Equipment for extracting and separating precious metal palladium from waste catalyst

By designing a device including a processing box, crushing roller, screening module, quantification module and circulation leaching module, the problem of inaccurate determination of material quantity and acid solution in the prior art is solved, and efficient extraction and separation of precious metal palladium and acid liquid savings are achieved.

CN119932322AInactive Publication Date: 2025-05-06YANTAI YINUO ELECTRONIC MATERIALS CO LTD
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Patent Information

Application Number
CN202510428203.9
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-04-08
Publication Date
2025-05-06
Estimated Expiration
Not applicable · inactive patent

AI Technical Summary

Technical Problem

In the prior art, the precious metal palladium extraction and separation equipment in the waste catalyst cannot accurately determine the amount of material and the amount of acidic solution, resulting in insufficient material leaching reaction or waste of acidic solution.

Method used

A device is designed including a processing box, a crushing roller, a screening module, a quantification module and a circulation leaching module. The material is screened through the screening module, the quantitative module quantifies the material, and leaching multiple times through the circulation leaching module to accurately control the amount of acidic solution usage.

Benefits of technology

It realizes efficient extraction and separation of precious metal palladium in waste catalysts, ensuring sufficient material leaching reaction, and reducing the waste of acid liquid.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention relates to the technical field of waste catalyst recycling, and particularly discloses waste catalyst precious metal palladium extraction and separation equipment which comprises a treatment box and a bottom plate, crushing rollers are arranged on the upper portion of an inner cavity of the treatment box in a bilateral symmetry mode, a screening module is arranged below the crushing rollers and comprises a screening plate, and the outer wall of the screening plate is connected with the treatment box; a quantifying module is arranged below the screening module and comprises turning plates, a quantifying plate piece and a first-stage pressure sensor, the turning plates are arranged below the screening plate in a bilateral symmetry mode, the quantifying plate piece is arranged below an inner cavity of the treatment box, and the periphery of the quantifying plate piece is in sliding fit with the inner wall of the treatment box; according to the equipment, crushing, screening and leaching dissolving equipment are integrated into one equipment, meanwhile, screened materials can be quantified, and the quantified materials are leached through a plurality of leaching boxes which operate independently, so that the amount of an acid solution can be accurately measured, and waste of the acid solution is not prone to being caused while it is guaranteed that the materials are fed and discharged to react sufficiently.
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Description

Technical Field

[0001] The invention belongs to the technical field of waste catalyst recycling, and in particular relates to a device for extracting and separating precious metal palladium from waste catalysts. Background Art

[0002] Extracting, separating and recovering precious metal palladium from waste catalysts can improve the utilization rate of palladium resources. When extracting palladium, the waste catalyst needs to be pretreated. In the prior art, in the equipment and method for extracting and separating precious metal palladium from waste catalysts with the published application number 202410160883.6, the crushing, screening and leaching and dissolving equipment are integrated into one equipment, which eliminates the process of material transfer, simplifies the process flow, and improves production efficiency. However, the material after fine screening is not quantified and transported. As the material continues to enter the leaching device, the required amount of acidic solution continues to increase. However, the equipment cannot determine the amount of material entering, and correspondingly, the amount of acidic solution that needs to be input cannot be determined. When the material is relatively more acidic, the leaching reaction of the material is insufficient. When the material is relatively less acidic, part of the acid does not participate in the reaction, resulting in a waste of acid when the palladium-containing solution after the transfer reaction. Summary of the invention

[0003] The object of the present invention is to provide a device for extracting and separating the precious metal palladium from waste catalysts to solve the problems raised in the above-mentioned background technology.

[0004] To achieve the above object, the present invention provides the following technical solutions: A device for extracting and separating precious metal palladium from waste catalysts comprises a processing box and a bottom plate, wherein crushing rollers are symmetrically arranged above the inner cavity of the processing box, a screening module is arranged below the crushing rollers, the screening module comprises a sieve plate, the outer wall of the sieve plate is connected to the processing box, a quantitative module is arranged below the screening module, the quantitative module comprises a flap, a quantitative plate and a primary pressure sensor, the flap is symmetrically arranged below the sieve plate, the quantitative plate is arranged below the inner cavity of the processing box, and the four sides of the quantitative plate are slidably matched with the inner wall of the processing box, the primary pressure sensor is connected between the bottom of the quantitative plate and the processing box, a circulating leaching module is connected between the bottom of the quantitative module and the bottom plate, the circulating leaching module comprises a primary driving motor, a rotating plate, a secondary pressure sensor and a leaching box, the primary driving motor is connected to the middle of the top of the bottom plate by positioning bolts, the rotating plate is arranged above the primary driving motor, and the output shaft at the top of the primary driving motor is connected to the middle of the bottom of the rotating plate, the secondary pressure sensor and the leaching box are arranged in a circular array on the top of the rotating plate, and the secondary pressure sensor is connected between the leaching box and the rotating plate.

