Multilayer shear microfluidic reactor

Abstract

The invention relates to the technical field of reactors, in particular to a multi-layer shearing microfluid reactor which comprises a connecting shaft, a reaction assembly and a temperature measuring assembly, the reaction assembly is arranged on the connecting shaft and comprises a rotor reaction part and a stator reaction part, the rotor reaction part is connected with the connecting shaft, and a second heat exchange cavity is formed in the stator reaction part; a first circulation area is arranged between the stator reaction part and the surface of the connecting shaft, a first reaction tooth set is arranged on the rotor reaction part, a second reaction tooth set is arranged on the stator reaction part, the first reaction tooth set is located in the second reaction tooth set, a second circulation area is arranged in the first reaction tooth set, and a jacket is arranged outside the rotor reaction part. And a third circulation area is arranged between the jacket and the second reaction tooth group. The rotating first reaction tooth set shears materials, the material reaction efficiency is improved, the materials pass through the first circulation area, the second circulation area and the third circulation area of each reaction assembly, stirring circulation is achieved, the reaction effect can be controlled by controlling the group number of the reaction assemblies, different materials can be adapted, and the materials can be discharged after penetrating through the multiple reaction assemblies; the reaction efficiency is relatively high.

Description

Technical Field

[0001] The invention relates to the technical field of reactors, and in particular to a multilayer shear microfluidic reactor. Background Art

[0002] Traditional reactors generally introduce materials to be reacted into the reactor, and then stir the materials through the stirring paddles in the reactor to speed up the reaction efficiency.

[0003] However, this method has limited stirring effect of the stirring paddle, which may result in incomplete reaction; on the other hand, it is necessary to wait until all materials in the reactor have reacted completely before all materials can be discharged, which is inefficient. Summary of the invention

[0004] The technical problem to be solved by the present invention is: in order to solve the technical problems in the prior art, the present invention provides a multilayer shear microfluidic reactor.

[0005] The technical solution adopted by the present invention to solve its technical problems is: a multilayer shear microfluidic reactor, comprising a connecting shaft, a reaction assembly is arranged on the connecting shaft, the reaction assembly comprises a rotor reaction piece and a stator reaction piece, the rotor reaction piece is arranged in contact with the surface of the connecting shaft and is connected to the connecting shaft, a first flow area is arranged between the stator reaction piece and the surface of the connecting shaft, and the reaction assembly is provided with multiple groups along the axial direction of the connecting shaft; a first reaction tooth group is arranged on the rotor reaction piece, a second reaction tooth group is arranged on the stator reaction piece, the first reaction tooth group is located in the second reaction tooth group, a second flow area is arranged in the first reaction tooth group, a jacket is arranged outside the rotor reaction piece, and a third flow area is arranged between the jacket and the second reaction tooth group; when working, the material passes through the first flow area, the second flow area and the third flow area of ​​each group of reaction assemblies in turn.

[0006] The multilayer shear microfluidic reactor of the present invention has a connecting shaft connected to a rotor reaction piece, so that the connecting shaft drives the rotor reaction piece to rotate. When the material passes through the first reaction tooth group and the second reaction tooth group, it is sheared by the rotating first reaction tooth group, thereby improving the reaction efficiency of the material. The material passes through the first flow area, the second flow area and the third flow area of ​​each group of reaction components in sequence to achieve a stirring cycle, and then the reaction effect can be controlled by controlling the number of reaction components to adapt to different materials. At the same time, the material can complete the reaction and be discharged by passing through multiple groups of reaction components in sequence, and the reaction efficiency is relatively high.

[0007] Further, the first reaction tooth group includes a plurality of first crushing teeth, a plurality of the first crushing teeth are arranged along the circumference of the rotor reaction piece, and a first shunt gap is arranged between adjacent first crushing teeth; the second reaction tooth group includes a plurality of second crushing teeth, a plurality of the second crushing teeth are arranged along the circumference of the stator reaction piece, and a second shunt gap is arranged between adjacent second crushing teeth.

[0008] Furthermore, a plurality of reaction components are passed through and fixed by a group of fastening bolts.

[0009] Furthermore, a rotor support sleeve is provided between adjacent rotor reaction pieces, the rotor support sleeve is sleeved on the connecting shaft and fits with the surface of the connecting shaft, and the first flow area is located between the rotor support sleeve and the stator reaction piece.

