Catalyst precipitation reactor

By connecting the cavity between the hot and cold pipes and the outer and inner pipes in the catalyst precipitation reaction kettle and connecting it with the interlayer of the observation box, the problem that it is difficult to know about the internal processing of the reactor is solved, and the effect of reducing the influence of temperature difference and improving observation accuracy is achieved.

CN115178216BActive Publication Date: 2025-03-25GUANGDONG CHANGHONG AIKAIYIN TECHNOLOGY CO LTD
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Patent Information

Application Number
CN202210919611.0
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2022-08-02
Publication Date
2025-03-25
Estimated Expiration
2042-08-02

AI Technical Summary

Technical Problem

When the existing catalyst precipitation reactor is used, personnel cannot understand the processing conditions inside the reactor, which leads to difficult to know about material waste and processing problems.

Method used

By communicating the cold pipe and the heat pipe with the cavity between the first outer pipe and the first inner pipe, and communicating the cavity between the second inner pipe and the second outer pipe with the interlayer inside the observation box through the first communication pipe, the raw materials are extracted and transported to the observation box by using the suction pump, and the influence of temperature difference is reduced by using the interlayer to improve the accuracy of observation and judgment.

Benefits of technology

The impact of temperature difference on raw material properties is reduced, the accuracy of observation and judgment of staff is improved, material waste is avoided, and energy utilization is improved.

✦ Generated by Eureka AI based on patent content.

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Abstract

The present invention discloses a catalyst precipitation reactor, which specifically relates to the technical field of reactors, including a tank outside the reactor body and a tank inside the reactor body, and a stirring mechanism installed inside the tank inside the reactor body, wherein the tank inside the reactor body is arranged inside the tank outside the reactor body, and spiral cold pipes and heat pipes are arranged between the tank outside the reactor body and the tank inside the reactor body, and materials used to cool the tank inside the reactor body flow in the cold pipes. The present invention connects the cold pipe and the heat pipe used to cool or heat the inside of the tank inside the reactor body with the cavity between the first outer tube and the first inner tube, and the cavity between the second inner tube and the second outer tube, and connects the cavity between the second inner tube and the second outer tube with the interlayer inside the observation box through the first connecting tube, so as to facilitate the liquid flowing in the tank inside the reactor body and the stirring shaft to heat the raw materials inside the first inner tube, the second inner tube and the observation box, so as to reduce the influence of temperature difference changes on the properties of the raw materials and improve the accuracy of observation and judgment of the staff.
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Description

Technical Field

[0001] The invention relates to the technical field of reactors, in particular to a catalyst precipitation reactor. Background Art

[0002] The reactor is a comprehensive reaction vessel. The design of the reactor structure, function and accessories is based on the reaction conditions. From the initial feeding-reaction-discharging, the pre-set reaction steps can be completed with a high degree of automation, and the important parameters such as temperature, pressure, mechanical control (stirring, blasting, etc.), reactant / product concentration, etc. during the reaction process are strictly regulated. Its structure is generally composed of a kettle body, a transmission device, a stirring device, a heating device, a cooling device, and a sealing device.

[0003] In the process of preparing catalysts by precipitation method, a reactor is required to mix the raw materials. However, when using the existing catalyst precipitation reactor, personnel cannot understand the processing conditions inside the reactor. If the material is not completely processed and the personnel opens the discharge pipe, a large amount of material will be wasted. If there is a problem during processing, the personnel will not be able to know it to the outside world. Therefore, in order to solve the above problems, the prior art uses a suction pump to extract the material in the reactor for observation. However, in the process of extracting the raw materials in the reactor, due to the temperature difference between the inside and outside of the reactor, the properties of the raw materials observed by the staff are different under the influence of the temperature difference, which can easily affect the staff's judgment.

[0004] Therefore, it is necessary to invent a catalyst precipitation reactor to solve the above problems. Summary of the invention

[0005] The purpose of the present invention is to provide a catalyst precipitation reaction kettle, which connects the cold pipe and the hot pipe used for cooling or heating the inside of the tank in the kettle body with the cavity between the first outer tube and the first inner tube and the cavity between the second inner tube and the second outer tube, and connects the cavity between the second inner tube and the second outer tube with the interlayer inside the observation box through the first connecting pipe, so as to facilitate the liquid flowing in the tank in the kettle body and the stirring shaft to heat the raw materials inside the first inner tube, the second inner tube and the observation box, so as to reduce the influence of the temperature difference on the properties of the raw materials, improve the accuracy of the staff's observation and judgment, and solve the above-mentioned deficiencies in the technology.

