Multi-effect white Chinese wolfberry fruit toothpaste for preventing gingival atrophy and preparation method of multi-effect white Chinese wolfberry fruit toothpaste

Abstract

The invention relates to the technical field of oral care, in particular to multi-effect pure white fructus lycii toothpaste for preventing gingival atrophy and a preparation method of the multi-effect pure white fructus lycii toothpaste. The lycium barbarum mask is prepared from the following components in percentage by weight: 3 to 5 percent of lycium barbarum compound active matter, 2 to 4 percent of carboxymethyl chitosan, 20 to 25 percent of hydrated silica, 3 to 5 percent of sodium pyrophosphate, 1 to 2 percent of sodium lauryl sulfate, 2 to 3 percent of sodium hyaluronate, 1 to 2 percent of allantoin, 15 to 20 percent of glycerol, 5 to 8 percent of propylene glycol, 1 to 2 percent of sodium carboxymethyl cellulose, 0.5 to 1 percent of xanthan gum, 0.1 to 0.3 percent of saccharin sodium salt and the balance of water. 0.5-1% of essence and 0.1-0.3% of a preservative sodium benzoate; according to the toothpaste disclosed by the invention, the fructus lycii compound active matter, various gingival care components and cleaning and whitening components are scientifically compounded, so that tooth stains can be effectively removed through hydrated silica, sodium pyrophosphate and the like, and multi-effect tooth whitening is realized; the components such as the fructus lycii composite active matter and the carboxymethyl chitosan can be used for resisting oxidation and inflammation, a protective film is formed on the surface of gingiva, gingival atrophy is effectively prevented, meanwhile, sodium hyaluronate and allantoin can relieve gingival inflammation, and multiple effects of oral cavity cleaning and nursing are achieved.

Description

Technical Field

[0001] The invention relates to the technical field of oral care, in particular to a wolfberry toothpaste for preventing gum atrophy and whitening teeth, and a preparation method thereof. Background Art

[0002] Gum recession is a common oral disease caused by factors including periodontitis, improper brushing techniques, irritation from poor restorations, and aging. Gum recession can lead to exposed tooth roots, tooth sensitivity, and, in severe cases, even loose teeth and loss, significantly impacting oral health and quality of life. Furthermore, as people become more aware of their personal appearance, tooth whiteness has become a key oral care requirement.

[0003] Currently, toothpaste products on the market have relatively simple functions. Most ordinary toothpastes only have basic cleaning effects and have little effect on preventing or improving gum atrophy. Some toothpastes claiming to have gum care functions, although containing some active ingredients, are not effective enough, and the synergy between the ingredients is poor. Among whitening toothpastes, some rely on high-strength abrasives to achieve tooth whitening, which can easily damage tooth enamel; some contain chemical ingredients that may irritate the oral mucosa with long-term use. Therefore, a wolfberry toothpaste with multiple effects for preventing gum atrophy and whitening, and a preparation method thereof, are proposed. Summary of the Invention

[0004] In view of this, the present invention provides a wolfberry toothpaste for preventing gum atrophy and whitening the teeth, and a preparation method thereof, so as to solve or alleviate the technical problems existing in the prior art and at least provide a beneficial choice.

[0005] The technical solution of the present invention is achieved as follows: a wolfberry toothpaste for preventing gum atrophy and achieving multiple effects and whitening, comprising the following ingredients in percentage by weight: 3-5% of wolfberry composite active ingredients, 2-4% of carboxymethyl chitosan, 20-25% of hydrated silica, 3-5% of sodium pyrophosphate, 1-2% of sodium lauryl sulfate, 2-3% of sodium hyaluronate, 1-2% of allantoin, 15-20% of glycerol, 5-8% of propylene glycol, 1-2% of sodium carboxymethyl cellulose, 0.5-1% of xanthan gum, 0.1-0.3% of sodium saccharin, 0.5-1% of flavor, and 0.1-0.3% of preservative sodium benzoate.

[0006] A method for preparing a wolfberry toothpaste for preventing gum atrophy and achieving multiple whitening effects, comprising the following steps:

[0007] S1, wolfberry compound active ingredient extraction;

[0008] S2, premixed moisturizing and thickening ingredients;

[0009] S3, add cleaning and whitening ingredients;

[0010] S4, adding active and functional ingredients;

[0011] S5. Post-processing.

