Chlorination kettle for producing phosphorus trichloride

By adding a protective shell, stirring components, and a gas purifier to the chlorination reactor, the problems of uneven raw material mixing, poor safety, and difficult cleaning were solved, resulting in more efficient phosphorus trichloride production and a safer operating environment.

CN223969979UActive Publication Date: 2026-03-06XUZHOU YONGLI FINE CHEM ENG CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-04-03
Publication Date
2026-03-06

AI Technical Summary

Technical Problem

Existing chlorination reactors suffer from uneven raw material mixing, poor safety, difficult cleaning, and unpurified gas emissions, resulting in low production efficiency, unstable product quality, and high environmental pollution and health risks.

Method used

A chlorination reactor with a protective shell, stirring components, gas purifier, and scraper was designed. Through bidirectional three-dimensional stirring, gas purification, and inner wall cleaning, the mixing uniformity, safety, and cleanliness are improved.

Benefits of technology

It achieves more efficient raw material mixing, a safer operating environment, a cleaner inner wall of the reactor, and more environmentally friendly gas treatment, thereby improving production efficiency and product quality and reducing safety risks.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a chlorination kettle for producing phosphorus trichloride, which comprises support legs, a kettle body, a kettle cover and a stirring component, and further comprises a protective shell, the protective shell is sleeved outside the kettle body, a plurality of groups of springs and connecting support columns are fixedly connected between interlayers of the kettle body and the protective shell, the support legs are arranged on the protective shell, and the stirring component is arranged on the support legs. The kettle cover is detachably arranged on the kettle body, and the stirring assembly is arranged on the kettle cover; the stirring assembly comprises a driving shaft, a sleeve shaft, a stirring rod and a stirring blade, the sleeve shaft is rotatably arranged on the kettle cover and extends downwards into the kettle body, the stirring rod is arranged on the sleeve shaft, a mounting seat is arranged on the kettle cover, and the driving shaft is rotatably arranged on the mounting seat and rotatably penetrates through the sleeve shaft. The utility model relates to the technical field of phosphorus trichloride processing auxiliary devices, and particularly provides a chlorination kettle for producing phosphorus trichloride, which is better in stirring effect, higher in safety and convenient to clean and has a gas purification function.
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Description

Technical Field

[0001] This utility model relates to the technical field of auxiliary devices for phosphorus trichloride processing, specifically a chlorination reactor for producing phosphorus trichloride. Background Technology

[0002] Chlorination reactors are essential equipment for phosphorus trichloride production, but existing chlorination reactors have several shortcomings. In the raw material mixing stage, the design of the stirring device is inadequate, with a simple structure and a single stirring direction, resulting in insufficient and uneven mixing of raw materials within the reactor. This affects the reaction process, leading to low production efficiency and unstable product quality. Furthermore, most existing chlorination reactors are single-layered structures, resulting in poor safety performance. Additionally, cleaning and maintenance of existing chlorination reactors are difficult, and residual reactants inside the reactor are hard to remove. Long-term accumulation of these reactants affects the reactor's performance, shortens its lifespan, and increases production costs. Moreover, the gases produced during the reaction cannot be effectively discharged and purified, causing environmental pollution and posing health risks to workers. Utility Model Content

[0003] In view of the above situation and to overcome the defects of the prior art, this utility model provides a chlorination kettle for the production of phosphorus trichloride that has better stirring effect, higher safety, is easy to clean, and has gas purification function.

[0004] The technical solution adopted by this utility model is as follows: This utility model provides a chlorination reactor for producing phosphorus trichloride, including support legs, reactor body, reactor cover and stirring assembly, and also includes a protective shell. The protective shell is sleeved on the outside of the reactor body. Multiple sets of springs and connecting pillars are fixedly connected between the reactor body and the protective shell. The support legs are provided on the protective shell. The reactor cover is detachably provided on the reactor body. The stirring assembly is provided on the reactor cover.