[0006] In order to achieve the above-mentioned purpose, the present invention provides the following technical scheme: a catalyst precipitation reaction kettle, comprising a kettle body tank and a kettle body tank and a stirring mechanism installed inside the kettle body tank, the kettle body tank is arranged inside the kettle body tank, and a spiral cold pipe and a heat pipe are arranged between the kettle body tank and the kettle body tank, the cold pipe flows with a material for cooling the kettle body tank, the heat pipe flows with a material for heating the kettle body tank, the bottom of the kettle body tank is fixedly connected with a first inner pipe, one end of the first inner pipe is fixedly connected with a suction pump for suction, the top outlet of the suction pump is fixedly connected with a second inner pipe, one end of the second inner pipe is fixedly connected with an observation box with a sandwich, the observation box is arranged at the top of the kettle body tank, and a raw material reflux mechanism is arranged inside the observation box, and the raw material reflux mechanism extends out of the top of the observation box;

[0007] The top end of the cold pipe is fixedly connected to a first input pipe, the bottom end of the cold pipe is fixedly connected to a first output pipe, the top end of the heat pipe is fixedly connected to a second input pipe, the bottom end of the heat pipe is fixedly connected to a second output pipe, the bottom ends of the first output pipe and the second output pipe are both connected to the cavity between the first outer pipe and the first inner pipe, a third connecting pipe is fixedly connected between the first outer pipe and the second outer pipe, the third connecting pipe is arranged at the rear side of the second outer pipe, the top of the second outer pipe is fixedly connected to the first connecting pipe, and one end of the first connecting pipe is connected to the inner interlayer of the observation box.

[0008] Preferably, the stirring mechanism includes a stirring shaft installed inside the kettle body tank, the top end of the stirring shaft penetrates the kettle body tank and the kettle body tank and extends out of the top of the kettle body tank, the top end of the stirring shaft is movably connected to the kettle body tank and the kettle body tank via a sealed bearing, the bottom end of the stirring shaft is movably connected to the inner wall of the kettle body tank via a bearing, a plurality of stirring rods are fixedly provided at the bottom end of the stirring shaft, the stirring rods are arranged inside the kettle body tank, a mechanical seal is provided outside the top end of the stirring shaft, the mechanical seal is provided on the top of the kettle body tank, a motor is provided on the top of the mechanical seal to drive the stirring shaft to rotate, and the stirring mechanism can stir and process the raw materials in the kettle body tank.

[0009] Preferably, a feed pipe is provided on one side of the top of the outer tank of the kettle body, and the bottom end of the feed pipe is fixedly connected to the inside of the tank in the kettle body; a discharge pipe is provided on one side of the bottom of the outer tank of the kettle body, and the top end of the discharge pipe is fixedly connected to the bottom end of the inside of the tank in the kettle body; the outer ends of the feed pipe and the discharge pipe are both fixedly provided with a first solenoid valve.

[0010] Preferably, the outer ends of the first input pipe, the first output pipe, the second input pipe and the second output pipe are all fixedly provided with a first switch valve, and the outer end of the first connecting pipe is fixedly provided with a second solenoid valve.

[0011] Preferably, a third output pipe and a fourth output pipe are provided on the rear side of the observation box, which are distributed vertically. One end of the third output pipe and one end of the fourth output pipe are both connected to the internal interlayer of the observation box. A second switch valve is fixedly provided at the outer end of the third output pipe and the outer end of the fourth output pipe.

[0012] Preferably, a transparent plate is fixedly provided on the front side of the observation box, and the transparent plate is embedded in the front wall of the observation box, so that the staff can conveniently observe the raw materials inside the observation box through the transparent plate.

[0013] Preferably, the raw material reflux mechanism includes a partition installed inside the observation box, a second connecting pipe is fixedly provided inside the partition, the bottom end of the second connecting pipe penetrates the outer tank of the kettle body and the inner tank of the kettle body and extends into the inner tank of the kettle body, the second connecting pipe is communicated with the inner tank of the kettle body, a piston plate is provided on the top of the partition, two threaded rods are fixedly provided on the top of the piston plate, the outer ends of the threaded rods are threadedly connected with hollow rods, the top ends of the hollow rods penetrate the observation box and extend out of the top of the observation box, the hollow rods are movably connected to the observation box through sealed bearings, one of the hollow rods is provided with a forward and reverse motor to drive it to rotate, a transmission assembly is provided between the two hollow rods to drive the two hollow rods to rotate synchronously, and the raw materials drawn into the observation box can be pushed downward by using the piston plate to squeeze through the first outer tube to flow back to the inner tank of the kettle body.

