A thin film silanization surface modification system

By designing a thin film silanized surface modification system, the problem of modification and treatment of large-size flexible film materials is solved, and the effective silanization and drying of the film is achieved, which avoids film damage and wrinkles and improves the processing efficiency.

CN116622111BActive Publication Date: 2025-07-11SHANGHAI INST OF CERAMIC CHEM & TECH CHINESE ACAD OF SCI
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Patent Information

Application Number
CN202310598021.7
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2023-05-25
Publication Date
2025-07-11
Estimated Expiration
2043-05-25

AI Technical Summary

Technical Problem

The prior art is difficult to effectively deal with surface modification of large-size flexible polymer film materials, and existing systems are prone to damage to the film.

Method used

A thin film silanization surface modification system is designed, including a thin film fixing device, a thin film silanization treatment device and a thin film heat treatment device. The thin film is fixed by clamping components, silanization treatment is performed using silane reagent, and dried by heating device to ensure that the film is not damaged during the treatment process.

Benefits of technology

Effective silanization treatment of large-size flexible film materials is achieved, avoiding film damage and wrinkles, and improving treatment efficiency and effect.

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Abstract

The present invention discloses a thin film silanization surface modification system, which includes a thin film fixing device, a thin film silanization treatment device, and a thin film heat treatment device. The thin film fixing device includes a fixing frame, and a plurality of clamping components are arranged on the inner frame of the fixing frame. The clamping components are used to fix and extend the thin film to be treated on the fixing frame. The thin film silanization treatment device includes a first housing, a first accommodating cavity is opened in the first housing, a reaction container is arranged in the first accommodating cavity, a reaction tank is opened in the reaction container, the reaction tank is filled with a silane reagent, and first heating devices are further arranged on both sides of the reaction container corresponding to the reaction tank. The reaction tank is matched with the fixing frame, so that the thin film to be treated can be unfolded in the reaction container through the fixing frame and subjected to silanization treatment. The thin film heat treatment device is used to heat and dry the thin film to be treated that has been silanized, solving the problem that the thin film silanization surface modification system in the prior art cannot process large-sized thin films.
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Description

Technical Field

[0001] The present invention relates to the technical field of surface modification, and further relates to a thin film silanization surface modification system. Background Art

[0002] Flexible polymer thin film materials such as polyimide, polyester, fluoroplastics, etc. are key materials for spacecraft surfaces due to their light weight, good processing performance, excellent mechanical properties, and excellent light and heat properties, and are used to effectively protect spacecraft from the adverse space environmental factors in low Earth orbit. There are a large number of highly oxidizing atomic oxygen in the space environment of low Earth orbit. The highly kinetic and highly oxidation-active atomic oxygen is likely to cause severe erosion to the polymer thin film materials on the surface of the spacecraft, thus seriously affecting the service life of the spacecraft. Therefore, it is necessary to carry out protective treatment on the polymer thin film materials of spacecraft components. The key technology developed recently is to form a protective layer with a gradually changing composition gradient through anti-atomic oxygen surface modification, which can solve the problem of atomic oxygen erosion of polymer thin film materials and retain the original use performance of the polymer materials.

[0003] With the continuous iterative development of spacecraft, higher requirements are put forward for the size and performance of polymer thin films. The surface modification systems in the prior art can only better complete the modification treatment of small-sized thin film materials, and the thin film fixing devices in the prior art surface modification systems are only suitable for processing semi-rigid materials, and it is difficult to complete the modification treatment of large-sized flexible thin film materials. There is a problem of substrate damage in the fixation of flexible thin film materials. Summary of the Invention

[0004] Aiming at the above technical problems, the purpose of the present invention is to provide a thin film silanization surface modification system and a use method, which solve the problems in the prior art.

