Hair heat protection pomade and preparation process thereof

Abstract

The invention discloses a hair heat protection pomade and a preparation process thereof, and belongs to the technical field of daily chemical products. According to the invention, caprylic acid / capric triglyceride, polydimethylsiloxane, trimethylsiloxy silicate and divinyl polydimethylsiloxane / polydimethylsiloxane cross-linked polymer are compounded to prepare the pomade, and the pomade has the advantage of high temperature insulation, and when hot tools such as a curling iron, a straight iron and the like are used for styling hair, the pomade has the advantages of high temperature resistance and high temperature resistance. High temperature of a heat tool can be effectively isolated from multiple aspects, heat damage of the high temperature to hair is greatly reduced, and health and luster of the hair are kept.

Description

Technical Field

[0001] The invention relates to the technical field of daily chemical products, in particular to a hair heat protection wax and a preparation process thereof. Background Art

[0002] In the related art, repeated use of hair wax may lead to problems such as clogged pores, dandruff, and hair damage. Moreover, it is difficult to reduce thermal damage to the hair while providing lasting styling effects, moisturizing hair, protecting hair scales, repairing damaged hair, increasing hair gloss, and resisting frizz. Summary of the invention

[0003] The main purpose of the invention is to provide a hair heat protection wax and a preparation process thereof, so as to solve the technical problem that the hair wax is difficult to reduce the heat damage to the hair.

[0004] To achieve the above object, the present invention provides a hair heat protection wax, comprising the following raw materials:

[0005] Caprylic / capric triglyceride, dimethicone, trimethylsiloxysilicate and divinyl dimethicone / dimethicone crosspolymer.

[0006] In some embodiments of the present invention, the hair heat protection wax further comprises at least one of a solvent, an emulsifier, an emulsion stabilizer, a hair conditioner, a preservative, a moisturizing emollient and a fragrance.

[0007] In some embodiments of the present invention, the hair heat protection wax includes a solvent, and the solvent includes at least one of water and propylene glycol;

[0008] And / or, the hair heat protection wax comprises an emulsifier, and the emulsifier comprises at least one of ceteareth-30, oleth-5, laureth-7, and trideceth-10;

[0009] And / or, the hair heat protection wax comprises an emulsion stabilizer, and the emulsion stabilizer comprises ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer.

[0010] In some embodiments of the present invention, the hair heat protection wax comprises a hair conditioning agent, and the hair conditioning agent comprises at least one of amodimethicone, hydrolyzed keratin, jojoba seed oil, and argania spinosa kernel oil.

[0011] In some embodiments of the present invention, the hair heat protection wax includes a preservative, and the preservative includes at least one of methylparaben, propylparaben, and phenoxyethanol;

[0012] And / or, the hair heat protection wax comprises a moisturizing emollient, wherein the moisturizing emollient comprises C 13-14 At least one of isoparaffins.

[0013] And / or, the heat protecting hair wax comprises a fragrance, and the fragrance comprises a perfume.

[0014] In some embodiments of the present invention, the hair heat protection wax comprises the following raw materials:

[0015] Caprylic / capric triglyceride, dimethicone, divinyl dimethicone / dimethicone crosspolymer, trimethylsiloxysilicate, propylene glycol, water, amodimethicone, oleth-5, laureth-7, trideceth-10, ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer, hydrolyzed keratin, jojoba seed oil, argania spinosa kernel oil, methylparaben, propylparaben, phenoxyethanol, ceteareth-30, C 13-14 Isoparaffin, flavor.

[0016] In some embodiments of the present invention, the hair heat protection wax comprises the following raw materials calculated by weight percentage:

[0017] Caprylic / capric triglyceride: 20%-40%,

[0018] Polydimethylsiloxane: 10%-30%,

[0019] Divinyl dimethicone / dimethicone crosspolymer: 5%-15%,

[0020] Trimethylsiloxysilicate: 5%-15%,

[0021] Propylene glycol: 5%-30%,

[0022] Water: 20%-50%,

[0023] Ceteareth-30: 2%-5%,

[0024] Oleth-5: 1%-5%,

[0025] Laureth-7: 0.5%-2%,

[0026] Trideceth-10: 0.1%-1%,

[0027] Ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer: 0.3%-2%,

[0028] Amodimethicone: 1%-5%,

[0029] Hydrolyzed keratin: 0.1%-1%,

[0030] Jojoba seed oil: 0.1%-2%,

[0031] Argania spinosa kernel oil: 0.05%-2%,

[0032] Methylparaben: 0.1%-0.25%,

[0033] Propylparaben: 0.05%-0.15%,

[0034] Phenoxyethanol: 0.3%-0.8%,

[0035] C 13-14 Isoparaffin: 0.5%-2%,

[0036] Fragrance: 0.1%-1%.

