Distillation kettle with gas-liquid separation device

Abstract

The utility model relates to the technical field of distillation kettles, and discloses a distillation kettle with a gas-liquid separation device, which comprises a kettle body, a gas outlet is arranged on the top end face of the kettle body, a heating pipe is fixedly connected to the inner wall of the kettle body, and a defoaming component is arranged on the inner wall of the kettle body. According to the distillation kettle with the gas-liquid separation device, foam can be crushed by the defoaming assembly and the vent plate slapping foam, the volume and the stability of the foam are reduced, the foam is prevented from being accumulated and upwards entering the gas outlet, the rotating rod rotates to capture bubbles suspended in steam, so that tiny bubbles suspended in gas flow are scattered and quickly broken, and the gas-liquid separation effect is improved. The separation efficiency of the bubbles and the steam is improved, the situation that the bubbles continue to rise to the air outlet due to pushing of the steam is avoided, condensation or breakage of the bubbles is accelerated through the arranged cooling pipe, and the bubble size is reduced or broken due to the fact that gas in the bubbles is shrunk by cooling the surfaces of the bubbles.

Description

TECHNICAL FIELD

[0001] The utility model relates to distillation kettle technical field, concretely to a distillation kettle with gas -liquid separation device. BACKGROUND

[0002] The liquid in the distillation kettle is prone to boiling suddenly during the vacuum distillation process. When the temperature of the solvent to be distilled is too high, the vacuum pressure in the distillation kettle has reached or exceeded the boiling point under the corresponding pressure. At this time, the distillation solvent will immediately form boiling after entering the distillation kettle, and carry a large amount of oil-containing solvent foam upward and into the distillation condenser, resulting in a decrease in the cleanliness of the distilled solvent.

[0003] According to the disclosed distillation kettle gas-liquid separation device (announcement number: CN217549028U), the above-mentioned application includes a first kettle body, a gas-liquid separation device arranged in the first kettle body, a second kettle body detachably connected with the first kettle body, and a heating coil detachably connected with the bottom of the second kettle body and extending towards the first kettle body. The first kettle body and the second kettle body form a distillation chamber, and the gas-liquid separation device is arranged in the first kettle body.

[0004] However, the above-mentioned device has the following problems in actual use: the gas outlet is fixed, and when there is too much foam, the foam can still move upward through the gas outlet. At the same time, due to the narrowing of the gas outlet, the foam accumulates at this point, which may completely block the gas outlet and affect the normal exhaust of the distillation kettle. In view of this, we propose a distillation kettle with a gas-liquid separation device. Utility model content

[0005] The utility model aims at providing a distillation kettle with a gas-liquid separation device to solve the problems raised in the background art.

[0006] To achieve the above-mentioned purpose, the utility model provides the following technical scheme: a distillation kettle with a gas-liquid separation device, comprising a kettle body, a gas outlet is formed in the top end face of the kettle body, a heating pipe is fixedly connected to the inner wall of the kettle body, a bubble removal assembly is arranged on the inner wall of the kettle body, and the bubble removal assembly comprises:

[0007] A fixed frame is fixedly connected to the top end face of the fixed frame, the fixed frame is rotatably connected to the vertical rod, the side wall of the vertical rod is fixedly connected to a blade, the outer wall of the vertical rod is fixedly connected to a rotating seat, the outer wall of the rotating seat is fixedly connected to a rotating rod, and the end face of the rotating rod is fixedly connected to a gas inlet plate.

[0008] A connecting block is provided with a limiting groove in the outer wall, the limiting groove is slidably connected to a limiting rod, the end face of the limiting rod is fixedly connected to a gas inlet plate, and the outer wall of the limiting rod is fixedly connected to a protruding block.

[0009] Preferably, the inner wall of the kettle body is fixedly connected with a fixed ring, the inner wall of the fixed ring is provided with a vertical groove, and the vertical groove is in sliding connection with the protrusion.

[0010] Preferably, the blade is movably connected with the inner wall of the guide cover, the axis of the guide cover coincides with the axis of the vertical rod, and the upward movement of the solution vapor pushes the blade and the vertical rod to rotate.