[0014] Preferably, the transmission assembly includes a pulley installed at the outer ends of the two hollow rods, a belt is provided between the two pulleys, and the pulley and the belt are both provided on the top of the observation box. The two hollow rods can be driven to rotate synchronously by utilizing the belt and the pulley. A limit frame is fixedly provided on the top of the observation box, and the top ends of the two hollow rods pass through the top of the limit frame and are movably connected to the limit frame through bearings. The limit frame can be used to support the hollow rods.

[0015] Preferably, a third solenoid valve is fixedly provided at the outer end of the second connecting pipe, and the third solenoid valve is arranged at the bottom end of the observation box. The third solenoid valve can prevent the raw materials drawn into the observation box from flowing downward through the second connecting pipe, and can also prevent the raw materials in the tank in the kettle from entering the observation box through the second connecting pipe.

[0016] Preferably, a cushion block is provided at the bottom of the suction pump, the bottom of which is in contact with the ground, and the cushion block is used to support the suction pump from the bottom so that the water suction port of the suction pump can be flush with the first outer tube.

[0017] In the above technical solution, the technical effects and advantages provided by the present invention are:

[0018] 1. The raw materials in the tank in the kettle body are extracted by using a suction pump and a first inner tube, and then the extracted raw materials are transported to the inside of the observation box through the second inner tube. In order to balance the temperature difference between the inside and outside of the tank in the kettle body, a first outer tube and a second outer tube are respectively wrapped outside the first inner tube and the second inner tube, and a cold tube and a hot tube used for cooling or heating the inside of the tank in the kettle body are connected with the cavity between the first outer tube and the first inner tube and the cavity between the second inner tube and the second outer tube, and the cavity between the second inner tube and the second outer tube is connected with the interlayer inside the observation box through the first connecting tube, so that the liquid flowing in the tank in the kettle body and the stirring shaft heats the raw materials inside the first inner tube, the second inner tube and the observation box, so as to reduce the influence of the temperature difference on the properties of the raw materials and improve the accuracy of observation and judgment of the staff;

[0019] 2. By introducing the materials used for heating or cooling in the inner tank of the kettle and the stirring shaft into the cavity between the first outer tube and the first inner tube and the cavity between the second inner tube and the second outer tube for reuse, the utilization rate of energy can be improved;

[0020] 3. By introducing the raw materials into the observation box for observation, and using the piston plate installed inside the observation box to squeeze the raw materials flowing into the observation box downward, the raw materials can flow downward into the inner tank of the kettle through the second connecting pipe to continue processing, thereby avoiding waste of raw materials. BRIEF DESCRIPTION OF THE DRAWINGS

[0021] In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings required for use in the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments recorded in the present invention. For ordinary technicians in this field, other drawings can also be obtained based on these drawings.

[0022] Figure 1 It is a schematic diagram of the overall structure of the present invention;

[0023] Figure 2 For the present invention Figure 1 Left view of

[0024] Figure 3 For the present invention Figure 2 Bottom view of

[0025] Figure 4 It is a schematic diagram of the structure of the kettle body outer tank after being cut open;

[0026] Figure 5 It is a schematic diagram of the structure of the kettle body outer tank and the kettle body tank after being cut apart;

[0027] Figure 6 For the present invention Figure 5 A magnified view of middle;

[0028] Figure 7 It is a schematic diagram of the structure of the cold pipe and the heat pipe of the present invention;

[0029] Figure 8 It is a schematic structural diagram of the observation box of the present invention after being cut open.