[0037] In some embodiments of the present invention, the hair heat protection wax comprises the following raw materials calculated by weight percentage:

[0038] Caprylic / capric triglyceride: 30%,

[0039] Polydimethylsiloxane: 20%,

[0040] Divinyl dimethicone / dimethicone crosspolymer: 5%,

[0041] Trimethylsiloxysilicate: 5%,

[0042] Propylene glycol: 10%,

[0043] Water: 20.59%,

[0044] Ceteareth-30: 2%,

[0045] Oleth-5: 1.5%,

[0046] Laureth-7: 0.68%,

[0047] Trideceth-10: 0.15%,

[0048] Ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer: 0.7%, amodimethicone: 1.925%,

[0049] Hydrolyzed keratin: 0.15%,

[0050] Jojoba seed oil: 0.1%,

[0051] Argania spinosa kernel oil: 0.05%,

[0052] Methylparaben: 0.2%,

[0053] Propylparaben: 0.1%,

[0054] Phenoxyethanol: 0.6%,

[0055] C 13-14 Isoparaffin: 0.85%,

[0056] Fragrance: 0.4%.

[0057] The present invention also provides a method for preparing the above-mentioned hair heat protection wax, comprising the following steps:

[0058] The raw materials are divided into water-soluble components and oil-soluble components according to their water solubility and oil solubility;

[0059] The water-soluble components are dissolved and mixed to obtain a water phase, and the oil-soluble components are dissolved and mixed to obtain an oil phase;

[0060] The water phase and the oil phase are mixed, homogenized and emulsified to obtain the hair heat protection wax.

[0061] In some embodiments of the present invention, the homogenization emulsification temperature of the water phase and the oil phase is 80°C to 85°C; and / or the discharge temperature of the hair heat protection wax is 40°C to 45°C.

[0062] The beneficial effects that can be achieved by the present invention are:

[0063] The invention prepares a hair wax by compounding caprylic acid / capric acid triglyceride, polydimethylsiloxane, trimethylsiloxysilicate and divinyl polydimethylsiloxane / polydimethylsiloxane crosslinked polymer. The hair wax has the advantage of isolating high temperature. When using hot tools such as curling irons and straightening irons to style hair, the high temperature of the hot tools can be effectively isolated from multiple aspects, greatly reducing the heat damage to the hair caused by the high temperature, and maintaining the health and luster of the hair. BRIEF DESCRIPTION OF THE DRAWINGS

[0064] In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the following briefly introduces the drawings required for use in the embodiments or the description of the prior art. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on the structures shown in these drawings without paying creative work.

[0065] Figure 1 This is a SEM picture of hair before and after using the hair wax of the present invention in accordance with an embodiment of the present invention.

[0066] Figure 2This is a comparison chart of the amount of lipid peroxides on hair before and after using the hair wax of the present invention in one embodiment of the present invention.

[0067] Figure 3 The average value of the work-to-break value of the hair before and after using the hair wax of the present invention in one embodiment of the present invention;

[0068] Figure 4 This is a diagram showing the difference in moisture content of hair before and after using the hair wax according to an embodiment of the present invention after the hair straightener of the present invention is damaged.

[0069] The realization of the purpose, functional features and advantages of the present invention will be further explained in conjunction with embodiments and with reference to the accompanying drawings. DETAILED DESCRIPTION

[0070] It should be understood that the specific embodiments described herein are only used to explain the present invention, and are not used to limit the present invention.

[0071] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0072] In the present invention, descriptions such as "first", "second", etc. are only used for descriptive purposes and cannot be understood as indicating or implying their relative importance or implicitly indicating the number of the indicated technical features. Therefore, the features defined as "first" and "second" may explicitly or implicitly include at least one of the features. In addition, the technical solutions between the various embodiments can be combined with each other, but they must be based on the ability of ordinary technicians in the field to implement them. When the combination of technical solutions is contradictory or cannot be implemented, it should be deemed that such a combination of technical solutions does not exist and is not within the scope of protection required by the present invention.

[0073] The present invention provides a hair heat protection wax, which comprises the following raw materials:

[0074] Caprylic / capric triglyceride, dimethicone, trimethylsiloxysilicate and divinyl dimethicone / dimethicone crosspolymer.

