Reaction kettle for producing perfluorononenoxy sodium benzenesulfonate
By designing a reactor for the production of perfluorononeneoxybenzenesulfonate, which includes stirring, cleaning and pressurized components, the material accumulation problem caused by the failure of reactants to fully react is solved, and a more efficient material reaction and production process is achieved. optimization.
Patent Information
- Application Number
- CN202411831245.9
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2024-12-12
- Publication Date
- 2025-02-14
AI Technical Summary
During the production process of perfluorononeneoxybenzenesulfonate, the reactants in the reactor fail to react completely, resulting in material accumulation, requiring frequent cleaning, which is time-consuming and labor-intensive.
A reactor for the production of perfluorononeneoxybenzenesulfonate is designed, including agitating parts, cleaning parts and pressurized parts. The mixing component realizes effective stirring of materials through the cooperation of rack and connecting slide; the cleaning component realizes cleaning of the inner wall of the device and the filter plate through the design of vertical sweeping plate and arc fan plate; the pressurized component is passed through the transmission belt and the inclined push plate Cooperate to enhance the air pressure in the device and promote material reaction.
Through the design of this reactor, it can effectively promote material reaction, reduce material accumulation, improve production efficiency, and reduce cleaning frequency and cost.
Smart Images

Figure CN119425586A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of sodium perfluorononenyloxybenzenesulfonate equipment, in particular to a reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate. Background Art
[0002] Sodium perfluorononenyloxybenzenesulfonate, referred to as OBS, is one of the common fluorinated surfactants on the market. It has low surface tension and critical micelle concentration and is the main active ingredient of the drainage agent in the oilfield fracturing system. The reactor for the production of sodium perfluorononenyloxybenzenesulfonate is a key equipment used in the production process of sodium perfluorononenyloxybenzenesulfonate.
[0003] In the reactor used for the production of sodium perfluorononenyloxybenzenesulfonate, its main function is to provide a closed environment so that the synthesis reaction of sodium perfluorononenyloxybenzenesulfonate can react well. When various reactants cannot react completely in the reactor, materials will accumulate and need to be cleaned up in time, which is time-consuming and laborious. Summary of the invention
[0004] The object of the present invention is to provide a reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate to solve the problems raised in the above background technology.
[0005] In order to solve the above technical problems, the present invention is achieved through the following technical solutions:
[0006] The present invention is a reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate, comprising a support, the end surface of the support is fixedly connected to a shell, the end surface of the shell away from the support is fixedly connected to a sealing cover, the end surface of the support close to the sealing cover is fixedly connected to a top cover, the end surface of the top cover is fixedly connected to a feed port, and further comprising:
[0007] A stirring component, the stirring component comprises an output shaft, a surface of the output shaft is fixedly connected with a periodic tooth plate, and a surface of the periodic tooth plate is meshingly connected with a rack;
[0008] A cleaning component, wherein the cleaning component comprises a vertical sweeping plate, a filter plate is arranged on the surface of the output shaft close to the vertical sweeping plate, and an arc fan plate is fixedly connected to the surface of the output shaft away from the filter plate;
[0009] The pressurizing component includes a motor positioning plate, and a transmission shaft is arranged on the end surface of the motor positioning plate away from one end of the motor, and a transmission belt is connected to the surface of the transmission shaft.
[0010] Furthermore, the end face of the support away from one end of the shell is fixedly connected with a discharge port, the surface of the discharge port is provided with an engine, the surface of the support close to the shell side is provided with a motor, the surface of the support close to one end of the engine is fixedly connected with a support rod, the number of the support rods is four, and the four support rods are symmetrically distributed on the surface of the support.
[0011] Furthermore, the stirring component includes a cross bar, the end face of the cross bar is fixedly connected to an auxiliary stirring fan, the end face of the output shaft away from the periodic tooth plate is fixedly connected to a positioning shaft, the end face of the positioning shaft away from the output shaft is fixedly connected to a top shaft, and the surface of the top shaft away from the positioning shaft is fixedly connected to a main stirring fan, and the number of the cross bars is two, and the two cross bars are symmetrically distributed around the surface center of the rack.
