Pet tooth cleaning gel and preparation process thereof

Abstract

The invention discloses pet tooth cleaning gel and a preparation process thereof, and relates to the technical field of pet supplies, and the pet tooth cleaning gel comprises the following components in parts by weight: 0.05-2 parts of an antibacterial preservative, 0.05-2 parts of a chelating agent, 0.03-5 parts of a taste regulator, 0.1-5 parts of a breath freshening raw material, 0.1-2 parts of an inflammation repairing raw material, 0.001-2 parts of essence, 0.1-5 parts of a pH regulator, 0.1-5 parts of an excipient and 100 parts of water. The preparation method comprises the following steps: dissolving carbomer in 25% of water, preparing sodium hydroxide into a 1% aqueous solution, and adding a formula amount to form gel for later use to obtain a premix A; dissolving the antibacterial preservative, the chelating agent, the taste regulator, the breath freshening raw material, the inflammation repairing raw material, the essence and the premix A in the residual water, and uniformly stirring; the pH value is detected to be 4-5. Cymene-5-alcohol is compounded with dichlorobenzyl alcohol to serve as a bacteriostatic agent, pet friendliness is achieved, rejection is avoided, and the bacteriostatic effect is good; and the compounded plant deodorant is used, so that the deodorization effect is good, the maintenance time is long, the raw materials and the product can be degraded, and the environmental pressure cannot be caused.

Description

Technical Field

[0001] The invention relates to the technical field of pet products, and in particular to a pet tooth cleaning gel and a preparation process thereof. Background Art

[0002] Loving pet owners often do everything they can to keep their pets in the best condition, such as: feeding their pets the most nutritious food and snacks; ensuring that their pets exercise every day and take them to professional pet exercise institutions; and visiting the veterinary hospital for regular check-ups for preventive care. However, oral care for pets is often overlooked. Just like us humans, pets are also affected by the accumulation of plaque and bacteria in their mouths, which can cause bad breath, gum disease, and even tooth decay. Proper oral care will make your pet's teeth healthier, while incorrect care can cause your pet to suffer from dental disease. Dental disease is a painful disease that occurs when bacteria, plaque, and tartar accumulate on the teeth and become trapped under the gum line. This bacteria can be absorbed into the bloodstream and wreak havoc on other major organs of the body, so maintaining oral health is essential to keeping your pet healthy and happy.

[0003] Daily cleaning of your pet's mouth will promote good oral health and prevent expensive surgeries that may be needed in the future. Pets cannot use human oral products, which may contain ingredients like xylitol that are toxic to animals, so special pet oral care products are needed, such as: tooth cleaning finger gloves, tooth cleaning pens, tooth cleaning water, toothpaste, tooth cleaning gel, tooth cleaning powder, tooth cleaning snacks, etc. Pet tooth cleaning gel is an antibacterial oral gel specially formulated to keep your pet's teeth healthy. The active ingredients can stay in contact with the oral and tooth surfaces for a long time to prevent bacterial attacks, and also help control the formation of dental plaque and the growth of tooth decay. Common oral gels on the market use quaternary ammonium salt antibacterial agents such as chlorhexidine. Quaternary ammonium salt antibacterial agents may cause severe staining of teeth and soft tissues, excessive deposition of supragingival calculus, etc., have poor antibacterial effects on some microorganisms, have many incompatibility taboos, and the bactericidal effect is greatly affected by other organic substances. Summary of the invention

[0004] The purpose of the present invention is to provide a pet tooth cleaning gel and a preparation process thereof in view of the defects and shortcomings of the prior art. Cymene-5-ol and dichlorobenzyl alcohol are used as antibacterial agents, which are pet-friendly and non-repulsive and have good antibacterial effects. A compounded plant deodorant is used, which has good deodorizing effects and a long maintenance time. Both the raw materials and the products can be degraded without causing environmental pressure, and the problem of inconvenient pet tooth cleaning operations is solved. The gel has the effects of antibacterial deodorization, softening stones, and relieving inflammation, thereby reducing pet dental diseases.