[0075] The INCI name of caprylic / capric triglyceride is CAPRYLIC / CAPRIC TRIGLYCERIDE, and the CAS number is 65381-09-1. It forms a protective film on the surface of the hair to help prevent the invasion of harmful external factors, including dryness and damage that may be caused by high temperature environments. In addition, caprylic / capric triglyceride can also improve the hair's own defense ability by promoting the renewal of epidermal cells and increasing the thickness of the stratum corneum, making it more resistant to heat stress. Furthermore, caprylic / capric triglyceride also has moisturizing and nourishing effects, because the fatty acids in caprylic / capric triglyceride can combine with the water in the stratum corneum, which can effectively increase the water content of the stratum corneum, thereby keeping the hair hydrated. This moisturizing effect helps to alleviate the dryness and dehydration of the skin caused by high temperature, allowing the hair to resist high-temperature dyeing and perming, and be healthier and more elastic.

[0076] The INCI name of polydimethylsiloxane is DIMETHICONE and its CAS number is 9006-65-9. As a special silicone polymer, its high temperature resistance is generally around 300°C. Polydimethylsiloxane can form a protective film on the surface of the hair, thereby reducing the damage to the hair caused by high temperature environment. At the same time, its good lubricity and moisturizing properties also help improve the hair texture.

[0077] The INCI name of divinyl dimethicone / dimethicone crosspolymer is DIVINYLDIMETHICONE / DIMETHICONE CROSSPOLYMER. It indirectly helps the hair stay healthy when facing external thermal stress by forming a protective film, lubricating and softening the hair, controlling moisture loss, repairing damaged hair, and reducing static electricity and flyaways.

[0078] The INCI name of trimethylsiloxysilicate is TRIMETHYLSILOXYSILICATE, and the CAS number is 104133-09-7. It mainly works by forming a protective film on the surface of hair, lubricating and softening, and assisting in repair and nourishment. Trimethylsiloxysilicate can effectively reduce the damage to hair caused by external factors such as high temperature, while improving hair quality and enhancing the protective properties of hair.

[0079] The invention prepares a hair wax by compounding caprylic acid / capric acid triglyceride, polydimethylsiloxane, trimethylsiloxysilicate and divinyl polydimethylsiloxane / polydimethylsiloxane crosslinked polymer. The hair wax has the advantage of isolating high temperature. When using hot tools such as curling irons and straightening irons to style hair, the high temperature of the hot tools can be effectively isolated from multiple aspects, greatly reducing the heat damage to the hair caused by the high temperature, and maintaining the health and luster of the hair.

[0080] In some embodiments, the hair heat protection wax further comprises at least one of a solvent, an emulsifier, an emulsion stabilizer, a hair conditioner, a preservative, a moisturizer, an emollient, and a fragrance.

[0081] The solvent plays a role in dissolving and dispersing various raw materials. In some embodiments, the hair heat protection wax includes a solvent, and the solvent includes at least one of water and propylene glycol.

[0082] The INCI name of water is WATER and its CAS number is 7732-18-5. It is a commonly used and better solvent.

[0083] The INCI name of propylene glycol is PROPYLENE GLYCOL, and its CAS number is 57-55-6. It can be used as a solvent in hair wax to help other ingredients dissolve and mix, making the texture of the hair wax more uniform. In addition, propylene glycol can also be used as a viscosity regulator to help adjust the viscosity and fluidity of the hair wax, making the hair wax easy to apply and easy to help shape the hair. Furthermore, propylene glycol also has good moisturizing properties. It can absorb moisture from the air, help maintain moisture in the hair wax, maintain long-lasting moisturizing effects for the hair, reduce frizziness of the hair, and increase the moisture in the hair film formed on the surface of the hair, which is equivalent to forming a layer of water film on the surface of the hair. It can not only improve the hair quality, but also improve the hair's resistance to high temperatures, further reduce the heat damage to the hair caused by the high temperature of hot tools, and maintain the health and luster of the hair. In addition,

[0084] Emulsifiers help mix oil and water in hair wax, stabilize the formula, and provide good styling effects.

[0085] In some embodiments, the emulsifier includes at least one of ceteareth-30, oleth-5, laureth-7, and trideceth-10.

[0086] The INCI name of Ceteareth-30 is CETEARETH-30, and the CAS number is 68439-49-6. It has good moisturizing properties, helps hair retain moisture, reduces dryness and frizz, provides a soft and smooth touch, and increases the moisture in the hair film formed on the hair surface, which not only improves hair quality, but also improves the hair's resistance to high temperatures, further reduces the heat damage to hair caused by high temperatures of hot tools, and maintains the health and luster of hair. In addition, Ceteareth-30 also has antistatic properties, which helps reduce the flying of hair caused by static electricity, making hair smoother and easier to comb.

[0087] The INCI name of Oleth-5 is OLETH-5 and the CAS number is 5353-27-5. It helps mix the oil phase and the water phase in the hair wax to form a uniform emulsion or paste, thereby improving the stability of the hair wax.