[0011] Preferably, the bottom end face of the kettle body is provided with a liquid outlet, the bottom of the liquid outlet is fixedly connected with an external valve body, and the heating pipe is located at the side of the inside of the kettle body close to the liquid outlet.

[0012] Preferably, the top end face of the vent plate is provided with through holes, the number of the through holes is provided with a plurality of groups, the plurality of groups of through holes are equidistantly arranged on the top end face of the vent plate, the connecting block is fixedly connected with the outer wall of the vertical rod, and the solution vapor can move upward through the through holes on the vent plate.

[0013] Preferably, the fixed frame is fixedly connected with the inner wall of the kettle body, and the guide cover is fixedly connected with the inner wall of the kettle body.

[0014] Preferably, the bottom end face of the fixed frame is fixedly connected with a fixed seat, the inner bottom face of the fixed seat is provided with an annular groove one and an annular groove two, the annular groove one is fixedly connected with the water inlet pipe, the annular groove two is fixedly connected with the drain pipe, the inner wall of the rotating seat and the rotating rod is fixedly connected with a cooling pipe, the two ends of the cooling pipe are movably connected with the annular groove one and the annular groove two respectively, and the fixed seat rotates with the rotating seat.

[0015] Compared with the prior art, the distillation kettle with the gas-liquid separation device has the following beneficial effects:

[0016] 1. The distillation kettle with the gas-liquid separation device, through the setting of the defoaming assembly, the beating of the vent plate on the foam can break the foam, reduce the volume and stability of the foam, prevent the accumulation of the foam and the upward entering of the gas outlet, the rotation of the rotating rod can capture the bubbles suspended in the steam, so that the small bubbles suspended in the airflow are dispersed, they are quickly broken, the separation efficiency of the bubbles and the steam is improved, and the bubbles are prevented from continuing to rise to the gas outlet due to the pushing of the steam.

[0017] 2. The distillation kettle with the gas-liquid separation device, through the setting of the cooling pipe, the surface temperature of the bubbles is reduced, the surface tension is increased, so that the condensation or rupture of the bubbles is accelerated, the gas in the bubbles is contracted by cooling the surface of the bubbles, the volume of the bubbles is reduced or broken, after the rupture of the bubbles, not only the number of the bubbles is reduced, but also they are prevented from further rising through the airflow and being brought into the gas outlet. BRIEF DESCRIPTION OF DRAWINGS

[0018] Figure 1The utility model discloses a main body structure schematic diagram;

[0019] Figure 2 The utility model discloses a kettle body section structure schematic diagram;

[0020] Figure 3 The utility model discloses a fixed frame structure schematic diagram;

[0021] Figure 4 The utility model discloses a vent plate explosion view;

[0022] Figure 5 The utility model discloses a blade structure schematic diagram.

[0023] In the drawing: 1, kettle body;2, gas outlet;3, liquid outlet;4, heating tube;5, bubble removing component;501, fixed frame;502, guide cover;503, vertical rod;504, blade;505, rotating seat;506, rotating rod;507, connecting block;508, limiting groove;509, vent plate;510, limiting rod;511, protruding block;512, fixed ring;513, vertical groove;6, fixed seat;7, water inlet pipe;8, drain pipe;9, cooling pipe. Specific implementation

[0024] As Figures 1-5 Indicated, the utility model provides a kind of technical scheme: a distillation kettle with gas-liquid separation device, including kettle body 1, the top end surface of kettle body 1 is equipped with gas outlet 2, the inner wall of kettle body 1 is fixedly connected with heating tube 4, the bottom end surface of kettle body 1 is equipped with liquid outlet 3, the bottom of liquid outlet 3 is fixedly connected with external valve body, heating tube 4 is located in the inside of kettle body 1 and is close to the side of liquid outlet 3, the inner wall of kettle body 1 is provided with bubble removing component 5, bubble removing component 5 includes fixed frame 501, guide cover 502, vertical rod 503, blade 504, rotating seat 505, rotating rod 506, connecting block 507, limiting groove 508, vent plate 509, limiting rod 510, protruding block 511, fixed ring 512, vertical groove 513.