[0005] To achieve the above purpose, the present invention provides a thin film silanization surface modification system, including:

[0006] A thin film fixing device, including a fixing frame, and a plurality of clamping components are arranged on the inner frame of the fixing frame. The clamping components are used to fix and extend the thin film to be processed on the fixing frame;

[0007] A thin film silanization treatment device, including a first housing, a first accommodation cavity is opened in the first housing, a reaction container is arranged in the first accommodation cavity, a reaction tank is opened in the reaction container, the reaction tank is filled with a silane reagent, and first heating devices are further arranged on both sides of the reaction container corresponding to the reaction tank. The first heating devices are used to heat the silane reagent to accelerate the silanization reaction. The reaction tank matches the fixing frame, so that the thin film to be processed can be unfolded in the reaction container through the fixing frame and undergo silanization treatment;

[0008] The film heat treatment device is used for heating and drying the film to be treated that has been silanized.

[0009] The film to be treated is fixed and unfolded in the inner frame under the clamping action of the clamping assembly, and then the fixed frame holding the film to be treated is transferred to the reaction tank manually or by a lifting mechanism, and is fully contacted with the silane reagent heated by the first heating device in the reaction tank, so that the surface of the film to be treated completes the activated silanization reaction, and then the film to be treated and the fixed frame that have completed the silanization reaction are transferred from the reaction tank to the film heat treatment device manually or by a lifting mechanism, and the silanized film to be treated is heated and dried, thereby completing the surface modification of the film to be treated.

[0010] In some embodiments, the fixing frame includes:

[0011] A concave connecting member, the concave connecting member being arranged on a side of the fixing frame close to the clamping assembly;

[0012] An L-shaped connector, the L-shaped connector is arranged on one side of the clamping assembly close to the concave connector, the L-shaped connector is provided with a strip hole, the concave connector is provided with a groove with a fixing hole, the strip hole and the fixing hole are connected through a tension screw, so that the L-shaped connector is connected and fitted in the groove of the concave connector, and can complete the sliding action when the tension screw is loosened.

[0013] The tightness of the film to be processed is adjusted by sliding the L-shaped connector on the concave connector to avoid damage to the film to be processed due to excessive clamping tension or wrinkles on the film to be processed due to insufficient clamping force.

[0014] In some embodiments, the clamping assembly comprises:

[0015] A clamp, comprising a first clamp and a second clamp, wherein the first clamp and the second clamp are hingedly connected by a plurality of hinge structures, a concave tooth structure is provided on a side of the first clamp close to the second clamp, and a convex tooth structure is provided on a side of the second clamp close to the first clamp, wherein the concave tooth structure is correspondingly engaged with the convex tooth structure;

[0016] A plurality of pressing members are clamped on the clamping members, and manual butterfly screws are arranged on the pressing members to adjust the pressure of the film to be processed clamped on the two groups of clamping strips.

[0017] By corresponding engagement of the concave tooth structure and the convex tooth structure, the film to be processed is effectively prevented from falling off. The clamping force of the pressing member is adjusted by manually adjusting the butterfly screw, and then the pressure of the film to be processed clamped on the two sets of clamping strips is adjusted, effectively avoiding the situation that the film to be processed falls off due to too small clamping force or the film to be processed is damaged due to too large clamping force.

[0018] In some embodiments,

[0019] The reaction tank includes an upper tank and a lower tank vertically communicating with the upper tank. The upper tank and the lower tank form a T-shaped tank. The opening of the upper tank corresponds to the opening of the first accommodation cavity. Chamfers are provided at the joints of the lower tank and the upper tank.

[0020] The lower tank and the upper tank form a T-shaped tank, which not only helps to reduce the usage amount of the silane reagent to effectively reduce the cost, but also effectively avoids the situation that the silane reagent expands and overflows after heating. The setting of the chamfer makes it easier to place the fixing frame into the lower tank.

[0021] In some embodiments, the first heating device includes a plurality of first heating tubes. The plurality of first heating tubes are closely arranged on the outer sides of the two side walls of the lower tank, and heat insulation cotton is arranged in the gaps between the plurality of first heating tubes.

[0022] The heating tubes are used to provide heat sources for heating the silane reagent in the reaction tank to accelerate the silanization reaction of the film to be processed. Heat insulation cotton is filled between the heating tubes to maintain the temperature of the silane reagent in the reaction tank, improve the heat insulation performance of the film silanization treatment device, and thus reduce the loss of heat energy.