[0012] Furthermore, a sliding rod is provided on the surface of the positioning shaft, the end surface of the rack close to one end of the sliding rod is fixedly connected to a connecting slide plate, the end surface of the connecting slide plate away from one end of the output shaft is fixedly connected to a push plate, the inner wall of the sliding rod close to one side of the connecting slide plate is rotatably connected to a transverse axis, the surface of the transverse axis is fixedly connected to a vertical fan, the surface of the transverse axis away from one end of the sliding rod is transmission-connected to an auxiliary belt, and the surface of the support close to one side of the auxiliary belt is fixedly connected to an auxiliary shell;
[0013] The number of the connecting slides is set to two, and the two connecting slides are symmetrically distributed on the surface of the rack, and the end face of the connecting slide is slidingly connected to the surface of the slide rod. The number of the vertical fans is set to two, and the two vertical fans are symmetrically distributed on the surface of the horizontal axis, and the surface of the horizontal axis passes through the inner wall of the support to the inner wall of the auxiliary shell. The number of the auxiliary belts is set to two, and the two auxiliary belts are symmetrically distributed on the surface of the support, and the inner wall of the auxiliary shell is fixedly connected to the surface of the support.
[0014] Furthermore, the cleaning component includes an adsorption plate, a half-leaf arc plate is fixedly connected to the surface of the top shaft away from the adsorption plate, a bottom arc plate is fixedly connected to the inner wall of the support close to the half-leaf arc plate, an arc groove plate is fixedly connected to the inner wall of the support close to the bottom arc plate, and a scraper is slidably connected to the surface of the arc groove plate;
[0015] The surface of the vertical sweeping plate contacts the end surface of the filter plate. There are three arc fan plates, which are symmetrically distributed around the surface center of the output shaft. The surface of the arc fan plate away from the filter plate contacts the end surface of the adsorption plate.
[0016] Further, a force-bearing plate is provided on the surface of the semi-leaf arc plate, the force-bearing plate is fixedly connected with a rotating shaft plate, the inner wall of the rotating shaft plate is rotatably connected with a rotating shaft, the surface of the rotating shaft is rotatably connected with a connecting shaft rod, the end surface of the force-bearing plate close to one end of the rotating shaft plate is fixedly connected with a return spring, and the surface of the force-bearing plate is slidably connected with a force-bearing groove plate;
[0017] The number of the force-bearing plates is four, and the four force-bearing plates are symmetrically distributed around the surface center of the half-leaf arc plate. The number of the rotating shaft plates is two, and the two rotating shaft plates are symmetrically distributed around the surface of the force-bearing plate. The number of the reset springs is two, and the two reset springs are symmetrically distributed around the surface of the force-bearing plate. The end face of the force-bearing slot plate away from one end of the force-bearing plate is fixedly connected to the inner wall of the support, the end face of the connecting shaft away from one end of the rotating shaft is fixedly connected to the end face of the scraper plate close to one end of the arc slot plate, and the surface of the force-bearing slot plate contacts the surface of the half-leaf arc plate.
[0018] Furthermore, the pressure-applying component includes a transmission plate, an end face of the transmission plate away from the motor positioning plate is fixedly connected to an inclined push plate, an end face of the inclined push plate away from the transmission plate is fixedly connected to a slider, the surface of the motor positioning plate is fixedly connected to the surface of the support, the inner wall of the transmission belt is rotatably connected to the surface of the transmission plate, two inclined push plates are provided, and the two inclined push plates are symmetrically distributed on the surface of the transmission plate, and two sliders are provided, and the two sliders are symmetrically distributed on the end face of the inclined push plate.
[0019] Furthermore, a push block is provided on the end face of the slider away from the inclined push plate, the inner wall of the slider is slidably connected to an arc slide plate, the end face of the push block away from the slider is fixedly connected to a box plate, the surface of the box plate is slidably connected to a box body, the surface of the box body close to the support is fixedly connected to an air outlet pipe, the end face of the arc slide plate close to the auxiliary shell is fixedly connected to a positioning block, and the inner wall of the box body is fixedly connected to the surface of the support.
[0020] The present invention has the following beneficial effects:
[0021] When the present invention is in operation, the required materials are poured into the device through the top cover and the feed port. At this time, the engine in the stirring component is started to drive the output shaft to rotate. When the output shaft rotates, it will drive the periodic tooth plate to rotate. When the periodic tooth plate rotates, it will drive the rack to operate periodically. The rack will drive the connecting slide plate to slide periodically along the surface of the slide rod. At the same time, when the rack is running, it will drive the cross bar to run, and the cross bar will drive the auxiliary stirring fan to run. The auxiliary stirring fan will stir the materials inside it to promote its reaction. At the same time, when the connecting slide plate is running, it will drive the push plate to run. When the push plate is running, it will collide with the vertical fan, thereby driving the vertical fan to rotate. The vertical fan passes through another The stirring force in one direction makes better use of the materials inside it. At the same time, when the vertical fan rotates, it will drive the horizontal axis to rotate along the inner wall of the slide bar. When the horizontal axis rotates, it will drive the auxiliary belt to transmit. When the auxiliary belt transmits, it will drive the horizontal axis of the inner wall of the other end to rotate. Therefore, when the device is in cyclic operation, the horizontal axis at the other end will not stop rotating. At the same time, when the output shaft rotates, it will drive the positioning shaft to rotate on the inner wall of the slide bar. When the positioning shaft rotates, it will drive the top shaft to rotate. When the top shaft rotates, it will drive the main stirring fan to rotate. The main stirring fan will perform initial stirring on the materials inside it, so that it can perform a good stirring effect.
