Synthesis production system of p-toluene sulfonamide sodium chloride salt

Abstract

The utility model belongs to the technical field of chemical production equipment, and particularly relates to a synthetic production system of p-toluene sulfonamide sodium chloride salt, which comprises a tank body, a filter cover and a flushing pipe, the filter cover is arranged in a cavity inside the tank body, an inner cylinder is integrally arranged in the middle of the filter cover, and filter holes are uniformly distributed on the inner cylinder. A feeding pipe is arranged on a top cover at the upper part of the tank body, a liquid outlet pipe is arranged at the bottom of the tank body, a flushing pipe is arranged on the top cover, a branch pipe communicated with the flushing pipe extends into an inner cavity of the filtering cover, and a water outlet hole is formed in the branch pipe. According to the utility model, the flushing pipeline is additionally arranged on the filtering equipment, solid impurities intercepted after filtering are flushed, and residual raw materials in the solid impurities are separated out and are re-injected into the solvent kettle for reuse, so that the loss of the raw materials is reduced, and the utilization rate of the raw materials and the production efficiency are improved.

Description

Technical Field

[0001] This utility model relates to the field of chemical production equipment technology, specifically to a synthesis production system for p-toluenesulfonamide sodium chloride. Background Technology

[0002] p-Toluenesulfonamide sodium chloride (chloramine T) is a white crystalline powder with a slight chlorine odor. It is not bitter and slowly decomposes when exposed to air, with only a 0.1% decrease in available chlorine per year. It gradually loses chlorine and turns yellow. As a disinfectant, this product is a broad-spectrum disinfectant for external use, containing 24-25% available chlorine. It is relatively stable and has a killing effect on bacteria, viruses, fungi, and spores.

[0003] A search revealed a production system for p-toluenesulfonamide sodium chloride salt in Chinese patent application number 201520989351.X. This system mainly includes a dissolving kettle, a first filter, a salt-forming reactor, a second filter, and a centrifugal dehydrator. The inlet of the dissolving kettle is connected to a liquid alkali storage tank and a p-toluenesulfonamide storage tank. The outlet of the dissolving kettle is connected to the inlet of the first filter. The liquid phase outlet of the first filter is connected to the inlet of the salt-forming reactor. The salt-forming reactor also has a sodium hypochlorite storage tank. The outlet of the salt-forming reactor is connected to the inlet of the second filter. The solid phase outlet of the second filter is connected to the inlet of the centrifugal dehydrator. The centrifugal dehydrator has a wastewater outlet and a product outlet. This p-toluenesulfonamide sodium chloride salt production system offers advantages such as low production cost, high production efficiency, high product purity, and minimal environmental pollution.

[0004] In the above technical solution, after the raw materials are dissolved, they are filtered by a filter to remove solid impurities. However, the solid impurities trapped in the filter will still leave raw materials, resulting in raw material loss and low production efficiency. Utility Model Content

[0005] (a) Technical problems to be solved

[0006] To address the shortcomings of existing technologies, this invention provides a synthesis and production system for p-toluenesulfonamide sodium chloride, which solves the problem that raw materials remain in the solid impurities trapped in the filter, leading to raw material loss and low production efficiency.

[0007] (II) Technical Solution

[0008] To achieve the above objectives, this utility model specifically adopts the following technical solution:

[0009] A synthesis production system for p-toluenesulfonamide sodium chloride includes a tank, a filter cover, and a rinsing pipe. The filter cover is installed in the cavity inside the tank. An inner cylinder is integrally formed in the middle of the filter cover. The inner cylinder has uniformly distributed filter holes. A feed pipe is installed on the top cover of the tank. A liquid outlet pipe is installed at the bottom of the tank. A rinsing pipe is installed on the top cover. A branch pipe connected to the rinsing pipe extends into the internal cavity of the filter cover. A water outlet hole is opened on the branch pipe.

[0010] Furthermore, a return pipe is connected to the liquid outlet pipe at the bottom of the tank. Both the liquid outlet pipe and the return pipe are equipped with quick-connect plugs at their ends. The feed pipe is installed through the top cover. The feed pipe is integrally provided with a connecting end plate at its end, and an anti-clogging cone is installed in the feed pipe.

[0011] The anti-clogging cone is fixedly connected to the feed pipe by a connecting rod. The lower end of the anti-clogging cone extends to the outside of the feed pipe and is fixedly connected to the diverter shroud. The diverter shroud abuts against the upper part of the inner cylinder, and the lower edge of the diverter shroud extends to the periphery of the inner cylinder.

[0012] Furthermore, a lifting lug is fixedly connected to the upper port of the filter cover.

