A nickel-plated reactor with diamond micropowder

Abstract

This utility model discloses a nickel plating reactor for diamond micron powder, comprising a reactor and an oil storage tank. The reactor has a jacketed structure, and a detachable lid is provided on the top of the reactor. A stirring element is provided on the lid, and a temperature regulating element is provided between the oil storage tank and the jacket of the reactor. This utility model belongs to the technical field of reactors, specifically referring to a nickel plating reactor for diamond micron powder.

Description

Technical Field

[0001] This utility model belongs to the field of reaction vessel technology, specifically referring to a diamond micron powder nickel plating reaction vessel. Background Technology

[0002] Nickel plating with diamond micropowder is an important surface treatment process that can significantly improve the wear resistance, oxidation resistance, and adhesion to the metal substrate of diamond micropowder. It is widely used in the field of superhard material tool manufacturing. In the nickel plating process with diamond micropowder, the reaction process has high requirements for conditions such as temperature and stirring effect.

[0003] Existing diamond micron nickel plating reactors can only be heated or cooled by a single method, which is not convenient for switching according to the temperature requirements of different stages of the nickel plating reaction. This can easily lead to excessive temperature fluctuations. In terms of stirring, unidirectional stirring can easily cause the micron powder to settle and agglomerate, resulting in incomplete coating. Utility Model Content

[0004] The technical problem this invention aims to solve is that existing diamond micron nickel plating reactors can only be heated or cooled by a single method, which is not convenient for switching the temperature according to the different stages of the nickel plating reaction. Furthermore, in terms of stirring, unidirectional stirring easily causes the micron powder to settle and agglomerate, resulting in incomplete coating.

[0005] To achieve the above functions, the technical solution adopted by this utility model is as follows: a diamond micron nickel plating reactor, including a reactor and an oil storage tank, wherein the reactor is a jacketed structure, the top of the reactor is detachably provided with a reactor cover, the reactor cover is provided with a stirring element, and a temperature regulating element is provided between the oil storage tank and the jacket of the reactor.

[0006] Preferably, the temperature regulating component includes a circulating pump, an electric three-way valve, a tubular electric heater, and a plate heat exchanger, and is installed at the bottom of the oil storage tank. Its output end extends out of the oil storage tank and is connected to the inlet of the electric three-way valve. The two outlets of the electric three-way valve are independently connected to the inlet of the tubular electric heater and the inlet of the plate heat exchanger, respectively. The outlets of the tubular electric heater and the plate heat exchanger are connected to the jacket. The top of the reactor is provided with an oil outlet, which is connected to the oil storage tank.

[0007] Preferably, a temperature sensor is provided inside the reactor, and a PLC controller is provided on the side wall of the reactor. The PLC controller is electrically connected to the temperature sensor and the electric three-way valve.

[0008] Preferably, the stirring component includes a paddle and a rotating frame. The top end of the paddle rotates through the lid and extends outward. A connecting sleeve is rotatably fitted onto the top of the paddle, and the connecting sleeve rotates outward from the top of the lid. The top of the rotating frame is fixedly fitted onto the connecting sleeve, and the bottom of the rotating frame is rotatably fitted onto the bottom of the paddle. The outer side of the paddle and the inner sidewall of the rotating frame are provided with staggered blades. The lid is provided with a driving component that drives the paddle and the rotating frame to rotate.

[0009] Preferably, the driving component includes a driven bevel gear one fixedly sleeved on the top of the connecting sleeve, and a driven bevel gear two fixedly sleeved on the top of the paddle rod. The top of the vessel cover is provided on a fixed plate. An active bevel gear that meshes with the driven bevel gear one and the driven bevel gear two is rotatably provided on the fixed plate. A drive motor is also provided on the fixed plate. The output end of the drive motor rotatably passes through the fixed plate and is connected to the active bevel gear.

[0010] Preferably, an expansion buffer tank is connected to the top of the oil storage tank.

