A distillation tower for producing furanone
By introducing stirring, speed limit, pre-cooling and vibration mechanisms into the distillation tower, the problems of uneven steam flow rate, low condensation efficiency and poor heat absorption efficiency during the condensation process are solved, and more efficient condensation and collection effects are achieved .
Patent Information
- Application Number
- CN202411666683.4
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-11-21
- Publication Date
- 2025-02-18
- Estimated Expiration
- 2044-11-21
AI Technical Summary
The existing distillation towers used for the production of furonone have problems such as uneven steam flow rate, low condensation efficiency and poor heat absorption efficiency of cooling water during the condensation process.
A distillation tower is designed, including a stirring mechanism, a speed limiting mechanism, a pre-cooling mechanism and a vibration mechanism. These mechanisms improve condensation efficiency and effect by adjusting the flow rate and path of cooling water, limiting the flow rate of steam, pre-cooling the cooling water, and vibrating the condensation tube.
Through these technical means, the efficiency and effect of condensation are improved, the collection effect of furanone is ensured, and the heat absorption efficiency of cooling water is improved.
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Figure CN119158288B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of distillation tower condensers, in particular to a distillation tower for producing furanone. Background Art
[0002] Furanone is a flavor enhancer widely used in food, tobacco, and beverage flavoring. The distillation tower used to produce furanone is a highly efficient, energy-saving, and environmentally friendly separation equipment, mainly used to separate miscible liquid mixtures. Its essence is multi-stage distillation. The steam rising from the top of the tower will enter the condenser and be completely condensed into saturated liquid, of which part of the liquid is used as reflux, and the rest of the liquid is used as the top product.
[0003] However, when the existing distillation tower for producing furanone is in use, when the condenser condenses the steam, the condensed water flows and absorbs heat, which is not uniform, affecting the efficiency and effect of condensation; when the reaction starts, the flow rate of the steam is very fast, so that the contact time between the steam and the cooling water is short, thereby affecting the efficiency and effect of condensation; when the reaction is about to end, the amount of steam becomes less, and the steam in the distillation tower cannot quickly and thoroughly enter the condenser for condensation, which also affects the efficiency and effect of condensation; after the condensation is completed, the liquid is easy to adhere to the inner wall of the pipe, thereby affecting the collection effect, and after the cooling water absorbs heat, it needs to be cooled by heat exchange through a heat exchanger, and the cooling efficiency is low and the effect is poor, which also affects the efficiency and effect of subsequent condensation. Summary of the invention
[0004] The object of the present invention is to provide a distillation tower for producing furanone to solve the problems raised in the above background technology.
[0005] To achieve the above-mentioned purpose, the present invention provides the following technical solutions: a distillation tower for producing furanone, comprising a condenser assembly arranged on a distillation tower body, the distillation tower body comprising a tower body and a steam pipe, and the condenser assembly comprising a shell, an inlet and an outlet, a condenser is fixedly inserted in the shell, and the two ends of the condenser are respectively fixed to the inlet and the outlet, a first fixed box is fixedly connected to the top of the inlet, and a first connecting pipe is fixedly connected to the top of the first fixed box, the other end of the steam pipe is fixed to the upper end of the first connecting pipe, and a speed reduction mechanism for speeding up steam is arranged in the first fixed box, a partition assembly is fixedly inserted in the shell, and the partition assembly comprises a plurality of first partitions arranged in an array and a plurality of second partitions arranged in an array, and The first partition and the second partition are arranged alternately, a plurality of first through holes arranged in an array are opened on one side of the top of the first partition, and a plurality of second through holes arranged in an array are opened on the other side of the top of the second partition, a circulation pump is fixedly connected to the side wall of the shell, and a water inlet pipe is fixedly connected to the side wall of the circulation pump, a heat exchanger is fixedly connected to the top of the heat exchanger, and a return pipe is fixedly connected between the second connecting pipe and the shell, a plurality of stirring mechanisms for stirring the cooling water are arranged between the first partition and the second partition, and a knocking mechanism for knocking and vibrating the condenser is arranged on the top of the partition assembly, and a pre-cooling mechanism for pre-cooling the cooling water is arranged on the side wall of the second connecting pipe.
[0006] Preferably, each of the stirring mechanisms comprises a rotating rod rotatably connected to the inner side wall of the shell, a plurality of blades arranged in an array are fixedly connected to the side wall of the rotating rod, and the rotation of the rotating rod is driven by a driving mechanism.
[0007] Preferably, the knocking mechanism includes a movable plate, and the side wall of the movable plate is fixedly connected to a first connecting plate, the side wall of the first connecting plate is connected to a plurality of rubber rods arranged in an array, the movable plate is connected to the top of the partition assembly through a reset mechanism, and the movement of the movable plate is driven by a pushing mechanism.
[0008] Preferably, the deceleration mechanism includes a first rotating shaft rotatably connected to a first fixed box, and the side wall of the first rotating shaft is fixedly connected to a plurality of first baffles arranged in an array, the side wall of the first fixed box is fixedly connected to a motor, and the output end of the motor is fixed to one end of the first rotating shaft, one end of the first rotating shaft is fixedly connected to a rotating disk, and the side wall of the rotating disk is provided with a scale mark, the top of the first fixed box is fixedly connected to an L-shaped block, and the top of the L-shaped block is fixedly inserted with a visual sensor, the side wall of the first fixed box is fixedly connected to an L-shaped plate, and the side wall of the L-shaped plate is connected to a moving block through a moving module, the side wall of the moving block is connected to a friction block through a moving mechanism, and the side wall of the moving block is fixedly inserted with a distance sensor.
