Separation device and process for purifying silymarin

By designing a separation device that integrates the pneumatic generation mechanism, filter mechanism and airflow cleaning mechanism, the problem of easy clogging of filter media and lack of dynamic cleaning mechanism in the traditional silymarin purification process is solved, and efficient silymarin purification and automated production are achieved.

CN120094282AActive Publication Date: 2025-06-06PANJIN TIANYUAN PHARMA

Patent Information

Application Number
CN202510592442.8
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-05-09
Publication Date
2025-06-06
Estimated Expiration
2045-05-09

AI Technical Summary

Technical Problem

In the traditional silymarin purification process, the filter media is prone to clogging, reducing separation efficiency, and lacking a dynamic cleaning mechanism, resulting in a decrease in filtration efficiency with running time and increasing maintenance costs.

Method used

A separation device including a pneumatic generator, a filter mechanism and an airflow cleaning mechanism is designed. Through the synergistic action of the water flow impeller and the airflow impeller, the industrial filter cloth is driven to rotate and clean with mechanical power and airflow, thereby achieving efficient filtration of silymarin stock liquid and separation of impurities.

Benefits of technology

It improves the efficiency and product purity of silymarin purification, reduces maintenance costs and energy consumption, and realizes the full process automation of filtration, slag discharge and cleaning.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention relates to the technical field of silymarin purification and separation, and discloses a separation device and process for silymarin purification, the device comprises a separation box assembly, the input end of the separation box assembly is communicated with a liquid conveying assembly, and the liquid conveying assembly is communicated with an external silymarin stock solution pipeline; a pneumatic generating mechanism is arranged on the outer side of the liquid conveying assembly and comprises a water flow impeller and an air flow impeller. According to the device, firstly, a dynamic filtering mechanism automatically forms an inclined concave surface, enlarges gaps of filter cloth and guides solid particles to be directionally discharged in the filtering process through telescopic industrial filter cloth and a rolling sliding block structure, the problem of filter screen blockage is effectively solved, continuous production is guaranteed, secondly, a self-cleaning system is combined with a knocking mechanism and an airflow back-blowing technology, and the production efficiency is improved. The impeller is driven by the flowing energy of the stock solution, the filter cloth is hammered alternately, airflow is blown synchronously, fluff thorns embedded into fibers are thoroughly removed, impurity residues are avoided, and the filter cloth cleaning efficiency is remarkably improved.
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Description

Technical Field

[0001] The invention relates to the technical field of silymarin purification and separation, and more specifically, to a separation device and process for silymarin purification. Background Art

[0002] Silymarin is an important medicinal ingredient extracted from the milk thistle plant and is widely used in the treatment of liver diseases and in the field of anti-oxidation. The purification process requires separating the active ingredient from the broken plant tissue. Traditional processes usually use multi-stage filtration and centrifugal separation, but the leaf fragments, seed particles and fine burrs mixed in the milk thistle stock solution can easily cause clogging of the filter medium and reduce separation efficiency. Especially in continuous production processes, frequent filter cloth cleaning and shutdown maintenance seriously restrict production capacity. At the same time, residual impurities may affect the purity of the final product.

[0003] Existing filtration devices mostly use fixed filter screens or static centrifugal structures, which are difficult to adapt to the complex characteristics of solid particles in milk thistle concentrate, especially leaf fuzz, which is easy to embed into the gaps between filter cloth fibers, causing irreversible blockage and reducing the filtration and purification efficiency. At the same time, manual disassembly and cleaning are required, which increases time costs. In addition, traditional equipment lacks a dynamic cleaning mechanism and cannot simultaneously remove attached impurities during the filtration process, resulting in a significant decrease in filtration efficiency with running time. Some improvement plans attempt to introduce mechanical vibration to assist in slag removal, but it is difficult to balance the vibration intensity and the life of the filter cloth, and the problem of retention of fine fuzz cannot be solved. Summary of the invention

[0004] In order to overcome the above technical problems, the present invention proposes a separation device and process for purifying silymarin.