[0088] The INCI name of Laureth-7 is LAURETH-7 and its CAS number is 3055-97-8. It can also help mix oil and water in hair wax, stabilize the formula, and provide good styling effects.

[0089] The INCI name of trideceth-10 is TRIDECETH-10 and its CAS number is 24938-91-8. It can also help mix oil and water in hair wax, stabilize the formula and provide good styling effects.

[0090] Emulsifier stabilizers can promote uniform dispersion of oil and water, enhance the shaping power of hair wax, and improve user experience.

[0091] In some embodiments, the emulsion stabilizer includes ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer.

[0092] The INCI name of ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer is AMMONIUMACRYLOYLDIMETHYLTAURATE / BEHENETH-25METHACRYLATE CROSSPOLYMER, and the CAS number is 1219698-43-7. It can effectively thicken the viscosity of the water-oil system, help improve the styling power and feel of the hair wax, and ensure the stability of the product.

[0093] Hair conditioners can specifically improve some of the properties of hair wax.

[0094] In some embodiments, the hair conditioning agent includes at least one of amodimethicone, hydrolyzed keratin, jojoba seed oil, and argania spinosa kernel oil.

[0095] The INCI name of aminodimethicone is AMODIMETHICONE, and the CAS number is 71750-80-6. It helps mix oil and water in hair wax, stabilizes the formula, and provides good styling effects. Moreover, aminodimethicone has good stability and can maintain its performance even under high temperature conditions. It is not easy to degrade or deteriorate, and is suitable for hair products treated at high temperatures. In addition, aminodimethicone has excellent film-forming properties and can form a protective film on the surface of hair, providing thermal protection for the hair and reducing hair breakage. Furthermore, aminodimethicone also has antistatic and defoaming effects. The antistatic property reduces the frizziness of hair caused by static electricity, making the hair easier to comb and style, and the defoaming effect can optimize the production process.

[0096] The INCI name of hydrolyzed keratin is HYDROLYZED KERATIN, and the CAS number is 69430-36-0. It is positively charged, while the surface of hair is negatively charged. The positive and negative charges attract each other, so that the hydrolyzed protein adheres to the surface of the hair, thereby achieving the purpose of repairing the surface of the hair and making the hair smooth and easy to comb. In addition, hydrolyzed protein can also enhance the strength of the hair and fill the tiny gaps in the hair shaft, including the cuticle, cortex and medulla oblongata. Filling these tiny gaps with decomposed protein can temporarily enhance the strength of the hair, thereby minimizing the destructive effects of sunlight exposure, heat setting, chemical treatment and mechanical operation (or combing). Furthermore, hydrolyzed protein can also nourish and improve the texture of the hair, provide good moisturizing and repairing effects, and can nourish the hair and improve the texture of the hair.

[0097] The INCI name of jojoba seed oil is SIMMONDSIA CHINENSIS (JOJOBA) SEED OIL, and the CAS number is 61789-91-1. It is rich in vitamins A, B, E and minerals such as calcium and magnesium. It can not only enhance the hair's absorption and maintenance of external moisture, prevent hair moisture loss, nourish and deeply protect hair, make hair shiny and elastic, but also improve rough hair, soften hair, prevent hair from sunburn, make hair darker and prevent split ends. In addition, jojoba seed oil is rich in vitamin B, and combined with hydrolyzed protein, it has the effects of protecting, weighting and conditioning hair, and can alleviate the damage of some chemical reagents in hair wax to the scalp and hair.

[0098] The INCI name of argania spinosakernel oil is ARGANIA SPINOSAKERNEL OIL, and the CAS number is 299184-75-1. It is rich in fatty acids, vitamin E, squalene and sterols. These ingredients can penetrate deep into the hair, nourish the hair, increase the water content of the hair, soften the hair, maintain the elasticity and luster of the hair, and have a nourishing and moisturizing effect. In addition, argania spinosakernel oil can also help repair damaged hair, reduce frizz and split ends, and improve the overall health of the hair. Moreover, because it is rich in vitamin E, it has an excellent antioxidant effect, which can reduce the aging of hair due to free radical damage and protect the hair from environmental damage. Furthermore, argania spinosakernel oil can also improve hair problems such as dryness, lack of luster and curling, making hair easier to manage.

[0099] Preservatives can inhibit the growth of bacteria, mold and other flora, and extend the life cycle and shelf life of hair wax.

[0100] In some embodiments, the preservative includes at least one of methylparaben, propylparaben, and phenoxyethanol.

