Asahi collagen king firming and Anti-aging essence capable of converting from solid to liquid and preparation method thereof

Abstract

To provide a plant extract essence having excellent anti-aging effect, and to provide a method for preparing the same.SOLUTION: The present invention relates to the field of cosmetics technology, in particular to ASAHI collagen king firming and anti-aging essence capable of converting from solid to liquid and to a method for preparing the same. Specifically, it includes mannitol, ASAHI collagen, biopolysaccharide gum, panthenol, trehalose, niacinamide, xanthan gum, 1,3-butylene glycol, sodium hyaluronate, ergothioneine, glycerin, honey, truffle extract, Centella asiatica extract, Lactobacillus culture lysate, tissue recombinant collagen peptide, pullulan and water. The solid-to-liquid convertible beauty essence product provided by the present invention has excellent anti-aging and firming effects and can obviously improve skin quality.SELECTED DRAWING: None

Description

[Technical field]

[0001] The present invention relates to the field of cosmetics technology, in particular to ASAHI Collagen King Firming & Anti-Aging Essence which can be converted from solid to liquid and its preparation method. [Background technology]

[0002] Although conventional skin care products with anti-aging and repair effects exist in various forms, their wrinkle improvement and anti-aging effects are not ideal and cannot meet the needs of consumers. The reason is that conventional anti-aging and anti-aging products all contain artificially synthesized active ingredients, such as peptide-based anti-aging and acetylated hexapeptides in anti-aging ingredients, which essentially suppress the occurrence of facial wrinkles and fine lines by blocking the transmission speed of muscle nerves, and such active ingredients often cause dependency after use, and if not used, the skin will return to its original state, and the skin will deteriorate because they have no effect of nourishing or conditioning the skin itself.

[0003] Some skin care products contain plant extracts, which have the advantage of being safe and having no side effects. However, the effectiveness of skin care products varies greatly depending on the plant composition, and the extraction method also results in significant differences in the extraction of active ingredients from plants. The active ingredients contained in the extracts have a significant impact on the effectiveness of skin care products.

[0004] Therefore, providing a plant extract having excellent anti-aging effects and further improving the use effect of anti-aging peptides are problems that must be solved as soon as possible by those skilled in the art. Summary of the Invention [Problem to be solved by the invention]

[0005] The object of the present invention is to provide an ASAHI Collagen King Firming & Anti-Aging Essence that can be converted from solid to liquid and its preparation method. [Means for solving the problem]

[0006] In order to achieve the above objectives, the present invention provides the following technical solutions:

[0007] The present invention provides an ASAHI Collagen King Tightening & Anti-Aging Essence that can be converted from a solid to a liquid, which is prepared from ingredients including 2 to 4 parts by mass of mannitol, 2 to 8 parts by mass of ASAHI collagen, 0.02 to 0.04 parts by mass of biopolysaccharide gum, 0.2 to 0.4 parts by mass of panthenol, 1 to 3 parts by mass of trehalose, 2 to 4 parts by mass of niacinamide, 0.1 to 0.3 parts by mass of xanthan gum, 1 to 3 parts by mass of 1,3-butylene glycol, 0.1 to 0.3 parts by mass of sodium hyaluronate, 0.4 to 0.6 parts by mass of ergothioneine, 2 to 4 parts by mass of glycerin, 3 to 20 parts by mass of honey, 0.4 to 0.6 parts by mass of truffle extract, 0.4 to 0.6 parts by mass of Centella asiatica extract, 1 to 3 parts by mass of lactobacillus culture lysate, 0.4 to 0.6 parts by mass of tissue recombinant collagen peptide, 0.4 to 0.6 parts by mass of pullulan, and 60 to 80 parts by mass of water.

[0008] Preferably, the method for preparing the truffle extract and the Centella asiatica extract comprises the steps of: 1) Mixing truffles and Centella asiatica with an extractant and then extracting to obtain a crude truffle extract and a crude Centella asiatica extract; 2) Mix the crude truffle extract and crude Centella asiatica extract with glyceryl tristearate respectively, stir, adjust the pH to neutral, and sterilize to obtain the truffle extract and Centella asiatica extract.

[0009] Preferably, the mass ratio of the truffle and Centella asiatica to the extractant described in step 1) is 1:20-30.