[0005] The present invention achieves the above-mentioned purpose through the following technical solutions:

[0006] A separation device for purifying silymarin, comprising a separation box assembly, wherein the input end of the separation box assembly is connected to an infusion assembly, wherein the infusion assembly is connected to an external silymarin stock solution pipeline, wherein a pneumatic generating mechanism is arranged on the outside of the infusion assembly, wherein the pneumatic generating mechanism comprises a water flow impeller and an air flow impeller, wherein the silymarin stock solution flows inside the infusion assembly and drives the water flow impeller to rotate to generate mechanical power, and the water flow impeller drives the air flow impeller to rotate to generate wind power;

[0007] A central axis is provided in the middle of the separation box assembly, and a filtering mechanism is provided on the outer side of the central axis, wherein the filtering mechanism comprises an industrial filter cloth, and the industrial filter cloth is used to filter the silymarin stock solution;

[0008] A striking mechanism is arranged at a position outside the central axis near the top of the filter mechanism, and the striking mechanism comprises a first hammer and a second hammer. The mechanical power generated by the water flow impeller drives the first hammer and the second hammer to alternately and reciprocally strike the top of the industrial filter cloth.

[0009] An airflow cleaning mechanism connected to a pneumatic generating mechanism is disposed on the top of the separation box assembly. The wind force generated by the airflow impeller drives the airflow to flow through the airflow cleaning mechanism and is transported to the interior of the separation box assembly, thereby performing airflow cleaning on the upper and lower end surfaces of the industrial filter cloth.

[0010] As a further optimization scheme of the present invention, the separation box assembly includes a filter separation box body, a liquid collecting bucket is provided at the bottom of the filter separation box body, a top plate is provided at the top of the filter separation box body, the central axis passes through the middle of the top of the top plate to the interior of the filter separation box body, the central axis is connected to the top plate bearing seat, the inner wall of the filter separation box body is provided with a slide groove, and the outer side of the filter separation box body is provided with a discharge port, the slide groove is an annular structure, and the slide groove stretches downward near the discharge port.

[0011] As a further optimization scheme of the present invention, the infusion component includes a solution delivery tube and an arc-shaped guide plate, the arc-shaped guide plate is arranged on one side of the inner wall of the solution delivery tube, the output end of the solution delivery tube is connected to the input end of the filtering and separation box, and a baffle corresponding to the output end of the solution delivery tube is arranged at the inner wall of the filtering and separation box, and the baffle is used to limit and block the silymarin stock solution delivered by the solution delivery tube to the inside of the filtering and separation box.

[0012] As a further optimization scheme of the present invention, the pneumatic generating mechanism also includes an air collecting cylinder fastened to the top of the solution delivery pipe, the bottom diameter of the air collecting cylinder is larger than the width of the solution delivery pipe, a support shaft penetrating into the solution delivery pipe is arranged in the middle of the interior of the air collecting cylinder, a water flow impeller is arranged on the outside of the support shaft located inside the solution delivery pipe, one side of the water flow impeller corresponds to the arc guide plate, an air flow impeller is arranged on the top of the support shaft, and a transmission unit connected to the central shaft is arranged on the outside of the support shaft.

[0013] As a further optimization scheme of the present invention, the airflow cleaning mechanism includes a main air pipe interconnected with the air collecting cylinder, and the output ends of the main air pipe are respectively provided with a first air pipe and a second air pipe, the output end of the first air pipe extends to the interior of the filter separation box and is provided with an upper exhaust port located at the top of the industrial filter cloth, and the output end of the second air pipe extends to the interior of the filter separation box and is provided with a lower exhaust port located at the bottom of the industrial filter cloth, and the output ends of the lower exhaust port and the upper exhaust port both correspond to the discharge port.

[0014] As a further optimization scheme of the present invention, the filtering mechanism also includes a mounting ring sleeved on the outside of the central axis, the outer side of the mounting ring is uniformly universally connected to a support frame, the end of the support frame away from the mounting ring is universally connected to a support block, a synchronous connection joint is connected between two adjacent groups of support blocks, the synchronous connection joint is ductile, and a rolling slider that rolls and displaces inside the slide groove is provided at a position of the support block close to the inside of the filter separation box, the support frame and the top of the support block jointly support an industrial filter cloth, and the inner side of the industrial filter cloth is sealed and connected to the outer side of the mounting ring, the industrial filter cloth is elastic, and the industrial filter cloth near the discharge port is stretched downward by the guiding action of the rolling slider to form a concave structure obliquely downward, and the output end of the concave structure corresponds to the discharge port.

[0015] As a further optimization scheme of the present invention, the knocking mechanism also includes a supporting ring sleeved on the outside of the central axis, and a guide groove is provided on the outside of the supporting ring. The guide groove is a continuous wavy groove structure that fits the outer wall of the supporting ring.