[0009] Preferably, the driving mechanism includes gears fixedly connected to the side walls of each rotating rod, and the side walls of the shell are connected to a plurality of movable rods arranged in an array through a lifting mechanism, connecting rods are fixedly connected between the movable rods, and racks are fixedly connected to both ends of each movable rod, and the racks are meshing with the gears.
[0010] Preferably, the lifting mechanism includes two symmetrically arranged fixed blocks fixedly connected to the side walls of the shell, and the side walls opposite to the two fixed blocks are fixedly connected to two symmetrically arranged guide rods, the side wall of each guide rod is sleeved with a slider, and the slider is fixed to the side wall of one of the moving rods, the side wall of each guide rod is sleeved with a first spring, and the side wall of one of the moving rods is fixedly connected to a push plate, the side wall of the return pipe is fixedly inserted with a second fixed box, and a plurality of second baffles arranged in an array are rotatably connected to the second fixed box through a second rotating shaft, one end of the second rotating shaft is fixedly connected to a disc, and the side wall of the disc is fixedly connected to a plurality of conical rods arranged in an array.
[0011] Preferably, the pre-cooling mechanism includes a fixed rod fixedly connected to the side wall of the shell, and the side wall of the fixed rod is fixedly connected to a fixed tube, a piston is slidably connected in the fixed tube, and a push rod is fixedly connected to the top of the piston, the upper end of the push rod is fixed to the bottom of the push plate, and the side wall of the fixed tube is fixedly connected to an air intake pipe, a first one-way valve is arranged in the air intake pipe, and a blowing pipe is fixedly connected to the side wall of the fixed tube, a second one-way valve is arranged in the blowing pipe, and the other end of the blowing pipe is fixedly connected to a hollow annular cover, the annular cover is sleeved on the side wall of the second connecting pipe, and a plurality of blowing holes arranged in an array are opened on the inner side wall of the annular cover, an annular absorbent cotton is fixedly inserted in the annular cover, and the side wall of the heat exchanger is fixedly connected to a water storage tank, and a cotton core is fixedly connected between the water storage tank and the absorbent cotton.
[0012] Preferably, the reset mechanism includes two symmetrically arranged T-shaped guide rods fixedly connected to the side walls of each movable plate, and the side walls of the T-shaped guide rods are sleeved with connecting blocks, the connecting blocks are fixed to the top of the partition assembly, and the side walls of each T-shaped guide rod are sleeved with a second spring.
[0013] Preferably, the pushing mechanism includes a second connecting plate fixedly connected to the side wall of the movable plate, and the side wall of the second connecting plate is fixedly connected to a pushing block, the side wall fixing sleeve of the rotating rod is provided with a cam, and the cam slides on the side wall of the pushing block.
[0014] Preferably, the moving mechanism includes two symmetrically arranged sleeves fixedly connected to the side walls of the moving block, and a sleeve rod is inserted in the sleeve, the other end of the sleeve rod is fixed to the side wall of the friction block, and the side wall of each sleeve is sleeved with a third spring, the top of the moving block is fixedly connected to an electromagnet, and the top of the friction block is fixedly connected to an iron block.
[0015] Compared with the prior art, the present invention has the following beneficial effects:
[0016] The distillation tower for producing furanone is provided with a stirring mechanism, etc., so that during distillation, the steam generated by the distillation of the tower body enters the first fixed box through the steam pipe and the first connecting pipe, and enters the condenser pipe through the inlet for condensation. At the same time, the circulation pump is started, so that the cooling water can enter the shell after being cooled by the heat exchange of the heat exchanger, and can pass through the first through hole on the first partition and the second through hole on the second partition from bottom to top in sequence, which can reduce the flow rate of the cooling water and increase the path of the cooling water, thereby improving the efficiency and effect of condensation. Moreover, when the cooling water flows out of the shell through the return pipe, it can enter the second fixed box and impact the surface of the second baffle. , so that the second rotating shaft and the disc rotate, when the conical rod abuts against the top of the pushing plate, the pushing plate and the moving rod can be pushed downward, and at the same time, the slider moves downward along the guide rod, and the first spring is compressed. When the conical rod passes over the top of the pushing plate, the moving rod and the connecting rod can move upward and reset under the action of the first spring, and so on, the rack can be reciprocated up and down, thereby pushing the gear and the rotating rod to reciprocate, and then the blades can reciprocate and stir the cooling water between the partition assemblies, so that the heat absorption efficiency of the cooling water is higher and the effect is better, thereby improving the efficiency and effect of condensation, and the condensed furanone liquid is collected through the outlet.