[0030] Description of reference numerals:

[0031] 1 kettle body outer tank, 2 kettle body inner tank, 3 stirring shaft, 4 mechanical seal, 5 motor, 6 stirring rod, 7 cold pipe, 8 hot pipe, 9 first input pipe, 10 first output pipe, 11 second input pipe, 12 second output pipe, 13 first outer pipe, 14 first inner pipe, 15 suction pump, 16 second inner pipe, 17 second outer pipe, 18 observation box, 19 first connecting pipe, 20 third output pipe, 21 fourth output pipe, 22 partition, 23 second connecting pipe, 24 piston plate, 25 threaded rod, 26 hollow rod, 27 forward and reverse motor, 28 pulley, 29 belt, 30 limit frame, 31 transparent plate, 32 feed pipe, 33 discharge pipe, 34 third connecting pipe. DETAILED DESCRIPTION

[0032] In order to enable those skilled in the art to better understand the technical solution of the present invention, the present invention will be further described in detail below with reference to the accompanying drawings.

[0033] The present invention provides Figure 1-3 The catalyst precipitation reactor shown comprises an outer tank 1 and an inner tank 2. The inner tank 2 is arranged inside the outer tank 1. If the catalyst is to be processed, the raw materials need to be added into the inner tank 2 for reaction. In order to facilitate feeding, a feed pipe 32 is provided on the top side of the outer tank 1. The bottom end of the feed pipe 32 is fixedly connected with the inner tank 2. A discharge pipe 33 is provided on the bottom side of the outer tank 1. The top end of the discharge pipe 33 is fixedly connected with the bottom end of the inner tank 2. The outer ends of the feed pipe 32 and the discharge pipe 33 are fixedly provided with a first solenoid valve. The raw materials are introduced into the inner tank 2 through the feed pipe 32 for easy processing. The processed raw materials can be discharged through the discharge pipe 33 to complete the entire catalyst processing feeding and discharging process.

[0034] Moreover, during the processing, it is necessary to stir the raw materials inside the kettle body tank 2. As shown in FIG5 , the present invention further includes a stirring mechanism installed inside the kettle body tank 2. Specifically, the stirring mechanism includes a stirring shaft 3 installed inside the kettle body tank 2. The top end of the stirring shaft 3 penetrates the kettle body tank 2 and the kettle body tank 1 and extends out of the top of the kettle body tank 1. The top end of the stirring shaft 3 is movably connected to the kettle body tank 2 and the kettle body tank 1 through a sealed bearing. The bottom end of the stirring shaft 3 is movably connected to the inner wall of the kettle body tank 2 through a bearing. A plurality of stirring rods 6 are fixedly provided at the bottom end of the stirring shaft 3. The stirring rods 6 are arranged inside the kettle body tank 2. A mechanical seal 4 is arranged outside the top end of the stirring shaft 3. The mechanical seal 4 is arranged at the top of the kettle body tank 1. A motor 5 that drives the stirring shaft 3 to rotate is provided at the top of the mechanical seal 4.

[0035] When processing the raw materials, the motor 5 is started, the motor 5 is used to drive the stirring shaft 3 to rotate, and the stirring shaft 3 is used to drive the stirring rod 6 to stir and process the raw materials in the inner tank 2 of the kettle body. In addition, the mechanical seal 4 set at the top of the stirring shaft 3 can also improve the overall sealing performance.

[0036] In addition, during the stirring process of the raw materials, the raw materials need to be cooled or heated depending on the type of catalyst, such as Figure 4 and 6 As shown, a spiral cold pipe 7 and a heat pipe 8 are provided between the outer tank 1 of the kettle body and the outer tank 2 of the kettle body. The cold pipe 7 flows with materials for cooling the inner tank 2 of the kettle body, and the heat pipe 8 flows with materials for heating the inner tank 2 of the kettle body. By injecting a low-temperature fluid into the cold pipe 7, the heat of the materials in the inner tank 2 of the kettle body can be absorbed during the reaction process to achieve the purpose of cooling. Moreover, by injecting a high-temperature fluid into the heat pipe 8, the inner tank 2 of the kettle body can be heated.

[0037] During the reaction, in order to facilitate the staff to observe the reaction of the raw materials in the tank 2 in the kettle, the staff needs to take out some of the raw materials for observation. Figure 5-8 As shown, the bottom end of the inner tank 2 of the kettle body is fixedly connected with a first inner tube 14, one end of the first inner tube 14 is fixedly connected with a suction pump 15 for suction, and a cushion block is provided at the bottom of the suction pump 15, the bottom of which is in contact with the ground, and the cushion block is used to support the suction pump 15 from the bottom, so that the water suction port of the suction pump 15 can be flush with the first outer tube 13, and the top outlet of the suction pump 15 is fixedly connected with a second inner tube 16, one end of the second inner tube 16 is fixedly connected with an observation box 18 with a interlayer, and the observation box 18 is arranged on the top of the outer tank 1 of the kettle body, and the suction pump 15 can be used to suck the raw materials in the tank 2 of the kettle body through the first inner tube 14 and the second inner tube 16 into the observation box 18 for observation by utilizing the suction of the suction pump 15, and since a transparent plate 31 is fixedly provided on the front side of the observation box 18, the transparent plate 31 is embedded in the front wall of the observation box 18, and the staff can observe the raw materials inside the observation box 18 through the transparent plate 31.

