Recovery device for methyl tert-butyl ether

By installing multiple sets of hollow tubes and nozzles inside the water washing tower, and adjusting the components to control the gas-liquid flow, the problem of low mass transfer efficiency caused by uneven gas distribution is solved, and the methanol recovery efficiency is improved.

CN121155302APending Publication Date: 2025-12-19ANHUI ZHONGHUIFA NEW MATERIALS CO LTD
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Patent Information

Application Number
CN202511349630.4
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-09-22
Publication Date
2025-12-19

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Abstract

The invention relates to the technical field of methyl tert-butyl ether, and discloses a methyl tert-butyl ether recovery device which comprises a tower body, a gas inlet pipeline, a pipeline and a plurality of observation windows are mounted on the surface of the tower body, an exhaust pipeline is mounted above the tower body, and a recovery mechanism is arranged on the inner wall of the tower body; the recovery mechanism comprises a chassis mounted in the inner wall of the tower body, a plurality of hollow pipes I are mounted on the inner wall of the chassis, and hollow pipes II are slidably connected to the inner walls of the hollow pipes I. According to the invention, the recovery mechanism is arranged, and a gas channel is formed by the plurality of groups of hollow pipes I and hollow pipes II, so that gas can uniformly enter the plurality of groups of hollow pipes I and hollow pipes II; according to the present invention, the adjusting assembly can control the movement of the upper disc and the hollow sleeve 2, the movement of the hollow sleeve 2 in the hollow sleeve 1, and the overall recovery rate can be significantly improved by adjusting the length of the gas path and prolonging the contact time with the liquid.
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Description

TECHNICAL FIELD

[0001] The present application relates to the technical field of methyl tert-butyl ether, in particular to a recovery device for methyl tert-butyl ether. BACKGROUND

[0002] Methyl tert-butyl ether (MTBE) is a colorless transparent liquid, has ether special smell, boiling point 55.2℃, slightly soluble in water, easily soluble in organic solvents, as a high octane gasoline additive, can improve the anti-knock, reduce exhaust pollution, has been widely used.

[0003] In the process of producing and manufacturing methyl tert-butyl ether, the methanol in the mixture of methanol and C4 needs to be recovered.

[0004] The prior art often uses water washing tower equipment to recover methanol. Methanol is a polar molecule and can be miscible with water (polar solvent) in any proportion. After the gaseous mixture containing methanol (such as reaction tail gas, volatile gas) enters the water washing tower, it is in countercurrent contact with the water from top to bottom. The methanol molecules quickly dissolve in the water due to the "like dissolves like" principle, forming a methanol aqueous solution, thereby separating from other gases (such as C4, hydrocarbons, etc.) that are not soluble in water. However, the existing water washing tower equipment generally uses a spray head to spray liquid downward and a gas flowing upward in a gas-liquid countercurrent contact mode. However, during actual operation, due to factors such as gas inlet structure design and uneven distribution of fluid resistance in the tower, the lateral distribution of gas in the tower is difficult to achieve an ideal uniform state, and local flow rate is prone to be too high or too low. In the area with high flow rate, the gas-liquid contact time is insufficient, and the methanol cannot be fully dissolved. In the area with low flow rate, there is liquid bias, which leads to a decrease in mass transfer efficiency and causes poor methanol recovery effect.

[0005] Therefore, we propose a recovery device for methyl tert-butyl ether. SUMMARY

[0006] (I) Technical problems solved

[0007] In view of the shortcomings of the prior art, the present application provides a recovery device for methyl tert-butyl ether, which solves the problem that the lateral distribution of gas in the tower is difficult to achieve an ideal uniform state, and local flow rate is prone to be too high or too low. In the area with high flow rate, the gas-liquid contact time is insufficient, and the methanol cannot be fully dissolved. In the area with low flow rate, there is liquid bias, which leads to a decrease in mass transfer efficiency and causes poor methanol recovery effect.