[0010] Furthermore, the jacket is located between adjacent stator reaction pieces, a first heat exchange cavity is provided in the jacket, and a first heat exchange inlet and a first heat exchange outlet communicating with the first heat exchange cavity are provided on the jacket.

[0011] Furthermore, a second heat exchange cavity is provided in the stator reaction piece, and a second heat exchange inlet and a second heat exchange outlet communicating with the second heat exchange cavity are provided on the stator reaction piece.

[0012] Furthermore, a temperature measuring component is provided on the stator reaction piece, and the temperature measuring component is communicated with the inner hole of the stator reaction piece to monitor the temperature of the first flow area.

[0013] Furthermore, a feed flange is provided at one end of the plurality of reaction components, and a discharge heat exchange jacket is provided at the other end, and a feed port is provided on the feed flange, and the feed port is communicated with the first flow zone;

[0014] The discharge heat exchange jacket is provided with a discharge pipe, and the discharge pipe is communicated with the third flow zone.

[0015] Furthermore, the discharge heat exchange jacket is connected to a base flange, and a sealing assembly is installed on the base flange.

[0016] Furthermore, the stator reaction piece is provided with a jacket fixing groove for the jacket to be inserted into.

[0017] The beneficial effects of the present invention are:

[0018] 1. The connecting shaft is connected to the rotor reaction piece, so that the connecting shaft drives the rotor reaction piece to rotate. When the material passes through the first reaction tooth group and the second reaction tooth group, it is sheared by the rotating first reaction tooth group, thereby improving the reaction efficiency of the material. The material passes through the first flow area, the second flow area and the third flow area of ​​each group of reaction components in turn, thereby realizing a stirring cycle. The reaction effect can be controlled by controlling the number of reaction components to adapt to different materials. At the same time, the material can complete the reaction and be discharged by passing through multiple groups of reaction components in turn, thereby achieving a high reaction efficiency.

[0019] 2. When the material passes through the second reaction tooth group and the first reaction tooth group, it is first dispersed by the second diversion gap, then enters the first diversion gap under the impact of the first crushing tooth, and then passes through the first diversion gap to converge into the third flow area. In the continuous dispersion, impact, and mixing cycle process, the reaction effect is improved, and this method can make the material react as completely as possible;

[0020] 3. By setting up the first heat exchange chamber and the second heat exchange chamber, it is convenient to control the temperature during the material reaction process to further improve the reaction efficiency and ensure the reaction effect. BRIEF DESCRIPTION OF THE DRAWINGS

[0021] The present invention is further described below in conjunction with the accompanying drawings and embodiments.

[0022] Figure 1 It is a schematic diagram of the overall structure of the multilayer shear microfluidic reactor in the present invention.

[0023] Figure 2 It is a schematic diagram of a rotor reaction member in the present invention.

[0024] Figure 3 It is a schematic diagram of the stator reaction element in the present invention.

[0025] Figure 4 It is a schematic diagram of the combination of two groups of first reaction tooth groups in the present invention.

[0026] Figure 5 It is a schematic end view showing that the first reaction tooth group has two groups in the present invention.

[0027] Figure 6 It is a schematic diagram of the combination of two groups of second reaction tooth groups in the present invention.

[0028] Figure 7 It is a schematic end view showing that the second reaction tooth group has two groups in the present invention.

[0029] Figure 8 It is a schematic diagram of the second heat exchange chamber in the present invention.

[0030] Fig. 9 It is a schematic diagram of the connecting shaft in the present invention.

[0031] Fig.10 It is a schematic diagram of a rotor support sleeve in the present invention.

[0032] Fig.11 It is a schematic diagram of a jacket in the present invention.

[0033] Fig.12 It is a schematic diagram of the temperature measurement component in the present invention.

[0034] Fig.13 It is a schematic diagram of the base flange in the present invention.

[0035] Fig.14 It is a schematic diagram of the feed flange in the present invention.

[0036] In the figure: 1. connecting shaft; 2. rotor reaction piece; 21. first reaction tooth group; 211. first crushing tooth; 212. first diversion gap; 3. stator reaction piece; 31. first flow area; 32. second flow area; 33. third flow area; 34. second reaction tooth group; 341. second crushing tooth; 342. second diversion gap; 35. jacket fixing groove; 36. temperature measuring component; 37. second heat exchange cavity; 371. second heat exchange inlet; 372. second heat exchange outlet; 4. rotor support sleeve; 5. jacket; 51. first heat exchange cavity; 52. first heat exchange inlet; 53. first heat exchange outlet; 6. feed flange; 61. feed port; 7. discharge heat exchange jacket; 71. discharge port; 8. base flange; 81. sealing component; 9. fastening bolts. DETAILED DESCRIPTION

[0037] The present invention will now be described in further detail with reference to the accompanying drawings. These drawings are simplified schematic diagrams, which only illustrate the basic structure of the present invention in a schematic manner, and therefore only show the components related to the present invention.