[0023] In some embodiments, the film heat treatment device includes a second housing. A second accommodation cavity is provided on the second housing. A placement container is arranged in the second accommodation cavity. A heating and drying tank is provided in the placement container. A second heating device is further arranged in the second housing. The second heating device is located outside the two side walls of the heating and drying tank. The heating and drying tank matches the fixing frame, so that the film to be processed that has been silanized is heat-treated by the second heating device in the placement container.

[0024] In some embodiments, a first opening is provided on the side wall of the placement container, and a first sealing door is detachably arranged at the first opening;

[0025] The film heat treatment device further includes a moving track and a moving bracket corresponding to the moving track. The moving track is arranged at the bottom of the placement container and extends outward through the first opening. A fixing seat for fixing the fixing frame is arranged on the moving bracket, so that the film to be treated can be transferred along the moving track to a predetermined position of the placement container.

[0026] The setting of the moving track enables the fixing frame fixed with the film to be treated to be quickly and stably conveyed into the heating and drying tank for subsequent heating and drying treatment of the film to be treated.

[0027] In some embodiments, a plurality of circulating air holes are opened on the side walls of the placement container parallel to the moving track;

[0028] The second heating device includes: a plurality of second heating tubes, which are respectively fixedly arranged on the outer sides of the two side walls of the placement container;

[0029] A plurality of circulating air impellers, which are all arranged on the top of the placement container.

[0030] Through the cooperation of the circulating air impellers and a plurality of circulating air holes, a hot air circulation can be formed in the placement tank after the first sealing door is closed to accelerate the heat treatment of the film to be treated.

[0031] In some embodiments, a second opening is opened on the other side wall of the second housing corresponding to the first opening, and a second sealing door is detachably connected to the second opening;

[0032] The number of the film heat treatment devices is two, and the two film heat treatment devices are connected by a plurality of connection components, and the first opening and the second opening are in contact correspondingly.

[0033] By combining and connecting two film heat treatment devices, a placement tank with a longer space is formed for heating and drying treatment of films to be treated with longer dimensions, so that the application range of the whole system is wider.

[0034] In some embodiments, the connection components include:

[0035] Two connecting pieces, which are respectively arranged at corresponding positions on the two film heat treatment devices;

[0036] A connecting bolt, which connects the two connecting pieces through a fastening nut.

[0037] Through a film silanization surface modification system provided by the present invention, at least one of the following beneficial effects can be brought:

[0038] 1. The thin film silanization surface modification system provided by the present invention solves the problem of fixing the thin film to be processed by adding a thin film fixing device. At the same time, a reaction vessel matching the fixing frame is set, so that the thin film to be processed can enter the reaction tank in the reaction vessel in a state of being unfolded and fixed, so that the thin film can fully contact with the silane reagent in the reaction tank, and then under the heating action of the first heating device, the silanization treatment is accelerated. Then, the thin film to be processed that has been silanized is put into the thin film heat treatment device for heating and drying treatment, so that the surface of the thin film to be processed after the activated silanization reaction is heat-stabilized.

[0039] 2. The thin film silanization surface modification system provided by the present invention adds a concave connecting piece and an L-shaped connecting piece, so that while the fixing frame can clamp and fix the thin film to be processed, the L-shaped connecting piece can be slid on the concave connecting piece to adjust the unfolding tightness of the thin film to be processed, so as to avoid damage to the thin film to be processed caused by excessive clamping force or wrinkles on the thin film to be processed caused by too small clamping force. BRIEF DESCRIPTION OF THE DRAWINGS

[0040] The above characteristics, technical features, advantages and their implementation manners of the present invention will be further described below in a clear and easy-to-understand manner in conjunction with the drawings in the preferred embodiments.