[0025] In an embodiment of the utility model, the top end surface of fixed frame 501 is fixedly connected with guide cover 502, fixed frame 501 is fixedly connected in the inner wall of kettle body 1, guide cover 502 is fixedly connected in the inner wall of kettle body 1, fixed frame 501 is rotatably connected with vertical rod 503, the side wall of vertical rod 503 is fixedly connected with blade 504, blade 504 is movably connected with the inner wall of guide cover 502, the axis of guide cover 502 coincides with the axis of vertical rod 503, solution vapor moves upwards and pushes blade 504 and vertical rod 503 to rotate, the outer wall of vertical rod 503 is fixedly connected with rotating seat 505, the outer wall of rotating seat 505 is fixedly connected with rotating rod 506.

[0026] The outer wall of the connecting block 507 is provided with a limiting groove 508, the limiting groove 508 is in sliding connection with a limiting rod 510, the end face of the limiting rod 510 is fixedly connected with a ventilation plate 509, the outer wall of the limiting rod 510 is fixedly connected with a protrusion 511, the inner wall of the kettle body 1 is fixedly connected with a fixed ring 512, the inner wall of the fixed ring 512 is provided with a vertical groove 513, the vertical groove 513 is in sliding connection with the protrusion 511, the top end face of the ventilation plate 509 is provided with a through hole, the number of the through hole is provided with several groups, and the several groups of through holes are equidistantly arranged on the top end face of the ventilation plate 509. The connecting block 507 is fixedly connected to the outer wall of the vertical rod 503. The solution vapor can move upward through the through hole on the ventilation plate 509.

[0027] The heating pipe 4 heats the kettle body 1, the solution in the kettle body 1 is heated, the vapor generated by heating moves upward, is discharged from the kettle body 1 through the gas outlet 2, reaches the downstream equipment, the upward movement of the vapor drives the blade 504 to rotate, and then drives the vertical rod 503 and the connecting block 507 to rotate, so that the limiting groove 508 rotates, and then guides the ventilation plate 509 to reciprocate longitudinally. The ventilation plate 509 hits the foam, which can break the foam, reduce the volume and stability of the foam, and prevent the foam from accumulating and entering the gas outlet 2 upward. This hitting action can help break the bubbles in the foam, so that they no longer rise with the airflow, thereby reducing the influence of the foam on the vapor flow. The rotation of the vertical rod 503 drives the rotating rod 506 to rotate, captures the bubbles suspended in the vapor, and disperses the small bubbles suspended in the airflow, so that they are quickly broken, improving the separation efficiency of the bubbles and the vapor, and avoiding the bubbles from continuing to rise to the gas outlet 2 due to the pushing of the vapor.

[0028] In addition, the bottom end face of the fixed frame 501 is fixedly connected with a fixed seat 6, the inner bottom surface of the fixed seat 6 is provided with an annular groove one and an annular groove two, the annular groove one is fixedly connected with the water inlet pipe 7, the annular groove two is fixedly connected with the drain pipe 8, the inner wall of the rotating seat 505 and the rotating rod 506 is fixedly connected with a cooling pipe 9, and the two ends of the cooling pipe 9 are movably connected with the annular groove one and the annular groove two respectively. The fixed seat 6 and the rotating seat 505 rotate, the cooling liquid enters the rotating rod 506 through the water inlet pipe 7, and then is discharged through the drain pipe 8, so as to cool the rotating rod 506. During the distillation process, especially in a vacuum environment, the bubbles may maintain a certain activity and buoyancy due to the high temperature. By cooling the rotating rod 506 and making it contact with the bubbles, the temperature of the bubbles can be effectively reduced. The cooling effect can reduce the surface temperature of the bubbles and increase the surface tension, thereby accelerating the coagulation or rupture of the bubbles. By cooling the surface of the bubbles, the gas in the bubbles contracts, causing the volume of the bubbles to shrink or rupture. After the bubbles rupture, not only the number of bubbles is reduced, but also they are prevented from further rising through the airflow and being brought into the gas outlet 2.

