Turnover type high-temperature uniform reaction device

Abstract

The utility model belongs to the technical field of catalytic equipment, and particularly relates to a turnover type high-temperature uniform reaction device which comprises a muffle furnace, a mounting plate is arranged on the side wall of the muffle furnace, a motor is fixedly arranged on the mounting plate, an output shaft of the motor is fixedly connected with one rotating shaft of a turnover assembly, and the other rotating shaft of the turnover assembly is fixedly connected with the other rotating shaft of the turnover assembly. The overturning assembly is installed in the muffle furnace, a reaction tank is fixedly installed on the overturning assembly, the overturning assembly is used for driving the reaction tank to rotate, and the reaction tank is used for containing reactants. The reaction tank can be overturned through the overturning assembly, so that reactants are continuously overturned in the muffle furnace, uniform heating of the reactants is guaranteed, the reaction efficiency is improved, meanwhile, the raising plate is arranged in the reaction tank, sufficient and uniform heating of the reactants can be further guaranteed, and the reaction efficiency is further improved.

Description

TECHNICAL FIELD

[0001] The utility model belongs to catalytic equipment technical field, concretely relates to a high temperature even reaction device. BACKGROUND

[0002] High temperature even reaction is the core process link of realizing material synthesis, catalyst preparation and energy conversion in chemical industry, metallurgy and new energy field. In prior art, this kind of reaction usually adopts static heating scheme: after the reaction kettle is sealed, it is directly placed in the heating equipment such as muffle furnace, and temperature rise is realized by heat radiation and natural convection. However, this scheme has the following technical defects:

[0003] 1. Uneven heat field distribution

[0004] Under the static heating mode, significant axial and radial temperature gradient is formed in the reaction kettle:

[0005] · The local temperature of the region near the heating source is over threshold value due to concentrated heat radiation (the highest temperature difference is up to ± 50 DEG C measured by experiment);

[0006] · The cold zone is formed in the reaction material accumulation area due to blocked heat conduction, leading to inconsistent reaction kinetics (such as abnormal grain growth, active component distribution deviation).

[0007] Such unevenness directly affects the product performance and increases the risk of side reaction.

[0008] 2. Low mass transfer efficiency

[0009] Under the static state, the reaction material only relies on natural diffusion or limited convection to realize mixing, and the following problems exist:

[0010] · Particle agglomeration and sedimentation: high-density or large-particle material is easy to accumulate on the bottom of the kettle, leading to more than 50% reduction of effective contact area;

[0011] · Low energy utilization rate: energy is wasted significantly in the local overheated area (30%-40% of the total energy consumption of the system), and the cold area needs to extend the heating time for compensation.

[0012] Experimental data show that the reaction time of static heating under the same condition is about 2-3 times of that of dynamic heating mode.

[0013] 3. Limited equipment applicability

[0014] The prior art scheme has the following structural contradictions:

[0015] · Poor material form adaptability: easy to cause bridging and wall sticking for non-uniform materials such as slurry and powder;

[0016] · Scale bottleneck: large reaction tanks are difficult to efficiently invert due to their weight and inertia, while small tanks cannot meet the needs of industrial continuous production.

[0017] The above defects result in that the prior art is difficult to meet the needs of high-end manufacturing in terms of reaction controllability (such as temperature uniformity within ±10℃), production efficiency (output per unit time), and product consistency (batch difference CV value ≥15%). Utility model content

[0018] The utility model provides a high temperature even reaction device for above -mentioned problem.

[0019] In order to achieve the above object, the utility model adopts the following technical scheme:

[0020] A kind of high temperature even reaction device, including muffle furnace, installation plate is arranged on the side wall of the muffle furnace, motor is fixedly arranged on the installation plate, the output shaft of the motor is fixedly connected with one of the rotating shafts of overturning assembly, the overturning assembly is installed in muffle furnace, reaction tank is fixedly installed on the overturning assembly, the overturning assembly is used to drive reaction tank to rotate, and the reaction tank is used to place reactant.

[0021] Further, the overturning assembly includes a base, two support seats are fixedly connected on the left and right sides of the base by bolts, rotating shafts are rotatably installed on the support seats, rotating discs are fixedly connected to the inner sides of the rotating shafts, at least two connecting rods are uniformly arranged in a ring shape between the two rotating discs, clamping mechanisms are arranged on the connecting rods, and the clamping mechanisms are used to clamp the reaction tank.