[0041] Figure 1 is an overall schematic diagram of the thin film silanization surface modification system of the embodiment of the present invention;

[0042] Figure 2 is a front view structural schematic diagram of the thin film fixing device of the embodiment of the present invention;

[0043] Figure 3 is a front view structural schematic diagram of the fixing structure of the embodiment of the present invention;

[0044] Figure 4 is a structural schematic diagram of the clamping assembly of the embodiment of the present invention;

[0045] Figure 5 is a front view perspective structural schematic diagram of the thin film silanization treatment device of the embodiment of the present invention;

[0046] Figure 6 is a side view perspective structural schematic diagram of the thin film silanization treatment device of the embodiment of the present invention;

[0047] Figure 7 is a front view perspective structural schematic diagram of the thin film heat treatment device of the embodiment of the present invention;

[0048] Figure 8 is an elevation structural schematic diagram of two thin film heat treatment devices of the embodiment of the present invention;

[0049] Figure 9 It is a schematic side perspective structure diagram of the thin film heat treatment device according to an embodiment of the present invention;

[0050] Figure 10 It is an enlarged structure schematic diagram of the connection structure between two thin film heat treatment devices according to an embodiment of the present invention.

[0051] Explanation of the reference numerals in the drawings:

[0052] Thin film to be processed 10, thin film fixing device 20, fixing frame 21, clamping member 22, pressing member 23, butterfly screw 231, concave connecting member 24, L-shaped connecting member 25, strip hole 251, tensioning screw 26, hinge structure 27, thin film silanization treatment device 30, first heating tube 31, first housing 32, upper groove 33, lower groove 34, sealing cover 35, thin film heat treatment device 40, moving track 41, moving bracket 42, first sealing door 43, second heating tube 44, circulating air impeller 45, circulating air hole 46, second housing 47, placing groove 48, second sealing door 49, connecting member 50, connecting bolt 51, fastening nut 52, flat gasket 53, baffle 54. Detailed implementation manners

[0053] In order to more clearly illustrate the technical solutions in the embodiments of the present invention or the prior art, the specific implementation manners of the present invention will be described below with reference to the accompanying drawings. Obviously, the drawings in the following description are only some embodiments of the present invention. For those of ordinary skill in the art, without creative efforts, other drawings can be obtained based on these drawings, and other implementation manners can also be obtained.

[0054] For the sake of simplicity of the drawings, only the parts related to the invention are schematically shown in each drawing, and they do not represent the actual structure of the product. In addition, for the sake of simplicity and easy understanding of the drawings, in some drawings, components with the same structure or function are only schematically shown for one of them, or only one of them is marked. In this document, "one" not only means "only this one", but also means "more than one" situation.

[0055] It should also be further understood that the term "and / or" used in the specification and appended claims of the present application refers to any combination and all possible combinations of one or more of the associated listed items, and includes these combinations.

[0056] In this document, it should be noted that, unless otherwise clearly specified and limited, the terms "installed", "connected", and "connected" should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection, or it can be indirectly connected through an intermediate medium, or it can be the internal communication of two components. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.

[0057] In addition, in the description of the present application, the terms "first", "second", etc. are only used to distinguish the description and cannot be understood as indicating or implying relative importance.

[0058] In one embodiment, the reference specification Figure 1 As shown, a thin film silanization surface modification system provided by the present invention includes a thin film fixing device 20, a thin film silanization treatment device 30 and a thin film heat treatment device 40, wherein the thin film fixing device 20 includes a fixing frame 21, and a plurality of clamping components are arranged on the inner frame of the fixing frame 21, and the clamping components are used to fix and extend the film 10 to be treated on the fixing frame 21, and the thin film silanization treatment device 30 includes a first shell 32, and the first shell 32 is provided with a first accommodating cavity, and a reaction container is arranged in the first accommodating cavity, and a reaction tank is arranged in the reaction container, and the reaction tank is filled with a silane reagent, and a first heating device is also arranged on both sides of the reaction container corresponding to the reaction tank, and the first heating device is used to heat the silane reagent to accelerate the silanization reaction, and the reaction tank is matched with the fixing frame 21, so that the film 10 to be treated can be unfolded in the reaction container through the fixing frame 21 and subjected to silanization treatment, and the thin film heat treatment device 40 is used to heat and dry the film 10 to be treated that has been subjected to silanization treatment.