[0022] When the present invention is in operation, in the cleaning component, when the output shaft rotates, it will drive the vertical sweeping plate to rotate, and the vertical sweeping plate will clean the materials remaining on the surface of the filter plate and the inner wall of the support to prevent the materials from accumulating in the device and causing damage to the device. After that, the reacted materials will fall below through the filter plate. At the same time, when the output shaft rotates, it will drive the arc fan plate to rotate along the inner wall of the support and clean the surface of the adsorption plate. Finally, the reacted materials will fall to the bottom through the adsorption plate and be discharged through the discharge port. At the same time, when the top shaft rotates, it will drive the half-leaf arc plate When the half-leaf arc plate rotates, it will push the force-bearing plate to slide along the inner wall of the force-bearing groove plate. When the force-bearing plate is running, it will drive the rotating shaft plate to run. When the rotating shaft plate is running, it will drive the connecting shaft rod to rotate along the surface of the rotating shaft. When the connecting shaft rod is running, it will drive the scraper to slide along the mutually approaching surface of the bottom arc plate and the arc groove plate. At the same time, it will run along the inner wall of the support, so that the scraper will clean the inner wall of the support. At the same time, when the force-bearing plate is running, it will push the reset spring to run. When the half-leaf arc plate does not push the force-bearing plate to run, the force-bearing plate will be reset by the reaction force of the reset spring.
[0023] When the present invention is running, the motor in the pressurizing component is started, driving the transmission shaft to rotate, and the transmission shaft will drive the transmission belt to transmit. When the transmission belt is transmitting, it will drive the transmission plate on the inner wall of the other end to rotate, and the transmission plate will drive the inclined push plate to operate. When the inclined push plate is operating, it will drive the slider to slide along the surface of the arc slide. At the same time, when the slider is operating, it will drive the push block to slide along the inner wall of the arc slide. When the push block runs to a certain position, it will collide and contact with the box plate, thereby driving the box plate to slide along the inner wall of the box body, thereby squeezing the gas in the box body, and finally ejecting gas through the outlet pipe, thereby enhancing the air pressure in the device, and making the material reaction therein more complete. At the same time, it will assist the main stirring fan, driving it to rotate better and enhancing the stirring effect.
[0024] Of course, any product implementing the present invention does not necessarily need to achieve all of the advantages described above at the same time. BRIEF DESCRIPTION OF THE DRAWINGS
[0025] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the accompanying drawings required for describing the embodiments will be briefly introduced below. Obviously, the accompanying drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other accompanying drawings can be obtained based on these accompanying drawings without paying creative work.
[0026] Figure 1 It is a schematic diagram of the overall structure of the present invention;
[0027] Figure 2 It is a cross-sectional view of the overall structure of the present invention;
[0028] Figure 3 This is a cross-sectional view of the stirring component structure of the present invention;
[0029] Figure 4 For the present invention Figure 3 A magnified view of part A in FIG.
[0030] Figure 5 It is a bottom view of the structure section of the cleaning component of the present invention;
[0031] Figure 6 This is a schematic diagram of the structure of a half-leaf arc plate of the present invention;
[0032] Figure 7 For the present invention Figure 6 A magnified view of part B in FIG.
[0033] Figure 8 This is a schematic diagram of the structure of the cleaning component of the present invention;
[0034] Fig. 9 For the present invention Figure 8 Enlarged view of part C in .