[0012] Further preferably, in S1, dried high-quality wolfberry is selected and crushed to 80-100 mesh, and an ethanol solution with a volume fraction of 60-70% is added at a material-liquid ratio of 1:8-1:10. Ultrasonic-assisted extraction is performed at 50-60°C for 1-1.5 hours, and the extract is collected by filtration. The extract is concentrated under reduced pressure at 40-50°C and a vacuum degree of 0.06-0.08MPa to obtain a wolfberry extract concentrate, and the concentrate is separated and purified by macroporous adsorption resin column chromatography, and the eluates rich in wolfberry polysaccharides, wolfberry flavonoids, and wolfberry polyphenols are collected respectively, and mixed to obtain wolfberry composite active substances.

[0013] Further preferably, in the S2, 70-80% of the total amount of deionized water is added to the batching pot, the agitator is turned on, the speed is adjusted to 200-300 r / min, glycerol and propylene glycol are added in sequence, and stirred for 10-15 minutes to fully dissolve them, sodium carboxymethyl cellulose, xanthan gum and an appropriate amount of deionized water are mixed into a paste, slowly added to the batching pot, and stirred for 20-30 minutes to form a uniform and stable colloidal solution.

[0014] Further preferably, in S3, hydrated silica, sodium pyrophosphate and sodium lauryl sulfate are added to the colloidal solution, the stirring speed is increased to 300-400 r / min, and the stirring is carried out for 30-40 minutes to ensure that the cleansing and whitening ingredients are evenly dispersed.

[0015] Further preferably, in S4, the prepared wolfberry composite active ingredient, carboxymethyl chitosan, sodium hyaluronate and allantoin are added and stirred for 40-50 minutes to allow the active ingredients to be fully dissolved and uniformly mixed with the system.

[0016] Further preferably, in the S5, sodium saccharin, sodium benzoate, and flavor are added and stirred for 15-20 minutes to completely dissolve and disperse them, and the pH value of the toothpaste is adjusted to 7-8 with citric acid or sodium hydroxide solution to ensure the stability and mildness of the toothpaste. The material is transferred to a vacuum deaerator and degassed at a pressure of -0.08-0.06MPa for 15-20 minutes to remove bubbles mixed in during the stirring process, and finally filled by a filling machine to obtain a finished wolfberry toothpaste with multiple effects and whitening for preventing gum atrophy.

[0017] The embodiment of the present invention adopts the above technical solution, which has the following advantages:

[0018] 1. The toothpaste of the present invention scientifically compounds wolfberry composite active ingredients, multiple gum care ingredients and cleaning and whitening ingredients. It can not only effectively remove tooth stains through hydrated silica, sodium pyrophosphate, etc., to achieve multi-effect teeth whitening; it can also use wolfberry composite active ingredients, carboxymethyl chitosan and other ingredients for antioxidant and anti-inflammatory effects to form a protective film on the gum surface, effectively preventing gum atrophy. At the same time, sodium hyaluronate and allantoin can relieve gum inflammation, achieving multiple effects of oral cleaning and care.

[0019] 2. The various ingredients of the present invention work synergistically with each other. The wolfberry composite active ingredient enhances the effects of other gum care ingredients; carboxymethyl chitosan and sodium hyaluronate jointly form a stable protective film on the gum surface; hydrated silica and sodium pyrophosphate are combined to enhance the cleaning and whitening effects while reducing damage to teeth, thereby improving the overall performance of the toothpaste.

[0020] The above summary is for illustrative purposes only and is not intended to be limiting in any way. In addition to the illustrative aspects, embodiments and features described above, further aspects, embodiments and features of the present invention will be readily apparent by reference to the accompanying drawings and the following detailed description. BRIEF DESCRIPTION OF THE DRAWINGS

[0021] In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the following briefly introduces the drawings required for use in the embodiments or the description of the prior art. Obviously, the drawings described below are only some embodiments of the present application. For ordinary technicians in this field, other drawings can be obtained based on these drawings without any creative work.