[0008] (II) Technical solutions

[0009] In order to achieve the above object, the present application is realized by the following technical scheme: A recovery device for methyl tert-butyl ether, comprising a tower body, a gas inlet pipeline, a pipeline and a plurality of observation windows are installed on the surface of the tower body, an exhaust pipeline is installed above the tower body, a recovery mechanism is arranged on the inner wall of the tower body;

[0010] The recovery mechanism comprises a bottom disc installed in the inner wall of the tower body, a plurality of hollow pipes I are installed on the inner wall of the bottom disc, a hollow pipe II is slidably connected to the inner wall of the hollow pipe I, a plurality of hollow pipes II are installed on the surface of the upper disc, an adjusting assembly is arranged on the tower body for moving the hollow pipe II in the hollow pipe I, adjusting the gas passing time, a frame I is installed on the surface of the upper disc, a frame II is installed above the frame I, a center pipe and a plurality of edge pipes are rotatably connected to the inner wall of the frame I, a nozzle is installed below the center pipe and the plurality of edge pipes and extends into the hollow pipe II, a driving assembly is arranged on the surface of the frame I for controlling the rotation of the center pipe and the plurality of edge pipes, and a conveying assembly is arranged on the surface of the frame II for conveying the liquid in the pipeline into the center pipe and the plurality of edge pipes.

[0011] The auxiliary device is arranged between the tower body and the pipeline for pretreating the entering gas, and a guide part is arranged between the bottom disc and the upper disc. Through the above components, when the gas containing methanol enters the tower body during the recovery process, it will move upward as a whole, the bottom disc can intercept the gas and make it enter the plurality of hollow pipes I and hollow pipes II uniformly, and the conveying assembly can convey the liquid in the pipeline to the center pipe and the edge pipe, and the nozzles can spray to realize more uniform and intensive spraying, which can better cover the area through which the gas flows, improve the water washing effect, the adjusting assembly can move the hollow pipe II in the hollow pipe I to increase the contact time of the gas and the liquid, and more effectively absorb the methanol, the driving assembly can also control the rotation of the center pipe and the edge pipe to make the nozzles rotate and spray, which can increase the spraying area and also atomize the liquid, so that the atomized liquid droplets fully contact with the gas to accelerate the dissolution of methanol and improve the recovery efficiency.

[0012] Preferably, the driving assembly comprises two hollow seats mounted on the surface of the frame, the inner wall of the hollow seat is rotationally connected with a shaft, one end of the shaft is fixedly connected with a bevel gear one, the surface of the central pipe is mounted with a bevel gear two, and is meshingly connected with the bevel gear one, the number of each group of the edge pipes is two, a synchronous belt is mounted between each group of the edge pipes, and a gear body is fixedly connected to the surface of the edge pipe close to the central pipe, the surface of the central pipe is fixedly connected with a gear ring, the gear ring is meshingly connected with the gear body, the outer surface of the tower body is mounted with a driving motor, the output end of the driving motor penetrates the tower body and is mounted on one end of the shaft, through the above-mentioned parts, when operating, the driving motor is turned on, the driving motor drives the shaft and the bevel gear one to rotate, the bevel gear one drives the central pipe to rotate in cooperation with the bevel gear two, the central pipe drives the gear ring to rotate in synchronization, the gear ring drives the edge pipe to rotate in cooperation with the gear body, and then another edge pipe is driven to rotate through the synchronous belt, so that the nozzle rotates and sprays in the hollow pipe two.

[0013] Preferably, the surface of the nozzle is provided with a plurality of spray holes, the plurality of spray holes are arranged on the bottom and the side surface of the nozzle, and the spray holes on the side surface are arranged in an inclined manner.