[0022] Still further, screw rods are fixedly arranged at both ends of the connecting rods, and the screw rods pass through corresponding locking nuts on the rotating discs and are connected thereto by threads.

[0023] Still further, the clamping mechanism includes two clamping discs mounted on the connecting rods, a plurality of wedge-shaped blocks are uniformly mounted in a ring shape on the inner sides of the clamping discs, and the clamping of the reaction tank is realized by the cooperation of the wedge-shaped blocks on both sides.

[0024] Still further, the clamping discs are slidably mounted on the connecting rods, locking bolts are threadedly connected to the clamping discs, and the clamping discs and the connecting rods are fixed by the locking bolts.

[0025] Still further, the wedge-shaped blocks are fixedly connected to the clamping discs by fixing bolts.

[0026] Still further, the reaction tank includes a tank body and an end cover, the tank body and the end cover are sealingly connected, a plurality of lifting plates are uniformly arranged in the tank body to facilitate the sufficient heating and mixing of the reactant and prevent the accumulation of the reactant in the lower part of the reaction tank.

[0027] Further, a speed regulator is arranged on the mounting plate, and the speed regulator is electrically connected with the motor, so as to adjust the rotating speed of the motor.

[0028] Compared with the prior art, the utility model has the following advantages:

[0029] The utility model discloses a turnover assembly can realize the turnover of the reaction tank, and the reaction material is constantly turned over in the muffle furnace, guarantees the heating of reaction material even, improves reaction efficiency, and the application sets up the material lifting plate in the reaction tank, can further guarantee the sufficient even heating of reaction material, and further improves reaction efficiency.

[0030] The utility model discloses a wedge block on left and right sides realizes the fixing to the tank body, can adapt to different specifications tank body, and the adaptability is wider. ACCURACY OF DRAWINGS

[0031] Fig. 1 It is the structure schematic diagram of the utility model;

[0032] Fig. 2 It is the structure schematic diagram of the utility model turnover assembly;

[0033] Fig. 3 It is the structure schematic diagram of the utility model reaction tank;

[0034] In the drawing, muffle furnace 1, mounting plate 2, motor 3, turnover assembly 4, reaction tank 5, speed regulator 6, base 401, support seat 402, pivot 403, turntable 404, connecting rod 405, screw 406, locking nut 407, clamping disc 408, wedge block 409, locking bolt 410, fixed bolt 411, tank body 501, end cover 502, material lifting plate 503. DETAILED DESCRIPTION

[0035] In order to further illustrate the technical scheme of the utility model, the utility model is further illustrated below through examples.

[0036] As Figs. 1 to 3 The utility model discloses a high temperature even reaction device, including muffle furnace 1, be provided with mounting plate 2 on the lateral wall of muffle furnace 1, be fixed with motor 3 on mounting plate 2, the output shaft of motor 3 is fixedly connected with one of the pivot 403 of turnover assembly 4, turnover assembly 4 installs in muffle furnace 1, be fixedly installed with reaction tank 5 on turnover assembly 4, turnover assembly 4 is used to drive reaction tank 5 to rotate, reaction tank 5 is used to place reaction material, still be provided with speed regulator 6 on mounting plate 2, the speed regulator 6 is electrically connected with motor 3, so as to adjust the rotating speed of motor 3.

[0037] The turnover assembly 4 comprises a base 401, two support seats 402 are fixedly connected on the left and right sides of the base 401 through bolts, a rotating shaft 403 is rotatably installed on the support seat 402, a rotating disc 404 is fixedly connected on the inner side of the rotating shaft 403, at least two connecting rods 405 are uniformly arranged in a ring shape between the two rotating discs 404, screw rods 406 are fixedly arranged on both ends of the connecting rod 405, the screw rods 406 pass through the corresponding locking nuts 407 on the rotating disc 404 through threaded connection, a clamping mechanism is arranged on the connecting rod 405, and the clamping mechanism is used for clamping the reaction tank 5.