[0017] The distillation tower for producing furanone is provided with a speed limiting mechanism, etc., so that during distillation, the steam generated by the distillation of the tower body enters the first fixed box through the steam pipe and the first connecting pipe, and enters the condenser through the inlet for condensation. When the steam enters the first fixed box, it impacts the surface of the first baffle, causing the first rotating shaft to rotate, and the rotation of the first rotating shaft drives the rotation of the rotating disk. At the same time, the rotation speed of the rotating disk can be determined by detecting the scale mark on the side wall of the rotating disk through the distance sensor, and then the flow rate of the steam can be determined. When the flow rate of the steam is too fast, the electromagnet is de-energized. At this time, the friction block can be abutted against the side wall of the rotating disk under the action of the third spring, so that the rotation speed of the rotating disk can be limited, thereby limiting the flow rate of the steam. , making the condensation more efficient and effective. At the same time, the moving block can be driven to move through the moving module, so as to adjust the distance between the moving block and the friction block, and the compression amount of the third spring can be adjusted, thereby adjusting the extrusion force between the friction block and the rotating disk, and the maximum flow rate of the steam can be adjusted, which has stronger applicability. After the reaction is completed, when the visual sensor detects that the rotation speed of the rotating disk is slow, the motor can be started, and at the same time, the electromagnet is energized. After the electromagnet is energized, the iron block is attracted, so that the friction block is separated from the rotating disk. At the same time, when the motor rotates, the first baffle is driven to rotate through the first rotating shaft, so that the vacuum operation can be performed, which accelerates the steam in the tower body to thoroughly enter the condenser assembly for condensation operation, thereby improving the efficiency and effect of condensation.
[0018] The distillation tower for producing furanone is provided with a pre-cooling mechanism, etc., so that during distillation, the cooling water after absorbing heat enters the second connecting pipe through the return pipe, and enters the heat exchanger for heat dissipation and cooling. At the same time, when the push plate moves up and down reciprocatingly, the piston is driven to move up and down reciprocatingly by the push rod. When the piston moves upward, negative pressure is generated in the fixed pipe. At the same time, the first one-way valve is opened and the second one-way valve is closed. At this time, external air enters the fixed pipe through the air inlet pipe. When the piston moves downward, the air in the fixed pipe can be squeezed. At the same time, the first one-way valve is closed and the second one-way valve is opened. At this time, the air in the fixed pipe is squeezed and enters the annular cover through the blowing pipe and is blown out through the blowing hole. At the same time, the cooling water in the water storage tank can enter the absorbent cotton through the cotton core, so that the second connecting pipe can be cooled, and then the cooling water is pre-cooled, which can improve the efficiency and effect of subsequent heat exchanger cooling.
[0019] The distillation tower for producing furanone is provided with a vibration mechanism, etc. When the rotating rod rotates, the cam is driven to rotate synchronously. When the tip of the cam abuts against the side wall of the push block, the movable plate is driven to move in a direction away from the condenser through the second connecting plate. At the same time, the second spring is compressed. When the tip of the cam passes over the push block, the movable plate can be moved and reset in a direction close to the condenser under the action of the second spring. In this way, the movable plate can be reciprocated. At the same time, the rubber rod is driven to reciprocate through the first connecting plate, so that the rubber rod reciprocates and vibrates the side wall of the condenser, thereby preventing the condensed furanone liquid from adhering to the inner wall of the condenser, so that the collection effect is better. BRIEF DESCRIPTION OF THE DRAWINGS
[0020] Figure 1 It is a schematic diagram of the overall structure of the present invention.
[0021] Figure 2 It is a schematic diagram of the overall structure from another perspective of the present invention.
[0022] Figure 3 It is a schematic diagram of the partial cross-sectional structure of the shell in the present invention.
[0023] Figure 4 It is a schematic diagram of the partial cross-sectional structure of the shell in another viewing angle of the present invention.
[0024] Figure 5 It is a schematic diagram of the partial cross-sectional structure of the annular cover and the fixed pipe in the present invention.
[0025] Figure 6 for Figure 1 Schematic diagram of the enlarged structure at point A in the middle.
[0026] Figure 7 for Figure 2 Schematic diagram of the enlarged structure at point B in the middle.
[0027] Figure 8 for Figure 3 Schematic diagram of the enlarged structure at point C in the middle.
[0028] Fig. 9 for Figure 5 Schematic diagram of the enlarged structure at D in the middle.
[0029] Fig.10 for Figure 5 Schematic diagram of the enlarged structure at E in the middle.
[0030] Fig.11 for Figure 5 Schematic diagram of the enlarged structure at F in the middle.
[0031] Fig.12 for Fig.10 Schematic diagram of the enlarged structure at G in the middle.