[0101] The INCI name of methylparaben is METHYLPARABEN, and its CAS number is 99-76-3. It can effectively inhibit the growth of microorganisms such as bacteria, molds and yeasts, protect hair wax from microbial contamination, and extend the shelf life of the product. It mainly plays an antibacterial role by destroying the cell membrane of microorganisms, denaturing the proteins in the cells, and inhibiting the activity of cell respiratory enzymes and transfer enzyme systems. The antibacterial effect of methylparaben is affected by the pH value in the system, and it can play a better preservative role in an acidic environment.

[0102] The INCI name of propylparaben is PROPYLPARABEN and the CAS number is 94-13-3. It is an effective antibacterial agent that can inhibit the growth of microorganisms such as bacteria, molds and yeasts, thereby protecting the hair wax from microbial contamination and extending the shelf life of the product.

[0103] The INCI name of phenoxyethanol is PHENOXYETHANOL and the CAS number is 122-99-6. It can prevent the growth of bacteria, fungi and yeast, ensuring that the hair wax product remains safe and effective during use. It helps maintain the stability of the hair wax, does not react with other ingredients, and will not degrade in air and light.

[0104] The addition of moisturizing emollients can improve the moisturizing effect of hair, enhance the hair's resistance to high temperatures, further reduce the heat damage to hair caused by high temperatures of hot tools, and maintain the health and luster of hair.

[0105] In some embodiments, the moisturizing emollient comprises C 13-14 Isoparaffins.

[0106] C 13-14 The INCI name for isoparaffin is C 13-14 ISOPARAFFIN, CAS No. 246538-79-4, has good emollient effect and can improve the sensitivity of scalp. 13-14 Isoparaffin can form a protective layer on the surface of hair, which helps to prevent the rapid evaporation of water in the hair film formed on the surface of hair. The combination of high temperature resistance, moisturizing and anti-evaporation properties can not only greatly improve the hair's resistance to high temperatures and reduce the thermal damage to the hair caused by high temperatures of hot tools, but also prolong the hair's resistance to high temperatures. Even if the hair is styled for a longer time, it can still maintain the health and luster of the hair.

[0107] In some embodiments, the hair heat protection wax comprises a fragrance comprising a perfume having the INCI name PARFUM.

[0108] In some embodiments, the hair heat protection wax comprises the following ingredients:

[0109] Caprylic / capric triglyceride, dimethicone, divinyl dimethicone / dimethicone crosspolymer, trimethylsiloxysilicate, propylene glycol, water, amodimethicone, oleth-5, laureth-7, trideceth-10, ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer, hydrolyzed keratin, jojoba seed oil, argania spinosa kernel oil, methylparaben, propylparaben, phenoxyethanol, ceteareth-30, C 13-14 Isoparaffin, essence. In this embodiment, the obtained hair wax can not only provide a long-lasting styling effect, moisturize and smooth hair, protect hair scales, repair damaged hair, increase hair gloss, resist frizz, and inhibit bacteria, but also effectively isolate high temperature and reduce heat damage when using hot tools such as curling irons and hair straighteners, so as to maintain the health and gloss of hair.

[0110] In some embodiments, the hair heat protection wax comprises the following raw materials, calculated by weight percentage: caprylic / capric triglyceride: 20%-40%, polydimethylsiloxane: 10%-30%, divinyl dimethicone / polydimethylsiloxane crosspolymer: 5%-15%, trimethylsiloxysilicate: 5%-15%, propylene glycol: 5%-30%, water: 20%-50%, ceteareth-30: 2%-5%, oleth-5: 1%-5%, laureth-7 : 0.5%-2%, Trideceth-10: 0.1%-1%, Ammonium Acryloyldimethyltaurate / Beheneth-25 / Methacrylate Crosspolymer: 0.3%-2%, Amodimethicone: 1%-5%, Hydrolyzed Keratin: 0.1%-1%, Jojoba Seed Oil: 0.1%-2%, Argania Spinosa Kernel Oil: 0.05%-2%, Methylparaben: 0.1%-0.25%, Propylparaben: 0.05%-0.15%, Phenoxyethanol: 0.3%-0.8%, C 13-14 Isoparaffin: 0.5%-2%, essence: 0.1%-1%. In this embodiment, it is beneficial to obtain a hair wax with good shape and stability, and can better play the following roles: provide a lasting styling effect, moisturize and smooth hair, protect hair scales, repair damaged hair, increase hair luster, resist frizz, inhibit bacteria, and effectively isolate high temperature when using hot tools such as curling irons and hair straighteners, reduce heat damage, and maintain the health and luster of hair.