[0010] Preferably, the extractant described in step 1) is propylene glycol and n-butanol, and the volume ratio is 2-6:15-19.

[0011] Preferably, the volume concentration of the propylene glycol is 40 to 50%, and the volume concentration of the n-butanol is 40 to 50%.

[0012] Preferably, the extraction time described in step 1) is 1 to 3 hours.

[0013] Preferably, the mass ratio of the crude truffle extract and crude Centella asiatica extract to glyceryl tristearate described in step 2) is 30-40:2-4.

[0014] The present invention relates to Step (1) of mixing water and xanthan gum and stirring them first at 65 to 75°C to obtain material 1; (2) cooling the material 1 to 35 to 40°C, adding 1,3-butylene glycol, panthenol, trehalose, niacinamide, honey, sodium hyaluronate and glycerin, and stirring the mixture a second time to obtain a material 2; and (3) cooling the material 2 to room temperature, adding mannitol, ASAHI collagen, bio-polysaccharide gum, ergothioneine, truffle extract, Centella asiatica extract, Lactobacillus culture lysate, tissue recombinant collagen peptide and pullulan, and homogenizing to obtain the solid-to-liquid convertible ASAHI collagen king firming & anti-aging essence.

[0015] Preferably, the rotation speeds of the primary stirring and secondary stirring are both 200 to 300 r / min, and the times of the primary stirring and secondary stirring are both 15 to 25 minutes.

[0016] Preferably, the homogenization speed in step (3) is 1000-2000 r / min, and the homogenization time is 3-7 min. Effect of the Invention

[0017] Compared with the prior art, the present invention has the following beneficial effects:

[0018] 1. The ASAHI Collagen King Tightening & Anti-Aging Essence, which can be converted from solid to liquid, provided by the present invention has excellent anti-aging & tightening effects. By extracting active ingredients from specific plants and applying them to the essence, the anti-aging and firming effects of the essence can be safely realized, and the combination of each ingredient can nourish the skin itself, essentially realize the anti-aging and firming effects, and obviously improve the skin quality.

[0019] 2. The trehalose, mannitol and panthenol added in the present invention can maintain the moisture of the skin, accelerate the moisture absorption of the skin, form a moisture protective film, effectively lock in the moisture, and make the skin more moist.

[0020] Biopolysaccharide gum is rich in natural physiological water and minerals and has high penetration power, and butanediol has a water-retaining and moisturizing effect on the skin, so the addition of the above ingredients has an excellent hydrating effect, thereby suppressing the occurrence of wrinkles and improving fine lines.

[0021] Sodium hyaluronate can improve skin elasticity and radiance by absorbing water, increasing volume, and moisturizing the inside of the skin. Sodium hyaluronate can also stimulate the growth of collagen and elastic fibers, and promote the repair and regeneration of skin tissue.

[0022] Niacinamide promotes skin cell turnover, while ergothioneine helps slow the skin aging process with its powerful antioxidant properties. The ingredients mentioned above reduce damage to the skin caused by free radicals, thereby reducing signs of aging such as wrinkles and pigmentation.

[0023] Truffle extract is rich in various amino acids, vitamins, unsaturated fatty acids and other nutrients, which can enhance the antioxidant ability of the skin and promote the elimination of free radicals in the body, thereby achieving the effects of anti-aging and strengthening skin elasticity.

[0024] Centella asiatica extract not only has the effect of replenishing collagen, but also has the effects of removing acne scars, anti-inflammatory and soothing. It can tighten the junction between the epidermis and dermis, soften the skin, beneficent for dealing with sagging skin, make the skin smooth and stretchy, promote the formation of collagen powder in the dermis layer, regenerate free fatty acids, recombine, tighten and smooth the skin respectively.

[0025] Lactobacillus culture lysate contains bacteria and all the active ingredients synthesized in the fermentation process, including peptide polyglucose, teichoic acid, protein, phospholipid, sterol, fatty acid, various enzymes, peptide, amino acid, nucleotide, extracellular polysaccharide, etc., which can provide rich nutrition to the skin, promote the rate of cell metabolism, rapidly regenerate skin cells, inhibit melanin deposition, and effectively improve the formation of freckles, age spots, etc., and continuous use of Lactobacillus can make the skin whiter and more transparent.