[0013] Furthermore, the flushing pipe is fixedly connected to the top cover by a connecting buckle, and the water inlet pipe connected to the flushing pipe extends through the top cover to the outside of the tank. The end of the water inlet pipe is equipped with a quick-connect connector, and the branch pipes are distributed in a ring array on the flushing pipe, with evenly distributed water outlet holes on the branch pipes.

[0014] (III) Beneficial Effects

[0015] Compared with the prior art, this utility model provides a synthesis and production system for p-toluenesulfonamide sodium chloride, which has the following beneficial effects:

[0016] This invention adds a rinsing pipe to the filtration equipment to rinse the solid impurities trapped after filtration, separate the raw materials remaining in the solid impurities, and then inject them back into the solvent tank for reuse, thereby reducing the loss of raw materials and improving the utilization rate of raw materials and production efficiency. Attached Figure Description

[0017] Figure 1 This is a schematic diagram of the structure of this utility model;

[0018] Figure 2 This is a cross-sectional view of the present invention;

[0019] Figure 3 This is a cross-sectional view of the tank body in this utility model;

[0020] Figure 4 This is a cross-sectional view of the filter cover in this utility model;

[0021] Figure 5 This is a schematic diagram of the flushing pipe in this utility model.

[0022] In the diagram: 1. Tank body; 101. Discharge pipe; 102. Top cover; 103. Feed pipe; 104. Anti-clogging cone; 105. Connecting rod; 106. Diverter hood; 107. Return pipe; 2. Filter cover; 201. Inner cylinder; 202. Filter holes; 203. Lifting lug; 3. Flushing pipe; 301. Branch pipe; 302. Water inlet pipe; 303. Connecting buckle; 304. Water outlet. Detailed Implementation

[0023] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0024] Example

[0025] like Figure 1 , Figure 2 , Figure 3 , Figure 4 and Figure 5 As shown in one embodiment of this utility model, a synthesis production system for p-toluenesulfonamide sodium chloride includes a tank 1, a filter hood 2, and a flushing pipe 3. The filter hood 2 is installed in the cavity inside the tank 1. An inner cylinder 201 is integrally formed in the middle of the filter hood 2. The inner cylinder 201 has uniformly distributed filter holes 202. The filter hood 2 filters the material entering the tank 1, thereby separating solid impurities from the material. The liquid material flows through the filter holes 202 on the inner cylinder 201 into the tank 1, and is then discharged from the outlet pipe 101 and transported to the next process equipment for subsequent preparation operations. The tank body 1 has a top cover 102 with a feed pipe 103, which facilitates the injection of the reacted raw materials from the dissolving kettle into the tank body 1 for processing. The bottom of the tank body 1 is equipped with a liquid outlet pipe 101 to ensure the smooth discharge of the processed raw materials. The top cover 102 is equipped with a rinsing pipe 3, and the branch pipes 301 connected to the rinsing pipe 3 extend into the internal cavity of the filter cover 2. The branch pipes 301 are provided with water outlet holes 304. Water is evenly distributed to each branch pipe 301 through the rinsing pipe 3 and discharged to rinse the impurities trapped in the filter cover 2, separate the raw materials remaining in the impurities, reduce the loss of raw materials, and improve production efficiency.

[0026] like Figure 2 and Figure 3As shown, in some embodiments, a return pipe 107 is connected to the liquid outlet pipe 101 at the bottom of the tank 1, which facilitates the smooth discharge of the rinsing liquid in the tank 1. With the valve on the return pipe 107 and the external pipe, the rinsing liquid is injected back into the dissolving kettle, improving the utilization rate of raw materials. The ends of the liquid outlet pipe 101 and the return pipe 107 are equipped with quick-connect plugs, which facilitates the quick connection of external pipes and improves the convenience of use. The feed pipe 103 is installed through the top cover 102. The end of the feed pipe 103 is integrally provided with a connecting end plate, which facilitates a stable connection with the outlet of the dissolving kettle, thereby injecting the product after reaction in the dissolving kettle into the tank 1 for filtration. In addition, an anti-clogging cone 104 is installed in the feed pipe 103 to prevent the feed pipe 103 from being blocked during the feeding process and ensure smooth use.

[0027] The anti-clogging cone 104 is fixedly connected to the feed pipe 103 by the connecting rod 105, which facilitates the stable installation of the anti-clogging cone 104 in the feed pipe 103 and ensures stable use. The lower end of the anti-clogging cone 104 extends to the outside of the feed pipe 103 and is fixedly connected to the diversion hood 106, which facilitates the stable installation of the diversion hood 106 directly below the feed pipe 103. The diversion hood 106 abuts against the upper part of the inner cylinder 201, and the lower edge of the diversion hood 106 extends to the periphery of the inner cylinder 201. The diversion hood 106 is used to divert the material injected into the tank 1 from the feed pipe 103, so that it can be evenly distributed in the filter cover 2, thereby improving the subsequent filtration efficiency.