[0038] In the process of pumping raw materials, in order to avoid the influence of the temperature difference between the inside and outside of tank 2 in the kettle on the properties of the raw materials, such as Figure 7 As shown, the top of the cold pipe 7 is fixedly connected to the first input pipe 9, the bottom of the cold pipe 7 is fixedly connected to the first output pipe 10, the top of the heat pipe 8 is fixedly connected to the second input pipe 11, the bottom of the heat pipe 8 is fixedly connected to the second output pipe 12, the bottom of the first output pipe 10 and the bottom of the second output pipe 12 are both connected to the cavity between the first outer pipe 13 and the first inner pipe 14, the first outer pipe 13 and the second outer pipe 17 are fixedly connected to the third connecting pipe 34, the third connecting pipe 34 is arranged at the rear side of the second outer pipe 17, the top of the second outer pipe 17 is fixedly connected to the first connecting pipe 19, one end of the first connecting pipe 19 is connected to the inner interlayer of the observation box 18, and the outer ends of the first input pipe 9, the first output pipe 10, the second input pipe 11 and the second output pipe 12 are fixedly provided with a first switch valve, and the first connecting pipe 19 A second solenoid valve is fixedly provided at the outer end, and the fluid injected into the cold pipe 7 and the hot pipe 8 can enter the cavity between the first outer pipe 13 and the first inner pipe 14 through the first output pipe 10 and the second output pipe 12 respectively, and can also enter the cavity between the second inner pipe 16 and the second outer pipe 17 through the third connecting pipe 34, and then enter the interlayer of the observation box 18 through the first connecting pipe 19, so that the fluid can be used to cool or heat the raw materials inside the first inner pipe 14, the second inner pipe 16 and the observation box 18, so that their temperature can be the same as that in the inner tank 2 of the kettle body, reduce the temperature difference, avoid the influence of the temperature difference change on the properties of the raw materials, and improve the accuracy of the staff's observation and judgment;

[0039] In order to ensure the circulation of low-temperature fluid or high-temperature fluid, Figure 2 As shown, the rear side of the observation box 18 is provided with a third output pipe 20 and a fourth output pipe 21 distributed up and down, one end of the third output pipe 20 and one end of the fourth output pipe 21 are both connected to the internal interlayer of the observation box 18, and the outer ends of the third output pipe 20 and the outer ends of the fourth output pipe 21 are fixedly provided with a second switch valve. During the reaction, the cold pipe 7 and the third output pipe 20 can be connected to the input pipeline and the output pipeline of the low-temperature fluid respectively, and the second input pipe 11 and the fourth output pipe 21 can be connected to the input pipeline and the output pipeline of the high-temperature fluid respectively, so as to ensure the circulation of the fluid.

[0040] After the observation, in order to be able to re-introduce the fluid in the observation box 18 into the interior of the kettle tank 2, as shown in FIG. Figure 5 and 8As shown, a raw material reflux mechanism is provided inside the observation box 18, and the raw material reflux mechanism extends out of the top of the observation box 18. Specifically, the raw material reflux mechanism includes a partition 22 installed inside the observation box 18, and a second connecting pipe 23 is fixedly provided inside the partition 22. The bottom end of the second connecting pipe 23 passes through the outer tank 1 of the kettle body and the inner tank 2 of the kettle body and extends into the inner tank 2 of the kettle body. The second connecting pipe 23 is connected to the inner tank 2 of the kettle body. A piston plate 24 is provided on the top of the partition 22, and two threaded rods 25 are fixedly provided on the top of the piston plate 24. The outer end of the threaded rod 25 is threadedly connected with a hollow rod 26. The top end of the hollow rod 26 passes through the observation box 18 and extends out of the top of the observation box 18. The hollow rod 26 is movably connected to the observation box 18 through a sealed bearing, and one of the hollow rods 26 is provided with a forward and reverse bearing on the top to drive it to rotate. A motor 27 and a transmission assembly are provided between the two hollow rods 26 to drive the two hollow rods 26 to rotate synchronously. Moreover, the transmission assembly includes a pulley 28 installed at the outer ends of the two hollow rods 26, and a belt 29 is provided between the two pulleys 28. The pulley 28 and the belt 29 are both provided at the top of the observation box 18. The two hollow rods 26 can be driven to rotate synchronously by using the belt 29 and the pulley 28. The raw materials drawn into the observation box 18 can be pushed back to the interior of the tank 2 in the kettle body through the first outer tube 13 by using the piston plate 24 to squeeze downward. A limit frame 30 is fixedly provided on the top of the observation box 18. The top ends of the two hollow rods 26 pass through the top of the limit frame 30 and are movably connected to the limit frame 30 through bearings. The limit frame 30 can be used to support the hollow rods 26.

