Industrial sewage sample pretreatment method and device
Through the combined device of the settlement tank and the emulsification tank, sediment and oil pollution in industrial sewage are treated using settlement and phacoemulsification technology, solving the problem of accuracy of sewage detection data, and achieving accurate monitoring of sewage components and emission standards.
Patent Information
- Application Number
- CN202410960322.4
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-07-17
- Publication Date
- 2024-12-27
AI Technical Summary
Industrial sewage contains a large amount of silt and oil-filled components, which leads to a reduction in the accuracy of the detection data and affects the monitoring results of the sewage components.
The combination device of the sedimentation tank and the emulsification tank is used to treat suspended solid particles and oil stains in the sewage sample separately through physical sedimentation and phacoemulsification technology to ensure the accuracy of the sewage sample during the detection process. In the settlement tank, the settlement monitoring sensor and control system are used to monitor the data of suspended solid particles, and the stirring parameters and settlement time are adjusted; in the emulsification tank, the oil pollution is treated with emulsification monitoring sensors and ultrasonic technology, and the emulsification parameters and particle size distribution are adjusted.
The silt and oil pollution that have high interference in the detection are effectively filtered, ensuring the accuracy of the detection data, avoiding the loss of monitoring substances required in the sewage, and improving the accuracy of sewage treatment and emission compliance rate.
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Figure CN119191396A_ABST
Abstract
Description
Technical Field
[0001] The present disclosure relates to the technical field of sewage treatment, and in particular to a method and device for pretreating industrial sewage samples. Background Art
[0002] Wastewater is often generated during industrial production, and it is necessary to recycle or discharge the wastewater generated during industrial production. Automatic water quality analyzers can monitor various pollutants in sewage, such as suspended solids, chemical oxygen demand, ammonia nitrogen, total phosphorus, etc., to help optimize sewage treatment and ensure that sewage discharge meets standards. The components contained in sewage samples are complex, and most of the polluting components are low in content and exist in various forms. Therefore, before analysis and determination, sample pretreatment corresponding to the analytical method is required to obtain the sample system that meets the form and concentration requirements of the measurement method and eliminates the interference of coexisting components. However, since sewage samples contain a large amount of particulate matter such as sediment, they have a high interference with detection; in addition, since sewage samples also contain oily components, they are easy to adhere to the detection equipment during the detection process, thereby causing the substances to be monitored in the sewage samples to be lost, affecting the accuracy of the test data. Summary of the invention
[0003] The present invention provides an industrial wastewater sample pretreatment method and device, which solves the problem that the accuracy of wastewater component detection data is reduced due to the presence of a large amount of particulate matter such as sediment and oil components in the wastewater sample.
[0004] In a first aspect, the present disclosure provides a method for pretreating industrial wastewater samples, comprising:
[0005] Input the sewage sample into the sedimentation tank and obtain the suspended solid particle data and oil concentration in the sewage sample;
[0006] Setting stirring parameters and settling time according to the suspended solid particle data, and performing stirring according to the stirring parameters during the settling process;
[0007] After reaching the settling time, extracting water samples from the settling tank and transporting them to the emulsification tank;
[0008] Adjusting emulsification parameters according to the oil concentration parameters in water and performing emulsification;
[0009] During the emulsification process, the particle size distribution of oil molecules is obtained in real time to obtain the emulsification degree;
[0010] Whether the emulsification is completed is determined based on the emulsification degree.
[0011] In some embodiments, after emulsification is completed, the emulsified water sample is analyzed to determine whether it meets the discharge standards.
[0012] In some embodiments, after the water sample in the extraction sedimentation tank is transported to the emulsification tank, the method further includes: cleaning the sedimentation tank; the cleaning of the sedimentation tank includes:
[0013] Pump air into the settling tank, and add cleaning water and cleaning liquid at the same time;
[0014] Stir the sedimentation tank and discharge the sewage sample and cleaning agent after a preset time;
[0015] Continue pumping air to dry the sedimentation tank.