[0005] Preferably, the screening module also includes a secondary drive motor, a secondary drive screw, a secondary stabilizing rod, a secondary push plate, a connecting plate, a secondary opening, a receiving box, a limiting plate and a vibration motor. The secondary push plates are symmetrically arranged on both sides of the top of the sieve plate, and the connecting plates are symmetrically arranged on both sides of the top of the sieve plate front and back, and the left and right sides of the connecting plates are connected to the secondary push plates, the secondary drive motor is connected to the right side of the processing box through a positioning bolt, the right end of the secondary drive screw is connected to the output end of the secondary drive motor, and the left end of the secondary drive screw passes through the right side of the processing box, the secondary push plate on the right side, and the secondary push plate on the left side in sequence, and the outer wall of the secondary drive screw is connected to the two groups of secondary The secondary push plates are threadedly connected, and the secondary stabilizing rods are symmetrically arranged on both sides of the secondary driving screw rod, and the right end of the secondary stabilizing rod passes through the two groups of secondary push plates in turn and is connected to the processing box. The outer wall of the secondary stabilizing rod and the secondary push plates are slidably matched. The secondary opening is opened on the left side of the processing box, and the secondary opening is at the top of the sieve plate. The receiving box is connected to the left side of the processing box, and the receiving box is below the secondary opening. The limiting plate is connected to the middle of the top of the secondary push plate on the right, and the vibration motor is connected to the middle of the bottom of the sieve plate by positioning bolts. Through the secondary push plate, unqualified materials that have not passed through the sieve plate can be pushed into the receiving box, which is convenient for the subsequent crushing of the unqualified materials.

[0006] Preferably, the quantitative module also includes a three-stage drive motor and a transmission shaft. The three-stage drive motor is symmetrically arranged on the rear side of the processing box, and the three-stage drive motor is connected to the processing box through positioning bolts. The transmission shaft is arranged in the middle of the flap, and the rear end of the transmission shaft passes through the flap and is connected to the output end on the front side of the three-stage drive motor. The three-stage drive motor drives the transmission shaft to rotate 90°, so that the flap changes from a vertical state to a horizontal state, which has a shielding effect and prevents the screened material from falling to the top of the quantitative plate.

[0007] Preferably, the quantitative module also includes a four-stage opening, a baffle, a primary vertical slot, a transverse plate, a longitudinal plate, an electric telescopic rod and an assembly plate, the four-stage opening is symmetrically opened at the bottom of both sides of the processing box, and the four-stage opening is at the top of the quantitative plate, the baffle is symmetrically arranged on both sides of the top of the quantitative plate, the primary vertical slot is symmetrically opened at the left and right sides of the processing box respectively, the transverse plate slidably fits in the primary vertical slot, and one side of the transverse plate passes through the primary vertical slot and is connected to the baffle, the longitudinal plate is connected to the side opposite to the transverse plate and the baffle, the assembly plate is symmetrically connected to both sides of the processing box by positioning bolts, the electric telescopic rod is connected to the bottom of the assembly plate, and the output end of the bottom of the electric telescopic rod is connected to the longitudinal plate, the longitudinal plate is pulled up through the output end of the bottom of the electric telescopic rod, thereby driving the baffle to rise through the transverse plate, and under the action of the secondary vertical slot and the tertiary vertical slot, the baffle will not affect each other with the fourth-stage driving screw and the fourth-stage stabilizing rod, and the baffle blocks the fourth-stage opening, which can prevent the material from passing through the fourth-stage opening and leaving the quantitative plate.

[0008] Preferably, the quantitative module also includes a four-stage drive motor, a four-stage drive screw, a four-stage stabilizing rod, a four-stage push plate, an outward extension plate, a secondary vertical slot and a tertiary vertical slot. The four-stage push plate is symmetrically arranged on the top of the quantitative plate, and two groups of four-stage push plates are between the two groups of baffles. The secondary vertical slot is opened above the middle of the baffle, and the tertiary vertical slot is symmetrically opened on the front and rear sides of the baffle, and the secondary vertical slot and the tertiary vertical slot both penetrate the baffle from left to right. The four-stage drive motor is connected to the right side of the processing box through a positioning bolt, and the right end of the four-stage drive screw is connected to the four-stage drive The output end on the left side of the driving motor is connected, the left end of the four-stage driving screw rod passes through the right side of the processing box, two groups of secondary vertical grooves and two groups of four-stage push plates, and is connected to the processing box bearing, and the outer wall of the four-stage driving screw rod is threadedly connected to the four-stage push plate through an external thread, and the extended plate is connected to the bottom of the opposite side of the two groups of four-stage push plates. The four-stage stabilizing rod is symmetrically arranged on both sides of the four-stage driving screw rod, and the left and right ends of the four-stage stabilizing rod both pass through the three-stage vertical groove and are connected to the processing box. The stability of the four-stage push plate during movement is improved through the four-stage stabilizing rod.

[0009] Preferably, the quantitative module also includes a material guide frame and a central frame. The material guide frame is connected to the bottom of the outer side of the processing box, and the material guide frame is connected to the left and right groups of four-level openings. The central frame is connected to the left side of the bottom of the material guide frame, and can guide the materials discharged from the two groups of four-level openings to the feed port.

