Stirring reaction device for preparing electronic-grade chemicals

Abstract

The utility model belongs to the technical field of electronic-grade chemicals, and particularly relates to a stirring reaction device for preparing electronic-grade chemicals, which comprises a rack and a stirring drum, the stirring drum is fixedly mounted in the rack, a stirring device is arranged in the stirring drum, a cleaning device is arranged above the stirring drum, and a stirring device is arranged above the cleaning device. The stirring device comprises a stirring motor, a stirring shaft, alternate blades and a supporting rod, and the cleaning device comprises a valve, a cleaning straight pipe, a nozzle, a rhombic pipeline, a large gear, a small gear and a rotating shaft. According to the stirring reaction device for preparing the electronic grade chemicals, the stirring purpose is achieved through mutual cooperation of the stirring motor, the stirring shaft, the supporting rods and the alternate blades, and the purpose of all-directional spraying and cleaning is achieved through mutual cooperation of a valve, a cleaning straight pipe, a nozzle, a rhombic pipeline, a large gear, a small gear and a rotating shaft; raw material liquid is directly pumped into the stirring barrel through the water pump, raw material leakage can be prevented, accidents and pollution are reduced, and the state of the materials is detected in real time through the monitor.

Description

Technical Field

[0001] This utility model relates to the field of electronic-grade chemicals technology, specifically a stirring reaction apparatus for the preparation of electronic-grade chemicals. Background Technology

[0002] Electronic-grade chemicals refer to chemical reagents whose main components have a purity greater than 99.99% and whose impurity ions, especially impurity cations and particle numbers, meet strict requirements. They mainly include hydrochloric acid, acetone, ultrapure water, isopropanol, etc.

[0003] Electronic-grade chemicals require reaction equipment during manufacturing, but existing reaction equipment is relatively simple and lacks comprehensive functionality.

[0004] For example, Chinese patent CN221245220U discloses a reactor for electronic-grade chemical reactions. By using a stirring paddle, the chemicals inside the reactor can be stirred to increase the reaction rate. At the same time, the stirring column can be rotated in the opposite direction by a motor, and the stirring column drives the entire inner reactor to rotate, which has a certain centrifugal separation effect.

[0005] However, the equipment is difficult to clean after the reaction is complete, and impurities are easily left behind, affecting the quality and effect of the next production. Utility Model Content

[0006] The purpose of this invention is to provide a stirring reaction apparatus for the preparation of electronic-grade chemicals, in order to solve the problem mentioned in the background art that the apparatus is difficult to clean after the reaction is completed, easily leaving impurities, which affects the quality and effect of the next production.

[0007] To achieve the above objectives, the present invention provides the following technical solution: a stirring reaction apparatus for the preparation of electronic-grade chemicals, comprising a frame and a stirring cylinder, wherein the stirring cylinder is fixedly installed inside the frame, a stirring device is provided inside the stirring cylinder, and a cleaning device is provided above the stirring cylinder;

[0008] The stirring device includes a stirring motor, a stirring shaft, alternating blades, and a support rod. The stirring motor is mounted on the top of the frame, the stirring shaft is connected to the output end of the stirring motor, the support rod is fixedly connected to the outer surface of the stirring shaft, and the alternating blades are fixedly connected to the top of the support rod. By starting the stirring motor, the stirring shaft is driven, and the support rod rotates with the stirring shaft, thereby causing the alternating blades to rotate around the stirring shaft as the axis to achieve the purpose of stirring.

[0009] The cleaning device includes a valve, a cleaning straight pipe, a nozzle, a diamond-shaped pipe, a large gear, a small gear, and a rotating shaft. The large gear is fitted onto the outer surface of the stirring shaft. The diamond-shaped pipe has four through holes at its top, through which the rotating shaft passes. The nozzle is fixedly connected to the bottom of the rotating shaft. The small gear is fitted onto the outer surface of the rotating shaft and contacts the large gear. The diamond-shaped pipe is fixedly installed above the stirring drum. The cleaning straight pipe is fixedly connected to the right side of the diamond-shaped pipe. The valve is fixedly connected between two cleaning straight pipes. The cleaning straight pipe is connected to a container containing cleaning liquid. When the valve is opened, the cleaning liquid is sprayed out from the nozzle through the cleaning straight pipe and the diamond-shaped pipe. Turning on the stirring motor drives the large gear to rotate, which in turn drives the small gear to rotate, causing the rotating shaft to rotate, thereby rotating the nozzle to achieve the purpose of all-round spraying cleaning.

[0010] Preferably, a threaded hole is provided on the top of the frame, and the stirring motor is threadedly connected to the frame bolt through the threaded hole. This connection method makes the installation and disassembly of the stirring motor simple and quick, and facilitates maintenance and replacement. At the same time, the threaded connection also provides good stability and firmness, ensuring the stable operation of the stirring motor during the working process and reducing the risk of failure caused by vibration or loosening.