[0016] In some embodiments, the method includes: cleaning the emulsification pool after emulsification is completed; the method further includes:
[0017] Pump air into the emulsification tank, and add cleaning water and cleaning liquid at the same time;
[0018] Perform ultrasonic cleaning on the emulsification tank and discharge the sewage sample and cleaning agent after a preset time;
[0019] Continue pumping to dry the emulsion pool.
[0020] In some embodiments, the water sample is in contact with only the pump tube during the process of transporting the water sample to the emulsification tank.
[0021] In some embodiments, the emulsification parameters include: ultrasound frequency, emulsification time and power.
[0022] In a second aspect, the present disclosure provides an industrial wastewater sample pretreatment device, comprising:
[0023] Settling tanks, used to settle sewage samples;
[0024] Emulsification tank, used for emulsifying sewage samples after sedimentation;
[0025] A power device, comprising a pump pipe connecting the sedimentation tank and the emulsification tank, wherein the power device is used to pump the settled sewage sample into the emulsification tank through the pump pipe;
[0026] Sedimentation monitoring equipment, arranged in the sedimentation tank, for monitoring suspended solid particle data and oil concentration in the sewage sample;
[0027] An emulsification monitoring device, arranged in the emulsification tank, for monitoring the particle size distribution of oil molecules;
[0028] An analysis device, connected to the emulsification tank, for analyzing the components of the pretreated sewage sample;
[0029] A control system is electrically connected to the sedimentation monitoring device, the emulsification monitoring device and the analysis device, and is used to set stirring parameters and filtration time according to the suspended solid particle data, adjust emulsification parameters according to the oil concentration parameter in water, and determine whether emulsification is completed based on the emulsification degree.
[0030] In some embodiments, the industrial wastewater sample pretreatment device further comprises:
[0031] An air compressor connected to the sedimentation tank and the emulsification tank through an air pipeline, and used to pump air into the sedimentation tank and the emulsification tank;
[0032] The storage device is connected with the sedimentation tank and the emulsification tank through a liquid pipeline, and is used to input the stored cleaning water and cleaning liquid into the sedimentation tank and the emulsification tank through the liquid pipeline.
[0033] In a third aspect, the present disclosure provides an electronic device, comprising a memory, a processor, and a computer program stored in the memory, wherein the processor executes the computer program to implement the steps of the method described in the above aspects.
[0034] In a fourth aspect, the present disclosure provides a computer-readable storage medium having a computer program stored thereon, which implements the steps of the method described in the above aspects when executed by a processor.
[0035] The present disclosure provides an industrial wastewater sample pretreatment method and device, which ensures the full sedimentation of suspended matter, silt and other solid particles in the wastewater sample by physically sedimenting the wastewater sample in a sedimentation tank and installing a sedimentation monitoring sensor in the sedimentation tank; the sedimentation monitoring sensor cooperates with the control system to ensure full sedimentation in the most appropriate time period; then, the settled wastewater sample is transported to an emulsification tank for ultrasonic emulsification, and an emulsification monitoring sensor is installed in the emulsification tank, which reduces the adhesion and blockage of oil in the analysis system pipeline, thereby solving the influence of oil pollution components in the water on the detection results. Through the above two steps, the present invention not only filters the silt and other particles that have high interference with the detection, but also ensures that the required monitoring substances in the water sample are not lost, making the detection data more accurate. BRIEF DESCRIPTION OF THE DRAWINGS
[0036] The present disclosure will be described in more detail below based on embodiments and with reference to the accompanying drawings:
[0037] Figure 1 A schematic flow chart of a method for pretreating industrial wastewater samples provided in an embodiment of the present disclosure.
[0038] Figure 2 A schematic diagram of the structure of an industrial wastewater sample pretreatment device provided in an embodiment of the present disclosure.