[0035] In the accompanying drawings, the components represented by the reference numerals are listed as follows:
[0036] In the figure: 1, stirring part; 2, cleaning part; 3, cleaning part; 4, engine; 5, motor; 6, discharge port; 7, support; 8, shell; 9, sealing cover; 10, top cover; 11, feed port; 12, support rod; 21, output shaft; 22, periodic tooth plate; 23, rack; 24, cross bar; 25, auxiliary stirring fan; 26, positioning shaft; 27, top shaft; 28, main stirring fan; 29, auxiliary belt; 30, auxiliary shell; 31, slide bar; 32, connecting slide plate; 33, push plate; 34, cross shaft; 35, vertical fan; 4 1. Vertical sweeping plate; 42. Filter plate; 43. Arc fan plate; 44. Adsorption plate; 45. Half-leaf arc plate; 46. Force plate; 47. Bottom arc plate; 48. Arc slot plate; 49. Scraper; 50. Rotating shaft plate; 51. Rotating shaft; 52. Connecting shaft; 53. Reset spring; 54. Force slot plate; 61. Motor positioning plate; 62. Transmission shaft; 63. Transmission belt; 64. Transmission plate; 65. Positioning block; 66. Exhaust pipe; 67. Oblique push plate; 68. Sliding block; 69. Push block; 70. Arc sliding plate; 71. Box plate; 72. Box body. DETAILED DESCRIPTION
[0037] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0038] See also Figure 1-Figure 9 As shown, the present invention is a reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate, comprising a support 7, a shell 8 is fixedly connected to the end face of the support 7, a sealing cover 9 is fixedly connected to the end face of the shell 8 away from the support 7, a top cover 10 is fixedly connected to the end face of the support 7 close to the sealing cover 9, and a feed port 11 is fixedly connected to the end face of the top cover 10, and further comprising:
[0039] The stirring component 1 includes an output shaft 21. The engine 4 is started to drive the output shaft 21 to rotate. When the output shaft 21 rotates, the periodic toothed plate 22 is driven to rotate. The surface of the output shaft 21 is fixedly connected with the periodic toothed plate 22. When the periodic toothed plate 22 rotates, the rack 23 is driven to perform periodic operation. The surface of the periodic toothed plate 22 is meshedly connected with the rack 23. The rack 23 drives the connecting slide 32 to slide periodically along the surface of the slide bar 31. At the same time, when the rack 23 runs, it drives the cross bar 24 to run.
[0040] The cleaning component 2 includes a vertical sweeping plate 41. When the output shaft 21 rotates, the vertical sweeping plate 41 is driven to rotate. The vertical sweeping plate 41 will clean the materials remaining on the surface of the filter plate 42 and the inner wall of the support 7 to prevent the materials from accumulating in the device and causing damage to the device. After that, the reacted materials will fall below through the filter plate 42. The surface of the output shaft 21 close to the vertical sweeping plate 41 is provided with a filter plate 42. The surface of the output shaft 21 away from the filter plate 42 is fixedly connected with an arc fan plate 43. At the same time, when the output shaft 21 rotates, the arc fan plate 43 is driven to rotate along the inner wall of the support 7. At the same time, the surface of the adsorption plate 44 is cleaned. Finally, the reacted materials fall to the bottom through the adsorption plate 44 and are transmitted through the discharge port 6.
[0041] The pressurizing component 3 includes a motor positioning plate 61, and a transmission shaft 62 is arranged on the end face of the motor positioning plate 61 away from the motor 5. When the motor 5 is started, the transmission shaft 62 is driven to rotate, and the transmission shaft 62 drives the transmission belt 63 to transmit the power. The surface transmission of the transmission shaft 62 is connected with the transmission belt 63. When the transmission belt 63 is transmitting the power, it drives the transmission plate 64 on the inner wall of the other end to rotate.
[0042] The end face of the support 7 away from the shell 8 is fixedly connected to the discharge port 6, the surface of the discharge port 6 is provided with the engine 4, the surface of the support 7 close to the shell 8 is provided with the motor 5, the surface of the support 7 close to the engine 4 is fixedly connected to the support rod 12, the number of the support rods 12 is four, and the four support rods 12 are symmetrically distributed on the surface of the support 7.
[0043] The stirring component 1 includes a cross bar 24, which will drive the auxiliary stirring fan 25 to operate. The end surface of the cross bar 24 is fixedly connected with the auxiliary stirring fan 25. The auxiliary stirring fan 25 will stir the material therein to promote its reaction. The end surface of the output shaft 21 away from the periodic tooth plate 22 is fixedly connected with a positioning shaft 26. At the same time, when the output shaft 21 rotates, it will drive the positioning shaft 26 to rotate on the inner wall of the sliding rod 31. When the positioning shaft 26 rotates, it will drive the top shaft 27 to rotate. The end surface of the positioning shaft 26 away from the end of the output shaft 21 is fixedly connected with the top shaft 27. When the top shaft 27 rotates, it will drive the main stirring fan 28 to rotate. The main stirring fan 28 will initially stir the material therein so that it has a good stirring effect. The surface of the top shaft 27 away from the end of the positioning shaft 26 is fixedly connected with the main stirring fan 28. There are two cross bars 24, and the two cross bars 24 are symmetrically distributed around the surface center of the rack 23.