[0005] Furthermore, the stirring assembly includes a drive shaft, a sleeve shaft, a stirring rod, and stirring blades. The sleeve shaft is rotatably mounted on the vessel lid and extends downward into the vessel body. The stirring rod is mounted on the sleeve shaft. The vessel lid is provided with a mounting seat. The drive shaft is rotatably mounted on the mounting seat and rotatably passes through the sleeve shaft. The stirring blades are mounted on the drive shaft. A first bevel gear is sleeved on the drive shaft. A second bevel gear is sleeved on the sleeve shaft. A third bevel gear is rotatably mounted on the mounting seat. Both the first and second bevel gears mesh with the third bevel gear.

[0006] Furthermore, it also includes a gas purifier, the gas purifier having an exhaust pipe connected to its air inlet, the exhaust pipe being located on the lid of the vessel and communicating with the interior of the vessel.

[0007] Furthermore, the stirring rod is equipped with a scraper, which contacts the inner wall of the vessel.

[0008] Furthermore, the vessel lid is provided with a feeding port, and the feeding port is detachably provided with a sealing cap.

[0009] Furthermore, a discharge pipe is provided at the bottom of the vessel body, the discharge pipe extends to the outside of the protective shell, and a solenoid valve is provided on the discharge pipe.

[0010] Furthermore, a motor is provided on the mounting base, and one end of the drive shaft is located on the output shaft of the motor.

[0011] Furthermore, the lid is detachably attached to the vessel body via a first bolt.

[0012] Furthermore, the sealing cap is detachably mounted on the feed port via a second bolt.

[0013] The beneficial effects of this utility model using the above structure are as follows: This solution provides a protective shell on the outside of the vessel body, and a spring and connecting support are installed between the vessel body and the protective shell, which can effectively enhance the anti-collision effect of the vessel body, reduce the risk of leakage of substances inside the vessel, and improve the safety of the vessel body in use; This solution includes a stirring assembly, which can perform bidirectional three-dimensional stirring of the substances inside the vessel, improving the stirring effect; This solution includes a gas purifier, which can purify the exhaust gas, avoiding harm to the environment and personnel; This solution includes a scraper, which can clean the inner wall of the vessel, reducing the residue of impurities inside the vessel. Attached Figure Description

[0014] The accompanying drawings are provided to further illustrate the present invention and form part of the specification. They are used together with the embodiments of the present invention to explain the present invention, but do not constitute a limitation thereof. In the drawings:

[0015] Figure 1 This is a perspective view of an embodiment of the present utility model;

[0016] Figure 2 This is an exploded view of an embodiment of the present utility model;

[0017] Figure 3 This is a front view of an embodiment of the present utility model;

[0018] Figure 4 This is a left view of an embodiment of the present utility model;

[0019] Figure 5 This is a top view of an embodiment of the present utility model;

[0020] Figure 6 for Figure 4 A sectional view along section AA;

[0021] Figure 7 for Figure 2Enlarged view of section A;

[0022] Figure 8 for Figure 6 Enlarged view of section B.

[0023] The components are as follows: 1. Support leg; 2. Vessel body; 3. Vessel cover; 4. Stirring assembly; 5. Protective shell; 6. Spring; 7. Connecting support column; 8. Mounting base; 9. Third bevel gear; 10. Drive shaft; 11. Sleeve shaft; 12. Stirring rod; 13. Stirring blade; 14. First bevel gear; 15. Second bevel gear; 16. Exhaust pipe; 17. Gas purifier; 18. Scraper; 19. Feed port; 20. Sealing cover; 21. Discharge pipe; 22. Solenoid valve; 23. Motor; 24. First bolt; 25. Second bolt. Detailed Implementation

[0024] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments of the present utility model. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. All other embodiments obtained by those skilled in the art based on the embodiments of the present utility model without creative effort are within the protection scope of the present utility model.

[0025] In the description of this utility model, it should be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings. They are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limitations on this utility model.