[0016] As a further optimization scheme of the present invention, two groups of supporting slide bars are symmetrically arranged at the bottom of the top plate near the outer side of the supporting sleeve ring, and the outer sides of the two groups of supporting slide bars are respectively sleeved with a first slide bar and a second slide bar of symmetrical structure, and the first slide bar and the second slide bar are provided with a limiting protrusion matched with the guide groove on the side close to the supporting sleeve ring, and the limiting protrusions respectively drive the first slide bar and the second slide bar to be displaced up and down, and the first slide bar and the second slide bar are both provided with a rack on the side away from the supporting sleeve ring.

[0017] As a further optimization scheme of the present invention, a support frame is arranged at the bottom of the top plate near the first slider and the second slider, a mounting shaft is arranged at the bottom of the support frame, two groups of symmetrically distributed first hammers and second hammers are arranged on the outer side of the mounting shaft, and the first hammers and the second hammers are respectively provided with incomplete gears at positions near the second slider and the first slider, and the incomplete gears are meshed with the rack.

[0018] A separation process for purifying silymarin, the separation process method steps are as follows:

[0019] Step 1: First, the infusion component is connected to the external silymarin stock solution pipeline, and the silymarin stock solution is transported to the interior of the separation box component for filtration;

[0020] Step 2: Then, the flow force of the silymarin stock solution drives the water flow impeller to generate mechanical power, and simultaneously drives the air flow impeller to rotate to generate wind power;

[0021] Step 3: The industrial filter cloth is driven to rotate by mechanical power to transport the filtered milk thistle residue to the output end of the separation box assembly for discharge;

[0022] Step 4: Use mechanical power to drive the first hammer and the second hammer to hammer the surface of the industrial filter cloth to separate the pubescent thorns of the milk thistle leaves;

[0023] Step 5: The wind force generated by the rotation of the airflow impeller blows the discharge of the silymarin residue, thereby completing the separation and purification process of silymarin.

[0024] The beneficial effects of the present invention are:

[0025] 1. The present invention improves the efficiency of silymarin purification and product purity through the coordinated action of the filtering mechanism, the airflow cleaning mechanism and the knocking mechanism, while reducing the maintenance cost and energy consumption. First, the dynamic filtering mechanism automatically forms an oblique concave surface during the filtering process through the retractable industrial filter cloth and the rolling slider structure, expands the filter cloth gap and guides the solid particles to be discharged in a directional manner, effectively solves the filter blockage problem and ensures continuous production. Secondly, the self-cleaning system combines the knocking mechanism with the airflow backblowing technology, uses the energy of the original liquid flow to drive the impeller, alternately hammers the filter cloth and simultaneously sprays the airflow, thoroughly removes the fluff burrs embedded in the fiber, avoids impurity residues, and significantly improves the filter cloth cleaning efficiency.

[0026] 2. The present invention adopts an energy recycling design. The mechanical power and airflow generated by the raw liquid flow driving the impeller are directly used in the filtering and cleaning process. No external power source is required, and the energy-saving effect is outstanding. The airflow cleaning system cooperates with the upper and lower two-way exhaust ports to enhance the impurity stripping effect, ensure the permeability of the filter cloth pores, and the silymarin liquid purity after separation is higher. The overall structural modular design takes into account stability and adaptability, and can flexibly adjust the filter cloth morphology and airflow intensity, which is suitable for complex working conditions of different batches of raw materials. The device realizes the full process automation of filtration, slag discharge, and cleaning, greatly reduces manual intervention, and provides an efficient and sustainable solution for the large-scale production of silymarin. BRIEF DESCRIPTION OF THE DRAWINGS

[0027] Figure 1 It is a three-dimensional structural schematic diagram of the present invention;

[0028] Figure 2 is a three-dimensional structural cross-sectional view of the present invention;

[0029] Figure 3 It is an enlarged cross-sectional schematic diagram of the internal structure of the filtering and separating box in the present invention;

[0030] Figure 4 It is an enlarged schematic diagram of the connection structure between the infusion assembly and the pneumatic generating mechanism in the present invention;

[0031] Figure 5 It is an enlarged cross-sectional view of the internal structure of the infusion assembly and the pneumatic generating mechanism in the present invention;

[0032] Figure 6 It is an enlarged schematic diagram of the connection structure between the filter mechanism and the central axis in the present invention;