[0044] The surface of the positioning shaft 26 is provided with a slide bar 31, and the end surface of the rack 23 close to the slide bar 31 is fixedly connected with a connecting slide plate 32. When the connecting slide plate 32 is running, it will drive the push plate 33 to run. The end surface of the connecting slide plate 32 away from the output shaft 21 is fixedly connected with the push plate 33. When the push plate 33 is running, it will collide with the vertical fan 35, thereby driving the vertical fan 35 to rotate. The vertical fan 35 uses the stirring force in another direction to make better use of the materials inside it. At the same time, when the vertical fan 35 rotates, it will drive the horizontal axis 34 along the inner side of the slide bar 31. The wall rotates, the inner wall of the sliding bar 31 near the sliding plate 32 is connected to the horizontal shaft 34, when the horizontal shaft 34 rotates, it will drive the auxiliary belt 29 to transmit, the surface of the horizontal shaft 34 is fixedly connected to the vertical fan 35, the surface of the horizontal shaft 34 away from one end of the sliding bar 31 is connected to the auxiliary belt 29, when the auxiliary belt 29 transmits, it will drive the horizontal shaft 34 of the inner wall at the other end to rotate, so that when the device is in periodic operation, the horizontal shaft 34 at the other end will not stop rotating, and the surface of the support 7 near the auxiliary belt 29 is fixedly connected to the auxiliary shell 30;
[0045] There are two connecting slides 32, which are symmetrically distributed on the surface of the rack 23. The end faces of the connecting slides 32 are slidingly connected to the surface of the slide rod 31. There are two vertical fans 35, which are symmetrically distributed on the surface of the transverse axis 34. The surface of the transverse axis 34 passes through the inner wall of the support 7 to the inner wall of the auxiliary shell 30. There are two auxiliary belts 29, which are symmetrically distributed on the surface of the support 7. The inner wall of the auxiliary shell 30 is fixedly connected to the surface of the support 7.
[0046] The cleaning component 2 includes an adsorption plate 44, and a half-leaf arc plate 45 is fixedly connected to the surface of the top shaft 27 away from one end of the adsorption plate 44. At the same time, when the top shaft 27 rotates, the half-leaf arc plate 45 will be driven to rotate. When the half-leaf arc plate 45 rotates, the force-bearing plate 46 will be pushed to slide along the inner wall of the force-bearing groove plate 54. The inner wall of the support 7 close to the half-leaf arc plate 45 is fixedly connected to the bottom arc plate 47. When the connecting shaft 52 runs, it will drive the scraper 49 to slide along the mutually approaching surface of the bottom arc plate 47 and the arc groove plate 48, and at the same time, it will run along the inner wall of the support 7, so that the scraper 49 will clean the inner wall of the support 7. The inner wall of the support 7 close to the bottom arc plate 47 is fixedly connected to the arc groove plate 48, and the surface of the arc groove plate 48 is slidably connected to the scraper 49;
[0047] The surface of the vertical sweeping plate 41 contacts the end surface of the filter plate 42. There are three arc fan plates 43, which are symmetrically distributed around the surface center of the output shaft 21. The surface of the arc fan plate 43 away from the filter plate 42 contacts the end surface of the adsorption plate 44.
[0048] A force-bearing plate 46 is provided on the surface of the semi-leaf arc plate 45. When the force-bearing plate 46 is in operation, it will drive the rotating shaft plate 50 to operate. At the same time, when the force-bearing plate 46 is in operation, it will push the return spring 53 to operate. When the semi-leaf arc plate 45 does not push the force-bearing plate 46 to operate, the force-bearing plate 46 will be reset by the reaction force of the return spring 53. The force-bearing plate 46 is fixedly connected with the rotating shaft plate 50. When the rotating shaft plate 50 is in operation, it will drive the connecting shaft rod 52 to rotate along the surface of the rotating shaft 51. The inner wall of the rotating shaft plate 50 is rotatably connected with the rotating shaft 51, and the surface of the rotating shaft 51 is rotatably connected with the connecting shaft rod 52. The end surface of the force-bearing plate 46 close to one end of the rotating shaft plate 50 is fixedly connected with the return spring 53, and the surface of the force-bearing plate 46 is slidably connected with the force-bearing groove plate 54.
[0049] There are four force-bearing plates 46, which are symmetrically distributed around the surface center of the half-leaf arc plate 45. There are two rotating shaft plates 50, which are symmetrically distributed around the surface of the force-bearing plate 46. There are two return springs 53, which are symmetrically distributed around the surface of the force-bearing plate 46. The end face of the force-bearing slot plate 54 away from the force-bearing plate 46 is fixedly connected to the inner wall of the support 7. The end face of the connecting shaft 52 away from the rotating shaft 51 is fixedly connected to the end face of the scraper 49 close to the arc slot plate 48. The surface of the force-bearing slot plate 54 contacts the surface of the half-leaf arc plate 45.