[0026] ASAHI Collagen and tissue-engineered collagen peptides maximize the effects of collagen, improving skin conditions in many ways, leading to plump, firm, clear, soft, moisturized, and elastic skin. Honey can moisturize the skin, making it more delicate and smooth.

[0027] Pullulan has adhesive, sticky, degradable and spinnable properties, and its main function is as a film-forming agent. When combined with xanthan gum, it will first form a colloidal mask on the face when using the essence, and then wait for another 20 minutes until the colloidal mask on the face disappears, indicating that the essence has been completely absorbed into the skin and the skin care process is completed.

[0028] As can be seen from the above, among the ingredients added in the present invention, trehalose, mannitol, and panthenol can lock moisture in the skin, trehalose, mannitol, panthenol, and sodium hyaluronate can replenish moisture in the skin, lactobacillus culture lysate, ergothioneine, and niacinamide can repair damaged skin cells, and truffle extract and Centella asiatica extract, combined with tissue recombinant collagen peptide, play a major anti-aging role. Honey moisturizes the skin. Pullulan and xanthan gum play a film-forming role. The combination of various ingredients in the present invention achieves the technical effects of anti-aging, tightening, and hydration. DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS

[0029] The present invention provides an ASAHI Collagen King Tightening & Anti-Aging Essence that can be converted from a solid to a liquid, which is prepared from ingredients including 2 to 4 parts by mass of mannitol, 2 to 8 parts by mass of ASAHI collagen, 0.02 to 0.04 parts by mass of biopolysaccharide gum, 0.2 to 0.4 parts by mass of panthenol, 1 to 3 parts by mass of trehalose, 2 to 4 parts by mass of niacinamide, 0.1 to 0.3 parts by mass of xanthan gum, 1 to 3 parts by mass of 1,3-butylene glycol, 0.1 to 0.3 parts by mass of sodium hyaluronate, 0.4 to 0.6 parts by mass of ergothioneine, 2 to 4 parts by mass of glycerin, 3 to 20 parts by mass of honey, 0.4 to 0.6 parts by mass of truffle extract, 0.4 to 0.6 parts by mass of Centella asiatica extract, 1 to 3 parts by mass of lactobacillus culture lysate, 0.4 to 0.6 parts by mass of tissue recombinant collagen peptide, 0.4 to 0.6 parts by mass of pullulan, and 60 to 80 parts by mass of water.

[0030] Preferably, it is prepared from ingredients including the following mass parts: 3 parts of mannitol, 3 to 7 parts of ASAHI collagen, 0.03 parts of biopolysaccharide gum, 0.3 parts of panthenol, 2 parts of trehalose, 3 parts of niacinamide, 0.2 parts of xanthan gum, 2 parts of 1,3-butylene glycol, 0.2 parts of sodium hyaluronate, 0.5 parts of ergothioneine, 3 parts of glycerin, 4 parts of honey, 0.5 parts of truffle extract, 0.5 parts of Centella asiatica extract, 2 parts of Lactobacillus culture lysate, 0.5 parts of tissue recombinant collagen peptide, 0.5 parts of pullulan, and 65 to 75 parts of water.

[0031] More preferably, it is prepared from ingredients including, by mass, 3 parts of mannitol, 5 parts of ASAHI collagen, 0.03 parts of biopolysaccharide gum, 0.3 parts of panthenol, 2 parts of trehalose, 3 parts of niacinamide, 0.2 parts of xanthan gum, 2 parts of 1,3-butylene glycol, 0.2 parts of sodium hyaluronate, 0.5 parts of ergothioneine, 3 parts of glycerin, 4 parts of honey, 0.5 parts of truffle extract, 0.5 parts of Centella asiatica extract, 2 parts of Lactobacillus culture lysate, 0.5 parts of tissue recombinant collagen peptide, 0.5 parts of pullulan, and 70 parts of water.

[0032] In the present invention, the method for preparing the truffle extract and the Centella asiatica extract comprises the steps of: 1) Mixing truffles and Centella asiatica with an extractant and then extracting to obtain a crude truffle extract and a crude Centella asiatica extract; 2) Mix the crude truffle extract and crude Centella asiatica extract with glyceryl tristearate respectively, stir, adjust the pH to neutral, and sterilize to obtain the truffle extract and Centella asiatica extract.

[0033] In the present invention, the mass ratio of truffle and Centella to the extractant described in step 1) is 1:20-30, preferably 1:22-28, more preferably 1:24-26, and even more preferably 1:25.