[0011] The beneficial effects achieved by adopting the above-described structure are as follows:

[0012] 1. The temperature regulating component design of this utility model includes a circulating pump, an electric three-way valve, a tubular electric heater, and a plate heat exchanger, forming two independent temperature control paths. The temperature sensor inside the reactor works in conjunction with the PLC controller to monitor in real time and automatically adjust according to the set temperature, thereby reducing temperature fluctuations.

[0013] 2. The stirring component adopts a combination of paddle and rotating frame, with the paddle blades arranged in an alternating manner. The driving component, through the cooperation of driven bevel gear one, driven bevel gear two, and driving bevel gear, drives the paddle and rotating frame to rotate in opposite directions, forming strong shear force and turbulence, breaking up diamond powder agglomeration, avoiding deposition, improving coating uniformity, and enabling more thorough mixing of materials in the reactor, so that diamond powder and plating solution are in uniform contact during nickel plating.

[0014] 3. The electric three-way valve can easily switch the connection between the tubular electric heater or heat exchanger and the jacket to meet the different temperature requirements of different reaction stages. Attached Figure Description

[0015] Figure 1 This is a schematic diagram of the overall structure of an embodiment of the present utility model;

[0016] Figure 2 This is a cross-sectional view of an embodiment of the present utility model;

[0017] Figure 3 for Figure 1 Enlarged view of section A in the middle;

[0018] Figure 4This is a perspective view of an embodiment of the present utility model.

[0019] Among them, 1. Reactor, 2. Oil storage tank, 3. Reactor cover, 4. Stirring component, 5. Temperature regulating component, 6. Circulating pump, 7. Electric three-way valve, 8. Tubular electric heater, 9. Plate heat exchanger, 10. Oil outlet, 11. Temperature sensor, 12. PLC controller, 13. Paddle rod, 14. Rotating frame, 15. Connecting sleeve, 16. Paddle blade, 17. Driving component, 18. Driven bevel gear one, 19. Driven bevel gear two, 20. Fixed plate, 21. Driving bevel gear, 22. Drive motor, 23. Expansion buffer tank. Detailed Implementation

[0020] The technical solution of this utility model will now be clearly and completely described with reference to the accompanying drawings. Obviously, the described embodiments are only some, not all, of the embodiments of this utility model. Based on the embodiments of this utility model, all other embodiments obtained by those skilled in the art without creative effort are within the scope of protection of this utility model.

[0021] In the description of this utility model, it should be noted that, unless otherwise explicitly specified and limited, the terms "set," "install," "connect," and "link" should be interpreted broadly. For example, they can refer to a fixed connection, a detachable connection, or an integral connection; they can refer to a mechanical connection or an electrical connection; they can refer to a direct connection or an indirect connection through an intermediate medium; and they can refer to the internal connection of two components. Those skilled in the art can understand the specific meaning of the above terms in this application based on the specific circumstances.

[0022] like Figure 1-4 As shown, the present invention proposes a diamond micron nickel plating reactor, comprising a reactor 1 and an oil storage tank 2. The reactor 1 is a jacketed structure, and the top of the reactor 1 is detachably equipped with a lid 3. The lid 3 is equipped with a stirring element 4. A temperature regulating element 5 is provided between the oil storage tank 2 and the jacket of the reactor 1. An expansion buffer tank 23 is connected to the top of the oil storage tank 2, which can effectively cope with the volume expansion caused by changes in oil temperature, ensure the safe and stable operation of the entire temperature regulation system, and reduce safety hazards caused by abnormal pressure. The oil storage tank 2 contains heat transfer oil. The temperature regulating element 5 regulates the temperature of the reactor 1, and the stirring element 4 mixes the materials in the reactor 1.