[0026] like Figures 1-8 As shown, this utility model discloses a chlorination reactor for producing phosphorus trichloride, comprising a support leg 1, a reactor body 2, a reactor lid 3, and a stirring assembly 4, and a protective shell 5. The protective shell 5 is fitted onto the outside of the reactor body 2. Multiple sets of springs 6 and connecting supports 7 are fixedly connected between the reactor body 2 and the protective shell 5. The support leg 1 is mounted on the protective shell 5. The reactor lid 3 is detachably mounted on the reactor body 2. The stirring assembly 4 is mounted on the reactor lid 3. The reactor lid 3 is detachably mounted on the reactor body 2 by a first bolt 24. The reactor lid 3 is provided with a feeding port 19, and a sealing cap 20 is detachably mounted on the feeding port 19. The sealing cap 20 is detachably mounted on the feeding port 19 by a second bolt 25. A discharge pipe 21 is provided at the bottom of the reactor body 2, extending to the outside of the protective shell 5. A solenoid valve 22 is provided on the discharge pipe 21.

[0027] The stirring assembly 4 includes a drive shaft 10, a sleeve shaft 11, a stirring rod 12, and a stirring blade 13. The sleeve shaft 11 is rotatably mounted on the vessel cover 3 and extends downward into the vessel body 2. The stirring rod 12 is mounted on the sleeve shaft 11. The vessel cover 3 is provided with a mounting seat 8. The drive shaft 10 is rotatably mounted on the mounting seat 8 and rotatably passes through the sleeve shaft 11. The stirring blade 13 is mounted on the drive shaft 10. A first bevel gear 14 is sleeved on the drive shaft 10. A second bevel gear 15 is sleeved on the sleeve shaft 11. A third bevel gear 9 is rotatably mounted on the mounting seat 8. Both the first bevel gear 14 and the second bevel gear 15 mesh with the third bevel gear 9. A motor 23 is provided on the mounting seat 8. One end of the drive shaft 10 is located on the output shaft of the motor 23.

[0028] It also includes a gas purifier 17, with an exhaust pipe 16 connected to the gas inlet of the gas purifier 17. The exhaust pipe 16 is located on the lid 3 and communicates with the interior of the vessel body 2.

[0029] The stirring rod 12 is equipped with a scraper 18, which contacts the inner wall of the vessel body 2.

[0030] In practical use, the raw materials are added into the vessel body 2 through the feeding port 19, then the sealing cover 20 is closed, and the motor 23 is started. The motor 23 drives the drive shaft 10 to rotate, which in turn drives the first bevel gear 14 to rotate. The first bevel gear 14 drives the third bevel gear 9 to rotate, which in turn drives the second bevel gear 15 to rotate. The second bevel gear 15 drives the sleeve shaft 11 to rotate, and the rotation direction of the sleeve shaft 11 is opposite to that of the drive shaft 10. The drive shaft 10 and the sleeve shaft 11 drive the stirring blade 13 and the stirring rod 12 to rotate in opposite directions, thereby mixing the raw materials more evenly and improving the reaction efficiency. During the rotation of the stirring rod 12, the scraper 18 will also rotate, and the scraper 18 can clean the impurities remaining on the inner wall of the vessel body 2.

[0031] During the reaction, the gas produced is discharged through exhaust pipe 16 and enters gas purifier 17 for purification. After the reaction is completed, the solenoid valve 22 is opened, and the material can be discharged through discharge pipe 21.

[0032] By setting a protective shell 5 on the outside of the vessel body 2, and setting a spring 6 and a connecting support 7 between the vessel body 2 and the protective shell 5, the anti-collision effect of the vessel body 2 can be effectively enhanced, the risk of material leakage inside the vessel body 2 can be reduced, and the safety of the vessel body 2 in use can be improved.

[0033] In summary, this design includes a protective shell 5 on the outside of the vessel body 2, and a spring 6 and a connecting support 7 between the vessel body 2 and the protective shell 5. This effectively enhances the anti-collision effect of the vessel body 2, reduces the risk of leakage of substances inside the vessel body 2, and improves the safety of the vessel body 2. This design also includes a stirring assembly 4, which can perform bidirectional three-dimensional stirring of the substances inside the vessel body 2, improving the stirring effect. Furthermore, this design includes a gas purifier 17, which can purify the exhaust gas to avoid harm to the environment and personnel. Finally, this design includes a scraper 18, which can clean the inner wall of the vessel body 2, reducing the residue of impurities inside the vessel body 2.