[0032] In the figure: 1, distillation tower body; 101, tower body; 102, steam pipe; 2, stirring mechanism; 201, rotating rod; 202, blade; 3, knocking mechanism; 301, moving plate; 302, first connecting plate; 303, rubber rod; 4, reset mechanism; 401, connecting block; 402, T-shaped guide rod; 403, second spring; 5, pushing mechanism; 501, second connecting plate; 502, pushing block; 503, cam; 6, speed reduction mechanism; 601, first rotating shaft; 602, first a baffle; 603, motor; 604, rotating disk; 605, scale mark; 606, distance sensor; 607, L-shaped plate; 608, moving module; 609, L-shaped block; 610, visual sensor; 611, moving block; 612, friction block; 7, moving mechanism; 701, sleeve; 702, sleeve rod; 703, third spring; 704, electromagnet; 705, iron block; 8, driving mechanism; 801, gear; 802, rack; 803, moving rod; 804, connecting rod Connecting rod; 9, lifting mechanism; 901, fixed block; 902, guide rod; 903, slider; 904, first spring; 905, second fixed box; 906, second rotating shaft; 907, second baffle; 908, disc; 909, conical rod; 910, push plate; 10, pre-cooling mechanism; 1001, annular cover; 1002, blowing hole; 1003, absorbent cotton; 1005, water storage tank; 1006, cotton core; 1007, fixed rod; 1008, fixed tube; 1009 , piston; 1010, push rod; 1011, blow pipe; 1012, air inlet pipe; 11, condenser assembly; 1101, shell; 1102, inlet; 1103, outlet; 1104, condenser; 1105, first partition; 1106, second partition; 1107, first through hole; 1108, second through hole; 12, return pipe; 13, second connecting pipe; 14, heat exchanger; 15, water inlet pipe; 16, circulation pump; 17, first fixed box; 18, first connecting pipe. DETAILED DESCRIPTION
[0033] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0034] See also Figure 1-Figure 12The present invention provides a technical solution: a distillation tower for producing furanone, comprising a condenser assembly 11 arranged on a distillation tower body 1, the distillation tower body 1 comprising a tower body 101 and a steam pipe 102, and the condenser assembly 11 comprising a shell 1101, an inlet 1102 and an outlet 1103, a condenser 1104 is fixedly inserted in the shell 1101, and both ends of the condenser 1104 are respectively fixed to the inlet 1102 and the outlet 1103, a first fixed box 17 is fixedly connected to the top of the inlet 1102, and a first connecting pipe 18 is fixedly connected to the top of the first fixed box 17, and the other end of the steam pipe 102 is connected to the upper end of the first connecting pipe 18 The first fixed box 17 is fixed, and a speed reducing mechanism 6 for reducing the speed of steam is arranged in the first fixed box 17. A partition assembly is fixedly inserted in the shell 1101, and the partition assembly includes a plurality of first partitions 1105 arranged in an array and a plurality of second partitions 1106 arranged in an array, and the first partitions 1105 and the second partitions 1106 are arranged alternately, and a plurality of first through holes 1107 arranged in an array are opened on one side of the top of the first partition 1105, and a plurality of second through holes 1108 arranged in an array are opened on the other side of the top of the second partition 1106, and a circulating pump 16 is fixedly connected to the side wall of the shell 1101, and a water inlet pipe 15 is fixedly connected to the side wall of the circulating pump 16, and the water inlet pipe The upper end of the heat exchanger 15 is fixedly connected to the heat exchanger 14, the top of the heat exchanger 14 is fixedly connected to the second connecting pipe 13, and the return pipe 12 is fixedly connected between the second connecting pipe 13 and the shell 1101, and a plurality of stirring mechanisms 2 for stirring the cooling water are arranged between the first partition 1105 and the second partition 1106, and a knocking mechanism 3 for knocking and vibrating the condensing pipe 1104 is arranged on the top of the partition assembly, and a pre-cooling mechanism 10 for pre-cooling the cooling water is arranged on the side wall of the second connecting pipe 13, which can reduce the flow rate of the cooling water and increase the path of the cooling water when condensing the steam, and at the same time, can The cooling water in the tower 101 is stirred back and forth, so that the heat absorption efficiency of the cooling water is higher and the effect is better, thereby improving the efficiency and effect of condensation; when the flow rate of the steam is too fast, it can be limited, and when the flow rate of the steam is slow, a vacuum operation can be performed to accelerate the steam in the tower body 101 to completely enter the condenser assembly 11 for condensation operation, thereby improving the efficiency and effect of condensation; the condensation tube 1104 can be knocked and vibrated back and forth to prevent the condensed furanone liquid from adhering to the inner wall, so that the collection effect is better; before the cooling water enters the heat exchanger 14, the cooling water can be pre-cooled, thereby improving the efficiency and effect of subsequent cooling of the heat exchanger 14.
[0035] Each stirring mechanism 2 includes a rotating rod 201 rotatably connected to the inner wall of the shell 1101, and the side wall of the rotating rod 201 is fixedly connected with a plurality of blades 202 arranged in an array, and the rotation of the rotating rod 201 is driven by a driving mechanism 8, and the driving mechanism 8 drives the rotating rod 201 to rotate reciprocatingly, so that the blades 202 can reciprocate and stir the cooling water between the partition assemblies, so that the heat absorption efficiency of the cooling water is higher and the effect is better.
[0036] The knocking mechanism 3 includes a movable plate 301, and the side wall of the movable plate 301 is fixedly connected to a first connecting plate 302, and the side wall of the first connecting plate 302 is connected to a plurality of rubber rods 303 arranged in an array, and the movable plate 301 is connected to the top of the partition assembly through a reset mechanism 4, and the movement of the movable plate 301 is pushed by a pushing mechanism 5, and the movable plate 301 is made to reciprocate by the pushing mechanism 5 and the reset mechanism 4, and at the same time, the rubber rod 303 is driven to reciprocate by the first connecting plate 302, so that the rubber rod 303 reciprocates and knocks and vibrates the side wall of the condenser 1104, thereby preventing the condensed furanone liquid from adhering to the inner wall of the condenser 1104, so that the collection effect is better.