[0050] The pressurizing component 3 includes a transmission plate 64, which will drive the inclined push plate 67 to operate. The end face of the transmission plate 64 away from the motor positioning plate 61 is fixedly connected with the inclined push plate 67. When the inclined push plate 67 operates, it will drive the slider 68 to slide along the surface of the arc slide 70. The end face of the inclined push plate 67 away from the transmission plate 64 is fixedly connected with the slider 68. At the same time, when the slider 68 operates, it will drive the push block 69 to slide along the inner wall of the arc slide 70. The surface of the motor positioning plate 61 is fixedly connected to the surface of the support 7, and the inner wall of the transmission belt 63 is rotatably connected to the surface of the transmission plate 64. There are two inclined push plates 67, which are symmetrically distributed on the surface of the transmission plate 64. There are two sliders 68, which are symmetrically distributed on the end face of the inclined push plate 67.
[0051] The end surface of the slider 68 away from the inclined push plate 67 is provided with a push block 69, and the inner wall of the slider 68 is slidably connected to the arc slide plate 70. When the push block 69 runs to a certain position, it will collide and contact with the box plate 71, thereby driving the box plate 71 to slide along the inner wall of the box body 72, thereby squeezing the gas in the box body 72 and finally ejecting the gas through the outlet pipe 66, thereby enhancing the gas pressure in the device and making the materials in the device react more completely. At the same time, it will assist the main stirring fan 28, drive it to rotate better, and enhance the stirring effect. The end surface of the push block 69 away from the slider 68 is fixedly connected to the box plate 71, and the surface of the box plate 71 is slidably connected to the box body 72. The surface of the box body 72 close to the support 7 is fixedly connected to the outlet pipe 66, and the end surface of the arc slide plate 70 close to the auxiliary shell 30 is fixedly connected to the positioning block 65, and the inner wall of the box body 72 is fixedly connected to the surface of the support 7.
[0052] When in use, the required material is poured into the device through the top cover 10 and the feed port 11. At this time, the engine 4 in the stirring component 1 is started to drive the output shaft 21 to rotate. When the output shaft 21 rotates, it will drive the periodic tooth plate 22 to rotate. When the periodic tooth plate 22 rotates, it will drive the rack 23 to run periodically. The rack 23 will drive the connecting slide plate 32 to slide periodically along the surface of the slide rod 31. At the same time, when the rack 23 is running, it will drive the cross bar 24 to run, and the cross bar 24 will drive the auxiliary stirring fan 25 to run. The auxiliary stirring fan 25 will stir the material inside it and promote its reaction. At the same time, when the connecting slide plate 32 is running, it will drive the push plate 33 to run. When the push plate 33 is running, it will collide with the vertical fan 35, thereby driving the vertical fan 35 to rotate. 35 makes better use of the materials therein through the stirring force in the other direction. At the same time, when the vertical fan 35 rotates, it will drive the horizontal shaft 34 to rotate along the inner wall of the slide bar 31. When the horizontal shaft 34 rotates, it will drive the auxiliary belt 29 to transmit. When the auxiliary belt 29 transmits, it will drive the horizontal shaft 34 on the inner wall of the other end to rotate, so that when the device is in periodic operation, the horizontal shaft 34 at the other end will not stop rotating. At the same time, when the output shaft 21 rotates, it will drive the positioning shaft 26 to rotate on the inner wall of the slide bar 31. When the positioning shaft 26 rotates, it will drive the top shaft 27 to rotate. When the top shaft 27 rotates, it will drive the main stirring fan 28 to rotate. The main stirring fan 28 will perform initial stirring on the materials therein, so that it can perform a good stirring effect. At this time, in the cleaning component 2, when the output shaft 21 rotates, it will drive the vertical sweeping plate 41 to rotate, and the vertical sweeping plate 41 will clean the materials remaining on the surface of the filter plate 42 and the inner wall of the support 7 to prevent the accumulation of materials in the device and damage to the device. After that, the reacted materials will fall below through the filter plate 42. At the same time, when the output shaft 21 rotates, it will drive the arc fan plate 43 to rotate along the inner wall of the support 7, and at the same time, clean the surface of the adsorption plate 44. Finally, the reacted materials will fall to the bottom through the adsorption plate 44 and be transmitted through the discharge port 6. At the same time, when the top shaft 27 rotates, it will drive the half-leaf arc plate 45 to rotate. When the bearing plate 46 rotates, it pushes the force-bearing plate 46 to slide along the inner wall of the force-bearing groove plate 54. When the bearing plate 46 moves, it drives the rotating shaft plate 50 to move. When the rotating shaft plate 50 