[0014] Preferably, the surface of the central pipe and the plurality of groups of edge pipes are fixedly connected with a shielding cover, a plurality of through holes are formed in the surface of the shielding cover, and the shielding cover is located in the central pipe, through the above-mentioned parts, the shielding cover cooperates with the through holes, the speed of the gas discharged from the hollow pipe two can be further blocked, and the contact time with the liquid is improved.

[0015] Preferably, the shielding cover is arranged in a conical shape.

[0016] Preferably, the adjusting assembly comprises an adjusting screw rotationally connected with the inner wall of the bottom disc, the surface of the upper disc is fixedly connected with a threaded sleeve, the adjusting screw is threadedly connected with the inner wall of the threaded sleeve, the surface of the adjusting screw is mounted with a bevel gear three, the outer surface of the tower body is mounted with an adjusting motor, the output end of the adjusting motor penetrates the tower body and is fixedly connected with a bevel gear four, the bevel gear three is meshingly connected with the bevel gear four, through the above-mentioned parts, when working, the adjusting motor is turned on, the adjusting motor drives the bevel gear four to rotate, the bevel gear four drives the adjusting screw to rotate in cooperation with the bevel gear three, the adjusting screw cooperates with the threaded sleeve to control the movement of the upper disc and the hollow pipe two, the hollow pipe two moves in the hollow pipe one, thereby prolonging the path of the gas.

[0017] Preferably, the guide part comprises a plurality of guide sleeves fixed on the surface of the bottom disc, the surface of the upper disc is fixedly connected with a plurality of guide rods, and the guide rods are slidingly connected with the inner wall of the guide sleeves, through the above-mentioned parts, when the upper disc and the hollow pipe two move, the plurality of guide rods cooperate with the guide sleeves to improve the stability of the whole.

[0018] Preferably, the conveying assembly comprises a connecting pipe fixed on the surface of the frame, the connecting pipe is rotatably connected with the inner wall of the center pipe and the plurality of edge pipes respectively, the surface of the connecting pipe is fixedly connected with an extension pipe, the other end of the extension pipe is connected with the pipeline, through the above-mentioned components, the pipeline can convey the liquid into the extension pipe, the extension pipe conveys the liquid into the connecting pipe, and the connecting pipe uniformly conveys the liquid to the center pipe and the edge pipes, so that the nozzle performs the spraying operation.

[0019] Preferably, the auxiliary device comprises a supporting ring installed in the inner wall of the tower body, a spraying pipe is installed on the upper surface of the supporting ring, an installation pipe is installed on the lower surface of the spraying pipe, the other end of the installation pipe is connected with the pipeline, through the above-mentioned components, the pipeline can convey the liquid to the spraying pipe through the installation pipe, and the spraying pipe can realize 360-degree water spraying to preliminarily process the entering gas.

[0020] Preferably, the spraying pipe comprises a cylindrical pipe and a plurality of nozzles, and the plurality of nozzles are uniformly installed on the outer surface of the cylindrical pipe.

[0021] In summary, the technical effects and advantages of the present application are as follows:

[0022] 1. In the present application, the recovery mechanism is provided, the gas passage is formed through the plurality of hollow pipes one and hollow pipes two, the gas can uniformly enter the plurality of hollow pipes one and hollow pipes two, and is contacted with the liquid sprayed by the nozzle, the problem of gas flow deviation of the traditional tower body is solved, the gas-liquid contact in each region is more balanced, and the adjusting assembly can control the movement of the upper disc and the hollow sleeve two, the hollow sleeve two moves in the hollow sleeve one, the contact time with the liquid is increased by adjusting the length of the gas path, and the overall recovery rate is significantly improved.

[0023] 2. In the present application, the conical shielding cover cooperates with the through hole, the speed of the gas discharge is further blocked when the gas is discharged through the hollow pipe two, the gas discharge speed is effectively reduced, the residence time of the gas in the hollow pipe two is additionally increased, and the recovery effect is further improved.