[0023] like Figure 1-2As shown, the temperature regulating component 5 includes a circulating pump 6, an electric three-way valve 7, a tubular electric heater 8, and a plate heat exchanger 9. The circulating pump 6 is an immersion circulating pump and is installed at the bottom of the oil storage tank 2. Its output end passes through the oil storage tank 2 and is connected to the inlet of the electric three-way valve 7. The two outlets of the electric three-way valve 7 are independently connected to the inlet of the tubular electric heater 8 and the inlet of the plate heat exchanger 9, respectively. The outlets of the tubular electric heater 8 and the plate heat exchanger 9 are connected to the jacket. The electric three-way valve 7 switches the connection between the tubular electric heater 8 or the plate heat exchanger 9 and the jacket of the reactor 1, forming two independent temperature control paths. The top of the reactor 1 is provided with an oil outlet 10, which is connected to the oil storage tank 2. The electric three-way valve 7 closes the branch of the plate heat exchanger 9. The heat transfer oil is heated by the tubular electric heater 8 and enters the jacket. The electric three-way valve 7 switches to the branch of the plate heat exchanger 9, and the cooling water and hot oil exchange heat in the plate heat exchanger.

[0024] like Figure 2 and 4 As shown, a temperature sensor 11 is installed inside the reactor 1, and a PLC controller 12 is installed on the side wall of the reactor 1. The PLC controller 12 is electrically connected to the temperature sensor 11 and the electric three-way valve 7. The temperature sensor 11 monitors the temperature inside the reactor and the jacket in real time and transmits the data to the PLC controller 12. The PLC executes a PID algorithm and automatically adjusts the temperature according to the set temperature. Heating mode: the cooling branch of the electric three-way valve 7 is closed, and the electric heater is started to raise the temperature. Cooling mode: the electric three-way valve 7 is switched to the plate heat exchanger 9 branch, and cooling water is circulated to lower the temperature.

[0025] like Figure 2 As shown, the stirring component 4 includes a paddle 13 and a rotating frame 14. The top end of the paddle 13 rotates through the lid 3 and extends outward. A connecting sleeve 15 is rotatably fitted onto the top of the paddle 13. The connecting sleeve 15 rotates out from the top of the lid 3. The top of the rotating frame 14 is fixedly fitted onto the connecting sleeve 15. The bottom of the rotating frame 14 is rotatably fitted onto the bottom of the paddle 13. The outer side of the paddle 13 and the inner sidewall of the rotating frame 14 are provided with staggered paddle blades 16. The lid 3 is provided with a driving component 17 that drives the paddle 13 and the rotating frame 14 to rotate.

[0026] like Figure 3 As shown, the driving component 17 includes a driven bevel gear 18 fixedly sleeved on the top of the connecting sleeve 15 and a driven bevel gear 19 fixedly sleeved on the top of the paddle rod 13. The top of the vessel cover 3 is located on a fixed plate 20. A driving bevel gear 21 is rotatably mounted on the fixed plate 20, meshing with the driven bevel gear 18 and the driven bevel gear 19. A drive motor 22 is also mounted on the fixed plate 20. The output end of the drive motor 22 rotatably passes through the fixed plate 20 and is connected to the driving bevel gear 21.

[0027] In practical use, when heating is required, the PLC controller receives the temperature signal from the temperature sensor 11, determines that the current temperature is lower than the set value, automatically controls the electric three-way valve 7 to close the branch of the plate heat exchanger 9, starts the tubular electric heater 8, and the circulating pump 6 draws out the heat transfer oil from the bottom of the oil storage tank 2 and delivers it to the tubular electric heater 8 through the electric three-way valve 7. After the heat transfer oil is heated in the tubular electric heater 8, it enters the jacket of the reactor 1 to heat the reactor 1, so that the reaction temperature gradually rises to the set value.

[0028] While the temperature is rising, the drive motor 22 is started. The drive motor 22 drives the active bevel gear 21 to rotate. The active bevel gear 21 meshes with the driven bevel gear 18 and the driven bevel gear 19, which in turn drives the connecting sleeve 15 and the paddle rod 13 to rotate in opposite directions, i.e., stirring in two directions. This causes the paddle blades 16 on the rotating frame 14 and the paddle rod 13 to rotate and stir the material in the reaction vessel 1, promoting uniform mixing of the material.

