A chlorohexadecane reaction device that can assist sampling

Abstract

The utility model belongs to chloro hexadecane reaction device technical field, concretely is a kind of chloro hexadecane reaction device of auxiliary sampling, including reation kettle main body, kettle cover, feeding pipe, driving motor and stirring shaft, the top of reation kettle main body is covered with kettle cover, and the top of kettle cover is respectively equipped with feeding pipe and driving motor.The utility model positive and negative motor positive rotation, rotate through output shaft and drive rotating rod, to drive gear to rotate, to move gear plate by meshing, when gear plate moves, drive moving block to move, to drive electric sampling pump to move to the direction close to kettle cover surface, baffle and sealing washer can be sealed to the sampler port, so that sampler can be unscrewed from the bottom of storage tank, prevent the irritating smell of sample in sampler to affect the health of staff.

Description

Technical Field

[0001] This invention belongs to the technical field of hexadecyl chloride reaction apparatus, specifically a hexadecyl chloride reaction apparatus that can assist in sampling. Background Technology

[0002] Hexadecane chloroform is an organic compound. At room temperature, it is a colorless, transparent liquid. It is readily soluble in organic solvents such as alcohols and ethers, but insoluble in water. Hexadecane chloroform can be used as an intermediate in the preparation of surfactants (such as quaternary ammonium salts), and it is also used in fine chemical fields such as detergents and cosmetic raw materials. The production of hexadecane chloroform requires a reaction apparatus, which typically refers to a reaction vessel.

[0003] In the existing technology, the hexadecane chlororeactor is a special equipment for synthesizing hexadecane chlororea. When the reactor is in use, a stirring shaft can mix and stir multiple raw materials to accelerate the reaction between the raw materials. After the reaction is completed, samples need to be taken for testing. Only after the test is qualified can the sample be transferred to the next process. The traditional manual sampling method is inconvenient. It requires opening the reactor lid to take samples, which makes the sampling process more troublesome. Moreover, it is difficult to take samples at different depths. Summary of the Invention

[0004] The purpose of this invention is to provide a hexadecyl chloride reaction apparatus that can assist in sampling, so as to solve the problems mentioned in the background art.

[0005] To achieve the above objectives, this utility model provides the following technical solution: a hexadecyl chloride reaction apparatus for assisted sampling, comprising a reaction vessel body, a vessel lid, a feeding pipe, a drive motor, and a stirring shaft. The top of the reaction vessel body is covered with a vessel lid, and a feeding pipe and a drive motor are respectively installed on the top of the vessel lid. A stirring shaft is connected to the output shaft of the drive motor. A fixed base and a guide column are respectively connected to the top of the reaction vessel body. A connecting cylinder is connected to the surface of the reaction vessel body near the fixed base and the guide column. A first rubber sealing ring is adhered to the inner wall of the vessel lid near the connecting cylinder. The front part of the fixed base... The device is equipped with a forward and reverse motor. A rotating rod is connected to the output shaft of the forward and reverse motor. A gear is connected to the outer side of the rotating rod. A slider is slidably connected to the outer side of the guide column. An electric sampling pump is connected to the side of the slider near the fixed base. A moving block is connected to the side of the electric sampling pump away from the slider. A toothed plate is connected to the side of the moving block near the fixed base. A sampling tube is connected to the bottom of the electric sampling pump. A delivery pipe is connected to the front of the electric sampling pump. A control valve is connected to the top of the delivery pipe. A storage box is connected to the end of the delivery pipe. A sampler is threadedly connected to the bottom of the storage box.

[0006] Preferably, the gear and the toothed plate form a meshing structure.

[0007] Preferably, the sampling tube movably passes through the first rubber sealing ring, the vessel lid, and the connecting cylinder.

[0008] Preferably, a second sealing ring is bonded to the inside of the sampler, and a support plate is connected to the inside of the sampler near the second sealing ring.

[0009] Preferably, a connecting rod is movably connected between the support plate and the second sealing ring, and one end of the connecting rod is connected to a magnetic block.

[0010] Preferably, a baffle is connected to the end of the connecting rod away from the magnetic block, and a sealing gasket is adhered to the surface of the baffle.

[0011] Compared with the prior art, the beneficial effects of this utility model are:

[0012] 1. The electric sampling pump of this utility model can extract and transport samples from the main body of the reactor into the delivery pipe through the sampling tube. At this time, the control valve is opened to transport the sample inside the delivery pipe to the storage tank. The sample inside the storage tank will flow into the sampler at the bottom of the tank, thus completing the sampling. The bottom position of the sampling tube can be adjusted appropriately according to the actual sampling position, so that samples at different depths inside the main body of the reactor can be sampled, which is convenient for subsequent testing and comparison. Sampling is convenient and does not require opening the reactor lid.

