 14, and the top of the outer periphery of the recovery bucket 14 is provided with a second pressure gauge 15.

[0023] In the embodiment, the top of the outer periphery of the base 2 is provided with three groups of support rods 3, and the inside of the collection hopper 4, the catalytic bucket 5 and the connecting ring 6 is communicated, and the inside of the collection hopper 4, the electric control valve 18, the catalytic bucket 5 and the touch screen 16 is electrically connected.

[0024] Specifically, the staff can take out the catalyzed material by clicking the touch screen 16 to control the touch screen 16 to open.

[0025] In the embodiment, the inside of the heating mechanism 22 arranged in the catalytic bucket 5 is provided with a heating lamp, and the inside of the catalytic bucket 5, the touch screen 16, the heating mechanism 22, the temperature sensor 19 and the alarm lamp 20 is electrically connected.

[0026] Specifically, the staff can control the heating lamp in the heating mechanism 22 to start by the motor touch screen 16, heat the inside of the catalytic bucket 5 to improve the catalytic efficiency, and when the temperature sensor 19 senses that the temperature in the catalytic bucket 5 is too high, the alarm lamp 20 emits a sound to remind the staff, so as to prevent the high temperature from affecting the catalytic result and ensure that the reaction is carried out in the best temperature range.

[0027] In the embodiment, the output end of the outer periphery of the driving motor 7 penetrates the catalytic bucket 5 and is connected with the stirring rod 21, the stirring rod 21 is rotationally connected with the driving shaft on the output end of the outer periphery of the driving motor 7, the inside of the first filtering mechanism 23 arranged in the purification mechanism 11 is provided with a filter screen, and the inside of the second filtering mechanism 24 arranged in the purification mechanism 11 is provided with activated carbon.

[0028] Specifically, the staff can control the start of the driving motor 7 by starting the driving motor 7, the driving shaft of the output end of the outer periphery of the driving motor 7 drives the stirring rod 21 to rotate, so that the rotation of the stirring rod 21 can bring better catalytic effect, and in the chlorination reaction process, the unreacted chlorine gas passes through the purification mechanism 11, the first filtering mechanism 23 in the purification mechanism 11 filters the unreacted chlorine gas for the first time, then the second filtering mechanism 24 in the purification mechanism 11 filters the unreacted chlorine gas for the second time, and finally the filtered unreacted chlorine gas is collected in the recovery bucket 14.

[0029] In summary, the p-aminophenylalanine chlorination catalytic reaction device, when using the whole device body 1, the stirring rod 21 is connected to the catalytic barrel 5 through the peripheral bottom output end of the driving motor 7, and the stirring rod 21 is rotatably connected to the driving shaft on the peripheral bottom output end of the driving motor 7, so that the staff controls the start of the driving motor 7 by starting the driving motor 7, and the driving shaft of the peripheral bottom output end of the driving motor 7 drives the stirring rod 21 to rotate, so that the rotation of the stirring rod 21 can bring better catalytic effect, the heating lamp is arranged in the heating mechanism 22 arranged in the catalytic barrel 5, and the catalytic barrel 5, the touch screen 16, the heating mechanism 22, the temperature sensor 19 and the alarm lamp 20 are electrically connected, so that the staff controls the heating lamp in the heating mechanism 22 to start by the motor touch screen 16, and the inside of the catalytic barrel 5 is heated and treated to improve the catalytic efficiency, and when the temperature sensor 19 senses that the temperature inside the catalytic barrel 5 is too high, the alarm lamp 20 gives an alarm to remind the staff, so as to prevent the temperature from being too high to affect the catalytic result, and ensure that the reaction is carried out in the best temperature range, the filter screen is arranged in the first filter mechanism 23 arranged in the purification mechanism 11, and the activated carbon is arranged in the second filter mechanism 24 arranged in the purification mechanism 11, so that during the chlorination reaction, the unreacted chlorine gas passes through the purification mechanism 11, the first filter mechanism 23 in the purification mechanism 11 filters the unreacted chlorine gas for the first time, then the second filter mechanism 24 in the purification mechanism 11 filters the unreacted chlorine gas for the second time, and finally the filtered unreacted chlorine gas is collected in the recovery barrel 14, effectively solving the problems of poor alarm function and collection effect of ordinary p-aminophenylalanine chlorination catalytic reaction device, three groups of supporting rods 3 are arranged on the peripheral top of the base 2, the collecting hopper 4, the catalytic barrel 5 and the connecting ring 6 are internally communicated, and the collecting hopper 4, the electric control valve 18, the catalytic barrel 5 and the touch screen 16 are electrically connected, so that the staff can take out the catalyzed material by clicking the touch screen 16 to control the touch screen 16 to open, so the utility model is a very practical product and is worth popularizing and applying.

