A method for synthesizing glycerol polyoxyethylene ether fatty acid ester

By controlling the reaction conditions of glycerol polyoxyethylene ether and natural oils, a glycerol polyoxyethylene ether fatty acid ester with a good hydrophilic-lipophilic balance was prepared, which solved the problem of product instability or ineffective adhesion in the prior art and achieved the skin moisturizing and hydrating effects in personal care products.

CN115650846BActive Publication Date: 2026-02-03SINOLIGHT SURFACTANTS TECH CO LTD
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Patent Information

Application Number
CN202211082875.1
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2022-09-06
Publication Date
2026-02-03
Estimated Expiration
2042-09-06

AI Technical Summary

Technical Problem

Existing glycerol polyoxyethylene ether fatty acid ester synthesis technology fails to effectively control the hydrophilic-lipophilic balance of the product, resulting in the product being unstable in water or unable to effectively adhere to the skin or hair, affecting the skin moisturizing and hydrating effects, and domestic production relies on imports.

Method used

Using glycerol polyoxyethylene ether and natural oils in a molar ratio of 3:1 as raw materials, the reaction was carried out under the action of an alkaline catalyst. By controlling the reaction conditions such as temperature, time and catalyst dosage, and selecting appropriate EO addition number and catalyst type, glycerol polyoxyethylene ether fatty acid esters were prepared.

Benefits of technology

A glycerol polyoxyethylene ether fatty acid ester with a good hydrophilic-lipophilic balance was prepared, forming a stable nanomicelle system suitable for personal care products and cosmetics, achieving skin moisturizing and hydrating effects.

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Abstract

The application discloses a synthesis method of glycerin polyoxyethylene ether fatty acid ester, which comprises the following steps: taking glycerin polyoxyethylene ether and natural oil with a molar ratio of 3:1 as raw materials, and under the action of an alkaline catalyst, the mass percentage content of the alkaline catalyst in the natural oil is 0.3-0.6%, so as to obtain glycerin polyoxyethylene ether fatty acid ester. The product glycerin polyoxyethylene ether fatty acid ester can form a transparent and stable nanometer micellar system with a little blue light in water, and can be applied to personal washing and protection products and cosmetic formulations as a fat agent.
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