[0059] Specifically, a placement opening is opened on the top of the first shell 32, and a sealing cover 35 is also provided on the placement opening. The film 10 to be treated is fixed and unfolded in the inner frame under the clamping action of the clamping assembly, and then the fixed frame 21 clamping the film 10 to be treated is transferred to the reaction tank manually or by a lifting mechanism, and then fully contacted with the silane reagent in the reaction tank. Under the heating action of the first heating device, a silanization reaction is quickly carried out to complete the activation silanization reaction on the surface of the film 10 to be treated, and then the film 10 to be treated and the fixed frame 21 that have completed the silanization reaction are transferred from the reaction tank to the film heat treatment device 40 manually or by a lifting mechanism, and the silanized film 10 to be treated is heated and dried, thereby completing the surface modification of the film 10 to be treated.

[0060] It should be noted that the maximum processing size of the thin film 10 to be processed is 3 m in length and 1 m in width. The inner frame size of the fixed frame 21 is slightly larger than that of the thin film 10 to be processed. The size of the fixed frame 21 can be 3.2 m in length and 1.2 m in width. The number of clamping components is 22. Among them, 8 clamping components are arranged on each of the two long sides of the inner frame, and 3 clamping components are arranged on each of the two short sides.

[0061] In one embodiment, referring to the attached drawings of the specification Figures 2 to 4 As shown, the fixed frame 21 includes a concave connecting member 24 and an L-shaped connecting member 25. The concave connecting member 24 is arranged on the side of the fixed frame 21 close to the clamping component, and the L-shaped connecting member 25 is arranged on the side of the clamping component close to the concave connecting member 24. A strip-shaped hole 251 is formed in the L-shaped connecting member 25, and a groove with a fixing hole is formed in the concave connecting member 24. The strip-shaped hole 251 and the fixing hole are connected through a tensioning screw 26, so that the L-shaped connecting member 25 can be slidably connected in the groove.

[0062] Specifically, there is a sliding groove on the concave connecting member 24, and the L-shaped connecting member 25 slides in the sliding groove. The strip-shaped hole 251 is arranged on the plate of the L-shaped connecting member 25 that slides, and the fixing hole is formed in the sliding groove. The tensioning screw 26 passes through the fixing hole and the strip-shaped hole 251 at the same time to tightly connect the L-shaped connecting member 25 and the concave connecting member 24. The specific operation steps are as follows: first loosen the tensioning screw 26, so that the L-shaped connecting member 25 slides in the sliding groove on the concave connecting member 24 to adjust the clamping opening degree of the thin film 10 to be processed to a predetermined degree, and then tighten the tensioning screw 26 to fixedly connect the L-shaped connecting member 25 and the concave connecting member 24, so as to realize the fine adjustment of the tension of the thin film 10 to be processed. It should be noted that the sliding range of the L-shaped connecting member 25 in the sliding groove on the concave connecting member 24 can be 0 mm to 12 mm.

[0063] In one embodiment, on the basis of the previous embodiment, referring to the attached drawings of the specification Figure 2 and Figure 3 As shown, the clamping component includes a clamping member 22 and a plurality of pressing members 23. Among them, the clamping member 22 includes a first clamping strip and a second clamping strip. The first clamping strip and the second clamping strip are hinged through a plurality of hinge structures 27. A concave tooth structure is arranged on the side of the first clamping strip close to the second clamping strip, and a convex tooth structure is arranged on the side of the second clamping strip close to the first clamping strip. The concave tooth structure and the convex tooth structure are correspondingly engaged. The pressing member 23 is clamped on the clamping member 22, and a manual butterfly screw 231 is arranged on the pressing member 23 to adjust the pressure of the thin film 10 to be processed clamped on the two clamping strips.

[0064] Specifically, through the corresponding engagement of the concave tooth structure and the convex tooth structure, the film 10 to be processed is effectively prevented from falling off. By adjusting the manual butterfly screw 231, the clamping force of the pressing member 23 is adjusted, and then the pressure of the film 10 to be processed clamped on the two sets of clamping strips is adjusted, effectively avoiding the situation that the film 10 to be processed falls off due to too small clamping force or the film 10 to be processed is damaged due to too large clamping force.