[0011] Preferably, the bottom of the mixing drum is conical, and a discharge port is provided at the bottom of the mixing drum. A sealing ring is fitted over the discharge port, and the outer surface of the discharge port is threaded. A sealing cap is connected to the outer surface of the discharge port through the thread. The conical bottom design facilitates the smooth discharge of materials and reduces the possibility of residue and blockage. The design of the discharge port and the sealing cap not only ensures the convenience of material discharge, but also effectively prevents material leakage when not in use, ensuring the cleanliness and safety of the production environment.

[0012] Preferably, a conveying device is provided on the right side of the mixing drum; the conveying device includes a water pump, a conveying pipe, a base, a raw material tank, and a sealing ring. The base is fixedly connected to the upper right side of the frame, the water pump is installed above the base, and the conveying pipe is fixedly connected to the left and right sides of the water pump. A through hole is opened on the right side of the mixing drum, and the through hole is fixedly connected to the left end of the conveying pipe. The right end of the conveying pipe is threaded, and the sealing ring is fitted onto the right end of the conveying pipe. A connecting pipe is opened on the left side of the raw material tank, and the right end of the conveying pipe is threadedly connected to the connecting pipe. Most chemical raw materials are corrosive or polluting. Directly drawing the raw material liquid into the mixing drum by the water pump can prevent raw material leakage and avoid direct contact with personnel, reducing the occurrence of accidents and pollution.

[0013] Preferably, a threaded hole is provided on the upper part of the base, and the water pump is threadedly connected to the upper part of the base through the threaded hole. This installation method makes the water pump more secure and reliable, reduces loosening and failure caused by vibration, and at the same time, the threaded connection facilitates the maintenance and replacement of the water pump, improving the overall reliability and service life of the equipment.

[0014] Preferably, the material of the raw material barrel is polypropylene (PP), which has excellent corrosion resistance and can resist the erosion of a variety of chemicals. It is suitable for the storage and transportation of liquid chemicals. In addition, polypropylene is relatively inexpensive, which reduces production costs. Therefore, choosing polypropylene as the material of the raw material barrel ensures both product quality and safety and economic benefits.

[0015] Preferably, the front of the mixing drum is provided with a threaded hole, and a monitoring instrument is fixedly installed on the front of the mixing drum through the threaded hole. The installation of the monitoring instrument allows the operator to understand the status and parameters of the material in the mixing drum (such as temperature, pressure, liquid level, etc.) in real time, providing an important basis for the control and adjustment of the production process. At the same time, the fixing method of the monitoring instrument also ensures its stability and accuracy, and improves the reliability of the monitoring data.

[0016] Compared with the prior art, the beneficial effects of this utility model are:

[0017] 1. The stirring reaction device for preparing electronic-grade chemicals, by starting the stirring motor to drive the stirring shaft, the support rod rotates with the stirring shaft, thereby causing the alternating blades to rotate around the stirring shaft to achieve the purpose of stirring. The cleaning straight pipe is connected to the container containing the cleaning liquid. When the valve is opened, the cleaning liquid will be sprayed out from the nozzle through the cleaning straight pipe and the diamond-shaped pipe. Turning on the stirring motor drives the large gear to rotate, which in turn drives the small gear to rotate, causing the rotating shaft to rotate, thereby causing the nozzle to rotate, achieving the purpose of all-round spraying cleaning.

[0018] 2. The stirring reaction device for the preparation of electronic-grade chemicals is designed for chemical raw materials that are mostly corrosive or polluting. By directly pumping the raw material liquid into the stirring drum through a water pump, leakage of raw materials can be prevented, and direct contact with personnel can be avoided, thus reducing the occurrence of accidents and pollution.

[0019] 3. The stirring reaction device for the preparation of electronic-grade chemicals, with the installation of monitoring instruments, allows operators to monitor the state and parameters of the materials inside the stirring drum in real time (such as temperature, pressure, liquid level, etc.), providing an important basis for the control and adjustment of the production process. Attached Figure Description

[0020] Figure 1 This is a schematic diagram of the overall structure of this utility model;

[0021] Figure 2This is a schematic diagram of the stirring device structure of this utility model;

[0022] Figure 3 This is a schematic diagram of the cleaning device structure of this utility model;

[0023] Figure 4 This is a schematic diagram of the raw material conveying device of this utility model;

[0024] Figure 5 This is a schematic diagram of the stirring cylinder structure of this utility model.