[0041] In order to prevent the liquid in the observation box 18 from automatically entering the interior of the kettle tank 2 through the second connecting pipe 23, as shown in FIG. Figure 8 As shown, a third solenoid valve is fixedly provided at the outer end of the second connecting pipe 23, and the third solenoid valve is arranged at the bottom end of the observation box 18. The third solenoid valve can prevent the raw materials drawn into the observation box 18 from flowing downward through the second connecting pipe 23, and can also prevent the raw materials in the inner tank 2 of the kettle from entering the observation box 18 through the second connecting pipe 23;

[0042] After the second inner tube 16 draws the raw materials into the observation box 18, the piston plate 24 is located at the top of the observation box 18, and the third solenoid valve outside the second connecting tube 23 is in a closed state. After observing the raw materials, the staff opens the second connecting tube 23 and starts the forward and reverse motor 27. The forward and reverse motor 27 is used to drive the threaded rod 25 and the piston plate 24 to move downward, so that the principle in the observation box 18 can be squeezed through the second connecting tube 23 to flow into the inner tank 2 of the kettle body to continue the reaction, thereby avoiding waste of raw materials.

[0043] The above description is only by way of illustration of certain exemplary embodiments of the present invention. It is undoubted that those skilled in the art can modify the described embodiments in various ways without departing from the spirit and scope of the present invention. Therefore, the above drawings and descriptions are illustrative in nature and should not be construed as limiting the scope of protection of the claims of the present invention.

Claims

1. A catalyst precipitation reaction kettle, comprising an outer kettle tank (1) and an inner kettle tank (2) and a stirring mechanism installed inside the inner kettle tank (2), wherein the inner kettle tank (2) is arranged inside the outer kettle tank (1), and characterized in that: A spiral cold pipe (7) and a heat pipe (8) are provided between the outer tank (1) of the kettle body and the inner tank (2) of the kettle body. The cold pipe (7) flows with materials for cooling the inner tank (2) of the kettle body, and the heat pipe (8) flows with materials for heating the inner tank (2) of the kettle body. The bottom of the inner tank (2) of the kettle body is fixedly connected with a first inner pipe (14). One end of the first inner pipe (14) is fixedly connected with a suction pump (15) for suction. The top outlet of the suction pump (15) is fixedly connected with a second inner pipe (16). One end of the second inner pipe (16) is fixedly connected with an observation box (18) with a sandwich layer. The observation box (18) is provided at the top of the outer tank (1) of the kettle body. A raw material reflux mechanism is provided inside the observation box (18). The raw material reflux mechanism extends out of the top of the observation box (18). The top end of the cold pipe (7) is fixedly connected to a first input pipe (9), the bottom end of the cold pipe (7) is fixedly connected to a first output pipe (10), the top end of the heat pipe (8) is fixedly connected to a second input pipe (11), the bottom end of the heat pipe (8) is fixedly connected to a second output pipe (12), the bottom end of the first output pipe (10) and the bottom end of the second output pipe (12) are both connected to the cavity between the first outer pipe (13) and the first inner pipe (14), a third connecting pipe (34) is fixedly connected between the first outer pipe (13) and the second outer pipe (17), the third connecting pipe (34) is arranged at the rear side of the second outer pipe (17), the top of the second outer pipe (17) is fixedly connected to a first connecting pipe (19), one end of the first connecting pipe (19) is connected to the inner interlayer of the observation box (18); The raw material reflux mechanism comprises a partition (22) installed inside the observation box (18), a second connecting pipe (23) is fixedly arranged inside the partition (22), the bottom end of the second connecting pipe (23) passes through the kettle body outer tank (1) and the kettle body inner tank (2) and extends into the kettle body inner tank (2), the second connecting pipe (23) is connected with the kettle body inner tank (2), and a piston plate (24) is arranged on the top of the partition (2).