[0065] In one embodiment, referring to the attached drawings of the specification Figure 6 As shown, the reaction tank includes an upper tank 33 and a lower tank 34 vertically communicating with the upper tank 33. The upper tank 33 and the lower tank 34 form a T-shaped tank. The opening of the upper tank 33 corresponds to the opening of the first accommodating cavity, and chamfers are provided at the joints of the lower tank 34 and the upper tank 33.

[0066] Specifically, the lower tank 34 can accommodate the fixing frame 21 to be completely placed therein. The lower tank 34 and the upper tank 33 form a T-shaped tank, which not only helps to reduce the usage amount of the silane reagent to effectively reduce the cost, but also effectively avoids the situation that the volume of the silane reagent expands and overflows after heating. The setting of the chamfer makes it easier for the fixing frame 21 to be placed into the lower tank 34.

[0067] In one embodiment, referring to the attached drawings of the specification Figure 6 As shown, the first heating device includes a plurality of first heating tubes 31. The plurality of first heating tubes 31 are closely arranged on the outer sides of the two side walls of the lower tank 34, and heat insulation cotton is arranged in the gaps between the plurality of first heating tubes 31.

[0068] Specifically, the heating tubes are used to provide heat sources for heating the silane reagent in the reaction tank. Heat insulation cotton is filled between the heating tubes to maintain the temperature of the silane reagent in the reaction tank, improve the heat insulation performance of the film silanization treatment device 30, thereby reducing the loss of heat energy. The heating tubes can be U-shaped heating tubes, and the number of U-shaped heating tubes can be 14, which are divided into two groups. Each group of heating tubes is symmetrically arranged side by side and attached to the two side walls of the reaction tank.

[0069] It should be noted that the film silanization treatment device 30 is also provided with a temperature control system, which is arranged on the first housing 32 and used to independently detect and control each group of heating tubes, so as to effectively reduce the temperature difference at both ends of the reaction tank and ensure the temperature uniformity when the film 10 to be processed is heated and silanized.

[0070] In one embodiment, referring to the attached drawings of the specification Figure 1 and Figure 7As shown, the thin film heat treatment device 40 includes a second housing 47. A second accommodation cavity is provided on the second housing 47. A placement container is arranged in the second accommodation cavity. A drying groove is provided on the placement container. A second heating device is further arranged in the second housing 47. The second heating device is located outside the two side walls of the drying groove. The drying groove matches with the fixing frame 21, so that the to-be-treated thin film 10 after silanization treatment is heated and dried in the placement container through the second heating device.

[0071] In one embodiment, on the basis of the above embodiment, referring to the attached drawings of the specification Figure 1 and Figure 7 As shown, a first opening is provided on the side wall of the placement container. A first sealing door 43 is detachably arranged at the first opening. The thin film heat treatment device 40 further includes a moving track 41 and a moving support 42 corresponding to the moving track 41. The moving track 41 is arranged at the bottom of the placement container and extends outwards through the first opening. A fixing seat for fixing the fixing frame 21 is arranged on the moving support 42, so that the to-be-treated thin film 10 can be transferred to a predetermined position of the placement container along the moving track 41.

[0072] Specifically, the opening of the drying groove is arranged on the side surface of the second housing 47 and is communicated with the first opening. The fixing frame 21 with the thin film 10 is fixed on the moving support 42. A plurality of wheels corresponding to the moving track 41 are arranged at the bottom of the moving support 42, so that the moving support 42 is transferred to a predetermined position of the placement container along the moving track 41, and then the first sealing door 43 is closed, so that the placement groove 48 forms a sealed space to make the heating and drying effect better. The moving track 41 enables the fixing frame 21 with the to-be-treated thin film 10 to be quickly and stably conveyed into the drying groove.

[0073] It should be noted that universal wheels are arranged at the bottoms of both the second housing 47 and the moving support 42 to facilitate the movement of the entire thin film heat treatment device 40.

[0074] In one embodiment, on the basis of the above embodiment, referring to the attached drawings of the specification Figure 7 and Figure 8 As shown, a plurality of circulating air holes 46 are provided on the side walls of the placement container parallel to the moving track 41. The second heating device includes a plurality of second heating tubes 44 and a plurality of circulating air impellers 45. The second heating tubes 44 are respectively fixedly arranged outside the two side walls of the placement container, and the circulating air impellers 45 are all arranged on the top of the placement container.