[0005] To achieve the above purpose, the pet tooth cleaning gel of the present invention is composed of the following components by weight: 0.05-2 parts of antibacterial preservatives, 0.05-2 parts of chelating agents, 0.03-5 parts of taste regulators, 0.1-5 parts of breath freshening raw materials, 0.1-2 parts of inflammation repairing raw materials, 0.001-2 parts of flavors, 0.1-5 parts of pH regulators, 0.1-5 parts of excipients, and 100 parts of water; the antibacterial preservative is O-cymene-5-ol combined with dichlorobenzyl alcohol.

[0006] Furthermore, the antibacterial preservative can also be one or more of O-cymene-5-ol, dichlorobenzyl alcohol, propyl parahydroxybenzoate and its sodium salt, methyl parahydroxybenzoate and its sodium salt, plant-derived microbial inhibitors, lysozyme, polylysine hydrochloride, nisin, potassium sorbate, and sodium benzoate.

[0007] Furthermore, the chelating agent is selected from one or more of citric acid and its salts, disodium oxalate tetraacetate, tartaric acid and its salts, sodium pyrophosphate, hexametaphosphate, phytate, and glycine.

[0008] Furthermore, the taste regulator is selected from one or more of aspartame, cyclamate, acesulfame potassium, steviol glycosides, sucralose, erythritol, maltitol, glycerol, and sorbitol.

[0009] Furthermore, the breath freshening raw material is selected from one or more combinations of green tea extract, persimmon extract, tromethamine, and complex plant deodorants (plant-derived amino acid complex, hydroxymethyl chitosan, persimmon tannin, catechin, sedge extract, fresh bamboo juice, chlorophyll, citrus extract, and pine needle leaf extract).

[0010] Furthermore, the composite plant deodorant is prepared by the following method: in a vacuum emulsifier, alkyl glucoside APG0810, hydrogenated castor oil polyoxyethylene ether and butanediol are added to deionized water, heated to 55-75°C, lauryl methacrylate and plant extract are added while stirring, a transparent microemulsion is formed after half an hour, sodium methyl paraben and sodium propyl paraben are added, stirred to dissolve, cooled, filtered, and the finished composite plant deodorant is obtained.

[0011] Furthermore, the inflammation repair raw material is selected from one or more combinations of zinc gluconate, calcium pantothenate, honeysuckle extract, turmeric extract, dipotassium glycyrrhizinate, vitamin E, niacinamide, vitamin B6, and lysozyme.

[0012] Furthermore, the flavor is a toothpaste flavor such as fruity flavor and milky flavor, which has the effects of cooling, correcting taste, masking breath, and lasting fragrance, and is not repulsive to pets.

[0013] Furthermore, the pet tooth cleaning gel is composed of the following components in parts by weight: 1 part of O-cymene-5-ol, 0.1 part of sodium propyl parahydroxybenzoate, 0.1 part of sodium methyl parahydroxybenzoate, 0.5 part of sodium pyrophosphate, 0.03 part of sucralose, 3 parts of sorbitol, 2 parts of green tea extract, 0.5 part of tromethamine, 0.5 part of vitamin E, 0.2 part of zinc gluconate, 0.2 part of dipotassium glycyrrhizinate, 0.5 part of cantaloupe essence, 0.03 part of sodium hydroxide, 1 part of carbomer, and 100 parts of water.

[0014] Furthermore, the pet tooth cleaning gel is composed of the following components in parts by weight: 0.5 parts of O-cymene-5-ol, 0.8 parts of plant-derived microbial inhibitors (natural preservatives), 1 part of disodium oxalate tetraacetate, 0.5 parts of steviol glycosides, 1 part of erythritol, 0.5 parts of persimmon extract, 1 part of tromethamine, 0.5 parts of vitamin E, 0.1 parts of niacinamide, 0.09 parts of vitamin B6, 0.3 parts of green apple flavor, 0.02 parts of sodium hydroxide, 1 part of carbomer, and 100 parts of water.

[0015] Furthermore, the pet tooth cleaning gel is composed of the following components in parts by weight: 0.5 parts of O-cymene-5-ol, 0.1 parts of potassium sorbate, 0.1 parts of sodium benzoate, 0.26 parts of citric acid, 0.3 parts of sodium citrate, 0.1 parts of sucralose, 0.2 parts of aspartame, 2 parts of composite plant deodorant (plant-derived amino acid complex, hydroxymethyl chitosan, persimmon tannin, catechin, spatholobus extract, fresh bamboo juice, chlorophyll, citrus extract, pine needle leaf extract), 1 part of honeysuckle extract, 1 part of turmeric extract, 0.1 parts of peach essence, 0.02 parts of sodium hydroxide, 1 part of carbomer, and 100 parts of water.