[0025] In the diagram: 1. Frame; 2. Agitator motor; 3. Valve; 4. Water pump; 5. Monitoring instrument; 6. Agitator drum; 201. Agitator shaft; 202. Alternating blades; 203. Support rod; 301. Cleaning straight pipe; 302. Nozzle; 303. Diamond-shaped pipe; 304. Large gear; 305. Small gear; 306. Rotating shaft; 401. Conveying pipe; 402. Base; 403. Raw material bucket; 404. Sealing ring one; 601. Sealing ring two; 602. Sealing cover; 603. Discharge port. Detailed Implementation

[0026] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0027] Please see Figures 1-5 This utility model provides a technical solution:

[0028] Example 1: A stirring reaction apparatus for the preparation of electronic-grade chemicals, comprising a frame 1 and a stirring drum 6, wherein the stirring drum 6 is fixedly installed inside the frame 1, a stirring device is provided inside the stirring drum 6, and a cleaning device is provided above the stirring drum 6;

[0029] The stirring device includes a stirring motor 2, a stirring shaft 201, alternating blades 202, and a support rod 203. The stirring motor 2 is mounted on the top of the frame 1. The stirring shaft 201 is connected to the output end of the stirring motor 2. The support rod 203 is fixedly connected to the outer surface of the stirring shaft 201. The alternating blades 202 are fixedly connected to the top of the support rod 203.

[0030] The cleaning device includes a valve 3, a cleaning straight pipe 301, a nozzle 302, a diamond-shaped pipe 303, a large gear 304, a small gear 305, and a rotating shaft 306. The large gear 304 is sleeved on the outer surface of the stirring shaft 201. Four through holes are opened on the top of the diamond-shaped pipe 303. The rotating shaft 306 passes through the through holes. The nozzle 302 is fixedly connected to the bottom of the rotating shaft 306. The small gear 305 is sleeved on the outer surface of the rotating shaft 306 and contacts the large gear 304. The diamond-shaped pipe 303 is fixedly installed above the stirring drum 6. The cleaning straight pipe 301 is fixedly connected to the right side of the diamond-shaped pipe 303. The valve 3 is fixedly connected between the two cleaning straight pipes 301.

[0031] In this embodiment, by starting the stirring motor 2, the stirring shaft 201 is driven, and the support rod 203 rotates with the stirring shaft 201, thereby causing the alternating blades 202 to rotate around the stirring shaft 201 to achieve the purpose of stirring. The cleaning straight pipe 301 is connected to the container containing the cleaning liquid, and the valve 3 is opened. The cleaning liquid will be sprayed out from the nozzle 302 through the cleaning straight pipe 301 and the diamond-shaped pipe 303. The stirring motor 2 is turned on to drive the large gear 304 to rotate, thereby driving the small gear 405 to rotate, causing the rotating shaft 306 to rotate, thereby causing the nozzle 302 to rotate, so as to achieve the purpose of all-round spraying cleaning.

[0032] Example 2: Based on Example 1, a conveying device is provided on the right side of the stirring cylinder 6;

[0033] The conveying device includes a water pump 4, a conveying pipe 401, a base 402, a raw material barrel 403, and a sealing ring 404. The base 402 is fixedly connected to the upper right side of the frame 1. The water pump 4 is installed above the base 402. The conveying pipe 401 is fixedly connected to the left and right sides of the water pump 4. A through hole is opened on the right side of the mixing drum 6, and the through hole is fixedly connected to the left end of the conveying pipe 401. The right end of the conveying pipe 401 is threaded. The sealing ring 404 is sleeved on the right end of the conveying pipe 401. A connecting pipe is opened on the left side of the raw material barrel 403. The material thickness of the raw material barrel 403 is selected as 2mm. The right end of the conveying pipe 401 is connected to the connecting pipe by thread.

[0034] In this embodiment, since most chemical raw materials are corrosive or polluting, the raw material liquid is directly pumped into the mixing drum 6 by the water pump 4 to prevent raw material leakage and avoid direct contact with personnel, thereby reducing the occurrence of accidents and pollution.

[0035] Example 3: Based on Example 1 and Example 2, a threaded hole is provided on the front side of the stirring cylinder 6, and a monitoring instrument 5 is fixedly installed on the front side of the stirring cylinder 6 through the threaded hole.

[0036] In this embodiment, the installation of the monitoring instrument 5 allows the operator to understand the status and parameters of the material in the mixing drum 6 in real time, such as temperature, pressure, and liquid level, providing an important basis for the control and adjustment of the production process.

[0037] Working principle: By starting the stirring motor 2, the stirring shaft 201 is driven, and the support rod 203 rotates with the stirring shaft 201, thereby causing the alternating blades 202 to rotate around the stirring shaft 201 to achieve the purpose of stirring.