[0075] It should be noted that the number of the circulating air impellers 45 can be four, which are arranged in parallel on the top of the placement container. When the first sealing door 43 is closed, the placement groove 48 forms a sealed space. The heating tubes and the circulating air impellers 45 are turned on, so that a hot air circulation is formed in the placement groove 48 to heat and dry the to-be-treated thin film 10.

[0076] In one embodiment, referring to the appended drawings of the specification Figure 8 and Figure 9 as shown, the second housing 47 is provided with a second opening corresponding to the other side wall of the first opening, and a second sealing door 49 is detachably connected to the second opening;

[0077] The number of the thin film heat treatment devices 40 is two, and the two thin film heat treatment devices 40 are connected by a plurality of connecting components, and the first opening and the second opening are in corresponding contact.

[0078] Specifically, when the length of the thin film 10 to be processed is less than 1.6 m and the number of thin films is large, the two thin film heat treatment devices 40 can work independently to improve the drying efficiency. When the length of the thin film 10 to be processed is 3.0 m, the two thin film heat treatment devices 40 are combined to extend the length of the placement groove 48, so as to dry the thin film 10 to be processed with a length of 3.0 m. The specific combination process is as follows: first, remove the first sealing door 43 of one thin film heat treatment device 40 and the second sealing door 49 of the other thin film heat treatment device 40, so that the first opening of one thin film heat treatment device 40 and the second opening of the other thin film heat treatment device 40 are in corresponding contact, and then complete the connection by setting the connecting components, so that the application range of the thin film heat treatment device 40 is wider.

[0079] In one embodiment, referring to the appended drawings of the specification Figure 10 as shown, the connecting component includes two connecting pieces 50 and a connecting bolt 51. The two connecting pieces 50 are respectively fixed at corresponding positions on the two thin film heat treatment devices 40, and the connecting bolt 51 connects the two connecting pieces 50 through a fastening nut 52.

[0080] Specifically, the two connecting pieces are respectively fixed at corresponding positions on the two thin film heat treatment devices 40. When the first opening of one thin film heat treatment device 40 and the second opening of the other thin film heat treatment device 40 are in corresponding contact, the two connecting pieces of each group of connecting components are in corresponding contact, and then the two connecting pieces are firmly connected together by the connecting bolt 51.

[0081] It should be noted that the connecting component further includes a flat gasket 53 and a baffle 54. The flat gasket 53 is sleeved on the connecting bolt 51 to make the fastening relationship between the two connecting pieces firmer. The connection part of the two thin film heat treatment devices 40 can also be sealed with a high-temperature resistant sealing rubber ring. The baffle 54 is sleeved on the connecting piece to beautify the appearance of the two thin film heat treatment devices 40.

[0082] It should be noted that the above embodiments can be freely combined as needed. The above are only the preferred embodiments of the present invention. It should be pointed out that for those of ordinary skill in the art, without departing from the principle of the present invention, several improvements and refinements can be made, and these improvements and refinements should also be regarded as the protection scope of the present invention.

Claims

1. A thin film silanization surface modification system, characterized in that Comprising: A film fixing device, including a fixing frame. A number of clamping components are arranged on the inner frame of the fixing frame, and the clamping components are used to fix and extend the film to be processed on the fixing frame; the fixing frame includes a concave connecting piece and an L-shaped connecting piece, and the L-shaped connecting piece can be slidably connected in the groove of the concave connecting piece and is fixed by a tightening screw passing through; the clamping component includes a clamping piece and a number of pressing pieces, the clamping piece includes a first clamping strip and a second clamping strip connected in a meshing manner, and the pressing piece is adapted to clamp the first clamping strip and the second clamping strip; A film silanization treatment device, including a first housing. The first housing is provided with a first accommodating cavity, a reaction container is arranged in the first accommodating cavity, a reaction groove is arranged in the reaction container, the reaction groove is filled with a silane reagent, and first heating devices are further arranged on both sides of the reaction container corresponding to the reaction groove. The first heating devices are used to heat the silane reagent to accelerate the silanization reaction. The reaction groove is matched with the fixing frame, so that the film to be processed can be unfolded in the reaction container through the fixing frame and undergo silanization treatment; A film heat treatment device for heating and drying the film to be processed that has undergone silanization treatment.