[0013] 2. The baffle and sealing gasket of this utility model can seal the sampler port, so that the sampler can be unscrewed from the bottom of the storage box to prevent the irritating odor of the sample inside the sampler from affecting the health of the staff. Attached Figure Description

[0014] Figure 1 This is a three-dimensional structural diagram of the present invention;

[0015] Figure 2 This is a three-dimensional cross-sectional structural diagram of the main body of the reaction vessel of this utility model;

[0016] Figure 3 This is a three-dimensional cross-sectional structural diagram of the fixing base of this utility model;

[0017] Figure 4 This is a three-dimensional cross-sectional structural diagram of the storage box of this utility model;

[0018] Figure 5 This is a three-dimensional structural diagram of the magnetic block of this utility model.

[0019] In the diagram: 1. Reactor body; 2. Reactor lid; 3. Feeding pipe; 4. Drive motor; 5. Stirring shaft; 6. Fixed base; 7. Guide column; 8. Connecting cylinder; 9. First rubber sealing ring; 10. Forward and reverse motor; 11. Rotating rod; 12. Gear; 13. Sliding block; 14. Electric sampling pump; 15. Moving block; 16. Toothed plate; 17. Sampling pipe; 18. Conveying pipe; 19. Control valve; 20. Storage tank; 21. Sampler; 22. Second sealing ring; 23. Connecting rod; 24. Magnetic block; 25. Baffle; 26. Sealing gasket; 27. Support plate. Detailed Implementation

[0020] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0021] Please see Figures 1-3 It is understood that this utility model provides a technical solution: a chlorohexadecane reaction device that can assist in sampling, including a reaction vessel body 1, a vessel cover 2, a feeding pipe 3, a drive motor 4, and a stirring shaft 5. The top of the reaction vessel body 1 is covered with a vessel cover 2. The top of the vessel cover 2 is respectively installed with a feeding pipe 3 and a drive motor 4. The output shaft of the drive motor 4 is connected to the stirring shaft 5. The top of the reaction vessel body 1 is respectively connected with a fixed seat 6 and a guide column 7. A connecting cylinder 8 is connected to the surface of the reaction vessel body 1 near the fixed seat 6 and the guide column 7. A first rubber sealing ring 9 is adhered to the inner wall of the vessel cover 2 near the connecting cylinder 8. A forward and reverse motor 10 is installed at the front of the fixed seat 6. A rotating rod 11 is connected to the output shaft of the forward and reverse motor 10. A gear 12 is connected to the outer side of the rotating rod 11.

[0022] The first rubber sealing ring 9 of this utility model can improve the sealing performance between the sampling tube 17 and the vessel lid 2.

[0023] exist Figures 1-4 In the middle: a slider 13 is slidably connected to the outer side of the guide column 7. An electric sampling pump 14 is connected to the side of the slider 13 near the fixed seat 6. A moving block 15 is connected to the side of the electric sampling pump 14 away from the slider 13. A toothed plate 16 is connected to the side of the moving block 15 near the fixed seat 6. A sampling tube 17 is connected to the bottom of the electric sampling pump 14. A delivery pipe 18 is connected to the front of the electric sampling pump 14. A control valve 19 is connected to the top of the delivery pipe 18. A storage box 20 is connected to the end of the delivery pipe 18. A sampler 21 is threadedly connected to the bottom of the storage box 20.

[0024] The sampling tube 17 and the delivery tube 18 of this utility model are both made of stainless steel.

[0025] exist Figures 1-3 In the middle: the gear 12 and the toothed plate 16 form a meshing structure, and the sampling tube 17 moves through the first rubber sealing ring 9, the lid 2 and the connecting cylinder 8 respectively.

[0026] The sampling tube 17 and the connecting tube 8 of this utility model form a sliding structure.

[0027] In practice, when sampling and testing of hexadecane inside the reactor body 1 is required, the forward and reverse motor 10 is started. When the forward and reverse motor 10 rotates forward, it drives the rotating rod 11 to rotate through the output shaft, thereby driving the gear 12 to rotate. In turn, the gear plate 16 moves through meshing. When the gear plate 16 moves, it drives the moving block 15 to move, thereby driving the electric sampling pump 14 to move towards the surface of the reactor cover 2. This causes the slider 13 to slide against the guide column 7. At the same time, the electric sampling pump 14 moves the sampling tube 17 and the delivery tube 18. When the sampling tube 17 moves, it can slide against the connecting cylinder 8 and the first rubber sealing ring 9. When the bottom end of the sampling tube 17 moves to the designated position inside the reactor body 1, the electric sampling pump 14 can be started, so that the electric sampling pump 14 can extract and deliver the sample from the reactor body 1 to the delivery tube 18 through the sampling tube 17. At this time, the control valve 19 is opened, so that the sample inside the delivery tube 18 can be delivered to the storage tank 20.

[0028] See Figures 1-4 It is known that the sample inside the storage tank 20 will flow into the sampler 21 at its bottom to complete the sampling. The bottom position of the sampling tube 17 can be adjusted appropriately according to the actual sampling position, so that samples at different depths inside the reactor body 1 can be sampled, which is convenient for subsequent testing and comparison. Sampling is convenient and does not require opening the reactor lid 2.

[0029] exist Figures 1-5 In the sampler 21, a second sealing ring 22 is bonded to the inside. A support plate 27 is connected to the sampler 21 near the second sealing ring 22. A connecting rod 23 is connected between the support plate 27 and the second sealing ring 22. A magnetic block 24 is connected to one end of the connecting rod 23.