[0038] The clamping mechanism comprises two clamping discs 408 which are slidingly installed on the connecting rod 405, locking bolts 410 are threadedly connected on the clamping disc 408, the clamping disc 408 and the connecting rod 405 are fixed through the locking bolts 410, a plurality of wedge blocks 409 are uniformly installed in a ring shape on the inner side of the clamping disc 408, the reaction tank 5 is clamped through the cooperation of the wedge blocks 409 on both sides, and the wedge blocks 409 are fixedly connected with the clamping disc 408 through fixing bolts 411.

[0039] The reaction tank 5 comprises a tank body 501 and an end cover 502, the tank body 501 and the end cover 502 are sealingly connected, a plurality of material lifting plates 503 are uniformly arranged in the tank body 501, so that the reaction material can be fully heated and uniformly mixed, and the reaction material is prevented from accumulating in the lower part of the reaction tank 5.

[0040] The material of the reaction tank 5 is any one of stainless steel, quartz, graphite and ceramic.

[0041] The main features and advantages of the utility model are shown and described above, and it is obvious for those skilled in the art that the utility model is not limited to the details of the above-mentioned exemplary embodiments, and the utility model can be realized in other specific forms without departing from the spirit or basic features of the utility model. Therefore, no matter from which point of view, the embodiments should be regarded as exemplary and non-limiting, and the scope of the utility model is defined by the appended claims instead of the above description, and therefore all changes falling within the meaning and scope of the equivalent elements of the claims should be included in the utility model.

[0042] In addition, it should be understood that, although the present specification is described in terms of embodiments, not every embodiment contains only one independent technical solution, and the description manner of the specification is only for the sake of clarity, and those skilled in the art should regard the specification as a whole, and the technical solutions in each embodiment can be properly combined to form other embodiments that can be understood by those skilled in the art.

Claims

1. A flip high temperature uniform reaction device, characterized in that: The utility model provides a kind of reaction tank rotating device, including muffle (1), mounting plate (2) is provided on the side wall of the muffle (1), motor (3) is fixedly provided on the mounting plate (2), the output shaft of the motor (3) is fixedly connected with one of the rotating shaft (403) of turnover assembly (4), the turnover assembly (4) is installed in muffle (1), reaction tank (5) is fixedly installed on the turnover assembly (4), the turnover assembly (4) is used to drive reaction tank (5) to rotate, and the reaction tank (5) is used to place reactant.

2. The inverted high temperature uniform reaction device of claim 1, wherein: The turnover assembly (4) includes base (401), two support seats (402) are fixedly connected on the left and right sides of the base (401) by bolt, rotating shaft (403) is rotatably installed on the support seat (402), rotating disc (404) is fixedly connected on the inner side of the rotating shaft (403), at least two connecting rods (405) are uniformly provided in ring shape between two rotating discs (404), clamping mechanism is provided on the connecting rod (405), and the clamping mechanism is used to clamp reaction tank (5).

3. The inverted high temperature uniform reaction device of claim 2, wherein: Screw rod (406) is fixedly provided at both ends of the connecting rod (405), the screw rod (406) passes through corresponding locking nut (407) connected by thread on rotating disc (404).

4. The inverted high temperature uniform reaction device of claim 2, wherein: The clamping mechanism includes two clamping discs (408) mounted on the connecting rod (405), a plurality of wedge blocks (409) are uniformly mounted in ring shape on the inner side of the clamping disc (408), and the clamping of reaction tank (5) is realized by the cooperation of wedge blocks (409) on both sides.

5. The inverted high temperature uniform reaction device of claim 4, wherein: The clamping disc (408) is slidably installed on the connecting rod (405), locking bolt (410) is threadedly connected on the clamping disc (408), and the fixation of clamping disc (408) and connecting rod (405) is realized by the locking bolt (410).

6. The inverted high temperature uniform reaction device of claim 4, wherein: The wedge block (409) is fixedly connected with the clamping disc (408) by fixing bolt (411).

7. The inverted high temperature uniform reaction device of claim 1, wherein: The reaction tank (5) includes tank body (501) and end cover (502), the tank body (501) is sealingly connected with the end cover (502), a plurality of material lifting plates (503) are uniformly provided in the tank body (501), so as to realize the full heating and mixing of reactant, and prevent the accumulation of reactant in the lower part of reaction tank (5).

8. The inverted high temperature uniform reaction device of claim 1, wherein: Speed regulator (6) is further provided on the mounting plate (2), and the speed regulator (6) is electrically connected with the motor (3) to adjust the rotating speed of the motor (3).

Images