[0010] Preferably, the circulating leaching module also includes a liquid inlet pipe, a first-level solenoid valve, a liquid discharge pipe, a second-level solenoid valve, a feed port, a feed frame, a blocking vertical plate, an arc-shaped plate, a first-level bracket, a cylinder and a second-level bracket. The liquid inlet pipe is connected to the top of the leaching tank, the first-level solenoid valve is arranged on the liquid inlet pipe, the liquid discharge pipe is connected to the bottom of the leaching tank, the second-level solenoid valve is arranged on the liquid discharge pipe, the feed port is opened in the middle of the top of the leaching tank, the cylinder is connected to the middle of the bottom of the material guide frame, the first-level bracket connection sleeve is arranged on the outer wall of the cylinder, the arc-shaped plate is arranged in a circular array on the outside of the cylinder, and the feed frame and the blocking vertical plate are connected to two adjacent groups of arc-shaped plates. There are four groups of arc-shaped plates, one group of feed frame, and three groups of blocking vertical plates. The inner cavity of the feed frame is connected with the central frame and the feed port. The first-level bracket is respectively connected with the feed frame and the blocking vertical plates. The second-level bracket is slidably sleeved on the outer wall of the cylinder, and the second-level bracket is connected with the outer wall of the leaching box. The first-level solenoid valve is opened to guide the solution into the leaching box through the liquid inlet pipe. The second-level solenoid valve is opened to discharge the leached solution through the liquid discharge pipe. The feed frame and the blocking vertical plates are fixed through the first-level bracket and the cylinder. The feed port is ensured to be more accurately at the bottom of the feed frame through the second-level bracket.

[0011] Preferably, the circulating leaching module also includes a reinforcing ring, a reinforcing rod and a roller. The reinforcing rod is connected in a circular array to the bottom of the leaching box in a circumferential manner. The reinforcing ring is slidably mounted on the outer wall of the reinforcing rod, and the bottom end of the reinforcing ring is connected to the rotating plate. The roller is connected in a circumferential array to the top of the bottom plate, and the top of the roller is connected to the rotating plate. Through the reinforcing ring and the reinforcing rod, the monitoring effect of the secondary pressure sensor can be not affected while ensuring the stability of the leaching box when it rotates with the rotating plate.

[0012] Compared with the prior art, the beneficial effect of the present invention is that when the present invention is in use, the device integrates the crushing, screening and leaching and dissolving equipment into one device, and can quantify the screened material, and leach the quantified material through a plurality of independently operated leaching boxes, so as to accurately measure the amount of the acid solution, ensure that the material leaching reaction is sufficient, and not easily cause waste of acid solution. Among them, through the screening module, not only the crushed material can be screened, but also the unqualified material that has not passed through the screen plate can be pushed into the receiving box through the secondary push plate, so as to facilitate the subsequent crushing of the unqualified material. When the quantified material is pushed from the fourth-level opening to the material guide frame through the fourth-level push plate, the flap is made horizontal to prevent the screened material from continuously falling to the top of the quantitative plate. The material guide frame guides the material from the centralized frame, the feed frame plate and the feed port to the leaching box. Through the primary drive motor, the rotating plate drives the leaching box to rotate to switch different leaching boxes. BRIEF DESCRIPTION OF THE DRAWINGS

[0013] Figure 1 The figure is a schematic diagram of the overall structure of a device for extracting and separating the precious metal palladium from waste catalysts.

[0014] Figure 2 The present invention is a schematic diagram of the bottom structure of a device for extracting and separating the precious metal palladium from waste catalysts.

[0015] Figure 3 The present invention is a schematic diagram of the rear structure of a device for extracting and separating the precious metal palladium from waste catalysts.

[0016] Figure 4 This is a schematic diagram of the left side structure of a device for extracting and separating the precious metal palladium from waste catalysts.

[0017] Figure 5 The present invention is a schematic diagram of the bottom structure of a sieve plate used in a device for extracting and separating precious metal palladium from waste catalysts.

[0018] Figure 6 The present invention is a schematic diagram of a flap used in a device for extracting and separating the precious metal palladium from waste catalysts.

[0019] Figure 7 The diagram is a schematic diagram of a four-stage drive screw for a device for extracting and separating the precious metal palladium from waste catalysts.

[0020] Figure 8 This is a schematic diagram of a primary pressure sensor used in a device for extracting and separating precious metal palladium from waste catalysts.

[0021] Fig. 9 This is a schematic diagram of a feed frame for a device for extracting and separating precious metal palladium from waste catalysts.

[0022] Fig.10 This is a schematic diagram of a feed port for a device for extracting and separating precious metal palladium from waste catalysts.

[0023] Fig.11 This is a schematic diagram of a secondary support for a device for extracting and separating the precious metal palladium from waste catalysts.

[0024] Fig.12 The present invention is a schematic diagram of the bottom structure of a rotating plate used in a device for extracting and separating precious metal palladium from waste catalysts.