[0028] like Figure 2 and Figure 4 As shown, in some embodiments, the upper port of the filter cover 2 is fixedly connected with a lifting lug 203, which facilitates the lifting of the entire filter cover 2 during the assembly and disassembly process, so that the filter cover 2 can be smoothly placed into the tank 1 or removed from the tank 1, thereby cleaning the impurities in the filter cover 2 and improving the convenience of use.

[0029] like Figure 2 and Figure 5 As shown, in some embodiments, the flushing pipe 3 is fixedly connected to the top cover 102 by a connecting buckle 303, which facilitates the stable installation of the flushing pipe 3 on the top cover 102 and ensures stable use. The water inlet pipe 302 connected to the flushing pipe 3 passes through the top cover 102 and extends to the outside of the tank 1. The end of the water inlet pipe 302 is equipped with a quick-connect connector, which facilitates the quick connection of the external flushing water supply pipe to the water inlet pipe 302, so that the two are stably connected together, thereby inputting flushing water into the flushing pipe 3 to flush the impurities accumulated in the filter cover 2, and then flushing down the raw materials remaining in the impurities, improving the utilization rate of raw materials and reducing losses. The branch pipes 301 are distributed in a ring array on the flushing pipe 3, and the branch pipes 301 are provided with evenly distributed water outlet holes 304 to facilitate the discharge of water, thereby completing the flushing of impurities.

[0030] In use, the tank body 1 and all external auxiliary pipes are stably connected. Then, the raw materials reacted in the dissolving vessel are injected into the tank body 1. The filter hood 2 inside the tank body 1 filters the raw materials, trapping solid impurities. The liquid is discharged from the outlet pipe 101 and input into the next process equipment for further processing. Then, the rinsing water is injected from the inlet pipe 302 into the rinsing pipe 3 and distributed to each branch pipe 301. The water is discharged from the outlet hole 304 on the branch pipe 301 to rinse the solid impurities trapped in the filter hood 2. The rinsed water is discharged from the return pipe 107 on the outlet pipe 101 and injected into the dissolving vessel through the connected conveying pipe, so that the raw materials remaining in the solid impurities can be reused.

[0031] Finally, it should be noted that the above description is merely a preferred embodiment of this utility model and is not intended to limit the utility model. Although the utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of this utility model should be included within the protection scope of this utility model.

Claims

1. A synthesis production system for p-toluenesulfonamide sodium chloride, comprising a tank (1), a filter hood (2), and a flushing pipe (3), characterized in that: The filter cover (2) is installed in the cavity inside the tank (1). The filter cover (2) has an inner cylinder (201) integrally installed in the middle part. The inner cylinder (201) has evenly distributed filter holes (202). The top cover (102) at the top of the tank (1) is equipped with a feed pipe (103). The bottom of the tank (1) is equipped with a liquid outlet pipe (101). The top cover (102) is equipped with a flushing pipe (3). The branch pipe (301) connected to the flushing pipe (3) extends into the cavity inside the filter cover (2). The branch pipe (301) has a water outlet hole (304).

2. The synthesis and production system for p-toluenesulfonamide sodium chloride according to claim 1, characterized in that: The liquid outlet pipe (101) at the bottom of the tank (1) is connected to a return pipe (107). Both the liquid outlet pipe (101) and the return pipe (107) are equipped with quick-connect plugs. The feed pipe (103) is installed through the top cover (102). The feed pipe (103) is integrally provided with a connecting end plate at its end. An anti-blocking cone (104) is installed in the feed pipe (103).

3. The synthesis and production system for p-toluenesulfonamide sodium chloride according to claim 2, characterized in that: The anti-blocking cone (104) is fixedly connected to the feed pipe (103) by the connecting rod (105). The lower end of the anti-blocking cone (104) extends to the outside of the feed pipe (103) and is fixedly connected to the diverter hood (106). The diverter hood (106) abuts against the upper part of the inner cylinder (201), and the lower edge of the diverter hood (106) extends to the periphery of the inner cylinder (201).

4. The synthesis and production system for p-toluenesulfonamide sodium chloride according to claim 1, characterized in that: The filter cover (2) is fixedly connected to a lifting lug (203) at its upper port.

5. The synthesis and production system for p-toluenesulfonamide sodium chloride according to claim 1, characterized in that: The flushing pipe (3) is fixedly connected to the top cover (102) by a connecting buckle (303). The water inlet pipe (302) connected to the flushing pipe (3) passes through the top cover (102) and extends to the outside of the tank (1). A quick-connect fitting is installed at the end of the water inlet pipe (302), and the branch pipes (301) are arranged in a ring array on the flushing pipe (3). The branch pipes (301) are provided with evenly distributed water outlet holes (304).

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