Petroleum resin degassing reaction kettle

Abstract

The utility model relates to the technical field of petroleum resin, in particular to a petroleum resin degassing reaction kettle which comprises a reaction kettle body, the device further comprises a vacuum pump and a fixing assembly. One side of the reaction kettle body is fixedly connected with a support frame; according to the device, a vacuum pump is started, the vacuum pump extracts all gas in the reaction kettle body through a connecting pipe, so that the interior of the reaction kettle body is in a vacuum state, a driving motor is started, the driving motor drives a connecting rod to rotate, the connecting rod drives a rotating rod to move, and the rotating rod drives a gear to move along a gear ring, so that the gear rotates; the gear drives the rotating rod to rotate on the inner side of the connecting rod, and the rotating rod drives the stirring blades to rotate, so that planetary rotation is performed, resin is uniformly stirred, heating is more uniform, the petroleum resin is heated to a certain temperature, volatile components in the resin are gasified, partial pressure of the volatile components is reduced in a vacuum environment, and the volatile components are promoted to be separated from the resin; through vacuum and stirring, rapid and thorough removal of volatile components is realized.

Description

Technical Field

[0001] This utility model relates to the field of petroleum resin technology, and in particular to a petroleum resin degassing reactor. Background Technology

[0002] During the production of petroleum resins, volatile substances, low molecular weight polymers, and gases such as oxygen are inevitably introduced due to polymerization reactions and other processes. The presence of these gases can adversely affect the quality of petroleum resins, such as causing the resin to darken in color, produce odors, and reduce thermal stability. Therefore, degassing treatment is necessary to remove these gases and improve the quality of petroleum resins.

[0003] Existing petroleum resin degassing reactors heat the petroleum resin to a certain temperature, causing the volatile components in the resin to vaporize. Then, a motor is started, which drives the stirring blades to rotate vertically, stirring the resin in the reactor. This ensures that the resin is heated evenly within the reactor, avoiding localized overheating that could lead to resin degradation, thereby achieving degassing.

[0004] However, the rotation of vertical stirring blades easily creates a fixed flow field, resulting in a large difference in resin mixing effect between the edge and center areas of the reactor. This leads to uneven heating and makes it difficult to effectively break down the viscous layer formed on the resin surface. Consequently, some volatile components are trapped inside the resin and cannot escape in time, prolonging the degassing time. This not only increases production energy consumption and reduces production efficiency, but may also affect the final quality of petroleum resin due to incomplete degassing. Utility Model Content

[0005] The existing petroleum resin degassing reactor has a significant difference in resin mixing effect between the edge area and the center area, resulting in uneven heating and difficulty in effectively breaking down the viscous layer formed on the resin surface. This causes some volatile components to be trapped inside the resin and unable to be discharged in time.

[0006] The technical solution of this utility model is as follows: a petroleum resin degassing reactor, including a reactor body; it also includes a vacuum pump and a fixing assembly; a support frame is fixedly connected to one side of the reactor body, a cover plate is provided at the upper end of the reactor body, a control device is fixedly connected to the outside of the reactor body, a heating device is provided inside the reactor body, a discharge pipe is fixedly connected to the lower end of the reactor body, an electric valve is provided on one side of the discharge pipe, a fixing assembly is provided on the reactor body, a vacuum pump for vacuuming is fixedly connected to the upper end of the cover plate, a connecting pipe is fixedly connected to the output end of the vacuum pump, the other end of the connecting pipe is fixedly connected to the cover plate, a drive motor is fixedly connected to the upper end of the cover plate, a gear ring is fixedly connected to the inside of the cover plate, a connecting rod is fixedly connected to the output end of the drive motor, a rotating rod is provided on one side of the connecting rod, a gear is fixedly connected to one side of the rotating rod, the gear meshes with the gear ring, and a stirring blade is fixedly connected to the outside of the rotating rod.

[0007] Preferably, the connecting rod has a groove, and the rotating rod is rotatably connected to the inner side of the connecting rod through the groove.

[0008] Preferably, multiple sets of stirring blades are provided, and the multiple sets of stirring blades are arranged in a linear array on the outside of the rotating rod.

[0009] Preferably, the fixing component includes a sealing ring, a sealing ring is fixedly connected to the upper end of the reactor body, a first fixing block is fixedly connected to one side of the cover plate, a second fixing block is provided on one side of the reactor body, a rotating block is rotatably connected to the inner side of the second fixing block, a threaded rod is threadedly connected to the inner side of the rotating block, and a fixing plate is fixedly connected to the upper end of the threaded rod.