[0037] The speed reduction mechanism 6 includes a first rotating shaft 601 rotatably connected to the first fixed box 17, and a plurality of first baffles 602 arranged in an array are fixedly connected to the side wall of the first rotating shaft 601, a motor 603 is fixedly connected to the side wall of the first fixed box 17, and the output end of the motor 603 is fixed to one end of the first rotating shaft 601, a rotating disk 604 is fixedly connected to one end of the first rotating shaft 601, and a scale mark 605 is arranged on the side wall of the rotating disk 604, and an L-shaped block 609 is fixedly connected to the top of the first fixed box 17. A visual sensor 610 is fixedly inserted on the top of the L-shaped block 609, an L-shaped plate 607 is fixedly connected to the side wall of the first fixed box 17, and the side wall of the L-shaped plate 607 is connected to a moving block 611 through a moving module 608, and the side wall of the moving block 611 is connected to a friction block 612 through a moving mechanism 7, and a distance sensor 606 is fixedly inserted on the side wall of the moving block 611. When distillation is performed, the steam generated by the distillation of the tower body 101 enters the first fixed box 17 through the steam pipe 102 and the first connecting pipe 18. , and enters the condenser 1104 through the inlet 1102 for condensation. When the steam enters the first fixed box 17, it will impact the surface of the first baffle 602, causing the first rotating shaft 601 to rotate. The rotation of the first rotating shaft 601 drives the rotation of the rotating disk 604. At the same time, the distance sensor 606 detects the 605 scale mark on the side wall of the rotating disk 604, so as to determine the rotation speed of the rotating disk 604 and then determine the flow rate of the steam. When the flow rate of the steam is too fast, the friction block 612 is abutted against the side wall of the rotating disk 604 through the moving mechanism 7, so as to limit the rotation speed of the rotating disk 604, thereby limiting the flow rate of the steam, so that the condensation efficiency is higher and the effect is better. After the reaction is completed, the motor 603 can be started. When the motor 603 rotates, the first baffle 602 is driven to rotate through the first rotating shaft 601, so as to perform the exhaust operation, accelerate the steam in the tower body 101 to thoroughly enter the condenser assembly 11 for condensation operation, thereby improving the efficiency and effect of condensation.
[0038] The driving mechanism 8 includes a gear 801 fixedly connected to the side wall of each rotating rod 201, and the side wall of the shell 1101 is connected to a plurality of movable rods 803 arranged in an array through a lifting mechanism 9, and connecting rods 804 are fixedly connected between the movable rods 803. Both ends of each movable rod 803 are fixedly connected with a rack 802, and the rack 802 is meshing with the gear 801. The movable rod 803 is driven to move up and down reciprocatingly through the lifting mechanism 9, thereby driving the rack 802 to move, thereby pushing the gear 801 and the rotating rod 201 to rotate reciprocatingly, so that the blades 202 can reciprocate and stir the cooling water between the partition assemblies.
[0039] The lifting mechanism 9 includes two symmetrically arranged fixed blocks 901 fixedly connected to the side walls of the shell 1101, and the opposite side walls of the two fixed blocks 901 are fixedly connected to two symmetrically arranged guide rods 902, the side wall of each guide rod 902 is sleeved with a slider 903, and the slider 903 is fixed to the side wall of one of the moving rods 803, the side wall of each guide rod 902 is sleeved with a first spring 904, and the side wall of one of the moving rods 803 is fixedly connected to a push plate 910, the side wall of the return pipe 12 is fixedly inserted with a second fixed box 905, and a plurality of second baffles 907 arranged in an array are rotatably connected in the second fixed box 905 through a second rotating shaft 906, one end of the second rotating shaft 906 is fixedly connected to a disc 908, and the disc 908 The side wall is fixedly connected with a plurality of tapered rods 909 arranged in an array. When the cooling water flows out of the shell 1101 through the return pipe 12, it can enter the second fixed box 905 and impact the surface of the second baffle 907, so that the second rotating shaft 906 and the disk 908 rotate. When the tapered rod 909 abuts against the top of the push plate 910, it can push the push plate 910 and the moving rod 803 to move downward. At the same time, the slider 903 moves downward along the guide rod 902, and the first spring 904 is compressed. When the tapered rod 909 passes over the top of the push plate 910, the moving rod 803 and the connecting rod 804 can move upward and reset under the action of the first spring 904, and so on and so forth, so that the rack 802 can move back and forth up and down.
[0040] The precooling mechanism 10 includes a fixed rod 1007 fixedly connected to the side wall of the shell 1101, and the side wall of the fixed rod 1007 is fixedly connected to a fixed tube 1008, a piston 1009 is slidably connected in the fixed tube 1008, and a push rod 1010 is fixedly connected to the top of the piston 1009, the upper end of the push rod 1010 is fixed to the bottom of the push plate 910, and the side wall of the fixed tube 1008 is fixedly connected to an air intake pipe 1012, a first one-way valve is arranged in the air intake pipe 1012, the conduction direction of the first one-way valve is from the outside to the fixed tube 1008, and the fixed tube 100 The side wall of the heat exchanger 14 is fixedly connected with an air blowing pipe 1011, and a second one-way valve is arranged in the air blowing pipe 1011. The conducting direction of the second one-way valve is from the fixed pipe 1008 to the annular cover 1001, and the other end of the air blowing pipe 1011 is fixedly connected with a hollow annular cover 1001, the annular cover 1001 is sleeved on the side wall of the second connecting pipe 13, and the inner side wall of the annular cover 1001 is provided with a plurality of air blowing holes 1002 arranged in an array, and a ring-shaped absorbent cotton 1003 is fixedly inserted in the annular cover 1001, and the side wall of the heat exchanger 14 is fixedly connected with a water storage tank 1005, and the water storage tank 1005 is fixedly connected to the side wall of the heat exchanger 14. A cotton core 1006 is fixedly connected between the box 1005 and the absorbent cotton 1003. During distillation, the cooling water after absorbing heat enters the second connecting pipe 13 through the return pipe 12, and enters the heat exchanger 14 for heat dissipation and cooling. At the same time, when the push plate 910 moves up and down, the piston 1009 is driven to move up and down through the push rod 1010. When the piston 1009 moves upward, negative pressure is generated in the fixed pipe 1008. At the same time, the first one-way valve is opened and the second one-way valve is closed. At this time, the external air enters the fixed pipe 1008 through the intake pipe 1012. When the piston 1009 moves downward, the air in the fixed tube 1008 can be squeezed. At the same time, the first one-way valve is closed and the second one-way valve is opened. At this time, the air in the fixed tube 1008 is squeezed and enters the annular cover 1001 through the blowing pipe 1011, and is blown out through the blowing hole 1002. At the same time, the cooling water in the water tank 1005 can enter the absorbent cotton 1003 through the cotton core 1006, so as to cool the second connecting tube 13, and then pre-cool the cooling water, which can improve the cooling efficiency and effect of the subsequent heat exchanger 14.