[0038] Connect the cleaning straight pipe 301 to the container containing the cleaning liquid, open the valve 3, and the cleaning liquid will be sprayed out from the nozzle 302 through the cleaning straight pipe 301 and the diamond-shaped pipe 303. Turn on the stirring motor 2 to drive the large gear 304 to rotate, which in turn drives the small gear 405 to rotate, causing the rotating shaft 306 to rotate, thereby causing the nozzle 302 to rotate, achieving the purpose of all-round spraying cleaning.

[0039] By directly drawing the raw material liquid into the mixing drum 6 through the water pump 4 along the conveying pipe 401, leakage of raw material can be prevented, and direct contact with personnel can be avoided, reducing the occurrence of accidents and pollution.

[0040] The installation of the monitoring instrument 5 allows operators to monitor the status and parameters of the material inside the mixing drum 6 in real time (such as temperature, pressure, liquid level, etc.), providing an important basis for the control and adjustment of the production process.

[0041] It should be noted that, in this document, relational terms such as "first" and "second" are used only to distinguish one entity or operation from another, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Furthermore, the terms "comprising," "including," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to such a process, method, article, or apparatus. Without further limitations, an element defined by the phrase "comprising one..." does not exclude the presence of other identical elements in the process, method, article, or apparatus that includes said element.

Claims

1. An agitated reaction apparatus for the production of electronic grade chemicals comprising a frame (1) and an agitated vessel (6), characterized in that: The stirring cylinder (6) is fixedly installed inside the rack (1), the inside of the stirring cylinder (6) is provided with a stirring device, and the upper portion of the stirring cylinder (6) is provided with a cleaning device; The stirring device comprises a stirring motor (2), a stirring shaft (201), an alternating blade (202) and a support rod (203), the stirring motor (2) is installed above the rack (1), the stirring shaft (201) is connected to the output end of the stirring motor (2), the support rod (203) is fixedly connected to the outer surface of the stirring shaft (201), and the alternating blade (202) is fixedly connected above the support rod (203); The cleaning device comprises a valve (3), a cleaning straight pipe (301), a nozzle (302), a rhombic pipe (303), a large gear (304), a small gear (305) and a rotating shaft (306), the large gear (304) is sleeved on the outer surface of the stirring shaft (201), four through holes are formed in the upper portion of the rhombic pipe (303), the rotating shaft (306) penetrates through the through holes, the nozzle (302) is fixedly connected to the bottom of the rotating shaft (306), the small gear (305) is sleeved on the outer surface of the rotating shaft (306) and is in contact with the large gear (304), the rhombic pipe (303) is fixedly installed above the stirring cylinder (6), the cleaning straight pipe (301) is fixedly connected to the right side of the rhombic pipe (303), and the valve (3) is fixedly connected between the two cleaning straight pipes (301).

2. An electronic grade chemical preparation stirring reaction device according to claim 1, characterized in that: Threaded holes are formed in the upper portion of the rack (1), and the stirring motor (2) is boltedly and threadedly connected with the rack (1) through the threaded holes.

3. An electronic grade chemical preparation stirring reaction device according to claim 1, characterized in that: The bottom of the stirring cylinder (6) is in a conical shape, a discharge port (603) is formed in the bottom of the stirring cylinder (6), a sealing ring two (601) is sleeved on the discharge port (603), threads are arranged on the outer surface of the discharge port (603), and a sealing cover (602) is threadedly connected to the outer surface of the discharge port (603).

4. An electronic grade chemical preparation stirring reaction device according to claim 1, characterized in that: A conveying device is arranged on the right side of the stirring cylinder (6); The conveying device comprises a water pump (4), a conveying pipe (401), a base (402), a raw material barrel (403) and a sealing ring one (404), the base (402) is fixedly connected to the upper right side of the rack (1), the water pump (4) is installed above the base (402), the conveying pipe (401) is fixedly connected to the left and right sides of the water pump (4) respectively, a through hole is formed in the right side of the stirring cylinder (6), the through hole is fixedly connected to the left end of the conveying pipe (401), threads are arranged on the right end of the conveying pipe (401), the sealing ring one (404) is sleeved on the right end of the conveying pipe (401), and a connecting pipe is formed in the left side of the raw material barrel (403).

5. An electronic grade chemical preparation stirring reaction device according to claim 4, characterized in that: The right end of the conveying pipe (401) is threadedly connected to the connecting pipe.

6. An electronic grade chemical preparation stirring reaction device according to claim 4, characterized in that: The material thickness of the raw material barrel (403) is 2 mm.

7. An electronic grade chemical preparation stirring reaction device according to claim 1, characterized in that: The front face of the stirring cylinder (6) is provided with a threaded hole, and the front face of the stirring cylinder (6) is fixedly installed with a monitor (5) through the threaded hole.

Images