[0025] In the figure: 1. Processing box; 2. Bottom plate; 3. Crushing roller; 4. Screening module; 41. Screen plate; 42. Secondary drive motor; 43. Secondary drive screw rod; 44. Secondary stabilizing rod; 45. Secondary push plate; 46. Connecting plate; 47. Secondary opening; 48. Undertaking box; 49. Limiting plate; 410. Vibrating motor; 5. Dosing module; 51. Turn plate; 52. Dosing plate; 53. Primary pressure sensor; 54. Third-stage drive motor; 55. Transmission shaft; 56. Fourth-stage opening; 57. Baffle; 58. Primary vertical slot; 59. Horizontal plate; 510. Longitudinal plate; 511. Electric telescopic rod; 512. Assembly plate; 513. Fourth-stage drive motor; 514. Four-stage driving screw; 515, four-stage stabilizing rod; 516, four-stage pushing plate; 517, extending plate; 518, two-stage vertical slot; 519, three-stage vertical slot; 520, material guide frame; 521, central frame; 6, circulating leaching module; 61, one-stage driving motor; 62, rotating plate; 63, two-stage pressure sensor; 64, leaching box; 65, liquid inlet pipe; 66, one-stage solenoid valve; 67, liquid discharge pipe; 68, two-stage solenoid valve; 69, feed port; 610, feed frame; 611, blocking vertical plate; 612, arc plate; 613, one-stage bracket; 614, cylinder; 615, two-stage bracket; 616, reinforcing ring; 617, reinforcing rod; 618, roller. DETAILED DESCRIPTION

[0026] Example 1 See also Figure 1-Figure 12As shown, a device for extracting and separating precious metal palladium from waste catalysts includes a processing box 1 and a bottom plate 2. Crushing rollers 3 are symmetrically arranged above the inner cavity of the processing box 1. A screening module 4 is arranged below the crushing rollers 3. The screening module 4 includes a sieve plate 41. The outer wall of the sieve plate 41 is connected to the processing box 1. A quantitative module 5 is arranged below the screening module 4. The quantitative module 5 includes a flap 51, a quantitative plate 52 and a primary pressure sensor 53. The flap 51 is symmetrically arranged below the sieve plate 41. The quantitative plate 52 is arranged below the inner cavity of the processing box 1, and the quantitative plate 52 is slidably matched with the inner wall of the processing box 1 around the periphery. The primary pressure sensor 53 is connected to the quantitative plate A circulating leaching module 6 is connected between the bottom of 52 and the processing box 1, and between the bottom of the quantitative module 5 and the bottom plate 2. The circulating leaching module 6 includes a primary driving motor 61, a rotating plate 62, a secondary pressure sensor 63 and a leaching box 64. The primary driving motor 61 is connected to the middle of the top of the bottom plate 2 by positioning bolts, the rotating plate 62 is arranged above the primary driving motor 61, and the output shaft at the top of the primary driving motor 61 is connected to the middle of the bottom of the rotating plate 62. The secondary pressure sensor 63 and the leaching box 64 are both arranged in a circular array on the top of the rotating plate 62, and the secondary pressure sensor 63 is connected between the leaching box 64 and the rotating plate 62.

[0027] refer to Figure 1-Figure 4 As shown, the screening module 4 also includes a secondary driving motor 42, a secondary driving screw rod 43, a secondary stabilizing rod 44, a secondary pushing plate 45, a connecting plate 46, a secondary opening 47, a receiving box 48, a limiting plate 49 and a vibration motor 410. The secondary pushing plates 45 are symmetrically arranged on both sides of the top of the sieve plate 41, and the connecting plates 46 are symmetrically arranged on both sides of the top of the sieve plate 41, and the left and right sides of the connecting plates 46 are connected to the secondary pushing plates 45. The secondary driving motor 42 is connected to the right side of the processing box 1 through a positioning bolt, and the right end of the secondary driving screw rod 43 is connected to the output end of the secondary driving motor 42. The left end of the secondary driving screw rod 43 passes through the right side of the processing box 1, the secondary pushing plate 45 on the right side, and the secondary pushing plate 45 on the left side in sequence, and the outer wall of the secondary driving screw rod 43 is connected to the two groups of The secondary push plate 45 is threadedly connected, and the secondary stabilizing rod 44 is symmetrically arranged on both sides of the secondary driving screw 43, and the right end of the secondary stabilizing rod 44 passes through the two groups of secondary push plates 45 in sequence and is connected to the processing box 1. The outer wall of the secondary stabilizing rod 44 slides with the secondary push plate 45. The secondary opening 47 is opened on the left side of the processing box 1, and the secondary opening 47 is at the top of the sieve plate 41. The receiving box 48 is connected to the left side of the processing box 1, and the receiving box 48 is below the secondary opening 47. The limiting plate 49 is connected to the middle of the top of the secondary push plate 45 on the right side, and the vibration motor 410 is connected to the middle of the bottom of the sieve plate 41 by positioning bolts. Through the secondary push plate 45, unqualified materials that have not passed through the sieve plate 41 can be pushed into the receiving box 48, which is convenient for the subsequent crushing of the unqualified materials.

[0028] refer to Figure 3 , Figure 4 and Figure 6 As shown, the quantitative module 5 also includes a three-stage drive motor 54 and a transmission shaft 55. The three-stage drive motor 54 is symmetrically arranged on the rear side of the processing box 1, and the three-stage drive motor 54 is connected to the processing box 1 through a positioning bolt. The transmission shaft 55 is arranged in the middle of the flap 51, and the rear end of the transmission shaft 55 passes through the flap 51 and is connected to the output end on the front side of the three-stage drive motor 54. The three-stage drive motor 54 drives the transmission shaft 55 to rotate 90°, so that the flap 51 changes from a vertical state to a horizontal state, which has a shielding effect and prevents the screened material from falling to the top of the quantitative plate 52.