[0039] In the drawings, the same reference numerals are used for the same components, and the drawings are not drawn to scale. DETAILED DESCRIPTION
[0040] In order to enable those skilled in the art to better understand the technical solution of the present disclosure, and to fully understand and implement how the present disclosure applies technical means to solve technical problems and achieve the corresponding technical effects, the technical solution in the embodiments of the present disclosure will be clearly and completely described below in conjunction with the drawings in the embodiments of the present disclosure. Obviously, the described embodiments are only embodiments of a part of the present disclosure, not all of the embodiments. The embodiments of the present disclosure and the various features in the embodiments can be combined with each other without conflict, and the technical solutions formed are all within the scope of protection of the present disclosure. Based on the embodiments in the present disclosure, all other embodiments obtained by ordinary technicians in this field without making creative work should fall within the scope of protection of the present disclosure.
[0041] It should be noted that the terms "first", "second", etc. in the specification and claims of the present disclosure and the above-mentioned drawings are used to distinguish similar objects, and are not necessarily used to describe a specific order or sequence. It should be understood that the data used in this way can be interchangeable where appropriate, so that the embodiments of the present disclosure described herein can be implemented in an order other than those illustrated or described herein. In addition, the terms "including" and "having" and any variations thereof are intended to cover non-exclusive inclusions, for example, a process, method, system, product, or device that includes a series of steps or units is not necessarily limited to those steps or units that are clearly listed, but may include other steps or units that are not clearly listed or inherent to these processes, methods, products, or devices.
[0042] It should be noted that the steps shown in the flowcharts of the accompanying drawings can be executed in a computer system such as a set of computer executable instructions, and that, although a logical order is shown in the flowcharts, in some cases, the steps shown or described can be executed in an order different from that shown here.
[0043] Embodiment 1
[0044] Figure 1 The following is a schematic diagram of a process for pre-treating industrial wastewater samples provided in an embodiment of the present disclosure. Figure 1 As shown, a method for pretreating industrial wastewater samples comprises:
[0045] Step 01: Input the sewage sample into the sedimentation tank and obtain the suspended solid particle data and oil concentration in the water of the sewage sample. Input the sewage sample into the sedimentation tank, which is used to sediment the sewage sample. The sedimentation monitoring sensor is set in the sedimentation tank. During the sedimentation process of the sewage sample, the sedimentation monitoring sensor monitors the suspended solid particle data and oil concentration in the sewage sample, and then transmits the monitored data to the control system.
[0046] Step 02: Set stirring parameters and settling time according to the suspended solid particle data, and stir according to the stirring parameters during the settling process.
[0047] The control system receives the suspended solid particle data and oil concentration in the water transmitted by the sedimentation monitoring sensor, and controls the stirring parameters and sedimentation time in the sedimentation tank according to the preset control program to ensure that the suspended matter, silt and other solid particles in the sedimentation tank are fully settled in the most appropriate time period, thereby achieving the initial separation and purification of sewage.
[0048] Step 03: After reaching the settling time, extract the water sample in the settling tank and transport it to the emulsification tank.
[0049] According to different water sample conditions and required sample requirements, after the sedimentation time is reached, the control system controls the opening and closing of the sedimentation tank discharge valve according to the preset control program, extracts part of the water sample from the top or middle of the sewage sample that has completed sedimentation, and transports it to the emulsification tank.
[0050] The control system controls the power equipment to extract water samples from the top or middle of the sedimentation tank and transport them to the emulsification tank. During the water sample transportation process, the liquid only contacts the pump tube, which can effectively avoid contamination during the water sample collection process and prevent corrosion and damage to the pump caused by corrosive water samples.
[0051] Step 04: Adjust the emulsification parameters according to the oil concentration parameters in water, and perform emulsification.
[0052] After the water sample is transported to the emulsification tank, the control system adjusts the ultrasonic emulsification parameters according to the requirements of the water sample, including frequency, time, power, etc. Ultrasonic waves are used to treat water samples containing oil. Under the action of ultrasonic energy, the oil droplets are broken up, and the immiscible liquids in the sewage water sample are mixed together to form an emulsion-like liquid. The emulsification device breaks up the oil contained in the sewage into particles, so that the treated samples are more uniform, reducing the adhesion and blockage of oil in the analysis system pipeline.