[0010] Preferably, the first fixing block has a second groove, and the fixing plate is engaged with the inner side of the first fixing block through the second groove.

[0011] Preferably, multiple sets of the first fixed block, the second fixed block, the rotating block, the threaded rod, and the fixed plate are provided, and multiple sets of the first fixed block, the second fixed block, the rotating block, the threaded rod, and the fixed plate are arranged in a circumferential array on the outside of the reactor body.

[0012] As a preferred material, the sealing ring is made of fluororubber, which has excellent high temperature resistance and chemical corrosion resistance.

[0013] The beneficial effects of this invention are as follows: Compared with traditional petroleum resin degassing reactors, the mixing effect of resin in the edge area and the center area of ​​the reactor is significantly different, resulting in uneven heating and difficulty in effectively breaking down the viscous layer formed on the resin surface. This leads to some volatile components being trapped inside the resin and unable to be discharged in time. This device starts a vacuum pump, which extracts all the gas inside the reactor body through a connecting pipe, creating a vacuum inside the reactor body. The drive motor is then started, which drives the connecting rod to rotate. The connecting rod drives the rotating rod to move, which in turn drives the gear along the gear ring. This causes the gear to rotate, which in turn drives the rotating rod to rotate inside the connecting rod. The rotating rod then drives the stirring blade to rotate, resulting in planetary rotation, which uniformly stirs the resin and makes the heating more uniform. When the petroleum resin is heated to a certain temperature, the volatile components in the resin are vaporized. In a vacuum environment, the partial pressure of the volatile components is reduced, promoting their release from the resin. Through vacuum and stirring, the volatile components are rapidly and thoroughly removed. Attached Figure Description

[0014] Figure 1 The diagram shown is a three-dimensional structural schematic of this utility model;

[0015] Figure 2 The diagram shown is a disassembled structural diagram of the reaction vessel body and cover plate of this utility model;

[0016] Figure 3The diagram shown is a cross-sectional view of the present invention.

[0017] Figure 4 The diagram shown is a cross-sectional view of the combined structure of the cover plate, vacuum pump, connecting pipe, drive motor, gear ring, connecting rod, rotating rod, gear and stirring blade of this utility model.

[0018] Figure 5 The diagram shown is a cross-sectional view of the fixing component of this utility model.

[0019] Explanation of reference numerals in the attached drawings: 1. Reactor body; 2. Support frame; 3. Cover plate; 4. Control device; 5. Heating device; 6. Discharge pipe; 7. Electric valve; 801. Vacuum pump; 802. Connecting pipe; 803. Drive motor; 804. Gear ring; 805. Connecting rod; 806. Rotating rod; 807. Gear; 808. Stirring blade; 901. Sealing ring; 902. First fixing block; 903. Second fixing block; 904. Rotating block; 905. Threaded rod; 906. Fixing plate. Detailed Implementation

[0020] The present invention will be further described below with reference to the accompanying drawings and embodiments.