[0034] In the present invention, the extractant in step 1) is propylene glycol and n-butanol, and the volume ratio is 2-6:15-19, preferably 3-5:16-18, more preferably 4:16-18, and further preferably 4:17.

[0035] In the present invention, the volume concentration of the propylene glycol is 40 to 50%, preferably 42 to 48%, more preferably 44 to 46%, and further preferably 45%.

[0036] In the present invention, the volume concentration of the n-butanol is 40 to 50%, preferably 42 to 48%, more preferably 44 to 46%, and further preferably 45%.

[0037] In the present invention, the extraction time described in step 1) is 1 to 3 hours, preferably 2 hours.

[0038] In the present invention, the mass ratio of the crude truffle extract and crude Centella asiatica extract to glyceryl tristearate described in step 2) is 30-40:2-4, preferably 32-38:2-4, more preferably 35:2-4, and even more preferably 35:3.

[0039] The present invention relates to Step (1) of mixing water and xanthan gum and stirring them first at 65 to 75°C to obtain material 1; (2) cooling the material 1 to 35 to 40°C, adding 1,3-butylene glycol, panthenol, trehalose, niacinamide, honey, sodium hyaluronate and glycerin, and stirring the mixture a second time to obtain a material 2; and (3) cooling the material 2 to room temperature, adding mannitol, ASAHI collagen, bio-polysaccharide gum, ergothioneine, truffle extract, Centella asiatica extract, Lactobacillus culture lysate, tissue recombinant collagen peptide and pullulan, and homogenizing to obtain the solid-to-liquid convertible ASAHI collagen king firming & anti-aging essence.

[0040] In the present invention, in step (1), the materials are mixed preferably at 67 to 73°C, more preferably at 69 to 71°C, and even more preferably at 70°C.

[0041] In the present invention, in step (2), the material 1 is cooled to preferably 36 to 39°C, more preferably 37°C.

[0042] In the present invention, the rotation speeds of the primary stirring and secondary stirring are both 200 to 300 r / min, preferably 220 to 280 r / min, more preferably 240 to 260 r / min, and further preferably 250 r / min.

[0043] In the present invention, the time for each of the primary stirring and secondary stirring is 15 to 25 minutes, preferably 17 to 23 minutes, more preferably 19 to 21 minutes, and further preferably 20 minutes.

[0044] In the present invention, the homogenization speed described in step (3) is 1000 to 2000 r / min, preferably 1200 to 1800 r / min, more preferably 1400 to 1600 r / min, and further preferably 1500 r / min.

[0045] In the present invention, the homogenization time described in step (3) is 3 to 7 minutes, preferably 4 to 6 minutes, and more preferably 5 minutes.

[0046] The technical solutions provided by the present invention are described in detail below with reference to the following examples.

[0047] Ingredients used in the present invention: mannitol is purchased from Mol Biological Technology Co., Ltd., biopolysaccharide gum (powder), tissue recombinant collagen peptide is purchased from Shanghai Yadai Biological Technology Co., Ltd., Lactobacillus culture lysate is purchased from Shanghai Yanfu Industry Co., Ltd., and ergothioneine is purchased from Shanxi Lishen Biological Technology Co., Ltd. EXAMPLES

[0048] A preparation method for ASAHI Collagen King Firming & Anti-Aging Essence, which can be converted from solid to liquid, comprising the steps of:

[0049] (1) The extractant was obtained by mixing 40% propylene glycol and 50% n-butanol in a volume ratio of 2:15.

[0050] (2) Truffles and Centella asiatica were mixed with an extractant in a mass ratio of 1:20, and then extracted for 1 hour. The filtrates were then filtered through a 0.45 μm microfiltration membrane, and the filtrates were truffle crude extract and Centella asiatica crude extract.

[0051] (3) In an environment of 55℃, the truffle crude extract and the Centella asiatica crude extract were mixed with glyceryl tristearate in a mass ratio of 30:2, respectively, and stirred at 150 r / min for 10 min., adjusted to a neutral pH, and sterilized at 105℃ for 20 s to obtain the truffle extract and the Centella asiatica extract.

[0052] (4) 60 parts of water and 0.1 parts of xanthan gum were mixed at 65°C and stirred at 200 rpm for 15 minutes to obtain material 1.