[0022] Figure 1 Flow chart of the method of the present invention. DETAILED DESCRIPTION

[0023] Hereinafter, only certain exemplary embodiments are briefly described. As will be appreciated by those skilled in the art, the described embodiments may be modified in various ways without departing from the spirit or scope of the present invention. Therefore, the drawings and description are to be considered as illustrative in nature and not restrictive.

[0024] The embodiments of the present invention are described in detail below with reference to the accompanying drawings.

[0025] like Figure 1As shown, an embodiment of the present invention provides a wolfberry toothpaste with multiple effects for preventing gum atrophy and whitening, which is composed of the following ingredients in weight percentage: 3-5% wolfberry composite active ingredient, 2-4% carboxymethyl chitosan, 20-25% hydrated silica, 3-5% sodium pyrophosphate, 1-2% sodium lauryl sulfate, 2-3% sodium hyaluronate, 1-2% allantoin, 15-20% glycerol, 5-8% propylene glycol, 1-2% sodium carboxymethyl cellulose, 0.5-1% xanthan gum, 0.1-0.3% sodium saccharin, 0.5-1% flavor and 0.1-0.3% preservative sodium benzoate.

[0026] A method for preparing a wolfberry toothpaste for preventing gum atrophy and achieving multiple whitening effects, comprising the following steps:

[0027] S1, wolfberry compound active ingredient extraction;

[0028] S2, premixed moisturizing and thickening ingredients;

[0029] S3, add cleaning and whitening ingredients;

[0030] S4, adding active and functional ingredients;

[0031] S5. Post-processing.

[0032] In one embodiment, in S1, dried high-quality wolfberries are selected and crushed to 80-100 mesh, and an ethanol solution with a volume fraction of 60-70% is added at a material-liquid ratio of 1:8-1:10. Ultrasonic-assisted extraction is performed at 50-60°C for 1-1.5 hours, and the extract is collected by filtration. The extract is concentrated under reduced pressure at 40-50°C and a vacuum degree of 0.06-0.08 MPa to obtain a wolfberry extract concentrate. The concentrate is separated and purified by macroporous adsorption resin column chromatography, and eluates rich in wolfberry polysaccharides, wolfberry flavonoids, and wolfberry polyphenols are collected respectively, and mixed to obtain a wolfberry composite active substance.

[0033] In one embodiment, in S2, 70-80% of the total amount of deionized water is added to the batching pot, the stirrer is turned on, the speed is adjusted to 200-300 r / min, glycerol and propylene glycol are added in sequence, and stirred for 10-15 minutes to fully dissolve them, sodium carboxymethyl cellulose and xanthan gum are mixed with an appropriate amount of deionized water to form a paste, which is slowly added to the batching pot and stirred for 20-30 minutes to form a uniform and stable colloidal solution.

[0034] In one embodiment, in S3, hydrated silica, sodium pyrophosphate, and sodium lauryl sulfate are added to the colloidal solution, the stirring speed is increased to 300-400 r / min, and the mixture is stirred for 30-40 minutes to ensure that the cleansing and whitening ingredients are evenly dispersed.

[0035] In one embodiment, in S4, the prepared wolfberry composite active ingredient, carboxymethyl chitosan, sodium hyaluronate, and allantoin are added and stirred for 40-50 minutes to allow the active ingredients to fully dissolve and mix evenly with the system.

[0036] In one embodiment, in S5, sodium saccharin, sodium benzoate, and flavor are added and stirred for 15-20 minutes to completely dissolve and disperse them. The pH value of the toothpaste is adjusted to 7-8 with citric acid or sodium hydroxide solution to ensure the stability and mildness of the toothpaste. The material is transferred to a vacuum deaerator and degassed at a pressure of -0.08-0.06 MPa for 15-20 minutes to remove bubbles mixed in during the stirring process. Finally, the material is filled by a filling machine to obtain a finished wolfberry toothpaste for preventing gum atrophy and whitening with multiple effects.

[0037] The above description is merely a specific embodiment of the present invention, but the scope of protection of the present invention is not limited thereto. Any person skilled in the art can easily conceive of various modifications and substitutions within the technical scope disclosed in the present invention, and such modifications and substitutions are intended to be within the scope of protection of the present invention. Therefore, the scope of protection of the present invention shall be subject to the scope of protection of the claims.

