The invention discloses a preparation method of a
vanadium-doped nanometer
tungsten oxide material and application of the preparation method. The preparation method is characterized by comprising the following steps: putting 4-10 parts of a
tungsten hexachloride solution with the concentration being 0.2-0.3mol / L in a
polytetrafluoroethylene reactor, adding 12-20 parts of secondary
distilled water, and stirring to enable the
tungsten hexachloride solution and the secondary
distilled water to be fully dissolved; adding 1-10 parts of a
sodium metavanadate solution with the concentration being 0.06-0.6mmol / L in the solution, continuously stirring, and fully mixing; then adding 1-5 parts of a
hydrochloric acid solution with the concentration being 2-4mol / L and 28-35 parts of an
ammonium sulfate solution with the concentration being 0.4-0.5mol / L in the
polytetrafluoroethylene reactor, and stirring for 0.5-1h; sealing the
polytetrafluoroethylene reactor, putting in a program oven with the temperature raising rate and the temperature falling rate being 1-2 DEG C / min, and carrying out hydro-
thermal treatment at the temperature of 150-200 DEG C for 24-48h; taking out the reactor, and cooling to
room temperature; and washing reaction products with
distilled water until neutral, putting the reaction products in an oven with the temperature being 80-100 DEG C, and
drying the reaction products for 24-48h to obtain the
vanadium-doped nanometer
tungsten oxide material.