[0024] 3. In the present application, a plurality of spray holes are arranged on the bottom and the side surface of the nozzle, the spray holes on the side surface are arranged in an inclined manner, the driving assembly drives the center pipe and the edge pipe to rotate, the rotation of the nozzle is controlled, the spraying area is increased, and the liquid can be atomized, the atomized liquid droplets are fully contacted with the gas, the dissolution of methanol is accelerated, and the recovery efficiency is improved.

[0025] 4. In the present application, the auxiliary device is provided, the spraying pipe (cylindrical pipe+multiple nozzles) on the supporting ring realizes 360-degree preliminary water washing, a certain amount of methanol in the gas entering the tower body is removed in advance, and the subsequent treatment load is reduced. BRIEF DESCRIPTION OF DRAWINGS

[0026] Figure 1It is the whole structure schematic diagram of the recovery device for methyl tert-butyl ether of the present application;

[0027] Figure 2 It is the sectional structure schematic diagram of the recovery device for methyl tert-butyl ether of the present application;

[0028] Figure 3 It is another visual sectional structure schematic diagram of the recovery device for methyl tert-butyl ether of the present application;

[0029] Figure 4 It is the side view structure schematic diagram of the recovery device for methyl tert-butyl ether of the present application;

[0030] Figure 5 It is the partial structure schematic diagram of the recovery mechanism of the recovery device for methyl tert-butyl ether of the present application;

[0031] Figure 6 It is the explosion structure schematic diagram of the recovery device for methyl tert-butyl ether of the present application; Figure 5

[0032] Figure 7 It is another visual structure schematic diagram of the recovery device for methyl tert-butyl ether of the present application; Figure 6

[0033] Figure 8 It is the drive assembly structure schematic diagram of the recovery device for methyl tert-butyl ether of the present application;

[0034] Figure 9 It is the nozzle sectional structure schematic diagram of the recovery device for methyl tert-butyl ether of the present application;

[0035] Figure 10 It is the auxiliary device structure schematic diagram of the recovery device for methyl tert-butyl ether of the present application.

[0036] ​​As shown in the figure: 1, tower body; 2, intake pipeline; 3, exhaust pipeline; 4, observation window; 5, pipeline; 6, recovery mechanism; 61, bottom disc; 62, hollow tube one; 63, upper disc; 64, hollow tube two; 65, frame one; 66, frame two; 67, conveying assembly; 671, telescopic pipe; 672, connecting pipe; 68, driving assembly; 681, driving motor; 682, hollow seat; 683, shaft; 684, bevel gear one; 685, bevel gear two; 686, synchronous belt; 687, gear body; 688, gear ring; 69, adjusting assembly; 691, adjusting motor; 692, adjusting screw; 693, bevel gear three; 694, threaded sleeve; 695, bevel gear four; 610, edge pipe; 611, spray head; 612, center pipe; 613, shielding cover; 614, through hole; 615, guide rod; 616, guide sleeve; 7, auxiliary device; 71, support ring; 72, spray pipe; 721, cylindrical pipe; 722, nozzle; 73, mounting pipe. DETAILED DESCRIPTION

[0037] The technical solutions in the embodiments of the present application will be clearly and completely described below with reference to the drawings in the embodiments of the present application. Obviously, the described embodiments are only part of the embodiments of the present application, rather than all the embodiments. Based on the embodiments in the present application, all other embodiments obtained by those skilled in the art without creative work fall within the scope of protection of the present application.

[0038] Reference Figure 1 - Figure 10 As shown in the figure, a methyl tert-butyl ether recovery device includes a tower body 1, the surface of the tower body 1 is provided with an intake pipeline 2, a pipeline 5 and a plurality of observation windows 4, an exhaust pipeline 3 is installed above the tower body 1, and a recovery mechanism 6 is arranged on the inner wall of the tower body 1.