[0053] (5) The material 1 was cooled to 35°C, and 1 part of 1,3-butylene glycol, 0.2 parts of panthenol, 1 part of trehalose, 2 parts of niacinamide, 8 parts of honey, 0.1 parts of sodium hyaluronate, and 2 parts of glycerin were added thereto, and the mixture was stirred at 200 r / min for 15 minutes to obtain material 2.

[0054] (6) The material 2 was cooled to room temperature, and 2 parts of mannitol, 2 parts of ASAHI collagen, 0.02 parts of biopolysaccharide gum, 0.4 parts of ergothioneine, 0.4 parts of truffle extract, 0.4 parts of Centella asiatica extract, 1 part of Lactobacillus culture lysate, 0.4 parts of tissue recombinant collagen peptide, and 0.4 parts of pullulan were added, and the mixture was homogenized at 1000 r / min for 3 minutes to obtain ASAHI Collagen King Tightening & Anti-Aging Essence, which can be converted from solid to liquid.

[0055] (7) When in use, the solid-to-liquid convertible ASAHI Collagen King firming & anti-aging essence is first applied to the mask base fabric to obtain the solid-to-liquid convertible ASAHI Collagen King firming & anti-aging mask, and then the skin care process is carried out. EXAMPLES

[0056] A preparation method for ASAHI Collagen King Firming & Anti-Aging Essence, which can be converted from solid to liquid, comprising the steps of:

[0057] (1) The extractant was obtained by mixing 50% propylene glycol and 50% n-butanol in a volume ratio of 6:19.

[0058] (2) Truffles and Centella asiatica were mixed with an extractant in a mass ratio of 1:30, and then extracted for 3 hours. The filtrates were then filtered through a 0.45 μm microfiltration membrane, and the filtrates were truffle crude extract and Centella asiatica crude extract.

[0059] (3) In an environment of 60℃, the truffle crude extract and the Centella asiatica crude extract were mixed with glyceryl tristearate in a mass ratio of 40:4, respectively, and stirred at 250 r / min for 20 min., adjusted to neutral pH, and sterilized at 106℃ for 22 s to obtain the truffle extract and the Centella asiatica extract.

[0060] (4) 80 parts of water and 0.3 parts of xanthan gum were mixed at 75°C and stirred at 300 rpm for 25 minutes to obtain material 1.

[0061] (5) The material 1 was cooled to 40°C, and 3 parts of 1,3-butylene glycol, 0.4 parts of panthenol, 3 parts of trehalose, 4 parts of niacinamide, 5 parts of honey, 0.3 parts of sodium hyaluronate, and 4 parts of glycerin were added thereto, and the mixture was stirred at 300 r / min for 25 minutes to obtain material 2.

[0062] (6) The material 2 was cooled to room temperature, and 4 parts of mannitol, 8 parts of ASAHI collagen, 0.04 parts of biopolysaccharide gum, 0.6 parts of ergothioneine, 0.6 parts of truffle extract, 0.6 parts of Centella asiatica extract, 3 parts of Lactobacillus culture lysate, 0.6 parts of tissue recombinant collagen peptide, and 0.6 parts of pullulan were added, and the mixture was homogenized at 2000 r / min for 7 minutes to obtain ASAHI Collagen King Tightening & Anti-Aging Essence, which can be converted from solid to liquid.

[0063] (7) When in use, the solid-to-liquid convertible ASAHI Collagen King firming & anti-aging essence is first applied to the mask base fabric to obtain the solid-to-liquid convertible ASAHI Collagen King firming & anti-aging mask, and then the skin care process is carried out. EXAMPLES

[0064] A preparation method for ASAHI Collagen King Firming & Anti-Aging Essence, which can be converted from solid to liquid, comprising the steps of:

[0065] (1) The extractant was obtained by mixing 45% propylene glycol and 45% n-butanol in a volume ratio of 4:17.

[0066] (2) Truffles and Centella asiatica were mixed with an extractant in a mass ratio of 1:25, and then extracted for 2 hours. The mixture was then filtered through a 0.45 μm microfiltration membrane, and the filtrate was obtained as truffle crude extract and Centella asiatica crude extract.