[0041] The reset mechanism 4 includes two symmetrically arranged T-shaped guide rods 402 fixedly connected to the side walls of each movable plate 301, and the side walls of the T-shaped guide rods 402 are sleeved with connecting blocks 401, the connecting blocks 401 are fixed to the top of the partition assembly, and the side walls of each T-shaped guide rod 402 are sleeved with second springs 403, which play a guiding and resetting role for the movement of the movable plate 301.
[0042] The pushing mechanism 5 includes a second connecting plate 501 fixedly connected to the side wall of the movable plate 301, and the side wall of the second connecting plate 501 is fixedly connected with a pushing block 502, the side wall fixed sleeve of the rotating rod 201 is provided with a cam 503, and the cam 503 slides on the side wall of the pushing block 502, when the rotating rod 201 rotates, it drives the cam 503 to rotate synchronously, when the tip of the cam 503 abuts against the side wall of the pushing block 502, the movable plate 301 is driven to move in a direction away from the condensation tube 1104 through the second connecting plate 501.
[0043] The moving mechanism 7 includes two symmetrically arranged sleeves 701 fixedly connected to the side wall of the moving block 611, and a sleeve rod 702 is inserted in the sleeve 701, the other end of the sleeve rod 702 is fixed to the side wall of the friction block 612, and the side wall of each sleeve 701 is sleeved with a third spring 703, the top of the moving block 611 is fixedly connected with an electromagnet 704, and the top of the friction block 612 is fixedly connected with an iron block 705. The moving block 611 can be driven to move through the moving module 608, so as to adjust the distance between the moving block 611 and the friction block 612, thereby adjusting the compression amount of the third spring 703, and then adjusting the extrusion force between the friction block 612 and the rotating disk 604, so as to adjust the maximum flow rate of the steam, and the applicability is stronger.
[0044] Working principle: When in use, the steam generated by the distillation of the tower body 101 enters the first fixed box 17 through the steam pipe 102 and the first connecting pipe 18, and enters the condenser pipe 1104 through the inlet 1102 for condensation. When the steam enters the first fixed box 17, it will impact the surface of the first baffle 602, causing the first rotating shaft 601 to rotate. The rotation of the first rotating shaft 601 drives the rotation of the rotating disk 604. At the same time, the distance sensor 606 detects the 605 scale mark on the side wall of the rotating disk 604, so as to determine the rotation speed of the rotating disk 604 and then determine the flow rate of the steam. When the flow rate of the steam is too fast, the electromagnet 704 is powered off. At this time, the friction block 612 can be abutted against the side wall of the rotating disk 604 under the action of the third spring 703, so as to limit the rotation speed of the rotating disk 604, thereby limiting the flow rate of the steam, so that the condensation efficiency is higher and the effect is better.
[0045] At the same time, the circulation pump 16 is started, so that the cooling water can enter the housing 1101 after being cooled by heat exchange in the heat exchanger 14, and can pass through the first through hole 1107 on the first partition 1105 and the second through hole 1108 on the second partition 1106 from bottom to top, which can reduce the flow rate of the cooling water and increase the path of the cooling water, thereby improving the efficiency and effect of condensation;
[0046] When the cooling water flows out of the shell 1101 through the return pipe 12, it can enter the second fixed box 905 and impact the surface of the second baffle 907, so that the second rotating shaft 906 and the disc 908 rotate. When the conical rod 909 abuts against the top of the push plate 910, the push plate 910 and the moving rod 803 can be pushed to move downward. At the same time, the slider 903 moves downward along the guide rod 902, and the first spring 904 is compressed. When the conical rod 909 passes over the top of the push plate 910, the moving rod 803 and the connecting rod 804 can move upward and reset under the action of the first spring 904. This reciprocating process can make the rack 802 reciprocate up and down, thereby pushing the gear 801 and the rotating rod 201 to reciprocate, and then the blade 202 can reciprocate and stir the cooling water between the partition assembly, so that the heat absorption efficiency of the cooling water is higher and the effect is better, thereby improving the efficiency and effect of condensation, and the condensed furanone liquid is collected through the outlet 1103;
[0047] At the same time, when the rotating rod 201 rotates, the cam 503 is driven to rotate synchronously. When the tip of the cam 503 abuts against the side wall of the pushing block 502, the moving plate 301 is driven to move away from the condensing tube 1104 through the second connecting plate 501. At the same time, the second spring 403 is compressed. When the tip of the cam 503 passes over the pushing block 502, the moving plate 301 can be reset in the direction close to the condensing tube 1104 under the action of the second spring 403. In this way, the moving plate 301 can be reciprocated. At the same time, the rubber rod 303 is driven to be reciprocated through the first connecting plate 302, so that the rubber rod 303 reciprocates and vibrates the side wall of the condensing tube 1104, thereby preventing the condensed furanone liquid from adhering to the inner wall of the condensing tube 1104, so that the collection effect is better.
