A residual ammonia separation tank
By designing a residual ammonia water separation tank containing anti-impact plate, baffle plate and separation partition, the problem of tar deposition in the remaining ammonia water in the coking plant is solved, effective separation of tar and extended ammonia water circulation time are achieved, distillation efficiency is improved and maintenance costs are reduced.
Patent Information
- Application Number
- CN202110436859.7
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2021-04-22
- Publication Date
- 2025-04-11
- Estimated Expiration
- 2041-04-22
AI Technical Summary
The tar present in the remaining ammonia water in the coking plant will be deposited in the ammonia distillation tower and heat exchange equipment, resulting in reduced distillation efficiency, blockage of equipment, increased maintenance costs and labor intensity, and the prior art cannot effectively separate tar.
A residual ammonia water separation tank is designed, including the tank body, inlet, outlet, light tar adjustment device, separation partition and baffle plate. Through the combination of horizontal anti-impact plate, baffle plate and separation partition plate, the ammonia water circulation time is extended and the tar is separated.
Effective separation of tar extends the circulation time of ammonia water, prevents tar deposition, improves distillation efficiency, and reduces maintenance costs and labor intensity.
Smart Images

Figure CN113262526B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of tar ammonia water separation equipment, and in particular to a residual ammonia water separation tank. Background Art
[0002] The residual ammonia water in the coking plant is the product of the tar-ammonia water mixture that enters the gas purification system with the raw coal gas and passes through the tar-ammonia water separation device. It generally contains a small amount of tar. In the subsequent ammonia distillation process, the tar in the residual ammonia water is deposited on the trays of the ammonia distillation tower and the heat exchange equipment, which reduces the distillation efficiency and blocks the heat exchange equipment, affecting normal operation and increasing maintenance costs and labor intensity. At present, the residual ammonia water storage tank of the coking plant has a storage function and cannot separate the tar-ammonia water. Summary of the invention
[0003] In order to overcome the deficiencies of the prior art, the present invention provides a residual ammonia water separation tank, which not only has a storage function, but also can prolong the circulation time and has the function of separating tar and ammonia water.
[0004] In order to achieve the above object, the present invention adopts the following technical solutions:
[0005] A residual ammonia water separation tank comprises a tank body, a residual ammonia water inlet, a tar discharge outlet, a residual ammonia water outlet, a light tar regulating device, a light tar separation baffle, a tar ammonia water separation baffle, and a tar ammonia water separation baffle; the residual ammonia water inlet is fixedly connected to the lower part of the tank body, the tar discharge outlet is fixedly connected to the lowest part of the tank body, and the residual ammonia water outlet is fixedly connected to the upper part of the tank body; the light tar regulating device is fixedly connected to the tank body and is located at the upper part; the light tar separation baffle and the tar ammonia water separation baffle are both cylindrical and fixedly connected to the tank body; the tar ammonia water separation baffle is fixedly connected between the tar ammonia water separation baffle and the tank body wall plate.
[0006] It also includes a manhole, which is fixedly connected to the top of the trough body.
[0007] The trough body is a vaulted trough or a cone-topped trough.
[0008] The residual ammonia water inlet is provided with a horizontally arranged anti-collision plate, which is a semicircular tube.
[0009] The light tar separation partition is a cylindrical body or a spiral cylindrical body; the tar ammonia water separation partition is a cylindrical body with a hole at the inlet of the residual ammonia water.
[0010] The tar-ammonia-water separation baffles are arranged alternately up and down to support the tar-ammonia-water separation partitions. A distance is left above and below the baffles, and a whole connecting plate is arranged at the inlet of the remaining ammonia water.
[0011] The light tar separation partition is located on the top of the tar ammonia separation partition. The light tar separation partition includes a bottom plate, an ammonia separation cylinder, a light tar separation cylinder and a support plate. The bottom plate is fixedly connected to the trough body, the ammonia separation cylinder is fixedly connected to the bottom plate, the support plate is fixedly connected to the ammonia separation cylinder, and the light tar separation cylinder is fixedly connected to the support plate.
[0012] The light tar regulating device comprises a flange, a flange cover, a seamless steel pipe, a cone section, a shaft, bolts and a filler; the seamless steel pipe, the cone section and the shaft are connected in sequence, and the flange and the flange cover are fixedly connected to the seamless steel pipe.
[0013] Compared with the prior art, the present invention has the following beneficial effects:
[0014] 1. In the present invention, the residual ammonia water enters the tank through the residual ammonia water inlet from the lower part of the separation tank through the horizontally arranged anti-collision plate, which does not affect the tar deposition at the bottom.