[0067] (3) In an environment of 57℃, the truffle crude extract and the Centella asiatica crude extract were mixed with glyceryl tristearate in a mass ratio of 35:3, respectively, and stirred at 200 r / min for 15 min., adjusted to a neutral pH, and sterilized at 105℃ for 20 s to obtain the truffle extract and the Centella asiatica extract.

[0068] (4) 70 parts of water and 0.2 parts of xanthan gum were mixed at 70°C and stirred at 250 rpm for 20 minutes to obtain material 1.

[0069] (5) The material 1 was cooled to 37°C, and 2 parts of 1,3-butylene glycol, 0.3 parts of panthenol, 2 parts of trehalose, 3 parts of niacinamide, 4 parts of honey, 0.2 parts of sodium hyaluronate, and 3 parts of glycerin were added thereto, and the mixture was stirred at 250 r / min for 20 minutes to obtain material 2.

[0070] (6) The material 2 was cooled to room temperature, and 3 parts of mannitol, 5 parts of ASAHI collagen, 0.03 parts of biopolysaccharide gum, 0.5 parts of ergothioneine, 0.5 parts of truffle extract, 0.5 parts of Centella asiatica extract, 2 parts of Lactobacillus culture lysate, 0.5 parts of tissue recombinant collagen peptide, and 0.5 parts of pullulan were added, and the mixture was homogenized at 1500 r / min for 5 minutes to obtain ASAHI Collagen King Tightening & Anti-Aging Essence, which can be converted from solid to liquid.

[0071] (7) When in use, the solid-to-liquid convertible ASAHI Collagen King firming & anti-aging essence is first applied to the mask base fabric to obtain the solid-to-liquid convertible ASAHI Collagen King firming & anti-aging mask, and then the skin care process is carried out.

[0072] Experimental Example 1 1. Test subjects: A total of 140 female volunteers were selected and divided into seven groups with an average of 20 participants in each group. Their age range was 30-40 years old.

[0073] 2, How to use: The volunteers used the corresponding products once a day after cleansing their faces. The tests were carried out on the 10th and 20th days, respectively.

[0074] 3, Test equipment: Changes in the skin quality of the volunteers were measured using VISIA-CR (Facial Skin Image Analysis Device), which can evaluate the degree of reduction in wrinkle depth and length. The average test results are shown in Table 1.

[0075] The skin elasticity of both cheeks of the volunteers was tested using a skin tester (Derma-Expert MC760), and the average test results are shown in Table 2.

[0076] 4. Experimental grouping The product obtained by the method of Example 3 is the experimental group.

[0077] Control group 1: other methods are the same as in Example 3, the only difference is that no truffle extract or Centella asiatica extract was added.

[0078] Control group 2: other methods were the same as in Example 3, with the only difference being that truffle extract was replaced with commercially available truffle extract (Shanghai Yadai Biotechnology Co., Ltd.) and Centella asiatica extract (Shanghai Zhuoding Biology).

[0079] Control group 3: other methods are the same as in Example 3, the only difference is that no truffle extract was added.

[0080] Control group 4: other methods were the same as in Example 3, with the only difference being that no tissue recombinant collagen peptide was added.

[0081] Control group 5: other methods were the same as in Example 3, the only difference being that no ergothioneine was added.

[0082] The usage method for the experimental group and control groups 1 to 5 is as follows: after cleansing the face, apply the ASAHI Collagen King Firming & Anti-Aging Mask, which can be converted from solid to liquid, to the face, remove the mask base cloth, and the essence will form a "colloid mask" on the face. After waiting for another 10 minutes, when the "colloid mask" on the face disappears, it indicates that the essence has been completely absorbed into the skin and the skin care process is completed.

[0083] Prior art group: POLA Anti-Aging Essence (use according to the instructions).

[0084] [Table 1]

[0085] [Table 2]

[0086] As can be seen from the contents of Tables 1 and 2, the solid-to-liquid converting beauty serum product provided by the present invention has excellent anti-aging effects, and the reduction in skin surface wrinkles, the reduction in average wrinkle volume, and the increase in skin elasticity value are equivalent to the effects of using the products of the prior art.

[0087] As can be seen from the data of the control group, the truffle extract and Centella asiatica extract prepared by the method of the present invention also have excellent anti-aging effects, and their absence has a significant impact on the efficacy of the product. Whether or not tissue recombinant collagen peptide and ergothioneine are used also has a significant impact on the efficacy of the product.