[0038] In the description of the present invention, it should be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "up", "down", "front", "back", "left", "right", "vertical", "horizontal", "top", "bottom", "inside", "outside", "clockwise", "counterclockwise", "axial", "radial", "circumferential" and the like indicate positions or positional relationships based on the positions or positional relationships shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention. In addition, the features defined as "first" and "second" may explicitly or implicitly include one or more of the features. In the description of the present invention, unless otherwise specified, "multiple" means two or more. In the description of the present invention, it should be noted that, unless otherwise clearly specified and limited, the terms "installed", "connected" and "connected" should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection, or it can be indirectly connected through an intermediate medium, or it can be a connection between the two elements. For those skilled in the art, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.

[0039] The invention discloses a multilayer shear microfluid reactor.

[0040] Reference Figures 1 to 3 , Figures 8 to 14 , a multilayer shear microfluidic reactor, comprising a connecting shaft 1, on which a plurality of reaction components are arranged. The reaction components include a rotor reaction piece 2 and a stator reaction piece 3, the rotor reaction piece 2 is arranged in contact with the surface of the connecting shaft 1 and connected to the connecting shaft 1, and the rotor reaction piece 2 and the connecting shaft 1 can be connected by a key connection or a bolt connection, as long as the rotor reaction piece 2 can rotate with the connecting shaft 1. A rotor support sleeve 4 is arranged between adjacent rotor reaction pieces 2, and the rotor support sleeve 4 is convenient for controlling the distance between adjacent rotors. There are reaction holes on the stator reaction piece 3, the rotor support sleeve 4 is located in the reaction hole, and a first circulation area 31 is arranged between the inner wall of the reaction hole and the outer surface of the rotor support sleeve 4. A first reaction tooth group 21 is arranged on the rotor reaction piece 2, and a second reaction tooth group 34 is arranged on the stator reaction piece 3, the first reaction tooth group 21 is located in the second reaction tooth group 34, and a second circulation area 32 is arranged between the first reaction tooth group 21 and the rotor support sleeve 4, and a jacket 5 is arranged outside the rotor reaction piece 2, and a third circulation area 33 is arranged between the jacket 5 and the second reaction tooth group 34. During operation, the material passes through the first circulation area 31 , the second circulation area 32 and the third circulation area 33 of each reaction assembly in sequence. The material needs to pass through the first reaction tooth group 21 and the second reaction tooth group 34 to reach the third circulation area 33 from the second circulation area 32 .

[0041] The connecting shaft 1 is connected to the rotor reaction piece 2, so that the connecting shaft 1 can drive the rotor reaction piece 2 to rotate. When the material passes through the first reaction tooth group 21 and the second reaction tooth group 34, it is crushed and stirred by the rotating first reaction tooth group 21, thereby improving the reaction efficiency of the material. The material passes through the first flow area 31, the second flow area 32 and the third flow area 33 of each group of reaction components in turn to achieve a stirring cycle, and then the reaction effect can be controlled by controlling the number of reaction components to adapt to different materials. At the same time, the material can complete the reaction and be discharged by passing through multiple groups of reaction components in turn, and the reaction efficiency is relatively high.

[0042] Specifically, the first reaction tooth group 21 includes a plurality of first crushing teeth 211, and a plurality of the first crushing teeth 211 are arranged along the circumferential array of the rotor reaction piece 2, and a first shunt gap 212 is provided between adjacent first crushing teeth 211; the second reaction tooth group 34 includes a plurality of second crushing teeth 341, and a plurality of the second crushing teeth 341 are arranged along the circumferential array of the stator reaction piece 3, and a second shunt gap 342 is provided between adjacent second crushing teeth 341. When the material passes through the second reaction tooth group 34 and the first reaction tooth group 21, it is first dispersed by the second shunt gap 342, and then enters the first shunt gap 212 under the impact of the first crushing teeth 211, and then passes through the first shunt gap 212 and converges into the third flow area 33, and the reaction effect is improved in the continuous dispersion, impact, and mixing cycle process, and this method can make the material react as completely as possible.