[0039] The recovery mechanism 6 comprises a bottom disc 61 installed in the inner wall of the tower body 1, the inner wall of the bottom disc 61 is provided with a plurality of hollow tubes one 62, the inner wall of the hollow tube one 62 is slidably connected with a hollow tube two 64, the surface of the plurality of hollow tubes two 64 is provided with an upper disc 63, the tower body 1 is provided with an adjusting assembly 69 for moving the hollow tube two 64 in the hollow tube one 62, adjusting the gas passing time, the surface of the upper disc 63 is provided with a frame one 65, the upper frame two 66 is installed on the frame one 65, the inner wall of the frame one 65 is rotatably connected with a center tube 612 and a plurality of edge tubes 610, the lower surface of the center tube 612 and the plurality of edge tubes 610 is provided with a spray head 611, the surface of the spray head 611 is provided with a plurality of spray holes, the plurality of spray holes are arranged on the bottom and the side surface of the spray head 611, the spray holes on the side surface are arranged in an inclined manner and extend into the hollow tube two 64, the surface of the frame one 65 is provided with a driving assembly 68 for controlling the rotation of the center tube 612 and the plurality of edge tubes 610, the surface of the frame two 66 is provided with a conveying assembly 67 for conveying the liquid in the pipeline 5 into the center tube 612 and the plurality of edge tubes 610.

[0040] In the embodiment, during the recovery process, when the gas containing methanol enters the tower body 1, it moves upward as a whole, the bottom disc 61 can intercept the gas and make it enter the plurality of hollow tubes one 62 and the hollow tube two 64 uniformly, at the same time, the conveying assembly 67 conveys the liquid in the pipeline 5 to the center tube 612 and the edge tube 610, and the spray head 611 sprays to realize more uniform and intensive spraying, which can better cover the area through which the gas flows, improve the water washing effect, the adjusting assembly 69 can move the hollow tube two 64 in the hollow tube one 62 to increase the contact time of the gas and the liquid and more effectively absorb the methanol, the driving assembly 68 can also control the rotation of the center tube 612 and the edge tube 610 to make the spray head 611 rotate and spray to increase the spraying area, at the same time, the liquid can be atomized, the atomized liquid droplets fully contact with the gas to accelerate the dissolution of methanol and improve the recovery efficiency.

[0041] The driving assembly 68 comprises two hollow seats 682 installed on the surface of the frame one 65, the inner wall of the hollow seat 682 is rotatably connected with a shaft 683, one end of the shaft 683 is fixedly connected with a bevel gear one 684, the surface of the center tube 612 is provided with a bevel gear two 685 which is meshingly connected with the bevel gear one 684, the number of each group of edge tubes 610 is two, a synchronous belt 686 is installed between each group of edge tubes 610, and a gear body 687 is fixedly connected to the surface of the edge tube 610 close to the center tube 612, the surface of the center tube 612 is fixedly connected with a gear ring 688 which is meshingly connected with the gear body 687, the outer surface of the tower body 1 is provided with a driving motor 681, the output end of the driving motor 681 penetrates through the tower body 1 and is installed on one end of the shaft 683.

[0042] In the embodiment, when in operation, the driving motor 681 is turned on, the driving motor 681 drives the shaft 683 and the bevel gear one 684 to rotate, the bevel gear one 684 cooperates with the bevel gear two 685 to drive the central pipe 612 to rotate, the central pipe 612 synchronously drives the gear ring 688 to rotate through the synchronous belt 686, the gear ring 688 cooperates with the gear body 687 to drive the edge pipe 610 to rotate, and then another edge pipe 610 is driven to rotate through the synchronous belt 686, so that the nozzle 611 rotates and sprays in the hollow pipe two 64.

[0043] The surface of the central pipe 612 and the plurality of edge pipes 610 is fixedly connected with a shielding cover 613, a plurality of through holes 614 are formed in the surface of the shielding cover 613, the shielding cover 613 is located in the central pipe 612, and the shielding cover 613 is arranged in a conical shape.