moves, it drives the connecting shaft rod 52 to rotate along the surface of the rotating shaft 51. When the connecting shaft rod 52 moves, it drives the scraper 49 to slide along the mutually approaching surface of the bottom arc plate 47 and the arc groove plate 48, and at the same time, it moves along the inner wall of the support 7, so that the scraper 49 cleans the inner wall of the support 7. At the same time, when the bearing plate 46 moves, it pushes the reset spring 53 to move. When the half-leaf arc plate 45 does not push the bearing plate 46 to move, the bearing plate 46 will be reset by the reaction force of the reset spring 53.At this time, in the pressurizing component 3, the motor 5 is started, driving the transmission shaft 62 to rotate, and the transmission shaft 62 will drive the transmission belt 63 to transmit. When the transmission belt 63 is transmitting, it will drive the transmission plate 64 on the inner wall of the other end to rotate, and the transmission plate 64 will drive the inclined push plate 67 to operate. When the inclined push plate 67 is operating, it will drive the slider 68 to slide along the surface of the arc slide plate 70. At the same time, when the slider 68 is operating, it will drive the push block 69 to slide along the inner wall of the arc slide plate 70. When the push block 69 runs to a certain position, it will collide and contact with the box plate 71, thereby driving the box plate 71 to slide along the inner wall of the box body 72, thereby squeezing the gas in the box body 72, and finally ejecting the gas through the outlet pipe 66, thereby increasing the air pressure in the device, making the material reaction in the device more complete, and at the same time, it will assist the main stirring fan 28, driving it to rotate better and enhance the stirring effect.
[0053] The preferred embodiments of the present invention disclosed above are only used to help illustrate the present invention. The preferred embodiments do not describe all the details in detail, nor do they limit the invention to the specific implementation methods described. Obviously, many modifications and changes can be made according to the content of this specification. This specification selects and specifically describes these embodiments in order to better explain the principles and practical applications of the present invention, so that those skilled in the art can understand and use the present invention well. The present invention is limited only by the claims and their full scope and equivalents.
Claims
1. A reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate, comprising a support (7), the end surface of the support (7) being fixedly connected to a shell (8), the end surface of the shell (8) away from the support (7) being fixedly connected to a sealing cover (9), the end surface of the support (7) close to the sealing cover (9) being fixedly connected to a top cover (10), the end surface of the top cover (10) being fixedly connected to a feed port (11), characterized in that: Also includes: A stirring component (1), the stirring component (1) comprising an output shaft (21), a surface of the output shaft (21) being fixedly connected with a periodic tooth plate (22), and a surface of the periodic tooth plate (22) being meshingly connected with a rack (23); A cleaning component (2), the cleaning component (2) comprising a vertical sweeping plate (41), a filter plate (42) being arranged on a surface of the output shaft (21) close to the vertical sweeping plate (41), and an arc fan plate (43) being fixedly connected to a surface of the output shaft (21) away from the filter plate (42); A pressurizing component (3), the pressurizing component (3) comprising a motor positioning plate (61), the end surface of the motor positioning plate (61) away from the motor (5) is provided with a transmission shaft (62), and the surface of the transmission shaft (62) is connected to a transmission belt (63).
2. A reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate according to claim 1, characterized in that: The end surface of the support (7) away from the shell (8) is fixedly connected to a discharge port (6), and the surface of the discharge port (6) is provided with an engine (4). The surface of the support (7) close to the shell (8) is provided with a motor (5), and the surface of the support (7) close to the engine (4) is fixedly connected to a support rod (12), and the number of the support rods (12) is four, and the four support rods (12) are symmetrically distributed on the surface of the support (7).
3. A reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate according to claim 2, characterized in that: The stirring component (1) comprises a cross bar (24), the end surface of the cross bar (24) is fixedly connected to an auxiliary stirring fan (25), the end surface of the output shaft (21) away from the periodic tooth plate (22) is fixedly connected to a positioning shaft (26), the end surface of the positioning shaft (26) away from the output shaft (21) is fixedly connected to a top shaft (27), and the surface of the top shaft (27) away from the positioning shaft (26) is fixedly connected to a main stirring fan (28), and the number of the cross bars (24) is set to two, and the two cross bars (24) are symmetrically distributed around the surface center of the rack (23).