[0053] Step 05: During the emulsification process, obtain the particle size distribution of the oil molecules in real time to obtain the emulsification degree.
[0054] Step 06: Determine whether emulsification is completed based on the emulsification degree. Determine whether the particle size distribution of the obtained oil molecules reaches the preset particle size distribution, and if so, stop emulsification.
[0055] After the emulsification is completed, step 07 is also included: analyzing the emulsified water sample to determine whether it meets the discharge standard. After the emulsification stops, the emulsified water sample is transported to the analysis equipment for analysis to analyze whether the suspended solids, chemical oxygen demand, ammonia nitrogen, total phosphorus and other components in the sewage meet the discharge standard. If so, it is determined that the sewage can be discharged directly; if not, it is determined that the sewage needs to be optimized before discharge.
[0056] The method provided in this embodiment designs the process of pretreatment of industrial wastewater samples to ensure the effectiveness and accuracy of analytical data, optimize the detection concentration range of the components to be tested, increase the operation and maintenance cycle, and help optimize wastewater treatment and ensure that wastewater discharge meets standards.
[0057] Embodiment 2
[0058] On the basis of the above embodiment, after the water sample in the extraction sedimentation tank is transported to the emulsification tank, the method also includes: cleaning the sedimentation tank; the cleaning of the sedimentation tank includes: pumping air into the sedimentation tank, and adding cleaning water and cleaning liquid at the same time; stirring the sedimentation tank, and discharging the sewage sample and cleaning agent after a preset time; continuing to pump air to blow the sedimentation tank dry.
[0059] After each sample collection, the sedimentation tank needs to be cleaned and discharged before the next pretreatment process. As time goes by, the suspended matter and sediment in the tank will increase. In order not to affect the treatment effect, the control system controls the air compressor to pump air into the sedimentation tank, and at the same time, add cleaning water and cleaning liquid into the sedimentation tank respectively, and stir and clean it with a stirring rod. After cleaning, the water sample and cleaning agent are discharged, and then air is continued to be pumped into the sedimentation tank to dry the sedimentation tank.
[0060] Softened water or desalted water can be used for equipment cleaning. After each pipeline sampling or analysis, the pipeline or analysis module should be flushed 2 to 3 times with cleaning water and then blown dry with air. The equipment is set to use cleaning fluid for cleaning at a fixed period to remove residual particulate matter in the sedimentation tank.
[0061] Embodiment 3
[0062] On the basis of the above embodiment, after the emulsification is completed, the emulsification tank is cleaned; the method for cleaning the emulsification tank also includes: pumping air into the emulsification tank, and adding cleaning water and cleaning liquid respectively; ultrasonically cleaning the emulsification tank, discharging the sewage sample and cleaning agent after a preset time; and continuing to pump air to dry the emulsification tank.
[0063] After each sample collection, the emulsification tank needs to be cleaned and discharged before the next pretreatment process. When the water sample is emulsified, the air pump operates to pump air into the sedimentation tank, and at the same time, cleaning water and cleaning liquid are added to clean the emulsification tank. The emulsification tank can be cleaned under ultrasonic vibration. After cleaning, the emulsified water sample and cleaning agent are discharged, and then air is continued to be pumped into the sedimentation tank to dry the emulsification tank.
[0064] Softened water or desalted water can be used for equipment cleaning. After each pipeline sampling or analysis, the pipeline or analysis module should be flushed 2 to 3 times with cleaning water and then blown dry with air. The equipment should be cleaned with cleaning fluid at a fixed period to remove components such as oil attached to the emulsification tank, pipeline and analysis equipment.