[0044] In the embodiment, the shielding cover 613 cooperates with the through holes 614, so that the speed of the gas discharged from the hollow pipe two 64 can be further blocked, and the contact time with the liquid is improved.

[0045] The adjusting assembly 69 comprises an adjusting screw 692 rotationally connected with the inner wall of the bottom disc 61, the surface of the upper disc 63 is fixedly connected with a threaded sleeve 694, the adjusting screw 692 is threadedly connected with the inner wall of the threaded sleeve 694, the surface of the adjusting screw 692 is provided with a bevel gear three 693, the outer surface of the tower body 1 is provided with an adjusting motor 691, the output end of the adjusting motor 691 penetrates through the tower body 1 and is fixedly connected with a bevel gear four 695, and the bevel gear three 693 is meshingly connected with the bevel gear four 695.

[0046] In the embodiment, when in operation, the adjusting motor 691 is turned on, the adjusting motor 691 drives the bevel gear four 695 to rotate, the bevel gear four 695 cooperates with the bevel gear three 693 to drive the adjusting screw 692 to rotate, and the adjusting screw 692 cooperates with the threaded sleeve 694 to control the movement of the upper disc 63 and the hollow pipe two 64, so that the hollow pipe two 64 moves in the hollow pipe one 62, thereby prolonging the path of the gas.

[0047] The guiding part is arranged between the bottom disc 61 and the upper disc 63, and comprises a plurality of guiding sleeves 616 fixed to the surface of the bottom disc 61 and a plurality of guiding rods 615 fixed to the surface of the upper disc 63 and slidably connected with the inner wall of the guiding sleeves 616.

[0048] In the embodiment, when the upper disc 63 and the hollow pipe two 64 move, the plurality of guiding rods 615 cooperates with the guiding sleeves 616 to improve the stability of the whole.

[0049] The conveying assembly 67 comprises a connecting pipe 672 fixed on the surface of the frame two 66, the connecting pipe 672 is rotatably connected with the inner wall of the center pipe 612 and the plurality of edge pipes 610 respectively, the surface of the connecting pipe 672 is fixedly connected with an expansion pipe 671, and the other end of the expansion pipe 671 is connected with the pipeline 5.

[0050] In the embodiment, the pipeline 5 can convey the liquid into the expansion pipe 671, the expansion pipe 671 conveys the liquid into the connecting pipe 672, and the connecting pipe 672 uniformly conveys the liquid into the center pipe 612 and the edge pipes 610, so that the spray head 611 performs the spraying operation.

[0051] The auxiliary device 7 is arranged between the tower body 1 and the pipeline 5, the auxiliary device 7 comprises a supporting ring 71 installed in the inner wall of the tower body 1, a spraying pipe 72 is installed on the upper surface of the supporting ring 71, an installation pipe 73 is installed on the lower surface of the spraying pipe 72, the other end of the installation pipe 73 is connected with the pipeline 5, and the spraying pipe 72 comprises a cylindrical pipe 721 and a plurality of nozzles 722.

[0052] In the embodiment, the pipeline 5 can convey the liquid to the spraying pipe 72 through the installation pipe 73, the spraying pipe 72 can realize 360-degree water spraying, and the entering gas is preliminarily processed, so that the overall recovery effect is improved.

[0053] The working principle of the application is as follows: when working, first, the pipeline 5 is water-supplied through an external device, then the pipeline 5 conveys the liquid to the installation pipe 73 and the expansion pipe 671, the installation pipe 73 conveys the liquid to the spraying pipe 72, the spraying pipe 72 can realize 360-degree water spraying, the expansion pipe 671 conveys the liquid into the connecting pipe 672, and the connecting pipe 672 uniformly conveys the liquid into the center pipe 612 and the edge pipes 610, so that the spray head 611 performs the spraying operation in the hollow pipe two 64.