[0088] It should be noted that the above description is merely a preferred embodiment of the present invention, and those skilled in the art may make some improvements and modifications without departing from the principles of the present invention, and these improvements and modifications should also be considered as within the scope of the claims of the present invention.

Claims

1. The composition is prepared from components including 2-4 parts by mass of mannitol, 2-8 parts by mass of ASAHI collagen, 0.02-0.04 parts by mass of biopolysaccharide gum, 0.2-0.4 parts by mass of panthenol, 1-3 parts by mass of trehalose, 2-4 parts by mass of niacinamide, 0.1-0.3 parts by mass of xanthan gum, 1-3 parts by mass of 1,3-butylene glycol, 0.1-0.3 parts by mass of sodium hyaluronate, 0.4-0.6 parts by mass of ergothioneine, 2-4 parts by mass of glycerin, 3-20 parts by mass of honey, 0.4-0.6 parts by mass of truffle extract, 0.4-0.6 parts by mass of Centella asiatica extract, 1-3 parts by mass of Lactobacillus culture lysate, 0.4-0.6 parts by mass of tissue recombinant collagen peptide, 0.4-0.6 parts by mass of pullulan, and 60-80 parts by mass of water. ASAHI Collagen King Firming & Anti-Aging Essence is characterized by its ability to be converted from solid to liquid.

2. The method for preparing the truffle extract and the Centella asiatica extract comprises: 1) Mixing truffles and Centella asiatica with an extractant and then extracting to obtain a crude truffle extract and a crude Centella asiatica extract; 2) Mixing the crude truffle extract and crude Centella asiatica extract with glyceryl tristearate, stirring, adjusting the pH to neutral, and sterilizing to obtain the truffle extract and Centella asiatica extract; 2. The solid-to-liquid convertible ASAHI Collagen King Firming & Anti-Aging Essence according to claim 1.

3. The mass ratio of the truffle and Centella asiatica to the extractant described in step 1) is 1:20-30; 3. The solid-to-liquid convertible ASAHI Collagen King Firming & Anti-Aging Essence according to claim 2.

4. The extractant described in step 1) is propylene glycol and n-butanol, and the volume ratio is 2-6:15-19; 3. The solid-to-liquid convertible ASAHI Collagen King Firming & Anti-Aging Essence according to claim 2.

5. The volume concentration of the propylene glycol is 40 to 50%, and the volume concentration of the n-butanol is 40 to 50%.

5. The solid-to-liquid convertible ASAHI Collagen King Firming & Anti-Aging Essence according to claim 4.

6. The extraction time described in step 1) is 1 to 3 h; 2. The solid-to-liquid convertible ASAHI Collagen King Firming & Anti-Aging Essence according to claim 1.

7. The mass ratio of the crude truffle extract and the crude Centella asiatica extract to glyceryl tristearate described in step 2) is 30-40:2-4.

2. The solid-to-liquid convertible ASAHI Collagen King Firming & Anti-Aging Essence according to claim 1.

8. A method for preparing the solid-to-liquid convertible ASAHI Collagen King Firming & Anti-Aging Essence according to any one of claims 1 to 7, comprising: Step (1) of mixing water and xanthan gum and stirring them first under a condition of 65 to 75°C to obtain material 1; (2) cooling the material 1 to 35-40°C, adding 1,3-butylene glycol, panthenol, trehalose, niacinamide, honey, sodium hyaluronate and glycerin, and stirring the mixture to obtain a material 2; and (3) cooling the material 2 to room temperature, adding mannitol, ASAHI collagen, bio-polysaccharide gum, ergothioneine, truffle extract, Centella asiatica extract, Lactobacillus culture lysate, tissue recombinant collagen peptide and pullulan, and homogenizing to obtain ASAHI collagen king firming & anti-aging essence which can be converted from solid to liquid. A preparation method comprising the steps of:

9. The rotation speed of the primary stirring and the secondary stirring are both 200 to 300 r / min, and the time of the primary stirring and the secondary stirring are both 15 to 25 min. The method for preparing ASAHI Collagen King Firming & Anti-Aging Essence convertible from solid to liquid according to claim 8.

10. The homogenization speed in step (3) is 1000-2000 r / min, and the homogenization time is 3-7 min; The method for preparing ASAHI Collagen King Firming & Anti-Aging Essence convertible from solid to liquid according to claim 8.

Images