2. The thin film silanization surface modification system according to claim 1, characterized in that, The concave connecting piece is arranged on one side of the fixing frame close to the clamping component; The L-shaped connecting piece is arranged on one side of the clamping component close to the concave connecting piece. A strip-shaped hole is arranged on the L-shaped connecting piece, and a groove with a fixing hole is formed on the concave connecting piece. The strip-shaped hole and the fixing hole are connected through a tightening screw, so that the L-shaped connecting piece can be slidably connected in the groove.

3. The thin film silanization surface modification system according to claim 2, characterized in that, The first clamping strip and the second clamping strip are hinged through a number of hinge structures. A concave tooth structure is arranged on one side of the first clamping strip close to the second clamping strip, and a convex tooth structure is arranged on one side of the second clamping strip close to the first clamping strip. The concave tooth structure and the convex tooth structure are correspondingly engaged; The pressing piece is clamped on the clamping piece, and a manual butterfly screw is arranged on the pressing piece to be used for adjusting the pressure of the film to be processed clamped on the two clamping strips.

4. The film silanization surface modification system according to any one of claims 1-3, characterized in that The reaction groove includes an upper groove and a lower groove vertically communicating with the upper groove. The upper groove and the lower groove form a T-shaped groove. The opening of the upper groove corresponds to the opening of the first accommodating cavity, and chamfers are arranged at the connection of the lower groove and the upper groove.

5. The film silanization surface modification system according to claim 4, characterized in that The first heating device includes a number of first heating tubes. The number of first heating tubes are closely arranged on the outer sides of the two side walls of the lower groove, and heat insulation cotton is arranged in the gap between the number of first heating tubes.

6. The film silanization surface modification system according to claim 5, characterized in that The thin film heat treatment device includes a second housing, a second accommodation cavity is formed in the second housing, a placement container is arranged in the second accommodation cavity, a drying groove is formed in the placement container, a second heating device is further arranged in the second housing, the second heating device is located outside the two side walls of the drying groove, and the drying groove is matched with the fixed frame, so that the to-be-treated thin film after silanization treatment is heated and dried by the second heating device in the placement container.

7. The thin film silanization surface modification system according to claim 6, wherein a first opening is formed in the side wall of the placement container, and a first sealing door is detachably arranged at the first opening; the thin film heat treatment device further includes a moving track and a moving bracket corresponding to the moving track, the moving track is arranged at the bottom of the placement container and extends outward through the first opening, and a fixing seat for fixing the fixed frame is arranged on the moving bracket, so that the to-be-treated thin film can be transferred along the moving track to a predetermined position of the placement container.

8. The thin film silanization surface modification system according to claim 7, wherein a plurality of circulating air holes are formed in the side walls of the placement container parallel to the moving track; the second heating device includes: a plurality of second heating tubes, and the second heating tubes are respectively fixedly arranged outside the two side walls of the placement container; a plurality of circulating air impellers, and the circulating air impellers are all arranged on the top of the placement container.

9. The thin film silanization surface modification system according to claim 8, wherein a second opening is formed in the other side wall of the second housing corresponding to the first opening, and a second sealing door is detachably connected to the second opening; the number of the thin film heat treatment devices is two, and the two thin film heat treatment devices are connected by a plurality of connecting components, and the first opening and the second opening are in corresponding contact.

10. The thin film silanization surface modification system according to claim 9, wherein, The connecting component includes: two connecting pieces, and the two connecting pieces are respectively arranged and fixed at corresponding positions on the two thin film heat treatment devices; a connecting bolt, and the connecting bolt connects the two connecting pieces through a fastening nut.

Citation Information

Patent Citations

  • Chemical water-bath film-coating device

    CN109161875A

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    CN215217036U