[0030] The magnetic block 24 and the sampler 21 of this utility model form a magnetic attraction structure.

[0031] exist Figure 4 and Figure 5 In the middle: the end of the connecting rod 23 away from the magnetic block 24 is connected to a baffle 25, and a sealing gasket 26 is adhered to the surface of the baffle 25.

[0032] The sealing gasket 26 of this utility model can improve the sealing performance between the baffle 25 and the port of the sampler 21.

[0033] In practice, after the sample has completely flowed from the storage box 20 into the sampler 21, the magnetic block 24 can be pushed towards the sampler 21. When the magnetic block 24 moves, it drives the connecting rod 23 to move. When the connecting rod 23 moves, it can slide with the second sealing ring 22 and the support plate 27. The connecting rod 23 also drives the baffle 25 and the sealing gasket 26 to move. When the baffle 25 and the sealing gasket 26 move below the port of the sampler 21, one side of the magnetic block 24 can move to the outer surface of the sampler 21. The sampler 21 is made of iron, so that the magnetic block 24 can be attracted to the outside of the sampler 21.

[0034] See Figures 1-5 It is known that the baffle 25 and the sealing gasket 26 can seal the port of the sampler 21, so that the sampler 21 can be unscrewed from the bottom of the storage box 20 to prevent the irritating smell of the sample inside the sampler 21 from affecting the health of the staff.

[0035] In summary, when this utility model is in use, the forward and reverse motor 10 rotates forward, driving the rotating rod 11 to rotate via the output shaft, which in turn drives the gear 12 to rotate, and then drives the toothed plate 16 to move through meshing. The sample inside the storage tank 20 will flow into the sampler 21 at its bottom, thus completing the sampling. The bottom position of the sampling tube 17 can be appropriately adjusted according to the actual sampling position, so that samples at different depths inside the reactor body 1 can be sampled, which is convenient for subsequent testing and comparison. Sampling is convenient, without opening the reactor lid 2. The baffle 25 and the sealing gasket 26 can seal the port of the sampler 21, so that the sampler 21 can be unscrewed from the bottom of the storage tank 20 to prevent the irritating smell of the sample inside the sampler 21 from affecting the health of the staff. The contents not described in detail in this description are existing technologies known to those skilled in the art.

[0036] Although the present invention has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present invention should be included within the protection scope of the present invention.

Claims

1. A hexadecyl chloride reaction apparatus for assisted sampling, comprising a reaction vessel body (1), a vessel cover (2), a feeding pipe (3), a drive motor (4), and a stirring shaft (5), characterized in that: The reactor body (1) is covered with a lid (2), and a feeding pipe (3) and a drive motor (4) are respectively installed on the top of the lid (2). A stirring shaft (5) is connected to the output shaft of the drive motor (4). The top of the reactor body (1) is connected to a fixed base (6) and a guide column (7). A connecting cylinder (8) is connected to the surface of the reactor body (1) near the fixed base (6) and the guide column (7). A first rubber sealing ring (9) is bonded to the inner wall of the reactor cover (2) near the connecting cylinder (8). A forward and reverse motor (10) is installed at the front of the fixed base (6). A rotating rod (11) is connected to the output shaft of the forward and reverse motor (10). A gear (12) is connected to the outer side of the rotating rod (11). A slider (13) is slidably connected to the outer side of the guide column (7). The slider (13) is close to... An electric sampling pump (14) is connected to one side of the fixed base (6). A moving block (15) is connected to the side of the electric sampling pump (14) away from the slider (13). A toothed plate (16) is connected to the side of the moving block (15) close to the fixed base (6). A sampling tube (17) is connected to the bottom of the electric sampling pump (14). A delivery pipe (18) is connected to the front of the electric sampling pump (14). A control valve (19) is connected to the top of the delivery pipe (18). A storage box (20) is connected to the end of the delivery pipe (18). A sampler (21) is threadedly connected to the bottom of the storage box (20).

2. The hexadecyl chloride reaction apparatus with assisted sampling according to claim 1, characterized in that: The gear (12) and the toothed plate (16) form a meshing structure.

3. The hexadecyl chloride reaction apparatus with assisted sampling according to claim 1, characterized in that: The sampling tube (17) movably passes through the first rubber sealing ring (9), the kettle lid (2), and the connecting tube (8).

4. The hexadecyl chloride reaction apparatus with assisted sampling according to claim 1, characterized in that: The sampler (21) has a second sealing ring (22) bonded inside, and a support plate (27) is connected inside the sampler (21) near the second sealing ring (22).

5. The hexadecyl chloride reaction apparatus with assisted sampling according to claim 4, characterized in that: A connecting rod (23) is movably connected between the support plate (27) and the second sealing ring (22), and one end of the connecting rod (23) is connected to a magnetic block (24).

6. The hexachlorohexadecane reaction apparatus with assisted sampling according to claim 5, characterized in that: The end of the connecting rod (23) away from the magnetic block (24) is connected to a baffle (25), and a sealing gasket (26) is adhered to the surface of the baffle (25).

Images