[0029] In the utility model, when using, heating tube 4 heats cauldron body 1, the steam generated by heating moves upward, discharges cauldron body 1 through air outlet 2, steam upward movement promotes the rotation of blade 504, and further drives the rotation of vertical rod 503, and the rotation of limiting groove 508 guides the longitudinal reciprocating movement of breather plate 509, and breather plate 509 hits foam, reduces the volume and stability of foam, and rotation rod 506 rotates, disperses the tiny bubbles suspended in airflow, and improves the separation efficiency of bubbles and steam.

[0030] The above has made detailed description to the utility model in general, but can make some modification or improvement to it on the basis of the utility model, which is obvious to the general skilled in the technical field. Therefore, the modification or improvement without departing from the spirit of the utility model idea is within the protection scope of the utility model.

Claims

1. A distillation kettle with gas-liquid separation device, comprising a kettle body (1), a gas outlet (2) is arranged on the top end surface of the kettle body (1), and a heating pipe (4) is fixedly connected to the inner wall of the kettle body (1), characterized in that: The inner wall of the kettle body (1) is provided with a bubble removing assembly (5), which comprises: The top end surface of the fixed frame (501) is fixedly connected with a guide cover (502), the fixed frame (501) is rotatably connected with a vertical rod (503), the side wall of the vertical rod (503) is fixedly connected with a blade (504), the outer wall of the vertical rod (503) is fixedly connected with a rotating seat (505), the outer wall of the rotating seat (505) is fixedly connected with a rotating rod (506), and the outer wall of the connecting block (507) is provided with a limiting groove (508). The outer wall of the limiting rod (510) is fixedly connected with a ventilation plate (509), and the outer wall of the limiting rod (510) is fixedly connected with a protruding block (511).

2. A distillation kettle with a gas-liquid separation device according to claim 1, characterized in that: The inner wall of the kettle body (1) is fixedly connected with a fixed ring (512), the inner wall of the fixed ring (512) is provided with a vertical groove (513), and the vertical groove (513) is slidably connected with the protruding block (511).

3. A distillation kettle with a gas-liquid separation device according to claim 1, characterized in that: The inner wall of the kettle body (1) is fixedly connected with a fixed ring (512), the inner wall of the fixed ring (512) is provided with a vertical groove (513), and the vertical groove (513) is slidably connected with the protruding block (511).

4. The distillation kettle with a gas-liquid separation device according to claim 1, characterized in that: The bottom end surface of the kettle body (1) is provided with a liquid outlet (3), the bottom of the liquid outlet (3) is fixedly connected with an external valve body, and the heating pipe (4) is located inside the kettle body (1) and close to one side of the liquid outlet (3).

5. The distillation kettle with a gas-liquid separation device according to claim 1, characterized in that: The top end surface of the ventilation plate (509) is provided with a through hole, the number of the through holes is provided with several groups, and the through holes are arranged at equal intervals on the top end surface of the ventilation plate (509).

6. A distillation kettle with a gas-liquid separation device according to claim 1, characterized in that: The fixed frame (501) is fixedly connected to the inner wall of the kettle body (1), and the guide cover (502) is fixedly connected to the inner wall of the kettle body (1).

7. A distillation kettle with a gas-liquid separation device according to claim 1, characterized in that: The bottom end surface of the fixed frame (501) is fixedly connected with a fixed seat (6), the inner bottom surface of the fixed seat (6) is provided with an annular groove one and an annular groove two, the annular groove one is fixedly connected with a water inlet pipe (7), the annular groove two is fixedly connected with a drain pipe (8), the inner wall of the rotating seat (505) and the rotating rod (506) is fixedly connected with a cooling pipe (9), the two ends of the cooling pipe (9) are movably connected with the annular groove one and the annular groove two respectively, and the fixed seat (6) is rotatable with the rotating seat (505).

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