[0111] In some embodiments, the hair heat protection wax comprises the following raw materials, calculated by weight percentage: caprylic / capric triglyceride: 30%-40%, polydimethylsiloxane: 20-30%, divinyl dimethicone / polydimethylsiloxane crosspolymer: 5%-15%, trimethylsiloxysilicate: 5%-15%, propylene glycol: 10-30%, water: 20.29%-50%, ceteareth-30: 2%-5%, oleth-5: 1.5%-5%, laureth-7: 0.68%-2%, Trideceth-10: 0.15%-1%, Ammonium Acryloyldimethyltaurate / Beheneth-25 / Methacrylate Crosspolymer: 0.7%-2%, Amodimethicone: 1.925%-5%, Hydrolyzed Keratin: 0.15%-1%, Jojoba Seed Oil: 0.1%-2%, Argania Spinosa Kernel Oil: 0.05%-2%, Methylparaben: 0.2%-0.25%, Propylparaben: 0.1%-0.15%, Phenoxyethanol: 0.6%-0.8%, C 13-14 Isoparaffin: 0.85%-2%, essence: 0.4%-1%. In this embodiment, it is beneficial to obtain a hair wax with good shape and good stability, and can better play the following roles: provide a lasting styling effect, moisturize and smooth hair, protect hair scales, repair damaged hair, increase hair luster, resist frizz, inhibit bacteria, and effectively isolate high temperature when using hot tools such as curling irons and hair straighteners, reduce heat damage, and maintain the health and luster of hair.

[0112] The present invention also provides a method for preparing a hair heat protection wax, which is characterized by comprising the following steps:

[0113] S10: dividing the raw materials into water-soluble components and oil-soluble components according to their water solubility and oil solubility;

[0114] S20: dissolving and mixing water-soluble components to obtain a water phase, and dissolving and mixing oil-soluble components to obtain an oil phase;

[0115] S30: The water phase and the oil phase are mixed and homogenized to obtain a hair heat protection wax.

[0116] In some embodiments, the water-soluble components are dispersed in deionized water and dissolved by heating to obtain an aqueous phase.

[0117] In some embodiments, the oil-soluble components are mixed and dissolved by heating to obtain an oil phase.

[0118] In some embodiments, the water phase and the oil phase are homogenized and emulsified at 80° C. to 85° C. to promote uniform mixing of the water phase and the oil phase.

[0119] In some embodiments, the aqueous phase and the oil phase are mixed under stirring conditions.

[0120] In some embodiments, the water phase and the oil phase are mixed and homogenized to obtain the hair heat protection wax, and the hair heat protection wax is cooled to 40° C. to 45° C. before being discharged. Under the above temperature conditions, the hair heat protection wax has better stability.

[0121] In the present invention, the following raw materials are regarded as aqueous ingredients: propylene glycol, water, amodimethicone, oleth-5, trideceth-10, hydrolyzed keratin, methylparaben, phenoxyethanol, and ceteareth-30.

[0122] In the present invention, the following raw materials are regarded as oily ingredients: caprylic / capric triglyceride, dimethicone, divinyl dimethicone / dimethicone crosspolymer, trimethylsiloxysilicate, oleth-5, ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer, jojoba seed oil, argania spinosa kernel oil, C 13-14 Isoparaffin, propylparaben.

[0123] In the present invention, if the raw material is both water-soluble and oil-soluble, it can be added to either the water-soluble component or the oil-soluble component, such as ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate cross-linked polymer and fragrance.

[0124] In some embodiments, the heat-protective hair wax obtained by discharging is inspected, and after passing the inspection, it is filled and packaged to obtain a finished product, and the finished product is inspected and put into storage after passing the inspection.

[0125] The technical solution of the present invention is further described in detail below in conjunction with specific embodiments. It should be understood that the following specific embodiments are only used to explain the present invention, and are not used to limit the present invention.

[0126] Example 1 to Example 3

[0127] The preparation methods of the hair heat protection waxes of Examples 1 to 3 are as follows:

[0128] S10: Separating the raw materials in Table 1 into water-soluble components and oil-soluble components according to their water solubility and oil solubility;

[0129] S20: dissolving and mixing water-soluble components to obtain a water phase, and dissolving and mixing oil-soluble components to obtain an oil phase;

[0130] S30: The water phase and the oil phase are stirred and mixed at 80° C. to 85° C., and then homogenized to obtain a hair heat protection wax, and the heat protection wax is cooled to 40° C. to 45° C. and discharged.

[0131] Comparative Example 1 to Comparative Example 3

[0132] Comparative Examples 1 to 3 Hair wax was prepared by referring to the preparation methods of Examples 1 to 3, except that the addition amounts of various raw materials were different, as shown in Table 1.

[0133] Table 1

[0134]

[0135]

[0136] Performance Test 1

[0137] The following tests were performed on the hair wax according to the standards in Table 2: smoothness effect test, gloss effect test, moisturizing effect test, hair breaking strength test, hair lipid peroxidation test, heat resistance test, cold resistance test, cycle test and hygiene index test. The hygiene index mainly tested the total colony count, mold and yeast. The results are shown in Table 3.