[0029] refer to Figure 1-Figure 4 , Figure 6 and Figure 7 As shown, the quantitative module 5 also includes a four-stage opening 56, a baffle 57, a primary vertical slot 58, a horizontal plate 59, a longitudinal plate 510, an electric telescopic rod 511 and an assembly plate 512. The four-stage opening 56 is symmetrically opened at the bottom of both sides of the processing box 1, and the four-stage opening 56 is at the top of the quantitative plate 52. The baffle 57 is symmetrically arranged on both sides of the top of the quantitative plate 52. The primary vertical slot 58 is symmetrically opened on the left and right sides of the processing box 1 respectively. The horizontal plate 59 is slidably matched in the primary vertical slot 58, and one side of the horizontal plate 59 passes through the primary vertical slot 58 and is connected to the baffle 57. The longitudinal plate 510 is connected to the horizontal plate 59 and the baffle 57. On one side, the assembly plate 512 is symmetrically connected to the two sides of the processing box 1 through positioning bolts, the electric telescopic rod 511 is connected to the bottom of the assembly plate 512, and the output end of the bottom of the electric telescopic rod 511 is connected to the longitudinal plate 510. The longitudinal plate 510 is pulled up through the output end of the bottom of the electric telescopic rod 511, thereby driving the baffle 57 to rise through the transverse plate 59. Under the action of the secondary vertical groove 518 and the tertiary vertical groove 519, the baffle 57 will not affect each other with the fourth-level driving screw 514 and the fourth-level stabilizing rod 515, and the baffle 57 blocks the fourth-level opening 56, which can prevent the material from escaping from the quantitative plate 52 through the fourth-level opening 56.

[0030] refer to Figure 1 , Figure 2 , Figure 4 , Figure 6 and Figure 7As shown, the quantitative module 5 also includes a four-stage driving motor 513, a four-stage driving screw rod 514, a four-stage stabilizing rod 515, a four-stage pushing plate 516, an extending plate 517, a secondary vertical slot 518 and a tertiary vertical slot 519. The four-stage pushing plate 516 is symmetrically arranged on the top of the quantitative plate 52, and two groups of four-stage pushing plates 516 are located between two groups of baffles 57. The secondary vertical slot 518 is opened above the middle of the baffle 57, and the tertiary vertical slot 519 is symmetrically opened on the front and rear sides of the baffle 57, and the secondary vertical slot 518 and the tertiary vertical slot 519 both penetrate the baffle 57 from left to right. The four-stage driving motor 513 is connected to the right side of the processing box 1 through a positioning bolt, and the four-stage driving screw rod 514 is connected to the right side of the processing box 1 through a positioning bolt. The right end is connected to the output end on the left side of the four-stage drive motor 513, the left end of the four-stage drive screw rod 514 passes through the right side of the processing box 1, two groups of secondary vertical grooves 518 and two groups of four-stage push plates 516, and is connected to the bearing of the processing box 1, and the outer wall of the four-stage drive screw rod 514 is threadedly connected to the four-stage push plate 516 through an external thread, and the extended plate 517 is connected to the bottom of the opposite side of the two groups of four-stage push plates 516, and the four-stage stabilizing rod 515 is symmetrically arranged on both sides of the four-stage drive screw rod 514, and the left and right ends of the four-stage stabilizing rod 515 both pass through the three-stage vertical groove 519, and are connected to the processing box 1, and the stability of the four-stage push plate 516 during movement is improved through the four-stage stabilizing rod 515.

[0031] refer to Figure 1-Figure 4 and Figure 6-Figure 8 As shown, the quantitative module 5 also includes a material guide frame 520 and a central frame 521. The material guide frame 520 is connected to the outer bottom of the processing box 1, and the material guide frame 520 is connected to the left and right groups of four-level openings 56. The central frame 521 is connected to the left side of the bottom of the material guide frame 520, and can guide the materials discharged from the two groups of four-level openings 56 to the feed port 69.

[0032] refer to Figure 1-Figure 4 and Figure 9-12As shown, the circulating leaching module 6 also includes a liquid inlet pipe 65, a primary solenoid valve 66, a liquid discharge pipe 67, a secondary solenoid valve 68, a feed port 69, a feed frame 610, a blocking vertical plate 611, an arc plate 612, a primary bracket 613, a cylinder 614 and a secondary bracket 615. The liquid inlet pipe 65 is connected to the top of the leaching tank 64, the primary solenoid valve 66 is arranged on the liquid inlet pipe 65, the liquid discharge pipe 67 is connected to the bottom of the leaching tank 64, the secondary solenoid valve 68 is arranged on the liquid discharge pipe 67, the feed port 69 is opened in the middle of the top of the leaching tank 64, the cylinder 614 is connected to the middle of the bottom of the guide frame 520, the primary bracket 613 is connected and sleeved on the outer wall of the cylinder 614, the arc plate 612 is arranged in a circular array on the outside of the cylinder 614, and the feed frame 610 and the blocking vertical plate 611 are connected to two adjacent groups of arc plates. The arc-shaped plate members 612 are arranged between the two members, and four groups of arc-shaped plate members 612 are arranged between the two members, the feed frame 610 is arranged with one group, and the blocking vertical plates 611 are arranged with three groups. The inner cavity of the feed frame 610 is communicated with the central frame 521 and the feed port 69. The first-level bracket 613 is respectively connected with the feed frame 610 and the blocking vertical plates 611. The second-level bracket 615 is slidably sleeved on the outer wall of the cylinder 614, and the second-level bracket 615 is connected with the outer wall of the leaching box 64. The first-level solenoid valve 66 is opened to guide the solution into the leaching box 64 through the liquid inlet pipe 65. The second-level solenoid valve 68 is opened to discharge the leached solution through the liquid discharge pipe 67. The feed frame 610 and the blocking vertical plates 611 are fixed through the first-level bracket 613 and the cylinder 614. The feed port 69 is ensured to be more accurately located at the bottom of the feed frame 610 through the second-level bracket 615.