[0034] It should be noted that, in this document, relational terms such as "first" and "second" are used only to distinguish one entity or operation from another, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Furthermore, the terms "comprising," "including," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to such process, method, article, or apparatus.

[0035] The foregoing has shown and described the basic principles, main features, and advantages of this utility model. It will be apparent to those skilled in the art that this utility model is not limited to the details of the exemplary embodiments described above, and that it can be implemented in other specific forms without departing from the spirit or basic characteristics of this utility model. Therefore, the embodiments should be considered exemplary and non-limiting in all respects. The scope of this utility model is defined by the appended claims rather than the foregoing description, and thus all variations falling within the meaning and scope of equivalents of the claims are intended to be included within this utility model. No reference numerals in the claims should be construed as limiting the scope of the claims.

[0036] Furthermore, it should be understood that although this specification describes embodiments, not every embodiment contains only one independent technical solution. This narrative style is merely for clarity. Those skilled in the art should consider the specification as a whole, and the technical solutions in each embodiment can also be appropriately combined to form other embodiments that can be understood by those skilled in the art.

Claims

1. A chlorination kettle for producing phosphorus trichloride comprising a leg (1), a kettle body (2), a kettle cover (3) and an agitator assembly (4), characterized in that: Also include protective shell (5), the protective shell (5) is set on the kettle body (2) outside, the sandwich layer between the kettle body (2) and protective shell (5) is fixedly connected with multiple groups of spring (6) and connecting strut (7), the branch leg (1) is arranged on the protective shell (5), the kettle cover (3) is detachably arranged on the kettle body (2), and the stirring assembly (4) is arranged on the kettle cover (3).

2. The chlorination still for producing phosphorus trichloride according to claim 1, characterized by: The stirring assembly (4) includes a drive shaft (10), a sleeve shaft (11), a stirring rod (12) and a stirring blade (13), the sleeve shaft (11) is rotatably arranged on the kettle cover (3) and extends downward into the kettle body (2), the stirring rod (12) is arranged on the sleeve shaft (11), the kettle cover (3) is provided with a mounting seat (8), the drive shaft (10) is rotatably arranged on the mounting seat (8) and rotatably penetrates the sleeve shaft (11), the stirring blade (13) is arranged on the drive shaft (10), a first bevel gear (14) is sleeved on the drive shaft (10), a second bevel gear (15) is sleeved on the sleeve shaft (11), a third bevel gear (9) is rotatably arranged on the mounting seat (8), and the first bevel gear (14) and the second bevel gear (15) are engaged with the third bevel gear (9).

3. The chlorination still for producing phosphorus trichloride according to claim 1, characterized by: Also include gas purification machine (17), the gas purification machine (17) is connected with exhaust pipe (16) on the gas inlet, the exhaust pipe (16) is arranged on the kettle cover (3) and communicates with the inside of the kettle body (2).

4. The chlorination still for producing phosphorus trichloride according to claim 2, characterized by: The stirring rod (12) is provided with a scraper (18), and the scraper (18) is in contact with the inner wall of the kettle body (2).

5. The chlorination still for producing phosphorus trichloride according to claim 1, characterized by: The kettle cover (3) is provided with a charging port (19), and a sealing cover (20) is detachably arranged on the charging port (19).

6. The chlorination still for producing phosphorus trichloride according to claim 1, characterized by: The bottom of the kettle body (2) is provided with a discharge pipe (21), the discharge pipe (21) extends to the outside of the protective shell (5), and the discharge pipe (21) is provided with a solenoid valve (22).

7. The chlorination still for producing phosphorus trichloride according to claim 2, characterized by: The mounting seat (8) is provided with a motor (23), and one end of the drive shaft (10) is arranged on the output shaft of the motor (23).

8. The chlorination still for producing phosphorus trichloride according to claim 1, characterized by: The kettle cover (3) is detachably arranged on the kettle body (2) by the first bolt (24).

9. The chlorination still for producing phosphorus trichloride according to claim 5, characterized by: The sealing cover (20) is detachably arranged on the charging port (19) by the second bolt (25).