[0065] Embodiment 4
[0066] Figure 2 The schematic diagram of the structure of an industrial wastewater sample pretreatment device provided in the embodiment of the present disclosure. Figure 2 As shown, an industrial wastewater sample pretreatment device 100 includes: a sedimentation tank 10, an emulsification tank 20, a power device 30, a sedimentation monitoring device (not shown in the figure), an emulsification monitoring device (not shown in the figure), an analysis device 40 and a control system 50. Among them, the sedimentation tank 10 is used to sediment the sewage sample; the emulsification tank 20 is used to emulsify the sewage sample after sedimentation; the power equipment 30 includes a pump pipe connecting the sedimentation tank and the emulsification tank, and the power equipment is used to pump the settled sewage sample into the emulsification tank through the pump pipe; the sedimentation monitoring equipment 40 is arranged in the sedimentation tank, and is used to monitor the suspended solid particle data of the sewage sample and the oil concentration in the water; the emulsification monitoring equipment is arranged in the emulsification tank, and is used to monitor the particle size distribution of the oil molecules; the analysis equipment is connected to the emulsification tank, and is used to analyze the components of the pretreated sewage sample; the control system is electrically connected to the sedimentation monitoring equipment, the emulsification monitoring equipment and the analysis equipment, and is used to set the stirring parameters and the filtration time according to the suspended solid particle data, adjust the emulsification parameters according to the oil concentration parameters in the water, and judge whether the emulsification is completed based on the emulsification degree.
[0067] Furthermore, the analysis equipment is also used to analyze the emulsified water sample after the emulsification is completed to determine whether the discharge standards are met.
[0068] In addition to the above structure, the industrial wastewater sample pretreatment device also includes an air compressor and a storage device. The air compressor is connected to the sedimentation tank and the emulsification tank through an air pipeline and is used to pump air into the sedimentation tank and the emulsification tank; the storage device is connected to the sedimentation tank and the emulsification tank through a liquid pipeline and is used to input the stored cleaning water and cleaning liquid into the sedimentation tank and the emulsification tank through the liquid pipeline.
[0069] Optionally, the mechanical stirring device used for stirring in the sedimentation tank can perform cutting or magnetic stirring, and the stirring rod is an ultrasonic oscillating rod.
[0070] Optionally, high pressure air washing can be performed during cleaning.
[0071] Optionally, the sedimentation tank has a diameter of 150 mm and a height of 300 mm.
[0072] Optionally, during cleaning, the cleaning device also includes an automatic pressure drain (discharge valve), an overflow port, a pure water port, an upper injection three-way solenoid valve, a liquid level detection device, etc.
[0073] The industrial wastewater sample pretreatment device controls the electromagnetic valve switch on the flow path through the control system, as well as the automatic collection and continuous analysis of the sedimentation monitoring equipment and emulsification monitoring equipment to ensure the multi-channel and multi-parameter analysis function of the equipment. The wastewater sample passes through the sedimentation tank, peristaltic pump, emulsification tank, and analysis equipment in turn, and uses physical sedimentation technology, ultrasonic emulsification technology, and online cleaning technology to effectively reduce the interference of complex water quality substrate and oil components on detection. At the same time, it has cooling and decompression functions to provide qualified water samples for the chemical analysis module and extend the equipment operation and maintenance cycle.
[0074] Embodiment five:
[0075] Based on the above embodiment, the emulsified water sample is analyzed to determine whether it meets the discharge standard. If it does not meet the discharge standard, it is determined that the sewage needs to be optimized and then recycled or discharged. Currently, the sewage pretreatment technologies mainly include coagulation and sedimentation.
[0076] Coagulation is composed of two processes: coagulation and flocculation. Coagulation mainly refers to the process of destabilization of colloids after the double electrical layer is compressed; flocculation mainly refers to the process of colloids condensing into large flocs after destabilization. Coagulation is mainly used to remove suspended matter, colloidal substances and some soluble substances in water, and reduce the turbidity, color and part of the chemical oxygen demand of water.
[0077] Sedimentation method uses the natural sedimentation method. There are many suspended solids in sewage that are denser than water, so they can sink naturally. Using this principle to separate solids and liquids in sewage is called sedimentation method. Sedimentation devices for sewage treatment are generally divided into two categories: one is mainly used to settle inorganic solids, called sand settling tanks; the other is mainly used to settle organic solids, called sedimentation tanks. Sedimentation method is mainly used to remove sediment and suspended matter produced after coagulation to further improve water quality.