[0043] In another embodiment, referring to Figure 4 and Figure 5 The first reaction tooth set 21 may be provided with two sets, the two sets of first reaction tooth sets 21 are arranged along the radial direction of the rotor reaction member 2 , and the second reaction tooth set 34 is located between the two sets of first reaction tooth sets 21 .

[0044] In another embodiment, referring to Figure 6 and Figure 7 The second reaction tooth set 34 may be provided with two sets, the two sets of second reaction tooth sets 34 are arranged along the radial direction of the stator reaction member 3 , and the first reaction tooth set 21 is located between the two sets of second reaction tooth sets 34 .

[0045] In other embodiments, more groups of the first reaction tooth groups 21 and the second reaction tooth groups 34 may be provided, and the more groups of the first reaction tooth groups 21 and the second reaction tooth groups 34 there are, the better the reaction effect of the material will be.

[0046] The jacket 5 is located between adjacent stator reaction pieces 3, and the stator reaction piece 3 is provided with a jacket 5 fixing groove 35 for inserting the jacket 5 so as to limit and seal the jacket 5. A first heat exchange cavity 51 is provided in the jacket 5, and a first heat exchange inlet 52 and a first heat exchange outlet 53 communicating with the first heat exchange cavity 51 are provided on the jacket 5. A second heat exchange cavity 37 is provided in the stator reaction piece 3, and a second heat exchange inlet 371 and a second heat exchange outlet 372 communicating with the second heat exchange cavity 37 are provided on the stator reaction piece 3. The first heat exchange cavity 51 and the second heat exchange cavity 37 facilitate the introduction of cooling medium so as to control the temperature of the material.

[0047] In addition, a temperature measuring component 36 is provided on one of the stator reaction parts 3, and the temperature measuring component 36 is connected to the inner hole of the stator reaction part 3, and is used to monitor the temperature of the first flow area 31. The stator reaction part 3 with the temperature measuring component 36 can be installed in the middle position of the entire reactor, or can be installed at the feed position and the discharge position of the reactor. The temperature measuring component 36 can be a temperature sensor.

[0048] One end of the multiple reaction components is provided with a feed flange 6, and the other end is provided with a discharge heat exchange jacket 7. The feed flange 6 is provided with a feed port 61, which is connected to the first flow area 31 of one group of reaction components; the discharge heat exchange jacket 7 is provided with a discharge pipe, which is connected to the third flow area 33 of one group of reaction components, so as to realize the entry and outflow of materials. The discharge heat exchange jacket 7 is also provided with a heat exchange cavity, a heat exchange inlet and a heat exchange outlet.

[0049] It should be noted that the connecting shaft 1 does not extend to the stator reaction member 3 close to the feed flange 6, that is, the first flow area 31 of the stator reaction member 3 is the entire inner hole thereof, so that the material can enter.

[0050] The discharge heat exchange jacket 7 is fixedly connected to a base flange 8, and a sealing assembly 81 is installed on the base flange 8 to facilitate sealing the end of the discharge heat exchange jacket 7 away from the reaction assembly. The feed flange 6, the discharge heat exchange jacket 7 and multiple groups of reaction assemblies are penetrated by a group of fastening bolts 9 and fixed by the fastening bolts 9 to realize the assembly of the reactor.

[0051] Working principle: The connecting shaft 1 is connected to the rotor reaction part 2, so that the connecting shaft 1 can drive the rotor reaction part 2 to rotate. When the material passes through the first reaction tooth group 21 and the second reaction tooth group 34, it is crushed and stirred by the rotating first reaction tooth group 21, thereby improving the reaction efficiency of the material. The material passes through the first circulation area 31, the second circulation area 32 and the third circulation area 33 of each group of reaction components in turn to achieve a stirring cycle, and then the reaction effect can be controlled by controlling the number of reaction components to adapt to different materials. At the same time, the material can complete the reaction and be discharged by passing through multiple groups of reaction components in turn, and the reaction efficiency is relatively high. The setting of the first heat exchange chamber 51 and the second heat exchange chamber 37 facilitates the control of the temperature during the material reaction process to further improve the reaction efficiency and ensure the reaction effect.

[0052] In addition, the overall volume of this solution is smaller, and the space occupied by the factory is smaller. At the same time, multiple connecting shafts 1 can be connected through a transmission mechanism to achieve synchronous transmission, thereby improving the reaction efficiency.

[0053] The materials in this solution react in a relatively small space, and the reaction is more complete, so the reaction effect far exceeds that of traditional reaction tanks.