[0016] The preparation process of the pet tooth cleaning gel of the present invention comprises the following steps: Step 1, dissolve carbomer in 25% water, prepare sodium hydroxide into a 1% aqueous solution, add the formula amount to form a gel for standby use to obtain premix A; Step 2, dissolve the remaining water-soluble antibacterial preservative, chelating agent, flavor regulator, breath freshening raw material, inflammation repair raw material, flavor, and premix A, and stir evenly; Step 3: Check pH 4-5, if it is qualified.

[0017] Compared with the prior art, the beneficial effects of the present invention are as follows: the present invention provides a pet tooth cleaning gel and a preparation process thereof, uses cymene-5-ol combined with dichlorobenzyl alcohol as an antibacterial agent, is pet-friendly and non-repulsive, and has a good antibacterial effect; uses a compounded plant deodorant, has a good deodorizing effect and a long maintenance time, is degradable from raw materials to products, does not cause environmental pressure, solves the problem of inconvenient pet tooth cleaning operation, has the effects of antibacterial and deodorizing, softening stones, and relieving inflammation, thereby reducing pet dental diseases. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] Figure 1 This is a data table of hydrogen sulfide removal rate testing of pet tooth cleaning gels prepared in Examples 1-4.

[0019] Figure 2 This is a data table of antibacterial effect testing of the pet tooth cleaning gel prepared in Examples 1-4.

[0020] Figure 3 This is a microbiological test and sensory evaluation data table for test sample 1, test sample 1-1, test sample 1-2, and test sample 1-3.

[0021] Figure 4 This is a table showing the usage and sensory evaluation data of Test Sample 1, Test Sample 1-1, Test Sample 1-2, and Test Sample 1-3. DETAILED DESCRIPTION

[0022] The technical solution of the present invention will be clearly and completely described below in conjunction with the accompanying drawings. The preferred embodiments in the description are only used as examples, and all other embodiments obtained by those skilled in the art without making any creative work are within the scope of protection of the present invention.

[0023] Embodiment 1:

[0024] The ingredients of the pet tooth cleaning gel in this embodiment are as follows: 0.5 parts of O-cymene-5-ol, 0.1 parts of sodium propyl parahydroxybenzoate, 0.1 parts of sodium methyl parahydroxybenzoate, 0.5 parts of sodium pyrophosphate, 0.03 parts of sucralose, 3 parts of sorbitol, 2 parts of green tea extract, 0.5 parts of tromethamine, 0.5 parts of vitamin E, 0.2 parts of zinc gluconate, 0.2 parts of dipotassium glycyrrhizinate, 0.5 parts of cantaloupe flavor, 0.03 parts of sodium hydroxide, 1 part of carbomer, and 100 parts of water.

[0025] The preparation process is as follows: 1) Dissolve carbomer in 25% water, prepare sodium hydroxide into a 1% aqueous solution, add the formula amount to form a gel for use to obtain premix A; 2) O-cymene-5-ol, sodium propyl paraben, sodium methyl paraben, sodium pyrophosphate, sucralose, sorbitol, green tea extract, tromethamine, vitamin E, zinc gluconate, dipotassium glycyrrhizate, cantaloupe flavor, premix A, stir evenly. 3) Detect pH 4-5, and pass.

[0026] Embodiment 2:

[0027] The ingredients of the pet tooth cleaning gel in this embodiment are as follows: 0.5 parts of O-cymene-5-ol, 0.8 parts of plant-derived microbial inhibitors (natural preservatives), 1 part of disodium oxalate tetraacetate, 0.5 parts of steviol glycosides, 1 part of erythritol, 0.5 parts of persimmon extract, 1 part of tromethamine, 0.5 parts of vitamin E, 0.1 parts of niacinamide, 0.09 parts of vitamin B6, 0.3 parts of green apple flavor, 0.02 parts of sodium hydroxide, 1 part of carbomer, and 100 parts of water.