[0078] Embodiment six:
[0079] On the basis of the above embodiments, this embodiment provides an electronic device, including a memory, a processor, and a computer program stored in the memory, wherein the processor executes the computer program to implement the steps of the method described in the above embodiments.
[0080] In some implementations of this embodiment, a computer-readable storage medium is provided, on which a computer program is stored. When the computer program is executed by a processor, the steps of the method described in the above embodiment are implemented.
[0081] In some implementations of this embodiment, a computer program product is provided, including a computer program / instructions, characterized in that when the computer program is executed by a processor, the steps of the method described in the above embodiment are implemented.
[0082] The processor may include, but is not limited to, one or more processors or microprocessors. Each processor may be an application specific integrated circuit (ASIC), a digital signal processor (DSP), a digital signal processing device (DSPD), a programmable logic device (PLD), a field programmable gate array (FPGA), a controller, a microcontroller, a microprocessor or other electronic components to execute the method in the above embodiments.
[0083] The computer-readable storage medium may be implemented by any type of volatile or non-volatile storage device or a combination thereof, and the computer-readable storage medium may include but is not limited to, for example, random access memory (RAM), read-only memory (ROM), flash memory, EPROM memory, EEPROM memory, registers, computer storage media (e.g., hard disk, floppy disk, solid-state drive, removable disk, CD-ROM, DVD-ROM, Blu-ray disc, etc.).
[0084] The computer-readable storage medium may also store at least one computer executable program / instruction, which may be, for example, a computer-readable instruction. The computer-readable storage medium includes, but is not limited to, for example, a volatile memory and / or a non-volatile memory. The volatile memory may include, for example, a random access memory (RAM) and / or a cache memory (cache), etc. The computer-readable storage medium may include, for example, a read-only memory (ROM), a hard disk, a flash memory, etc. For example, a non-transitory computer-readable storage medium may be connected to a computing device such as a computer, and then, when the computing device runs the computer-readable instructions stored on the computer-readable storage medium, the various methods described above may be performed.
[0085] In addition, the electronic device may also include (but not limited to) a data bus, an input / output (I / O) bus, a display, and input / output devices (eg, keyboard, mouse, speaker, etc.), etc.
[0086] The processor may communicate with external devices via an I / O bus via a wired or wireless network.
[0087] In one embodiment, the at least one computer executable instruction may also be compiled into or constitute a software product / computer program product, wherein one or more computer executable instructions are executed by a processor to perform the various functions and / or method steps in the embodiments described in the present technology.
[0088] In the embodiments provided in the present disclosure, it should be understood that the disclosed devices and methods can also be implemented in other ways. The device embodiments described above are merely schematic. For example, the flowcharts and block diagrams in the accompanying drawings show the possible architecture, functions and operations of the devices, methods and computer program products according to multiple embodiments of the present disclosure. In this regard, each box in the flowchart or block diagram can represent a module, a program segment or a part of a code, and the above-mentioned module, program segment or a part of the code contains one or more executable instructions for implementing the specified logical function. It should also be noted that in some alternative implementations, the functions marked in the box can also occur in a different order from the order marked in the accompanying drawings. For example, two consecutive boxes can actually be executed substantially in parallel, and they can sometimes be executed in the opposite order, depending on the functions involved. It should also be noted that each box in the block diagram and / or flowchart, and the combination of boxes in the block diagram and / or flowchart can be implemented with a dedicated hardware-based system that performs a specified function or action, or can be implemented with a combination of dedicated hardware and computer instructions.
[0089] It should be noted that in the present disclosure, the terms "include", "comprises" or any other variations thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device. In the absence of further restrictions, an element limited by the sentence "includes a ..." does not exclude the existence of other identical elements in the process, method, article or device including the element.
