一种适用于超高真空系统的冷冻溶液样品制备装置
By freezing and transferring solution samples to an ultra-high vacuum system using a cryo-solution sample preparation device, the problems of transfer compatibility and cleanliness of solution samples in an ultra-high vacuum environment are solved, enabling high-resolution analysis and making it suitable for a variety of solution systems.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- PEKING UNIV
- Filing Date
- 2024-01-04
- Publication Date
- 2026-07-17
AI Technical Summary
Existing technologies make it difficult to transfer solution samples to an ultra-high vacuum environment for high-resolution analysis without damaging their intrinsic properties, and existing methods also have compatibility and cleanliness issues.
A cryogenic solution sample preparation device was designed, including a sample preparation stage, a compressible linear introducer, a sample transfer chamber, a gate valve, and a vacuum pump. The solution sample is frozen on the sample collection device by a refrigeration device and then transferred and characterized in an ultra-high vacuum system, avoiding the heating and evaporation process.
It enables the high-purity transfer and characterization of solution samples in an ultra-high vacuum environment, preserving the original information, applicable to various solution systems, and safe transfer of unstable molecules, providing atomic-scale structural and compositional information.
Smart Images
Figure CN117782742B_ABST