[0028] The preparation process is the same as that of Example 1.

[0029] Embodiment 3:

[0030] The ingredients of the pet tooth cleaning gel in this embodiment are as follows: 0.5 parts of O-cymene-5-ol, 0.1 parts of potassium sorbate, 0.1 parts of sodium benzoate, 0.26 parts of citric acid, 0.3 parts of sodium citrate, 0.1 parts of sucralose, 0.2 parts of aspartame, 1 part of composite plant deodorant (plant-derived amino acid complex, hydroxymethyl chitosan, persimmon tannin, catechin, deer hoof grass extract, fresh bamboo juice, green leaf alcohol, citrus extract, pine needle leaf extract), 1 part of honeysuckle extract, 1 part of turmeric extract, 0.1 parts of peach essence, 0.02 parts of sodium hydroxide, 1 part of carbomer, and 100 parts of water.

[0031] The preparation process is as follows: 1) In a vacuum emulsifier, add alkyl glucoside APG0810, hydrogenated castor oil polyoxyethylene ether and butanediol to deionized water, heat to 55-75°C, add lauryl methacrylate and plant extract while stirring, and form a transparent microemulsion after half an hour, then add sodium methylparaben and sodium propylparaben, stir to dissolve, cool, and filter to obtain the finished composite plant deodorant. 2) Take 25% water to dissolve carbomer, prepare sodium hydroxide into a 1% aqueous solution, add the formula amount to form a gel for standby use to obtain premix A; 3) O-cymene-5-ol, potassium sorbate, sodium benzoate, citric acid, sodium citrate, sucralose, aspartame, composite plant deodorant, honeysuckle extract, turmeric extract, peach essence, premix A, stir evenly. 4) Detect pH 4-5, and it is qualified.

[0032] Embodiment 4:

[0033] The ingredients of the pet tooth cleaning gel in this embodiment are as follows: 0.5 parts of O-cymene-5-ol, 0.1 parts of dichlorobenzyl alcohol, 0.3 parts of disodium ethylenediaminetetraacetic acid, 0.1 parts of sucralose, 0.2 parts of aspartame, 3 parts of composite plant deodorant (plant-derived amino acid complex, hydroxymethyl chitosan, persimmon tannin, catechin, spatholobus extract, fresh bamboo juice, leaf alcohol, citrus extract, pine needle leaf extract), 1 part of honeysuckle extract, 1 part of turmeric extract, 0.1 parts of peach essence, 0.02 parts of sodium hydroxide, 1 part of carbomer, and 100 parts of water.

[0034] The preparation process is the same as that of Example 3.

[0035] Performance Testing: 1. The pet tooth cleaning gel prepared in Examples 1-4 was tested for hydrogen sulfide removal rate (hydrogen sulfide removal rate is in accordance with GB / T 11742-89, QB / T 2761-2006). The results are as follows: Figure 1 As shown, it can be seen that the hydrogen sulfide removal rates in Example 2 and Example 4 are higher.

[0036] 2. The antibacterial effect of the pet tooth cleaning gel prepared in Examples 1-4 was tested. The results are as follows: Figure 2 As shown, it can be seen that the antibacterial effect in Example 4 is better.

[0037] 3. The pet tooth cleaning gel in Example 4 is used as the test sample 1; The flavor content in the formula of Example 4 was reduced to 0.05 parts, and purified water was used to reduce the content by 0.05 parts to prepare test sample 1-1; The flavor content of Example 4 was increased to 0.2 parts, and purified water was used to make up 0.1 parts to prepare test sample 1-2; The flavor content of Example 4 was increased to 0.4 parts, and purified water was used to make up to 0.3 parts to prepare test samples 1-3.

[0038] 3.1. The above-mentioned test samples 1, 1-1, 1-2 and 1-3 were filled and sealed in 120 ml pointed-mouth plastic bottles, and placed in an accelerated box at 40°C and 75% humidity for 1 month. After that, they were taken out for microbial testing and sensory evaluation. The results were as follows: Figure 3 As shown, result analysis: there is no obvious abnormality in the stability of the test samples.