2. The catalyst precipitation reactor according to claim 1, characterized in that: The stirring mechanism comprises a stirring shaft (3) installed inside the kettle body tank (2); the top end of the stirring shaft (3) penetrates the kettle body tank (2) and the kettle body tank (1) and extends out of the top of the kettle body tank (1); the top end of the stirring shaft (3) is movably connected to the kettle body tank (2) and the kettle body tank (1) via a sealed bearing; the bottom end of the stirring shaft (3) is movably connected to the inner wall of the kettle body tank (2) via a bearing; a plurality of stirring rods (6) are fixedly provided at the bottom end of the stirring shaft (3); the stirring rods (6) are arranged inside the kettle body tank (2); a mechanical seal (4) is provided outside the top end of the stirring shaft (3); the mechanical seal (4) is arranged at the top of the kettle body tank (1); and a motor (5) for driving the stirring shaft (3) to rotate is provided at the top of the mechanical seal (4).

3. The catalyst precipitation reactor according to claim 1, characterized in that: A feed pipe (32) is provided on one side of the top of the outer tank (1) of the kettle body, and the bottom end of the feed pipe (32) is fixedly connected to the inside of the inner tank (2) of the kettle body. A discharge pipe (33) is provided on one side of the bottom of the outer tank (1) of the kettle body, and the top end of the discharge pipe (33) is fixedly connected to the bottom end of the inner tank (2) of the kettle body. The outer ends of the feed pipe (32) and the discharge pipe (33) are both fixedly provided with a first solenoid valve.

4. The catalyst precipitation reactor according to claim 1, characterized in that: The outer ends of the first input pipe (9), the first output pipe (10), the second input pipe (11), and the second output pipe (12) are all fixedly provided with a first switch valve, and the outer end of the first connecting pipe (19) is fixedly provided with a second solenoid valve.

5. The catalyst precipitation reactor according to claim 1, characterized in that: A third output pipe (20) and a fourth output pipe (21) are arranged on the rear side of the observation box (18) and are distributed up and down; one end of the third output pipe (20) and one end of the fourth output pipe (21) are both connected to the inner interlayer of the observation box (18); and a second switch valve is fixedly provided at the outer end of the third output pipe (20) and the outer end of the fourth output pipe (21).

6. The catalyst precipitation reactor according to claim 1, characterized in that: A transparent plate (31) is fixedly provided on the front side of the observation box (18), and the transparent plate (31) is embedded in the front wall of the observation box (18).

7. The catalyst precipitation reactor according to claim 1, characterized in that: Two threaded rods (25) are fixedly provided on the top of the piston plate (24), and the outer ends of the threaded rods (25) are threadedly connected to hollow rods (26). The top ends of the hollow rods (26) penetrate the observation box (18) and extend out of the top of the observation box (18). The hollow rods (26) are movably connected to the observation box (18) via sealed bearings. A forward and reverse motor (27) is provided at the top of one of the hollow rods (26) to drive the hollow rods (26) to rotate, and a transmission assembly is provided between the two hollow rods (26) to drive the two hollow rods (26) to rotate synchronously.

8. The catalyst precipitation reactor according to claim 7, characterized in that: The transmission assembly comprises a pulley (28) mounted on the outer ends of two hollow rods (26), a belt (29) being arranged between the two pulleys (28), the pulley (28) and the belt (29) being arranged on the top of an observation box (18), a limiting frame (30) being fixedly arranged on the top of the observation box (18), the top ends of the two hollow rods (26) both passing through the top of the limiting frame (30) and being movably connected to the limiting frame (30) via bearings.

9. The catalyst precipitation reactor according to claim 7, characterized in that: A third solenoid valve is fixedly provided at the outer end of the second connecting pipe (23), and the third solenoid valve is arranged at the bottom end inside the observation box (18).

10. The catalyst precipitation reactor according to claim 1, characterized in that: A cushion block is provided at the bottom of the suction pump (15), and the bottom of the cushion block is in contact with the ground.

Citation Information

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