[0033] refer to Figure 1-Figure 4 and Figure 9-12 As shown, the circulating leaching module 6 also includes a reinforcing ring 616, a reinforcing rod 617 and a roller 618. The reinforcing rod 617 is connected to the bottom of the leaching box 64 in a circumferential array. The reinforcing ring 616 is slidably sleeved on the outer wall of the reinforcing rod 617, and the bottom end of the reinforcing ring 616 is connected to the rotating plate 62. The roller 618 is connected to the top of the bottom plate 2 in a circumferential array, and the top of the roller 618 is connected to the rotating plate 62. Through the reinforcing ring and the reinforcing rod, the stability of the leaching box 64 when rotating with the rotating plate 62 can be ensured without affecting the monitoring effect of the secondary pressure sensor 63.

[0034] Working principle: the material is thrown in through the top of the processing box 1, and the passing material is crushed by two sets of crushing rollers 3. The crushed material falls to the top of the screen plate 41, and is screened by the vibration motor 410 and the screen plate 41. The material passing through the screen plate 41 falls to the top of the quantitative plate 52 and is monitored by the primary pressure sensor 53. When the weight of the material on the top of the quantitative plate 52 reaches a preset value, the primary pressure sensor 53 transmits the data to the peripheral terminal, and the peripheral terminal controls the three-stage drive motor 54 to start. The three-stage drive motor 54 drives the transmission shaft 55 to rotate 90°, so that the flap 51 changes from a vertical state to a horizontal state, which has a shielding effect and prevents the screened material from falling to the top of the quantitative plate 52. After the transmission shaft 55 rotates 90°, the three-stage drive motor 54 drives the transmission shaft 55 to rotate 90°. The four-stage drive motor 54 transmits a signal to the peripheral terminal, the peripheral terminal receives the signal, and the electric telescopic rod 511 is turned on. The longitudinal plate 510 is pulled up through the output end at the bottom of the electric telescopic rod 511, thereby driving the baffle 57 to rise through the transverse plate 59. Under the action of the secondary vertical groove 518 and the tertiary vertical groove 519, the baffle 57 will not affect each other with the four-stage drive screw rod 514 and the four-stage stabilizing rod 515. After the top surface of the transverse plate 59 contacts the processing box 1, the transverse plate 59 cannot continue to rise, the electric telescopic rod 511 senses, and transmits a signal to the external terminal. The external terminal receives the signal and controls the four-stage drive motor 513 to turn on. The four-stage drive motor 513 drives the four-stage drive screw rod 514 to rotate. The opposite threads on the left and right outer walls of the driving screw 514 cause the two groups of four-stage push plates 516 to move in opposite directions until the outwardly extending plate 517 pushes the material through the four-stage opening 56 into the material guide frame 520, and the material falls into the leaching box 64 through the central frame 521, the feeding frame 610, and the feeding port 69. After the material on the top of the quantitative plate 52 is cleared, the primary pressure sensor 53 transmits data to the peripheral terminal, which receives the data and controls the four-stage driving motor 513 to drive the four-stage driving screw 514 to reverse, until the two groups of four-stage pushing plates 516 fit together and cannot move further, and the four-stage driving motor 513 cannot drive the four-stage driving screw 514 to rotate, and the four-stage driving motor 513 transmits the signal to the peripheral terminal, which receives the signal and controls the four-stage driving The motor 513 is turned off, and the weight of the material falling in the leaching box 64 is monitored through the secondary pressure sensor 63. After the material has fallen, the weight of the material reaches the preset value of the secondary pressure sensor 63, and the secondary pressure sensor 63 transmits the data to the external terminal. The external terminal receives the data and controls the primary drive motor 61 to start. The output shaft at the top of the primary drive motor 61 drives the rotating plate 62 to rotate 90°, so that another group of leaching boxes 64 with acidic solution pre-set are moved to the bottom of the centralized frame 521, and the switching of the leaching boxes 64 is completed. The setting of the arc plate 612 and the blocking vertical plate 611 can block the feed port 69 to prevent the inner cavity of the leaching box 64 from being connected to the external environment, thereby affecting the reaction between the material and the acidic solution; Larger materials cannot pass through the sieve plate 41. When a large amount of materials are piled up, the material is observed through the observation window on the front side of the processing box 1, the rotation of the crushing roller 3 is suspended, the secondary drive motor 42 is turned on, and the secondary drive screw 43 is driven to rotate, thereby driving the secondary push plate 45 to move left. The secondary push plate 45 on the left side is separated from the processing box 1 through the secondary opening 47. The materials between the two groups of secondary push plates 45 are pushed out of the secondary opening 47 and fall into the receiving box 48, completing the unqualified material discharge, and contacting the processing box 1 on the left side of the limiting plate 49. Afterwards, the movement of the limiting plate 49 is blocked, and the secondary driving screw 43 cannot rotate. The secondary driving motor 42 transmits a signal to the external terminal, and the external terminal receives the signal and controls the secondary driving motor 42 to drive the secondary driving screw 43 to rotate in the opposite direction until the right side of the limiting plate 49 contacts the processing box 1. The movement of the limiting plate 49 is blocked, and the secondary driving screw 43 cannot rotate. The secondary driving motor 42 transmits a signal to the external terminal, and the external terminal controls the secondary driving motor 42 to shut down, so that the unqualified materials can be exported in a short time.