[0138] Table 2

[0139]

[0140] Table 3

[0141]

[0142]

[0143]

[0144] From the performance test 1, it can be known that the hair wax of the present invention not only has good stability and can provide a lasting styling effect, but also can moisturize and smooth hair, protect hair scales, repair damaged hair, increase hair gloss, resist frizz, and also has an antibacterial effect.

[0145] Performance Test 2

[0146] After the hair bundles were treated, the process of using a hair straightener to simulate high temperature damage was as follows: the product of Test Example 1 was evenly applied to the hair at an amount of 0.2 g / g hair, balanced and dried for 4 hours in an environment of temperature 21±1° C. and relative humidity 50±10% RH, heated for 10 seconds using a 230° C. straightener, and repeated 10 times.

[0147] Thermal protection efficacy test: After the hair bundles were treated, a hair straightener was used to simulate high temperature damage, and the degree of hair scale curling before and after using the hair wax of Example 1 was analyzed by scanning electron microscope SEM, and the moisture content of the hair bundles before and after using the hair wax was analyzed by thermogravimetric analyzer, and the tensile strength of the hair before and after using the hair wax was tested by a hair multifunctional tester. The group using the hair wax of Example 1 was the test group, and the group not using it was the control group.

[0148] The degree of hair scale lifting before and after using the hair wax of Example 1 was analyzed by scanning electron microscope (SEM). Figure 1 As shown, Figure 1 The left side in the middle is the SEM image of the hair after using hair wax. Figure 1 The right side of the middle is the SEM image of the hair before using the hair wax. Figure 1 It can be seen that when the hair using the hair wax of Example 1 is compared with the hair not using the hair wax, the hair using the hair wax has a much less damaged degree of hair cuticle than the hair not using the hair wax.

[0149] Comparison of lipid peroxidation before and after using hair wax Figure 2 As shown, the number of lipid peroxidation of the hair using hair wax is 0.23, while the number of lipid peroxidation before using hair wax is 2.98. The number of lipid peroxidation of the hair using hair wax is much smaller than that of the hair not using hair wax.

[0150] The comparison of the tensile strength test of the hair bundle before and after using the hair wax is shown in the figure below. Figure 3 As shown, compared with the control group, the pulling-off work of the test group's hair bundles was significantly higher than that of the control group by 22.95%, indicating that the test product has the effect of improving the pulling-off work of hair bundles damaged by hair straighteners.

[0151] The test results of moisture content difference are as follows Figure 4 As shown, compared with the control group, the moisture content of the hair in the test group was significantly higher than that in the control group, indicating that the test product has the effect of improving the moisture content of the hair strands damaged by the straightening iron.

[0152] It can be known from Performance Test 2 that the hair wax of the present invention can effectively block high temperature, reduce heat damage to hair, and has the effect of heat protection for hair.

[0153] Combining performance test 1 and performance test 2, it can be seen that the hair wax of the present invention not only has good stability and can provide a long-lasting styling effect, but also can moisturize and smooth hair, protect hair scales, repair damaged hair, increase hair gloss, resist frizz, and has an antibacterial effect. In addition, it can also effectively block high temperatures, reduce thermal damage to hair, and has the effect of thermal protection of hair.

[0154] In Comparative Example 1, the added amounts of caprylic / capric triglyceride, dimethicone, and trimethylsiloxysilicate were small, and no divinyl dimethicone / dimethicone cross-linked polymer was added. The heat resistance test was unqualified, and the moisturizing effect and hair breaking strength test were affected.

[0155] Although the added amounts of caprylic / capric triglyceride and polydimethicone in Comparative Example 2 are sufficient, without adding divinyl dimethicone / polydimethicone crosspolymer and trimethylsiloxysilicate, the heat resistance test failed, and the moisturizing effect and hair breaking strength test were affected.

[0156] Although sufficient caprylic / capric triglyceride and trimethylsiloxysilicate were added to Comparative Example 3, polydimethylsiloxane, divinyl dimethicone / polydimethylsiloxane crosspolymer and trimethylsiloxysilicate were not added. The heat resistance test was unqualified, and the moisturizing effect and hair breaking strength test were affected.

[0157] The above are only preferred embodiments of the present invention, and are not intended to limit the patent scope of the present invention. Any equivalent structure or equivalent process transformation made using the contents of the present invention specification and drawings, or directly or indirectly applied in other related technical fields, are also included in the patent protection scope of the present invention.

Claims

1. A hair heat protection wax, characterized in that: Including the following ingredients: Caprylic / capric triglyceride, dimethicone, trimethylsiloxysilicate and divinyl dimethicone / dimethicone crosspolymer.