[0030] Although the embodiments of the utility model have been shown and described, it can be understood by those skilled in the art that various changes, modifications, replacements and modifications can be made to these embodiments without departing from the principles and spirits of the utility model, and the scope of the utility model is defined by the appended claims and their equivalents.

Claims

1. A catalytic apparatus for the chlorination of aminomethylbenzoic acid, comprising a monolithic body (1) of the apparatus, characterized in that: The whole device body (1) includes a base (2), wherein the base (2) is located at the bottom of the whole device body (1), the outer peripheral top of the base (2) is provided with a support rod (3), the outer peripheral top of the support rod (3) is provided with a collecting hopper (4), the outer peripheral bottom center of the collecting hopper (4) is provided with a collecting pipe (17), the outer ring surface of the collecting pipe (17) is provided with an electric control valve (18), the outer peripheral top of the collecting hopper (4) is provided with a catalytic barrel (5), one side of the outer ring surface of the catalytic barrel (5) is provided with a touch screen (16), one side of the outer ring surface of the catalytic barrel (5) is provided with a temperature sensor (19), one side of the outer ring surface of the catalytic barrel (5) is provided with an alarm lamp (20), the inside of the catalytic barrel (5) is provided with a heating mechanism (22), the outer peripheral top of the catalytic barrel (5) is provided with a connecting ring (6), the outer peripheral top of the connecting ring (6) is provided with a driving motor (7), the outer peripheral bottom output end of the driving motor (7) is movably connected with a stirring rod (21), the outer peripheral top of the connecting ring (6) is provided with a first connecting piece (8) near the outer edge, the outer peripheral top of the first connecting piece (8) is provided with a connecting pipe (9); The outer end of the connecting pipe (9) away from the first connecting piece (8) is provided with a second connecting piece (10), the outer peripheral bottom of the second connecting piece (10) is provided with a purification mechanism (11), the inside of the purification mechanism (11) is provided with a first filtering mechanism (23), the inside of the purification mechanism (11) is provided with a second filtering mechanism (24), the outer peripheral top of the purification mechanism (11) is provided with a first pressure gauge (12), the outer peripheral shorter side of the purification mechanism (11) is connected with a discharge pipe (13), the outer end of the discharge pipe (13) away from the purification mechanism (11) is connected with a recovery barrel (14), the outer peripheral top of the recovery barrel (14) is provided with a second pressure gauge (15).

2. A device for catalytic chlorination of aminomethylbenzoic acid according to claim 1, characterized in that: The outer peripheral top of the base (2) is provided with three groups of support rods (3), and the inside of the collecting hopper (4), the catalytic barrel (5) and the connecting ring (6) is interconnected.

3. A device for catalytic chlorination of aminomethylbenzoic acid according to claim 1, characterized in that: The inside of the collecting hopper (4), the electric control valve (18), the catalytic barrel (5) and the touch screen (16) is electrically connected.

4. A device for catalytic chlorination of aminomethylbenzoic acid according to claim 1, characterized in that: The inside of the heating mechanism (22) provided in the catalytic barrel (5) is provided with a heating lamp, and the inside of the catalytic barrel (5), the touch screen (16), the heating mechanism (22), the temperature sensor (19) and the alarm lamp (20) is electrically connected.

5. A device for catalytic chlorination of aminomethylbenzoic acid according to claim 1, characterized in that: The outer peripheral bottom output end of the driving motor (7) penetrates through the catalytic barrel (5) and is connected with the stirring rod (21), wherein the stirring rod (21) is rotationally connected with the driving shaft on the outer peripheral bottom output end of the driving motor (7).

6. A device for catalytic chlorination of aminomethylbenzoic acid according to claim 1, characterized in that: The inside of the first filtering mechanism (23) provided in the purification mechanism (11) is provided with a filter screen, and the inside of the second filtering mechanism (24) provided in the purification mechanism (11) is provided with activated carbon.

Images