[0048] After the reaction is completed, when the visual sensor 610 detects that the rotation speed of the rotating disk 604 is slow, the motor 603 can be started, and at the same time, the electromagnet 704 is energized. After the electromagnet 704 is energized, the iron block 705 is attracted, so that the friction block 612 is separated from the rotating disk 604. At the same time, when the motor 603 rotates, the first baffle 602 is driven to rotate through the first rotating shaft 601, so that the air extraction operation can be performed, and the steam in the tower body 101 is accelerated to completely enter the condenser assembly 11 for condensation operation, so as to improve the efficiency and effect of condensation;
[0049] Furthermore, the moving block 611 can be driven to move by the moving module 608, so as to adjust the distance between the moving block 611 and the friction block 612, and thus adjust the compression amount of the third spring 703, and further adjust the extrusion force between the friction block 612 and the rotating disk 604, so as to adjust the maximum flow rate of the steam, and the applicability is stronger;
[0050] The cooling water after absorbing heat enters the second connecting pipe 13 through the return pipe 12, and enters the heat exchanger 14 for heat dissipation and cooling. At the same time, when the push plate 910 moves up and down, the piston 1009 is driven to move up and down through the push rod 1010. When the piston 1009 moves upward, negative pressure is generated in the fixed pipe 1008. At the same time, the first one-way valve is opened and the second one-way valve is closed. At this time, the external air enters the fixed pipe 1008 through the intake pipe 1012. When the piston 1009 moves downward, it can press the fixed pipe 1008. The air inside is squeezed, and at the same time, the first one-way valve is closed and the second one-way valve is opened. At this time, the air in the fixed pipe 1008 is squeezed and enters the annular cover 1001 through the blowing pipe 1011, and is blown out through the blowing hole 1002. At the same time, the cooling water in the water storage tank 1005 can enter the absorbent cotton 1003 through the cotton core 1006, which can accelerate the evaporation of water, causing it to absorb heat and cool down, thereby cooling the second connecting pipe 13, and then pre-cooling the cooling water, which can improve the efficiency and effect of the subsequent cooling of the heat exchanger 14.
Claims
1. A distillation tower for producing furanone, comprising a condenser assembly (11) arranged on a distillation tower body (1), wherein the distillation tower body (1) comprises a tower body (101) and a steam pipe (102), and the condenser assembly (11) comprises a shell (1101), an inlet (1102) and an outlet (1103), characterized in that: A condenser (1104) is fixedly inserted in the shell (1101), and the two ends of the condenser (1104) are respectively fixed to the inlet (1102) and the outlet (1103), the top of the inlet (1102) is fixedly connected to a first fixed box (17), and the top of the first fixed box (17) is fixedly connected to a first connecting pipe (18), the other end of the steam pipe (102) is fixed to the upper end of the first connecting pipe (18), and a deceleration mechanism (6) for decelerating steam is arranged in the first fixed box (17), a partition assembly is fixedly inserted in the shell (1101), and the partition assembly includes a plurality of first partitions (1105) arranged in an array and a plurality of second partitions (1106) arranged in an array, and the first partitions (1105) and the second partitions (1106) are arranged alternately, and a plurality of first through holes (1106) arranged in an array are opened on one side of the top of the first partition (1105). 107), and a plurality of second through holes (1108) arranged in an array are provided on the other side of the top of the second partition (1106), a circulation pump (16) is fixedly connected to the side wall of the shell (1101), and a water inlet pipe (15) is fixedly connected to the side wall of the circulation pump (16), the upper end of the water inlet pipe (15) is fixedly connected to the heat exchanger (14), the top of the heat exchanger (14) is fixedly connected to the second connecting pipe (13), and a return pipe (12) is fixedly connected between the second connecting pipe (13) and the shell (1101), a plurality of stirring mechanisms (2) for stirring cooling water are provided between the first partition (1105) and the second partition (1106), and a knocking mechanism (3) for knocking and vibrating the condenser (1104) is provided on the top of the partition assembly, and a pre-cooling mechanism (10) for pre-cooling cooling water is provided on the side wall of the second connecting pipe (13); The speed reduction mechanism (6) comprises a first rotating shaft (601) rotatably connected in a first fixed box (17), and a plurality of first baffles (602) arranged in an array are fixedly connected to the side wall of the first rotating shaft (601), a motor (603) is fixedly connected to the side wall of the first fixed box (17), and an output end of the motor (603) is fixed to one end of the first rotating shaft (601), a rotating disk (604) is fixedly connected to one end of the first rotating shaft (601), and a scale mark (605) is arranged on the side wall of the rotating disk (604), The top of the first fixed box (17) is fixedly connected to an L-shaped block (609), and the top of the L-shaped block (609) is fixedly inserted with a visual sensor (610), the side wall of the first fixed box (17) is fixedly connected to an L-shaped plate (607), and the side wall of the L-shaped plate (607) is connected to a moving block (611) via a moving module (608), the side wall of the moving block (611) is connected to a friction block (612) via a moving mechanism (7), and the side wall of the moving block (611) is fixedly inserted with a distance sensor (606).