2. The hair heat protection wax according to claim 1, characterized in that: The hair heat protection wax further comprises at least one of a solvent, an emulsifier, an emulsion stabilizer, a hair conditioner, a preservative, a moisturizing emollient and a fragrance.

3. The hair heat protection wax according to claim 2, characterized in that: The hair heat protection wax includes a solvent, and the solvent includes at least one of water and propylene glycol; And / or, the hair heat protection wax comprises an emulsifier, and the emulsifier comprises at least one of ceteareth-30, oleth-5, laureth-7, and trideceth-10; And / or, the hair heat protection wax comprises an emulsion stabilizer, and the emulsion stabilizer comprises ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer.

4. The hair heat protection wax according to claim 2, characterized in that: The hair heat protection wax comprises a hair conditioner, and the hair conditioner comprises at least one of amino dimethicone, hydrolyzed keratin, jojoba seed oil and argania spinosa kernel oil.

5. The hair heat protection wax according to claim 2, characterized in that: The hair heat protection wax includes a preservative, and the preservative includes at least one of methylparaben, propylparaben, and phenoxyethanol; And / or, the hair heat protection wax comprises a moisturizing emollient, wherein the moisturizing emollient comprises C 13-14 At least one of isoparaffins. And / or, the heat protecting hair wax comprises a fragrance, and the fragrance comprises a perfume.

6. The hair heat protection wax according to claim 1, characterized in that: The hair heat protection wax comprises the following raw materials: Caprylic / capric triglyceride, dimethicone, divinyl dimethicone / dimethicone crosspolymer, trimethylsiloxysilicate, propylene glycol, water, amodimethicone, oleth-5, laureth-7, trideceth-10, ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer, hydrolyzed keratin, jojoba seed oil, argania spinosa kernel oil, methylparaben, propylparaben, phenoxyethanol, ceteareth-30, C 13-14 Isoparaffin, flavor.

7. The hair heat protection wax according to claim 6, characterized in that: The hair heat protection wax comprises the following raw materials calculated by weight percentage: Caprylic / capric triglyceride: 20%-40%, Polydimethylsiloxane: 10%-30%, Divinyl dimethicone / dimethicone crosspolymer: 5%-15%, Trimethylsiloxysilicate: 5%-15%, Propylene glycol: 5%-30%, Water: 20%-50%, Ceteareth-30: 2%-5%, Oleth-5: 1%-5%, Laureth-7: 0.5%-2%, Trideceth-10: 0.1%-1%, Ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer: 0.3%-2%, Amodimethicone: 1%-5%, Hydrolyzed keratin: 0.1%-1%, Jojoba seed oil: 0.1%-2%, Argania spinosa kernel oil: 0.05%-2%, Methylparaben: 0.1%-0.25%, Propylparaben: 0.05%-0.15%, Phenoxyethanol: 0.3%-0.8%, C 13-14 Isoparaffin: 0.5%-2%, Fragrance: 0.1%-1%.

8. The hair heat protection wax according to claim 7, characterized in that: The hair heat protection wax comprises the following raw materials calculated by weight percentage: Caprylic / capric triglyceride: 30%, Polydimethylsiloxane: 20%, Divinyl dimethicone / dimethicone crosspolymer: 5%, Trimethylsiloxysilicate: 5%, Propylene glycol: 10%, Water: 20.59%, Ceteareth-30: 2%, Oleth-5: 1.5%, Laureth-7: 0.68%, Trideceth-10: 0.15%, Ammonium acryloyldimethyltaurate / beheneth-25 / methacrylate crosspolymer: 0.7%, amodimethicone: 1.925%, Hydrolyzed keratin: 0.15%, Jojoba seed oil: 0.1%, Argania spinosa kernel oil: 0.05%, Methylparaben: 0.2%, Propylparaben: 0.1%, Phenoxyethanol: 0.6%, C 13-14 Isoparaffin: 0.85%, Fragrance: 0.4%.

9. A method for preparing the hair heat protection wax according to any one of claims 1 to 8, characterized in that: The following steps are involved: The raw materials are divided into water-soluble components and oil-soluble components according to their water solubility and oil solubility; The water-soluble components are dissolved and mixed to obtain a water phase, and the oil-soluble components are dissolved and mixed to obtain an oil phase; The water phase and the oil phase are mixed, homogenized and emulsified to obtain the hair heat protection wax.

10. The method for preparing the heat-protective hair wax according to claim 9, characterized in that: The homogenization emulsification temperature of the water phase and the oil phase is 80°C to 85°C; and / or the discharge temperature of the hair heat protection wax is 40°C to 45°C.

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