[0021] Please see Figures 1-5This utility model provides an embodiment of a petroleum resin degassing reactor, including a reactor body 1; it also includes a vacuum pump 801 and a fixing assembly; a support frame 2 is fixedly connected to one side of the reactor body 1, a cover plate 3 is provided at the upper end of the reactor body 1, a control device 4 is fixedly connected to the outer side of the reactor body 1, a heating device 5 is provided at the inner side of the reactor body 1, a discharge pipe 6 is fixedly connected to the lower end of the reactor body 1, an electric valve 7 is provided on one side of the discharge pipe 6, a fixing assembly is provided on the reactor body 1, a vacuum pump 801 for vacuuming is fixedly connected to the upper end of the cover plate 3, and a connecting pipe 802 is fixedly connected to the output end of the vacuum pump 801. The other end of 802 is fixedly connected to the cover plate 3. A drive motor 803 is fixedly connected to the upper end of the cover plate 3. A gear ring 804 is fixedly connected to the inner side of the cover plate 3. A connecting rod 805 is fixedly connected to the output end of the drive motor 803. A rotating rod 806 is provided on one side of the connecting rod 805. A gear 807 is fixedly connected to one side of the rotating rod 806. The gear 807 meshes with the gear ring 804. A stirring blade 808 is fixedly connected to the outer side of the rotating rod 806. A groove is provided on the connecting rod 805. The rotating rod 806 is rotatably connected to the inner side of the connecting rod 805 through the groove. The groove on the connecting rod 805 allows the rotating rod 806 to be rotatably connected to the inner side of the connecting rod 802. 5. The inner side of the rotating rod 806 is used to limit the movement of the rotating rod 806. Multiple sets of stirring blades 808 are arranged in a linear array on the outer side of the rotating rod 806. The multiple sets of stirring blades 808 make the resin mixing more uniform. Petroleum resin is added to the reactor body 1. The heating device 5 is started by the control device 4 to heat the resin inside the reactor body 1. The vacuum pump 801 is started. The vacuum pump 801 extracts all the gas in the reactor body 1 through the connecting pipe 802, so that the inside of the reactor body 1 is in a vacuum state. The drive motor 803 is started. The drive motor 803 drives the connecting rod 805 to rotate. The connecting rod 805 drives the rotating rod 806 to move, and the rotating rod 806 drives the gear 807 to move along the gear ring 804, causing the gear 807 to rotate. The gear 807 drives the rotating rod 806 to rotate inside the connecting rod 805, and the rotating rod 806 drives the stirring blade 808 to rotate, thus performing planetary rotation to uniformly stir the resin and make the heating more uniform. When the petroleum resin is heated to a certain temperature, the volatile components in the resin are vaporized. Under vacuum, the partial pressure of the volatile components is reduced, promoting their release from the resin. Through vacuum and stirring, the volatile components are quickly and thoroughly removed. After degassing is completed, the electric valve 7 is activated, and the resin is discharged from the discharge pipe 6.

[0022] Please see Figure 5In this embodiment, the fixing assembly includes a sealing ring 901. The sealing ring 901 is fixedly connected to the upper end of the reactor body 1. A first fixing block 902 is fixedly connected to one side of the cover plate 3. A second fixing block 903 is provided on one side of the reactor body 1. A rotating block 904 is rotatably connected to the inner side of the second fixing block 903. A threaded rod 905 is threadedly connected to the inner side of the rotating block 904. A fixing plate 906 is fixedly connected to the upper end of the threaded rod 905. A second groove is provided on the first fixing block 902. The fixing plate 906 is engaged with the inner side of the first fixing block 902 through the second groove. The second groove on the first fixing block 902 allows the fixing plate 906 to be engaged with the inner side of the first fixing block 902. The cover plate 3 is fixed to the inner side of the fixing block 902. Multiple sets of the first fixing block 902, the second fixing block 903, the rotating block 904, the threaded rod 905 and the fixing plate 906 are arranged in a circumferential array on the outer side of the reactor body 1. The multiple sets of the first fixing block 902, the second fixing block 903, the rotating block 904, the threaded rod 905 and the fixing plate 906 make the fixing of the cover plate 3 more stable and firm. The sealing ring 901 is made of fluororubber, which has excellent high temperature resistance and chemical corrosion resistance.

[0023] During operation, petroleum resin is added to the reactor body 1. The heating device 5 is activated via the control device 4 to heat the resin inside the reactor body 1. The vacuum pump 801 is activated, extracting all gas from the reactor body 1 through the connecting pipe 802, creating a vacuum inside the reactor body 1. The drive motor 803 is activated, rotating the connecting rod 805. The connecting rod 805 moves the rotating rod 806, which in turn moves the gear 807 along the gear ring 804, causing the gear 807 to rotate. The gear 807 then rotates the rotating rod 806 inside the connecting rod 805, which in turn rotates the stirring blade 808, resulting in planetary rotation that evenly stirs the resin and ensures more uniform heating. When the petroleum resin reaches a certain temperature, the volatile components in the resin vaporize. Under vacuum conditions, the partial pressure of these volatile components is reduced, promoting... The resin is extracted from the resin. Through vacuum and stirring, the volatile components are quickly and thoroughly removed. After degassing, the electric valve 7 is activated, and the resin is discharged from the discharge pipe 6. By rotating the fixed plate 906, the fixed plate 906 drives the threaded rod 905 to rotate inside the rotating block 904, thereby causing the fixed plate 906 to disengage from the groove on the first fixed block 902, releasing the limiting fixation of the first fixed block 902. Then, the rotating block 904 is rotated to move the fixed plate 906 away from the top of the first fixed block 902. Then, the cover plate 3 is pulled to open it. When fixing the cover plate 3, the fixed plate 906 is rotated to the top of the first fixed block 902 by rotating the rotating block 904. Then, the fixed plate 906 is rotated, and the fixed plate 906 drives the threaded rod 905 to rotate. The threaded rod 905 drives the fixed plate 906 to move, so that the fixed plate 906 engages with the groove on the first fixed block 902, thereby fixing the cover plate 3.