[0054] When the gas containing methanol enters the tower body 1, the gas moves upward as a whole, is preliminarily processed by the liquid sprayed by the spraying pipe 72, and a certain amount of methanol in the gas entering the tower body is removed in advance, so that the subsequent processing load is reduced, then the gas continues to move upward, the bottom disc 61 can intercept the gas, so that the gas enters the plurality of hollow pipes one 62 and the hollow pipe two 64 uniformly, the liquid sprayed by the spray head 611 in the hollow pipe two 64 can better contact the gas, and when the gas is discharged from the hollow pipe two 64, the shielding cover 613 cooperates with the through hole 614, so that the speed of the gas discharged from the hollow pipe two 64 is further blocked, and the contact time with the liquid is improved.

[0055] During the spraying process of the spray head 611, the driving motor 681 can be turned on to drive the shaft 683 and the bevel gear one 684 to rotate, the bevel gear one 684 cooperates with the bevel gear two 685 to drive the center pipe 612 to rotate, the center pipe 612 synchronously drives the gear ring 688 to rotate through the synchronous belt 686, the gear ring 688 cooperates with the gear body 687 to drive the edge pipe 610 to rotate, and then another edge pipe 610 is driven to rotate through the synchronous belt 686, so that the spray head 611 rotates in the hollow pipe two 64 to improve the spraying area, and the liquid can be atomized, the atomized liquid droplets can fully contact with the gas, the dissolution of the methanol is accelerated, and the recovery efficiency is improved;

[0056] When it is necessary to adjust the positions of the upper disc 63 and the hollow pipe two 64, the adjusting motor 691 is turned on to drive the bevel gear four 695 to rotate, the bevel gear four 695 cooperates with the bevel gear three 693 to drive the adjusting screw 692 to rotate, the adjusting screw 692 cooperates with the threaded sleeve 694 to control the movement of the upper disc 63 and the hollow pipe two 64, and the hollow pipe two 64 moves in the hollow pipe one 62 to lengthen the path of the gas passing through.

[0057] The methanol dissolved in water flows into the bottom of the tower body 1 along with the liquid and is discharged through the liquid discharge port at the bottom of the tower body 1 (not shown in the figure), so as to realize collection.

[0058] The electrical elements appearing in the text are all connected with the main controller and 220V mains, and the main controller can be a conventional known device such as a computer.

[0059] Finally, it should be noted that the above only describes the preferred embodiments of the present application and is not used to limit the present application, although the present application has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions recorded in the foregoing embodiments or make equivalent replacement for some technical features, and any modification, equivalent replacement or improvement made within the spirit and principles of the present application should be included in the protection scope of the present application.

Claims

1. A recovery device for methyl tert-butyl ether, comprising a tower body (1), characterized in that: The surface of the tower body (1) is equipped with an air inlet pipe (2), a pipeline (5) and multiple observation windows (4), an exhaust pipe (3) is installed on the top of the tower body (1), and a recycling mechanism (6) is provided on the inner wall of the tower body (1). The recycling mechanism (6) includes a chassis (61) installed in the inner wall of the tower body (1). Multiple hollow tubes (62) are installed on the inner wall of the chassis (61). Hollow tubes (64) are slidably connected to the inner walls of the hollow tubes (62). An upper plate (63) is installed on the surface of each of the hollow tubes (64). An adjustment assembly (69) is provided on the tower body (1) for moving the hollow tubes (64) within the hollow tubes (62) to adjust the gas passage time. A frame (65) is installed on the surface of the upper plate (63), and a frame (64) is installed above the frame (65). 6) The inner wall of the first frame (65) is rotatably connected to a central tube (612) and multiple sets of edge tubes (610). A nozzle (611) is installed below the central tube (612) and multiple sets of edge tubes (610) and extends into the hollow tube (64). The surface of the first frame (65) is provided with a drive assembly (68) for controlling the rotation of the central tube (612) and multiple sets of edge tubes (610). The surface of the second frame (66) is provided with a conveying assembly (67) for conveying the liquid in the pipeline (5) to the central tube (612) and multiple sets of edge tubes (610). An auxiliary device (7) is provided between the tower body (1) and the pipeline (5) for pre-treating the incoming gas. A guide is provided between the base plate (61) and the upper plate (63).