[0033] Figure 7 It is a bottom view schematic diagram of the filtering mechanism in the present invention;

[0034] Figure 8 It is a schematic diagram of the decomposed structure of the filtering mechanism in the present invention;

[0035] Fig. 9 yes Figure 8 A schematic diagram of the structure at A;

[0036] Fig.10 It is an enlarged schematic diagram of the connection structure between the airflow cleaning mechanism and the knocking mechanism in the present invention;

[0037] Fig.11 It is an enlarged schematic diagram of the connection structure of the knocking mechanism in the present invention;

[0038] Fig.12 It is an enlarged schematic diagram of the connection structure at the second sliding block in the present invention.

[0039] In the figure:

[0040] 100, separation box assembly; 200, central axis; 300, airflow cleaning mechanism; 400, pneumatic generating mechanism; 500, infusion assembly; 600, filtering mechanism; 700, knocking mechanism;

[0041] 101, filtering and separating box; 102, liquid collecting hopper; 103, top plate; 104, baffle; 105, chute; 106, discharge port;

[0042] 301, first gas pipeline; 302, main gas pipeline; 303, second gas pipeline; 304, lower exhaust port; 305, upper exhaust port;

[0043] 401, gas collecting cylinder; 402, transmission unit; 403, water flow impeller; 404, support shaft; 405, air flow impeller;

[0044] 501, solution delivery pipe; 502, arc guide plate;

[0045] 601, industrial filter cloth; 602, rolling slider; 603, synchronous connection joint; 604, support block; 605, mounting ring; 606, support frame;

[0046] 701, support collar; 702, guide groove; 703, support frame; 704, first hammer; 705, second hammer; 706, mounting shaft; 707, support slide bar; 708, rack; 709, first slider; 710, incomplete gear; 711, limit protrusion; 712, second slider. DETAILED DESCRIPTION

[0047] The subject matter described herein will now be discussed with reference to example embodiments. It should be understood that the discussion of these embodiments is only to enable those skilled in the art to better understand and implement the subject matter described herein, and the functions and arrangements of the elements discussed may be changed without departing from the scope of protection of the contents of this specification. Each example may omit, replace or add various processes or components as needed. In addition, the features described relative to some examples may also be combined in other examples.

[0048] Example 1

[0049] like Figure 1 , Figure 2 , Figure 3 As shown, a separation device for purifying silymarin includes a separation box assembly 100, the separation box assembly 100 includes a filtering and separating box body 101, a liquid collecting hopper 102 is arranged at the bottom of the filtering and separating box body 101, a top plate 103 is arranged at the top of the filtering and separating box body 101, a central axis 200 penetrates from the middle of the top of the top plate 103 to the inside of the filtering and separating box body 101, the central axis 200 is connected to the bearing seat of the top plate 103, a chute 105 is arranged on the inner wall of the filtering and separating box body 101, and a discharge port 106 is arranged on the outer side of the filtering and separating box body 101, the chute 105 is an annular structure, and the chute 105 is stretched downward at a position close to the discharge port 106;

[0050] like Figures 1 to 5 As shown, the input end of the separation box assembly 100 is connected with the infusion assembly 500, and the infusion assembly 500 is connected with the external silymarin stock solution pipeline. The infusion assembly 500 includes a solution delivery pipe 501 and an arc guide plate 502. The arc guide plate 502 is arranged on one side of the inner wall of the solution delivery pipe 501. The output end of the solution delivery pipe 501 is connected with the input end of the filtration separation box 101. A baffle 104 corresponding to the output end of the solution delivery pipe 501 is arranged at the inner wall position of the filtration separation box 101. The baffle 104 is used to limit and block the silymarin stock solution delivered to the inside of the filtration separation box 101 by the solution delivery pipe 501;

[0051] The pneumatic generating mechanism 400 is arranged outside the infusion component 500, and the pneumatic generating mechanism 400 includes a water flow impeller 403 and an air flow impeller 405. The silymarin stock solution flows inside the infusion component 500 and drives the water flow impeller 403 to rotate to generate mechanical power, and the water flow impeller 403 drives the air flow impeller 405 to rotate to generate wind power.