Claims

1. A wolfberry toothpaste for preventing gum atrophy and achieving multi-effect whitening, characterized by: The invention is composed of the following ingredients in percentage by weight: 3-5% of wolfberry compound active ingredients, 2-4% of carboxymethyl chitosan, 20-25% of hydrated silica, 3-5% of sodium pyrophosphate, 1-2% of sodium lauryl sulfate, 2-3% of sodium hyaluronate, 1-2% of allantoin, 15-20% of glycerol, 5-8% of propylene glycol, 1-2% of sodium carboxymethyl cellulose, 0.5-1% of xanthan gum, 0.1-0.3% of sodium saccharin, 0.5-1% of flavor and 0.1-0.3% of preservative sodium benzoate.

2. A method for preparing a wolfberry toothpaste for preventing gum atrophy and whitening teeth, which is used in conjunction with the wolfberry toothpaste for preventing gum atrophy and whitening teeth as claimed in claim 1, characterized in that: The following steps are involved: S1, wolfberry compound active ingredient extraction; S2, premixed moisturizing and thickening ingredients; S3, add cleaning and whitening ingredients; S4, adding active and functional ingredients; S5. Post-processing.

3. The method for preparing a multi-effect whitening wolfberry toothpaste for preventing gum atrophy according to claim 2, characterized in that: In the S1, dry high-quality wolfberries are selected and crushed to 80-100 meshes, and an ethanol solution with a volume fraction of 60-70% is added at a material-liquid ratio of 1:8-1:

10. Ultrasonic-assisted extraction is performed at 50-60° C. for 1-1.5 hours, and the extract is filtered and collected. The extract is concentrated under reduced pressure at 40-50° C. and a vacuum degree of 0.06-0.08 MPa to obtain a wolfberry extract concentrate. The concentrate is separated and purified by macroporous adsorption resin column chromatography, and eluates rich in wolfberry polysaccharides, wolfberry flavonoids, and wolfberry polyphenols are collected respectively, and mixed to obtain a wolfberry composite active substance.

4. The method for preparing a multi-effect whitening wolfberry toothpaste for preventing gum atrophy according to claim 2, characterized in that: In S2, 70-80% of the total amount of deionized water is added to the batching pot, the stirrer is turned on, the speed is adjusted to 200-300 r / min, glycerol and propylene glycol are added in sequence, and stirred for 10-15 minutes to fully dissolve them. Sodium carboxymethyl cellulose and xanthan gum are mixed with an appropriate amount of deionized water to form a paste, which is slowly added to the batching pot and stirred for 20-30 minutes to form a uniform and stable colloidal solution.

5. The method for preparing the multi-effect whitening wolfberry toothpaste for preventing gum atrophy according to claim 2, characterized in that: In S3, hydrated silica, sodium pyrophosphate, and sodium lauryl sulfate are added to the colloidal solution, the stirring speed is increased to 300-400 r / min, and the mixture is stirred for 30-40 minutes to ensure that the cleansing and whitening ingredients are evenly dispersed.

6. The method for preparing the multi-effect whitening wolfberry toothpaste for preventing gum atrophy according to claim 2, characterized in that: In the S4, the prepared wolfberry composite active ingredient, carboxymethyl chitosan, sodium hyaluronate, and allantoin are added and stirred for 40-50 minutes to allow the active ingredients to fully dissolve and mix evenly with the system.

7. The method for preparing the multi-effect whitening wolfberry toothpaste for preventing gum atrophy according to claim 2, characterized in that: In the S5, sodium saccharin, sodium benzoate, and flavor are added and stirred for 15-20 minutes to completely dissolve and disperse them. The pH value of the toothpaste is adjusted to 7-8 with citric acid or sodium hydroxide solution to ensure the stability and mildness of the toothpaste. The material is transferred to a vacuum deaerator and degassed at a pressure of -0.08-0.06 MPa for 15-20 minutes to remove bubbles mixed in during the stirring process. Finally, the material is filled by a filling machine to obtain a finished wolfberry toothpaste for preventing gum atrophy and whitening with multiple effects.

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