2. The methyl tert-butyl ether recovery device according to claim 1, characterized in that: The drive assembly (68) includes two hollow seats (682) mounted on the surface of the first frame (65). A shaft (683) is rotatably connected to the inner wall of each hollow seat (682). One end of the shaft (683) is fixedly connected to a bevel gear (684). A second bevel gear (685) is mounted on the surface of the central tube (612) and meshes with the first bevel gear (684). Each set of edge tubes (610) consists of two tubes. A synchronous belt (686) is installed between them, and a gear body (687) is fixedly connected to the surface of the edge tube (610) near the central tube (612). A gear ring (688) is fixedly connected to the surface of the central tube (612), and the gear ring (688) meshes with the gear body (687). A drive motor (681) is installed on the outer surface of the tower body (1). The output end of the drive motor (681) passes through the tower body (1) and is installed on one end of the shaft (683).

3. The methyl tert-butyl ether recovery device according to claim 1, characterized in that: The nozzle (611) has a plurality of spray holes on its surface. The spray holes are located on the bottom and sides of the nozzle (611), and the spray holes on the sides are arranged at an angle.

4. The methyl tert-butyl ether recovery device according to claim 1, characterized in that: The surface of the central tube (612) and the multiple sets of edge tubes (610) are all fixedly connected with shields (613), and the surface of the shields (613) is provided with multiple through holes (614), and the shields (613) are located inside the central tube (612).

5. The methyl tert-butyl ether recovery device according to claim 4, characterized in that: The shield (613) is cone-shaped.

6. The methyl tert-butyl ether recovery device according to claim 1, characterized in that: The adjustment assembly (69) includes an adjustment screw (692) rotatably connected to the inner wall of the chassis (61), a threaded sleeve (694) fixedly connected to the surface of the upper plate (63), the adjustment screw (692) being threadedly connected to the inner wall of the threaded sleeve (694), a bevel gear three (693) mounted on the surface of the adjustment screw (692), an adjustment motor (691) mounted on the outer surface of the tower body (1), the output end of the adjustment motor (691) penetrating the tower body (1) and fixedly connected to a bevel gear four (695), and the bevel gear three (693) meshing with the bevel gear four (695).

7. The methyl tert-butyl ether recovery device according to claim 1, characterized in that: The guide section includes multiple guide sleeves (616) fixed on the surface of the chassis (61), and multiple guide rods (615) fixedly connected to the surface of the upper plate (63). The guide rods (615) are slidably connected to the inner wall of the guide sleeves (616).

8. The methyl tert-butyl ether recovery device according to claim 1, characterized in that: The conveying assembly (67) includes a connecting pipe (672) fixed on the surface of the second frame (66). The connecting pipe (672) is rotatably connected to the inner walls of the central pipe (612) and multiple sets of edge pipes (610). A telescopic pipe (671) is fixedly connected to the surface of the connecting pipe (672). The other end of the telescopic pipe (671) is connected to the pipeline (5).

9. The methyl tert-butyl ether recovery device according to claim 1, characterized in that: The auxiliary device (7) includes a support ring (71) installed in the inner wall of the tower body (1). A spray pipe (72) is installed on the upper surface of the support ring (71), and an installation pipe (73) is installed on the lower surface of the spray pipe (72). The other end of the installation pipe (73) is connected to the pipeline (5).

10. A recovery device for methyl tert-butyl ether according to claim 9, characterized in that: The spray pipe (72) includes a cylindrical pipe (721) and a plurality of nozzles (722), which are evenly mounted on the outer surface of the cylindrical pipe (721).