[0015] 2. A baffle is arranged between the tar-ammonia separation baffle and the tank wall or spiral separation baffle to extend the circulation time of the remaining ammonia water, which is beneficial to the deposition of tar.
[0016] 3. The present invention is provided with a light tar separation partition and a light tar regulating device, which is conducive to separating the light tar. BRIEF DESCRIPTION OF THE DRAWINGS
[0017] Figure 1 It is a schematic diagram of the structure of the present invention;
[0018] Figure 2 This is a schematic diagram of the structure of the tar-ammonia water separation partition of the present invention;
[0019] Figure 3 This is a schematic diagram of the structure of the tar-ammonia water separation connecting plate of the present invention;
[0020] Figure 4 This is a schematic diagram of the structure of the tar-ammonia water separation baffle of the present invention;
[0021] Figure 5 This is a schematic diagram of the structure of the tar-ammonia water separation baffle of the present invention;
[0022] Figure 6 This is a schematic diagram of the opening of the tar-ammonia-water separation partition of the present invention;
[0023] Figure 7 This is a schematic diagram of the structure of the light tar separation partition of the present invention;
[0024] Figure 8 It is a schematic diagram of the structure of the light tar regulating device of the present invention.
[0025] In the figure: 1-tank body; 2-residual ammonia water inlet; 3-tar outlet; 4-residual ammonia water outlet; 5-light tar regulating device; 6-light tar separation baffle; 7-tar ammonia water separation baffle; 8-tar ammonia water separation baffle; 9-manhole; 10-connecting plate; 11-bottom plate; 12-ammonia water separation cylinder; 13-light tar separation cylinder; 14-support plate; 15-flange; 16-flange cover; 17-seamless steel pipe; 18-cone section; 19-shaft; 20-bolt; 21 nut; 22-filler. DETAILED DESCRIPTION
[0026] The specific implementation of the present invention will be further described below in conjunction with the accompanying drawings:
[0027] like Figure 1-8 As shown, a residual ammonia water separation tank includes a tank body 1, a residual ammonia water inlet 2, a tar discharge outlet 3, a residual ammonia water outlet 4, a light tar regulating device 5, a light tar separation baffle 6, a tar ammonia water separation baffle 7, a tar ammonia water separation baffle 8 and a manhole 9.
[0028] The tank body 1 is a vault tank or a cone-top tank. The residual ammonia water inlet 2 is fixedly connected to the lower part of the side wall of the tank body 1 and communicated with the inside of the tank body 1. The residual ammonia water inlet 2 is provided with a horizontally arranged anti-collision plate, which is a semicircular tube and does not affect the tar deposition at the bottom. The manhole 9 is fixedly connected to the top of the tank body 1 and communicated with the inside of the tank body 1. The tar discharge port 3 is fixedly connected to the lowest part of the side wall of the tank body 1 and communicated with the inside of the tank body 1 to facilitate the discharge of tar. The residual ammonia water outlet 4 is fixedly connected to the upper part of the side wall of the tank body 1 and communicated with the inside of the tank body 1.
[0029] The tar-ammonia-water separation baffle 7 is a cylindrical body, which is fixed to the bottom surface of the tank body 1 and has a hole at the residual ammonia water inlet 2 .
[0030] The light tar separation partition 6 is a cylindrical body or a spiral cylindrical body. The light tar separation partition 6 is located on the top of the tar ammonia water separation partition 7. The light tar separation partition 6 includes a bottom plate 11, an ammonia water separation cylinder 12, a light tar separation cylinder 13 and a support plate 14. The bottom plate 11 is fixedly connected to the trough wall of the trough body 1, the ammonia water separation cylinder 12 is fixedly connected to the bottom plate 11, the support plate 14 is fixedly connected to the ammonia water separation cylinder 12, and the light tar separation cylinder 13 is fixedly connected to the support plate 14.
[0031] The tar-ammonia separation baffles 8 are arranged alternately up and down to support the separation partitions. A distance is left above and below the baffles, and a whole connecting plate 10 is arranged at the remaining ammonia inlet 2.