[0035] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A device for extracting and separating precious metal palladium from waste catalysts, comprising a processing box (1) and a bottom plate (2), characterized in that: Crushing rollers (3) are symmetrically arranged above the inner cavity of the processing box (1), and a screening module (4) is arranged below the crushing rollers (3). The screening module (4) includes a screening plate (41), and the outer wall of the screening plate (41) is connected to the processing box (1). A quantitative module (5) is arranged below the screening module (4), and the quantitative module (5) includes a flap (51), a quantitative plate (52) and a primary pressure sensor (53). The flap (51) is symmetrically arranged below the screening plate (41), and the quantitative plate (52) is arranged below the inner cavity of the processing box (1), and the four sides of the quantitative plate (52) are slidably matched with the inner wall of the processing box (1). The primary pressure sensor (53) is connected between the bottom of the quantitative plate (52) and the processing box (1). A circulating leaching module (6) is connected between the bottom of the module (5) and the bottom plate (2). The circulating leaching module (6) comprises a primary drive motor (61), a rotating plate (62), a secondary pressure sensor (63) and a leaching box (64). The primary drive motor (61) is connected to the middle of the top of the bottom plate (2) via positioning bolts. The rotating plate (62) is arranged above the primary drive motor (61), and the output shaft at the top of the primary drive motor (61) is connected to the middle of the bottom of the rotating plate (62). The secondary pressure sensor (63) and the leaching box (64) are arranged in a circumferential array at the top of the rotating plate (62), and the secondary pressure sensor (63) is connected between the leaching box (64) and the rotating plate (62).

2. The device for extracting and separating precious metal palladium from waste catalysts according to claim 1, characterized in that: The screening module (4) further comprises a secondary driving motor (42), a secondary driving screw rod (43), a secondary stabilizing rod (44), a secondary pushing plate (45), a connecting plate (46), a secondary opening (47), a receiving box (48), a limiting plate (49) and a vibration motor (410); the secondary pushing plate (45) is symmetrically arranged on both sides of the top of the sieve plate (41); the connecting plate (46) is symmetrically arranged on both sides of the top of the sieve plate (41); and the left and right sides of the connecting plate (46) are connected to the secondary pushing plate (45); the secondary driving motor (42) is connected to the right side of the processing box (1) by means of a positioning bolt; the right end of the secondary driving screw rod (43) is connected to the output end of the secondary driving motor (42); and the left end of the secondary driving screw rod (43) passes through the right side of the processing box (1), the secondary pushing plate (45) on the right side, and the secondary pushing plate (45) on the left side in sequence. The secondary push plate (45) is provided with a secondary drive screw (43), and the outer wall of the secondary drive screw (43) is threadedly connected to the two groups of secondary push plates (45) through an external thread. The secondary stabilizing rod (44) is symmetrically arranged on both sides of the secondary drive screw (43) front and back, and the right end of the secondary stabilizing rod (44) passes through the two groups of secondary push plates (45) in sequence and is connected to the processing box (1). The outer wall of the secondary stabilizing rod (44) and the secondary push plate (45) are slidably matched. The secondary opening (47) is provided on the left side of the processing box (1), and the secondary opening (47) is located at the top of the sieve plate (41). The receiving box (48) is connected to the left side of the processing box (1), and the receiving box (48) is located below the secondary opening (47). The limiting plate (49) is connected to the middle of the top of the secondary push plate (45) located on the right side. The vibration motor (410) is connected to the middle of the bottom of the sieve plate (41) through a positioning bolt.

3. The device for extracting and separating precious metal palladium from waste catalyst according to claim 1, characterized in that: The quantitative module (5) further comprises a three-stage drive motor (54) and a transmission shaft (55); the three-stage drive motor (54) is symmetrically arranged at the rear side of the processing box (1), and the three-stage drive motor (54) is connected to the processing box (1) via positioning bolts; the transmission shaft (55) is arranged in the middle of the flap (51), and the rear end of the transmission shaft (55) passes through the flap (51) and is connected to the output end of the front side of the three-stage drive motor (54).