4. A reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate according to claim 3, characterized in that: The surface of the positioning shaft (26) is provided with a sliding rod (31); the end surface of the rack (23) close to one end of the sliding rod (31) is fixedly connected to a connecting slide plate (32); the end surface of the connecting slide plate (32) away from the output shaft (21) is fixedly connected to a push plate (33); the inner wall of the sliding rod (31) close to the connecting slide plate (32) is rotatably connected to a transverse axis (34); the surface of the transverse axis (34) is fixedly connected to a vertical fan (35); the surface of the transverse axis (34) away from one end of the sliding rod (31) is transmission-connected to an auxiliary belt (29); the surface of the support (7) close to the auxiliary belt (29) is fixedly connected to an auxiliary shell (30); The number of the connecting slides (32) is two, and the two connecting slides (32) are symmetrically distributed on the surface of the rack (23). The end face of the connecting slide (32) is slidably connected to the surface of the slide rod (31). The number of the vertical fans (35) is two, and the two vertical fans (35) are symmetrically distributed on the surface of the transverse axis (34). The surface of the transverse axis (34) passes through the inner wall of the support (7) to the inner wall of the auxiliary shell (30). The number of the auxiliary belts (29) is two, and the two auxiliary belts (29) are symmetrically distributed on the surface of the support (7). The inner wall of the auxiliary shell (30) is fixedly connected to the surface of the support (7).
5. A reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate according to claim 4, characterized in that: The cleaning component (2) comprises an adsorption plate (44), a half-leaf arc plate (45) is fixedly connected to the surface of the top shaft (27) at one end away from the adsorption plate (44), a bottom arc plate (47) is fixedly connected to the inner wall of the support (7) on the side close to the half-leaf arc plate (45), an arc groove plate (48) is fixedly connected to the inner wall of the support (7) on the side close to the bottom arc plate (47), and a scraper (49) is slidably connected to the surface of the arc groove plate (48); The surface of the vertical sweeping plate (41) contacts the end surface of the filter plate (42), the number of the arc fan plates (43) is three, the three arc fan plates (43) are symmetrically distributed around the surface center of the output shaft (21), and the surface of the arc fan plate (43) at one end away from the filter plate (42) contacts the end surface of the adsorption plate (44).
6. A reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate according to claim 5, characterized in that: A force-bearing plate (46) is provided on the surface of the semi-leaf arc plate (45), the force-bearing plate (46) is fixedly connected to a rotating shaft plate (50), the inner wall of the rotating shaft plate (50) is rotatably connected to a rotating shaft (51), the surface of the rotating shaft (51) is rotatably connected to a connecting shaft rod (52), the end surface of the force-bearing plate (46) close to one end of the rotating shaft plate (50) is fixedly connected to a return spring (53), and the surface of the force-bearing plate (46) is slidably connected to a force-bearing groove plate (54); The number of the force-bearing plates (46) is four, and the four force-bearing plates (46) are symmetrically distributed around the surface center of the half-leaf arc plate (45). The number of the rotating shaft plates (50) is two, and the two rotating shaft plates (50) are symmetrically distributed around the surface of the force-bearing plate (46). The number of the reset springs (53) is two, and the two reset springs (53) are symmetrically distributed around the surface of the force-bearing plate (46). The end face of the force-bearing slot plate (54) away from the force-bearing plate (46) is fixedly connected to the inner wall of the support (7). The end face of the connecting shaft (52) away from the rotating shaft (51) is fixedly connected to the end face of the scraper (49) close to the arc slot plate (48). The surface of the force-bearing slot plate (54) contacts the surface of the half-leaf arc plate (45).
7. A reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate according to claim 6, characterized in that: The pressurizing component (3) includes a transmission plate (64), the end surface of the transmission plate (64) away from the motor positioning plate (61) is fixedly connected to an inclined push plate (67), the end surface of the inclined push plate (67) away from the transmission plate (64) is fixedly connected to a slider (68), the surface of the motor positioning plate (61) is fixedly connected to the surface of the support (7), the inner wall of the transmission belt (63) is rotatably connected to the surface of the transmission plate (64), the number of the inclined push plates (67) is two, and the two inclined push plates (67) are symmetrically distributed on the surface of the transmission plate (64), the number of the sliders (68) is two, and the two sliders (68) are symmetrically distributed on the end surface of the inclined push plate (67).
8. A reaction kettle for producing sodium perfluorononenyloxybenzenesulfonate according to claim 7, characterized in that: A push block (69) is provided on the end surface of the slider (68) away from the inclined push plate (67); an arc slide plate (70) is slidably connected to the inner wall of the slider (68); an end surface of the push block (69) away from the slider (68) is fixedly connected to a box plate (71); a surface of the box plate (71) is slidably connected to a box body (72); a surface of the box body (72) close to the support (7) is fixedly connected to an air outlet pipe (66); an end surface of the arc slide plate (70) close to the auxiliary shell (30) is fixedly connected to a positioning block (65); and an inner wall of the box body (72) is fixedly connected to the surface of the support (7).
Citation Information
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