[0032] The light tar regulating device 5 includes a flange 15, a flange cover 16, a seamless steel pipe 17, a cone section 18, a shaft 19, a bolt 20, a nut 21 and a packing 22. The seamless steel pipe 17, the cone section 18 and the shaft 19 are connected in sequence, and the flange 15 and the flange cover 16 are fixed to the seamless steel pipe 17. The bolts 20 and the nuts 21 are installed on the shaft 19, and a sleeve and a handle are provided on the upper part of the shaft 19, and the packing 22 is placed in the sleeve. The density of light tar of each manufacturer is different. The upper handle is adjusted according to the position of the light tar, and the position of the cone section 18 is controlled. When light tar is detected by the discharge liquid through the flange cover 16, the regulating device is fixed; if the position is low and ammonia water is detected, the position of the cone section 18 is adjusted upward to ensure that light tar is detected; if the position is too high, the light tar is discharged with the ammonia water.
[0033] The working principle and working process of the present invention are:
[0034] The remaining ammonia water enters the tank through the residual ammonia water inlet 2 from the bottom of the separation tank through the horizontally arranged anti-collision plate, which does not affect the tar deposition at the bottom. The ammonia water flow rate is reduced, and a gap is left at the bottom of the tar-ammonia water separation baffle 8. The ammonia water flows upward in the tank without affecting the strength of the equipment and the internal partition. A gap is left at the top of the tar-ammonia water separation baffle 8, which does not affect the gas flow at the top and finally fills the tar-ammonia water separation baffle 7. The flow of ammonia water changes the flow direction at the tar-ammonia water separation baffle 8, prolonging the flow time, which is conducive to the separation of tar-ammonia water, and the bottom tar discharge port 3 regularly discharges heavy tar.
[0035] The separated light tar floats on the ammonia water at the light tar separation partition 6, gathers in the light tar separation cylinder 13, and is discharged from the equipment through the light tar regulating device 5; the ammonia water with light and heavy tar removed flows through the ammonia water separation cylinder 12, and is discharged from the equipment through the remaining ammonia water outlet 4 for subsequent processing. The light tar regulating device 5 has the function of regulating the range, and the regulating range is adjusted according to the discharged tar content.
[0036] The invention not only has the storage function, but also can prolong the circulation time and has the effect of separating tar and ammonia water.
[0037] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.
Claims
1. A residual ammonia separation tank, characterized in that: It includes a tank body, a residual ammonia water inlet, a tar discharge outlet, a residual ammonia water outlet, a light tar regulating device, a light tar separation baffle, a tar ammonia water separation baffle, and a tar ammonia water separation baffle; the residual ammonia water inlet is fixedly connected to the lower part of the tank body, the tar discharge outlet is fixedly connected to the lowest part of the tank body, and the residual ammonia water outlet is fixedly connected to the upper part of the tank body; the light tar regulating device is fixedly connected to the tank body and is located at the upper part; the light tar separation baffle and the tar ammonia water separation baffle are both cylindrical and fixedly connected to the tank body; the tar ammonia water separation baffle is fixedly connected between the tar ammonia water separation baffle and the tank body wall plate; The residual ammonia water inlet is provided with a horizontally arranged anti-collision plate, which is a semicircular tube; The light tar regulating device comprises a flange, a flange cover, a seamless steel pipe, a cone section, a shaft, bolts and a filler; the seamless steel pipe, the cone section and the shaft are connected in sequence, and the flange and the flange cover are fixedly connected to the seamless steel pipe; The light tar separation partition is a cylindrical body or a spiral cylindrical body; the tar ammonia water separation partition is a cylindrical body with a hole at the inlet of the residual ammonia water; The tar-ammonia-water separation baffles are arranged in an alternating manner up and down to support the tar-ammonia-water separation baffles. A distance is left between the baffles up and down, and a whole connecting plate is provided at the inlet of the remaining ammonia water. The light tar separation partition is located on the top of the tar ammonia separation partition. The light tar separation partition includes a bottom plate, an ammonia separation cylinder, a light tar separation cylinder and a support plate. The bottom plate is fixedly connected to the trough body, the ammonia separation cylinder is fixedly connected to the bottom plate, the support plate is fixedly connected to the ammonia separation cylinder, and the light tar separation cylinder is fixedly connected to the support plate.
2. The excess ammonia separation tank according to claim 1, characterized in that: It also includes a manhole, which is fixedly connected to the top of the trough body.
3. The excess ammonia separation tank according to claim 1, characterized in that: The trough body is a vaulted trough or a cone-topped trough.
Citation Information
Patent Citations
Residual ammonia water oil-removal groove
CN105417629A
Tar removing method and device for ammonia distilling tower
CN105819610A
Profit mud three -phase separation device
CN208003503U
Residual ammonia water separating tank
CN216092339U