4. The device for extracting and separating precious metal palladium from waste catalyst according to claim 1, characterized in that: The quantitative module (5) further comprises a four-stage opening (56), a baffle (57), a first-stage vertical slot (58), a transverse plate (59), a longitudinal plate (510), an electric telescopic rod (511) and an assembly plate (512), wherein the four-stage opening (56) is symmetrically disposed at the bottom of both sides of the processing box (1), and the four-stage opening (56) is located at the top of the quantitative plate (52), the baffle (57) is symmetrically disposed at both sides of the top of the quantitative plate (52), and the first-stage vertical slot (58) is symmetrically disposed at the left and right sides of the processing box (1). The horizontal plate (59) is slidably fitted in the primary vertical groove (58), and one side of the horizontal plate (59) passes through the primary vertical groove (58) and is connected to the baffle (57). The longitudinal plate (510) is connected to the side of the horizontal plate (59) opposite to the baffle (57). The assembly plate (512) is symmetrically connected to the two sides of the processing box (1) through positioning bolts. The electric telescopic rod (511) is connected to the bottom of the assembly plate (512), and the output end of the bottom of the electric telescopic rod (511) is connected to the longitudinal plate (510).

5. The device for extracting and separating precious metal palladium from waste catalysts according to claim 4, characterized in that: The quantitative module (5) further comprises a four-stage drive motor (513), a four-stage drive screw rod (514), a four-stage stabilizing rod (515), a four-stage push plate (516), an extended plate (517), a secondary vertical slot (518) and a tertiary vertical slot (519), wherein the four-stage push plate (516) is symmetrically arranged on the top of the quantitative plate (52), and two groups of four-stage push plates (516) are located between two groups of baffles (57), the secondary vertical slot (518) is opened above the middle of the baffle (57), the tertiary vertical slot (519) is symmetrically opened on the front and rear sides of the baffle (57), and the secondary vertical slot (518) and the tertiary vertical slot (519) both penetrate the baffle (57) from left to right, and the four-stage drive motor (513) is connected to the baffle (57) by positioning bolts. On the right side of the processing box (1), the right end of the four-stage drive screw (514) is connected to the output end of the left side of the four-stage drive motor (513), the left end of the four-stage drive screw (514) passes through the right side of the processing box (1), the two groups of secondary vertical slots (518) and the two groups of four-stage push plates (516), and is connected to the bearing of the processing box (1), and the outer wall of the four-stage drive screw (514) is threadedly connected to the four-stage push plates (516) through external threads, and the extended plate (517) is connected to the bottom of the opposite side of the two groups of four-stage push plates (516), and the four-stage stabilizing rod (515) is symmetrically arranged on both sides of the four-stage drive screw (514), and the left and right ends of the four-stage stabilizing rod (515) both pass through the three-stage vertical slot (519) and are connected to the processing box (1).

6. The device for extracting and separating precious metal palladium from waste catalysts according to claim 4, characterized in that: The quantitative module (5) further comprises a material guide frame (520) and a centralizing frame (521); the material guide frame (520) is connected to the outer bottom of the processing box (1), and the material guide frame (520) is connected to the left and right groups of four-level openings (56); the centralizing frame (521) is connected to the left side of the bottom of the material guide frame (520).

7. The device for extracting and separating precious metal palladium from waste catalysts according to claim 6, characterized in that: The circulating leaching module (6) further comprises a liquid inlet pipe (65), a first-level solenoid valve (66), a liquid discharge pipe (67), a second-level solenoid valve (68), a feed port (69), a feed frame (610), a blocking vertical plate (611), an arc-shaped plate (612), a first-level bracket (613), a cylinder (614) and a second-level bracket (615); the liquid inlet pipe (65) is connected to the top of the leaching tank (64); the first-level solenoid valve (66) is arranged on the liquid inlet pipe (65); the liquid discharge pipe (67) is connected to the bottom of the leaching tank (64); the second-level solenoid valve (68) is arranged on the liquid discharge pipe (67); the feed port (69) is opened in the middle of the top of the leaching tank (64); the cylinder (614) is connected to the middle of the bottom of the material guide frame (520); The first-stage bracket (613) is connected and sleeved on the outer wall of the cylinder (614); the arc-shaped plate members (612) are arranged in a circular array on the outer side of the cylinder (614); the feed frame (610) and the blocking vertical plates (611) are connected between two adjacent groups of arc-shaped plate members (612); there are four groups of arc-shaped plate members (612), one group of the feed frame (610), and three groups of the blocking vertical plates (611); the inner cavity of the feed frame (610) is connected to the central frame (521) and the feed port (69); the first-stage bracket (613) is connected to the feed frame (610) and the blocking vertical plates (611) respectively; the second-stage bracket (615) is slidably sleeved on the outer wall of the cylinder (614), and the second-stage bracket (615) is connected to the outer wall of the leaching box (64).

8. The device for extracting and separating precious metal palladium from waste catalysts according to claim 1, characterized in that: The circulating leaching module (6) further comprises a reinforcing ring (616), a reinforcing rod (617) and a roller (618); the reinforcing rod (617) is connected in a circular array to the bottom of the leaching box (64); the reinforcing ring (616) is slidably sleeved on the outer wall of the reinforcing rod (617); the bottom end of the reinforcing ring (616) is connected to the rotating plate (62); the roller (618) is connected in a circular array to the top of the bottom plate (2); and the top of the roller (618) is connected to the rotating plate (62).

Citation Information

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