2. A distillation tower for producing furanone according to claim 1, characterized in that: Each stirring mechanism (2) comprises a rotating rod (201) rotatably connected to the inner wall of the shell (1101), a plurality of blades (202) arranged in an array are fixedly connected to the side wall of the rotating rod (201), and the rotation of the rotating rod (201) is driven by a driving mechanism (8).
3. A distillation tower for producing furanone according to claim 2, characterized in that: The knocking mechanism (3) comprises a movable plate (301), and the side wall of the movable plate (301) is fixedly connected to a first connecting plate (302), and the side wall of the first connecting plate (302) is connected to a plurality of rubber rods (303) arranged in an array, and the movable plate (301) is connected to the top of the partition assembly via a reset mechanism (4), and the movement of the movable plate (301) is driven by a driving mechanism (5).
4. A distillation tower for producing furanone according to claim 2, characterized in that: The driving mechanism (8) comprises a gear (801) fixedly connected to the side wall of each rotating rod (201), and the side wall of the housing (1101) is connected to a plurality of movable rods (803) arranged in an array via a lifting mechanism (9), connecting rods (804) are fixedly connected between the movable rods (803), and racks (802) are fixedly connected at both ends of each movable rod (803), and the racks (802) are meshed with the gears (801).
5. A distillation tower for producing furanone according to claim 4, characterized in that: The lifting mechanism (9) comprises two symmetrically arranged fixed blocks (901) fixedly connected to the side walls of the shell (1101), and two symmetrically arranged guide rods (902) are fixedly connected to the opposite side walls of the two fixed blocks (901), the side wall of each guide rod (902) is sleeved with a slider (903), and the slider (903) is fixed to the side wall of one of the moving rods (803), the side wall of each guide rod (902) is sleeved with a first spring (904), and the side wall of one of the moving rods (803) is fixedly connected with a push plate (910), the side wall of the return pipe (12) is fixedly inserted with a second fixed box (905), and a plurality of second baffles (907) arranged in an array are rotatably connected in the second fixed box (905) via a second rotating shaft (906), one end of the second rotating shaft (906) is fixedly connected with a disk (908), and the side wall of the disk (908) is fixedly connected with a plurality of conical rods (909) arranged in an array.
6. A distillation tower for producing furanone according to claim 5, characterized in that: The pre-cooling mechanism (10) comprises a fixed rod (1007) fixedly connected to the side wall of the shell (1101), and the side wall of the fixed rod (1007) is fixedly connected to a fixed tube (1008), a piston (1009) is slidably connected in the fixed tube (1008), and a push rod (1010) is fixedly connected to the top of the piston (1009), the upper end of the push rod (1010) is fixed to the bottom of the push plate (910), and the side wall of the fixed tube (1008) is fixedly connected to an air inlet pipe (1012), a first one-way valve is provided in the air inlet pipe (1012), and the side wall of the fixed tube (1008) is fixedly connected to an air blowing valve (1012). The air blowing pipe (1011) is provided with a second one-way valve, and the other end of the air blowing pipe (1011) is fixedly connected to a hollow annular cover (1001), the annular cover (1001) is sleeved on the side wall of the second connecting pipe (13), and the inner side wall of the annular cover (1001) is provided with a plurality of air blowing holes (1002) arranged in an array, an annular absorbent cotton (1003) is fixedly inserted in the annular cover (1001), and the side wall of the heat exchanger (14) is fixedly connected to a water storage tank (1005), and a cotton core (1006) is fixedly connected between the water storage tank (1005) and the absorbent cotton (1003).
7. A distillation tower for producing furanone according to claim 3, characterized in that: The reset mechanism (4) comprises two symmetrically arranged T-shaped guide rods (402) fixedly connected to the side walls of each movable plate (301), and the side walls of the T-shaped guide rods (402) are sleeved with a connecting block (401), the connecting block (401) is fixed to the top of the partition assembly, and the side walls of each T-shaped guide rod (402) are sleeved with a second spring (403).
8. A distillation tower for producing furanone according to claim 3, characterized in that: The pushing mechanism (5) comprises a second connecting plate (501) fixedly connected to the side wall of the moving plate (301), and the side wall of the second connecting plate (501) is fixedly connected to a pushing block (502), and the side wall fixing sleeve of the rotating rod (201) is provided with a cam (503), and the cam (503) slides on the side wall of the pushing block (502).
9. A distillation tower for producing furanone according to claim 1, characterized in that: The moving mechanism (7) comprises two symmetrically arranged sleeves (701) fixedly connected to the side wall of the moving block (611), and a sleeve rod (702) is inserted into the sleeve (701), the other end of the sleeve rod (702) is fixed to the side wall of the friction block (612), and the side wall of each sleeve (701) is sleeved with a third spring (703), the top of the moving block (611) is fixedly connected to an electromagnet (704), and the top of the friction block (612) is fixedly connected to an iron block (705).
Citation Information
Patent Citations
Distillation tower with steam buffering function
CN110694294A
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CN217709357U
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CN219897102U
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