[0024] Through the above steps, petroleum resin is added to the reactor body 1. The heating device 5 is activated by the control device 4 to heat the resin inside the reactor body 1. The vacuum pump 801 is activated, and the vacuum pump 801 extracts all the gas inside the reactor body 1 through the connecting pipe 802, making the inside of the reactor body 1 a vacuum state. The drive motor 803 is activated, and the drive motor 803 drives the connecting rod 805 to rotate. The connecting rod 805 drives the rotating rod 806 to move, and the rotating rod 806 drives the gear 807 to move along the gear ring 804. The gear 807 rotates, which in turn drives the rotating rod 806 to rotate inside the connecting rod 805. The rotating rod 806 then drives the stirring blade 808 to rotate, thus performing planetary rotation to uniformly stir the resin and make the heating more uniform. When the petroleum resin is heated to a certain temperature, the volatile components in the resin are vaporized. Under vacuum conditions, the partial pressure of the volatile components is reduced, promoting their removal from the resin. Through vacuum and stirring, the volatile components are quickly and thoroughly removed. After degassing is completed, the electric valve 7 is activated, and the resin is discharged from the discharge pipe 6.

Claims

1. A petroleum resin degassing reactor, comprising a reactor body (1); characterized in that: It also includes a vacuum pump (801) and a fixing assembly; a support frame (2) is fixedly connected to one side of the reactor body (1), a cover plate (3) is provided at the upper end of the reactor body (1), a control device (4) is fixedly connected to the outside of the reactor body (1), a heating device (5) is provided at the inside of the reactor body (1), a discharge pipe (6) is fixedly connected to the lower end of the reactor body (1), an electric valve (7) is provided on one side of the discharge pipe (6), a fixing assembly is provided on the reactor body (1), and a vacuum pump (801) for vacuuming is fixedly connected to the upper end of the cover plate (3). The output end is fixedly connected to a connecting pipe (802), the other end of the connecting pipe (802) is fixedly connected to a cover plate (3), the upper end of the cover plate (3) is fixedly connected to a drive motor (803), the inner side of the cover plate (3) is fixedly connected to a gear ring (804), the output end of the drive motor (803) is fixedly connected to a connecting rod (805), a rotating rod (806) is provided on one side of the connecting rod (805), a gear (807) is fixedly connected on one side of the rotating rod (806), the gear (807) meshes with the gear ring (804), and a stirring blade (808) is fixedly connected to the outer side of the rotating rod (806).

2. The petroleum resin degassing reactor of claim 1, wherein: A groove is provided on the connecting rod (805), and the rotating rod (806) is rotatably connected to the inner side of the connecting rod (805) through the groove.

3. The petroleum resin degassing reactor of claim 1, wherein: Multiple sets of stirring blades (808) are provided, and multiple sets of stirring blades (808) are arranged in a linear array on the outside of the rotating rod (806).

4. The petroleum resin degassing reactor of claim 1, wherein: The fixing components include a sealing ring (901), the upper end of the reactor body (1) is fixedly connected to the sealing ring (901), the cover plate (3) is fixedly connected to one side of the first fixing block (902), the reactor body (1) is provided with a second fixing block (903), the inner side of the second fixing block (903) is rotatably connected to a rotating block (904), the inner side of the rotating block (904) is threadedly connected to a threaded rod (905), and the upper end of the threaded rod (905) is fixedly connected to a fixing plate (906).

5. The petroleum resin degassing reactor of claim 4, wherein: The first fixing block (902) has a second groove, and the fixing plate (906) is engaged with the inner side of the first fixing block (902) through the second groove.

6. The petroleum resin degassing reactor of claim 4, wherein: The first fixed block (902), the second fixed block (903), the rotating block (904), the threaded rod (905) and the fixed plate (906) are all provided in multiple sets. The multiple sets of the first fixed block (902), the second fixed block (903), the rotating block (904), the threaded rod (905) and the fixed plate (906) are arranged in a circumferential array on the outside of the reactor body (1).

7. The petroleum resin degassing reactor of claim 4, wherein: The sealing ring (901) is made of fluororubber, which has excellent high temperature resistance and chemical corrosion resistance.

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