[0029] If cooling is required during the reaction, the PLC controller controls the electric three-way valve 7 to switch to the plate heat exchanger 9 branch based on the feedback from the temperature sensor 11. At this time, the high-temperature heat transfer oil flows out from the jacket of the reactor 1 and enters the plate heat exchanger 9 to exchange heat with the cooling water. The cooled heat transfer oil then returns to the oil storage tank 2. At the same time, the circulation pump 6 continues to work to maintain the circulation of the heat transfer oil, so that the temperature inside the reactor 1 is reduced to a suitable range.

[0030] The present invention and its embodiments have been described above. This description is not restrictive, and the accompanying drawings are only one embodiment of the present invention; the actual structure is not limited thereto. In conclusion, if those skilled in the art are inspired by this description and design similar structures and embodiments without departing from the inventive spirit of the present invention, such designs should fall within the protection scope of the present invention.

Claims

1. A nickel-plating reactor for diamond micron powder, characterized in that: The reactor includes a reaction vessel (1) and an oil storage tank (2). The reaction vessel (1) has a jacketed structure. The top of the reaction vessel (1) is detachably equipped with a vessel cover (3). The vessel cover (3) is equipped with a stirring element (4). A temperature regulating element (5) is provided between the oil storage tank (2) and the jacket of the reaction vessel (1). The temperature regulating element (5) includes a circulating pump (6), an electric three-way valve (7), a tubular electric heater (8), and a plate heat exchanger (9). The circulating pump (6) is... An immersion circulating pump is installed at the bottom of the oil storage tank (2). Its output end passes through the oil storage tank (2) and is connected to the inlet of the electric three-way valve (7). The two outlets of the electric three-way valve (7) are independently connected to the inlet of the tubular electric heater (8) and the inlet of the plate heat exchanger (9). The outlet of the tubular electric heater (8) and the outlet of the plate heat exchanger (9) are connected to the jacket. The top of the reactor (1) is provided with an oil outlet (10), which is connected to the oil storage tank (2).

2. The diamond micron powder nickel plating reactor according to claim 1, characterized in that: The reactor (1) is equipped with a temperature sensor (11) and a PLC controller (12) is provided on the side wall of the reactor (1). The PLC controller (12) is electrically connected to the temperature sensor (11) and the electric three-way valve (7).

3. The diamond micron powder nickel plating reactor according to claim 2, characterized in that: The stirring component (4) includes a paddle (13) and a rotating frame (14). The top end of the paddle (13) rotates through the lid (3) and extends out. A connecting sleeve (15) is rotatably fitted onto the top of the paddle (13). The connecting sleeve (15) rotates out from the top of the lid (3). The top of the rotating frame (14) is fixedly fitted onto the connecting sleeve (15). The bottom of the rotating frame (14) is rotatably fitted onto the bottom of the paddle (13). The outer side of the paddle (13) and the inner side wall of the rotating frame (14) are provided with staggered blades (16). The lid (3) is provided with a driving component (17) that drives the paddle (13) and the rotating frame (14) to rotate.

4. The diamond micron powder nickel plating reactor according to claim 3, characterized in that: The driving component (17) includes a driven bevel gear one (18) fixedly sleeved on the top of the connecting sleeve (15) and a driven bevel gear two (19) fixedly sleeved on the top of the paddle rod (13). The top of the lid (3) is located on the fixed plate (20). The fixed plate (20) is rotatably provided with a driving bevel gear (21) that meshes with the driven bevel gear one (18) and the driven bevel gear two (19). The fixed plate (20) is also provided with a drive motor (22). The output end of the drive motor (22) rotatably passes through the fixed plate (20) and is connected to the driving bevel gear (21).

5. A nickel-plating reactor for diamond micron powder according to any one of claims 1 to 4, characterized in that: An expansion buffer tank (23) is connected to the top of the oil storage tank (2).

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