[0039] 3.2. Squeeze the above test samples 1, 1-1, 1-2 and 1-3 into a size of soybean and apply them on the back teeth of cats for use and sensory evaluation. The results are as follows: Figure 4 As shown, the result analysis: as the flavor content of the test samples increases, too much flavor added to samples 1-2 and 1-3 will cause cats to accept the product. Test sample 1 is not as effective as test sample 1-1 after use by cats, so test sample 1-1 is preferred.

[0040] Compared with the prior art, the beneficial effects of the present invention are as follows: the present invention provides a pet tooth cleaning gel and a preparation process thereof, uses cymene-5-ol combined with dichlorobenzyl alcohol as an antibacterial agent, is pet-friendly and non-repulsive, and has a good antibacterial effect; uses a compounded plant deodorant, has a good deodorizing effect and a long maintenance time, is degradable from raw materials to products, does not cause environmental pressure, solves the problem of inconvenient pet tooth cleaning operation, has the effects of antibacterial and deodorizing, softening stones, and relieving inflammation, thereby reducing pet dental diseases.

[0041] For those skilled in the art, they can modify the technical solutions described in the aforementioned embodiments and make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. A pet tooth cleaning gel, characterized in that: The invention is composed of the following components in parts by weight: 0.05-2 parts of antibacterial preservative, 0.05-2 parts of chelating agent, 0.03-5 parts of flavor regulator, 0.1-5 parts of breath freshening raw material, 0.1-2 parts of inflammation repairing raw material, 0.001-2 parts of flavor, 0.1-5 parts of pH regulator, 0.1-5 parts of excipient and 100 parts of water; the antibacterial preservative is O-cymene-5-ol compounded with dichlorobenzyl alcohol.

2. A pet tooth cleaning gel according to claim 1, characterized in that: The antibacterial preservative can also be one or more of O-cymene-5-ol, dichlorobenzyl alcohol, propyl parahydroxybenzoate and its sodium salt, methyl parahydroxybenzoate and its sodium salt, plant-derived microbial inhibitors, lysozyme, polylysine hydrochloride, nisin, potassium sorbate, and sodium benzoate.

3. A pet tooth cleaning gel according to claim 2, characterized in that: The chelating agent is selected from one or more of citric acid and its salts, disodium oxalate tetraacetate, tartaric acid and its salts, sodium pyrophosphate, hexametaphosphate, phytate, and glycine.

4. A pet tooth cleaning gel according to claim 3, characterized in that: The taste regulator is selected from one or more of aspartame, cyclamate, acesulfame potassium, steviol glycosides, sucralose, erythritol, maltitol, glycerol, and sorbitol.

5. The pet tooth cleaning gel according to claim 4, characterized in that: The breath freshening raw material is selected from one or more combinations of green tea extract, persimmon extract, tromethamine, and composite plant deodorant.

6. The pet tooth cleaning gel according to claim 5, characterized in that: The composite plant deodorant is prepared by the following method: in a vacuum emulsifier, alkyl glucoside APG0810, hydrogenated castor oil polyoxyethylene ether and butanediol are added into deionized water, heated to 55-75° C., lauryl methacrylate and plant extract are added while stirring, a transparent microemulsion is formed after half an hour, sodium methylparaben and sodium propylparaben are added, stirred to dissolve, cooled, filtered, and the finished composite plant deodorant is obtained.

7. A pet tooth cleaning gel according to claim 6, characterized in that: The inflammation repair raw materials are selected from one or more combinations of zinc gluconate, calcium pantothenate, honeysuckle extract, turmeric extract, dipotassium glycyrrhizinate, vitamin E, niacinamide, vitamin B6, and lysozyme.

8. The pet tooth cleaning gel according to claim 7, characterized in that: The flavor is a toothpaste flavor such as fruity and milky, which has the effects of cooling, correcting the taste, masking breath, and leaving a lasting fragrance, and is not repelled by pets.

9. A preparation process of a pet tooth cleaning gel, comprising the following steps: Step (1), dissolving carbomer in 25% water, preparing a 1% aqueous solution of sodium hydroxide, and adding a formula amount to form a gel for standby use to obtain premix A; Step (2), the remaining water-soluble antibacterial preservative, chelating agent, flavor regulator, breath freshening raw material, inflammation repair raw material, flavor, premix A, and stir evenly; Step (3), test pH 4-5, if it is qualified.

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