[0090] Although the embodiments disclosed in the present disclosure are as above, the above contents are only embodiments adopted for facilitating the understanding of the present disclosure and are not intended to limit the present disclosure. Any technician in the technical field to which the present disclosure belongs can make any modifications and changes in the form and details of the implementation without departing from the spirit and scope disclosed in the present disclosure, but the scope of patent protection of the present disclosure shall still be subject to the scope defined in the attached claims.
Claims
1. A method for pretreating industrial wastewater samples, characterized in that: include: Input the sewage sample into the sedimentation tank and obtain the suspended solid particle data and oil concentration in the sewage sample; Setting stirring parameters and settling time according to the suspended solid particle data, and performing stirring according to the stirring parameters during the settling process; After reaching the settling time, extracting water samples from the settling tank and transporting them to the emulsification tank; Adjusting emulsification parameters according to the oil concentration parameters in water and performing emulsification; During the emulsification process, the particle size distribution of oil molecules is obtained in real time to obtain the emulsification degree; Whether the emulsification is completed is determined based on the emulsification degree.
2. The industrial wastewater sample pretreatment method according to claim 1, characterized in that: After emulsification is completed, the emulsified water sample is analyzed to determine whether it meets the discharge standards.
3. The industrial wastewater sample pretreatment method according to claim 1, characterized in that: After the water sample in the extraction sedimentation tank is transported to the emulsification tank, the method further includes cleaning the sedimentation tank; the cleaning of the sedimentation tank includes: Pump air into the settling tank, and add cleaning water and cleaning liquid at the same time; Stir the sedimentation tank and discharge the sewage sample and cleaning agent after a preset time; Continue pumping air to dry the sedimentation tank.
4. The industrial wastewater sample pretreatment method according to claim 1, characterized in that: After the emulsification is completed, the method further includes cleaning the emulsification pool; the cleaning of the emulsification pool includes: Pump air into the emulsification tank, and add cleaning water and cleaning liquid at the same time; Perform ultrasonic cleaning on the emulsification tank and discharge the sewage sample and cleaning agent after a preset time; Continue pumping to dry the emulsion pool.
5. The industrial wastewater sample pretreatment method according to claim 1, characterized in that: include: When the water sample is transported to the emulsification tank, the water sample only contacts the pump tube.
6. The method according to claim 1, characterized in that The emulsification parameters include: ultrasonic frequency, emulsification time and power.
7. An industrial wastewater sample pretreatment device, characterized in that: include: Settling tanks, used to settle sewage samples; Emulsification tank, used for emulsifying sewage samples after sedimentation; A power device, comprising a pump pipe connecting the sedimentation tank and the emulsification tank, wherein the power device is used to pump the settled sewage sample into the emulsification tank through the pump pipe; Sedimentation monitoring equipment, arranged in the sedimentation tank, for monitoring suspended solid particle data and oil concentration in the sewage sample; An emulsification monitoring device, arranged in the emulsification tank, for monitoring the particle size distribution of oil molecules; An analysis device, connected to the emulsification tank, for analyzing the components of the pretreated sewage sample; A control system is electrically connected to the sedimentation monitoring device, the emulsification monitoring device and the analysis device, and is used to set stirring parameters and filtration time according to the suspended solid particle data, adjust emulsification parameters according to the oil concentration parameter in water, and determine whether emulsification is completed based on the emulsification degree.
8. The industrial wastewater sample pretreatment device according to claim 7, characterized in that: Also includes: An air compressor connected to the sedimentation tank and the emulsification tank through an air pipeline, and used to pump air into the sedimentation tank and the emulsification tank; The storage device is connected with the sedimentation tank and the emulsification tank through a liquid pipeline, and is used for inputting the stored cleaning water and cleaning liquid into the sedimentation tank and the emulsification tank through the liquid pipeline.
9. An electronic device comprising a memory, a processor and a computer program stored in the memory, characterized in that: The processor executes the computer program to implement the steps of the method according to any one of claims 1 to 6.
10. A computer-readable storage medium having a computer program stored thereon, characterized in that: When the computer program is executed by a processor, the steps of the method according to any one of claims 1 to 6 are implemented.
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