[0054] The rotor support sleeve 4 controls the distance between adjacent rotors and also ensures that there is a gap between the end of the rotor reaction element 2 away from the first reaction tooth set 21 and the stator reaction element 3, so as to facilitate the flow of materials between adjacent reaction components.

[0055] Based on the above ideal embodiments of the present invention, the relevant staff can make various changes and modifications without departing from the technical concept of the present invention through the above description. The technical scope of the present invention is not limited to the contents of the specification, and its technical scope must be determined according to the scope of the claims.

Claims

1. A multilayer shear microfluidic reactor, characterized in that The invention comprises a connecting shaft (1), wherein a reaction assembly is provided on the connecting shaft (1), wherein the reaction assembly comprises a rotor reaction piece (2) and a stator reaction piece (3), wherein the rotor reaction piece (2) is arranged in contact with the surface of the connecting shaft (1) and is connected to the connecting shaft (1), and a first flow area (31) is provided between the stator reaction piece (3) and the surface of the connecting shaft (1), and the reaction assembly is provided in multiple groups along the axial direction of the connecting shaft (1); The rotor reaction piece (2) is provided with a first reaction tooth group (21), the stator reaction piece (3) is provided with a second reaction tooth group (34), the first reaction tooth group (21) is located inside the second reaction tooth group (34), a second flow area (32) is provided inside the first reaction tooth group (21), a jacket (5) is provided outside the rotor reaction piece (2), and a third flow area (33) is provided between the jacket (5) and the second reaction tooth group (34); During operation, the material passes through the first circulation area (31), the second circulation area (32) and the third circulation area (33) of each group of reaction components in sequence.

2. The multilayer shear microfluidic reactor according to claim 1, characterized in that The first reaction tooth group (21) includes a plurality of first crushing teeth (211), a plurality of the first crushing teeth (211) are provided along the circumference of the rotor reaction piece (2), and a first diversion gap (212) is provided between adjacent first crushing teeth (211); The second reaction tooth group (34) includes a plurality of second crushing teeth (341), a plurality of the second crushing teeth (341) are provided along the circumference of the stator reaction piece (3), and a second diversion gap (342) is provided between adjacent second crushing teeth (341).

3. The multilayer shear microfluidic reactor according to claim 1, characterized in that A plurality of reaction components are passed through a group of fastening bolts (9) and are fixed by the fastening bolts (9).

4. The multilayer shear microfluidic reactor according to claim 3, characterized in that A rotor support sleeve (4) is provided between adjacent rotor reaction pieces (2); the rotor support sleeve (4) is sleeved on the connecting shaft (1) and fits the surface of the connecting shaft (1); and the first flow area (31) is located between the rotor support sleeve (4) and the stator reaction piece (3).

5. The multilayer shear microfluidic reactor according to claim 1, wherein The jacket (5) is located between adjacent stator reaction elements (3), a first heat exchange cavity (51) is provided in the jacket (5), and a first heat exchange inlet (52) and a first heat exchange outlet (53) communicating with the first heat exchange cavity (51) are provided on the jacket (5).

6. The multilayer shear microfluidic reactor according to claim 5, wherein A second heat exchange cavity (37) is provided in the stator reaction piece (3), and a second heat exchange inlet (371) and a second heat exchange outlet (372) communicating with the second heat exchange cavity (37) are provided on the stator reaction piece (3).

7. The multilayer shear microfluidic reactor according to claim 1, wherein The stator reaction piece (3) is provided with a temperature measuring component (36), and the temperature measuring component (36) is communicated with the inner hole of the stator reaction piece (3) to monitor the temperature of the first flow area (31).

8. The multilayer shear microfluidic reactor according to claim 7, wherein One end of the plurality of reaction components is provided with a feed flange (6), and the other end is provided with a discharge heat exchange jacket (7), the feed flange (6) is provided with a feed port (61), and the feed port (61) is communicated with the first flow zone (31); The discharge heat exchange jacket (7) is provided with a discharge pipe, and the discharge pipe is communicated with the third circulation area (33).

9. The multilayer shear microfluidic reactor according to claim 8, wherein The discharge heat exchange jacket (7) is connected to a base flange (8), and a sealing assembly (81) is installed on the base flange (8).

10. The multi-layer shear microfluidic reactor according to claim 1, wherein The stator reaction piece (3) is provided with a jacket (5) fixing groove (35) for the jacket (5) to be inserted.

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