[0052] The pneumatic generating mechanism 400 further includes a gas collecting cylinder 401 which is fastened to the top of the solution delivery pipe 501, the bottom diameter of the gas collecting cylinder 401 is larger than the width of the solution delivery pipe 501, a support shaft 404 which penetrates into the solution delivery pipe 501 is arranged in the middle of the gas collecting cylinder 401, a water flow impeller 403 is arranged on the outside of the support shaft 404 which is located inside the solution delivery pipe 501, one side of the water flow impeller 403 corresponds to the arc-shaped guide plate 502, an air flow impeller 405 is arranged on the top of the support shaft 404, and a transmission unit 402 which is transmission-connected to the central shaft 200 is arranged on the outside of the support shaft 404;

[0053] like Figures 1 to 9 As shown, a central axis 200 is disposed in the middle of the separation box assembly 100, and a filtering mechanism 600 is disposed outside the central axis 200. The filtering mechanism 600 includes an industrial filter cloth 601, and the industrial filter cloth 601 is used to filter the silymarin stock solution;

[0054] The filtering mechanism 600 also includes a mounting ring 605 sleeved on the outside of the central axis 200, the outside of the mounting ring 605 is uniformly connected to a support frame 606 by a universal joint, and one end of the support frame 606 away from the mounting ring 605 is universally connected to a support block 604, and a synchronous connection section 603 is connected between two adjacent groups of support blocks 604, and the synchronous connection section 603 is ductile, and a rolling slider 602 that rolls and displaces inside the slide groove 105 is provided at a position of the support block 604 close to the inner side of the filtering and separation box 101, and the top of the support frame 606 and the support block 604 jointly supports an industrial filter cloth 601, and the inner side of the industrial filter cloth 601 is sealed and connected to the outer side of the mounting ring 605, and the industrial filter cloth 601 is elastic, and the industrial filter cloth 601 near the discharge port 106 is guided by the rolling slider 602 to form a concave structure that is inclined downward, and the output end of the concave structure corresponds to the discharge port 106;

[0055] like Figures 1 to 12 As shown, a striking mechanism 700 is provided at a position outside the central axis 200 near the top of the filter mechanism 600, and the striking mechanism 700 includes a first hammer 704 and a second hammer 705. The mechanical power generated by the water flow impeller 403 drives the first hammer 704 and the second hammer 705 to alternately reciprocate and hammer the top of the industrial filter cloth 601;

[0056] The knocking mechanism 700 also includes a support ring 701 sleeved on the outside of the central axis 200, and a guide groove 702 is arranged on the outside of the support ring 701. The guide groove 702 is a continuous wavy groove structure that fits the outer wall of the support ring 701. Two groups of support slide bars 707 are symmetrically arranged at the bottom of the top plate 103 near the outside of the support ring 701. The outsides of the two groups of support slide bars 707 are respectively sleeved with a first slider 709 and a second slider 712 of symmetrical structure. The first slider 709 and the second slider 712 are provided with a limiting protrusion 711 that is adapted to the guide groove 702 on the side close to the support ring 701. The limiting protrusion 711 drives the first slider 709 and the second slider 712 to be in an up-and-down dislocation distribution state respectively. The first slider 709 and the second slider 712 are both provided with a rack 708 on the side away from the support ring 701.

[0057] A support frame 703 is provided at the bottom of the top plate 103 near the first slider 709 and the second slider 712. A mounting shaft 706 is provided at the bottom of the support frame 703. Two sets of symmetrically distributed first hammers 704 and second hammers 705 are provided on the outer side of the mounting shaft 706. Incomplete gears 710 are provided at the positions of the first hammer 704 and the second hammer 705 near the second slider 712 and the first slider 709 respectively. The incomplete gear 710 is meshed with the rack 708.

[0058] The top of the separation box assembly 100 is provided with an airflow cleaning mechanism 300 which is interconnected with the pneumatic generating mechanism 400. The wind force generated by the airflow impeller 405 drives the airflow to flow through the airflow cleaning mechanism 300 and transport it to the interior of the separation box assembly 100, thereby performing airflow cleaning on the upper and lower end surfaces of the industrial filter cloth 601.

[0059] The airflow cleaning mechanism 300 includes a main air pipe 302 interconnected with the air collecting cylinder 401, and the output ends of the main air pipe 302 are respectively provided with a first air pipe 301 and a second air pipe 303. The output end of the first air pipe 301 extends to the interior of the filtering and separating box 101 and is provided with an upper exhaust port 305 located on the top of the industrial filter cloth 601. The output end of the second air pipe 303 extends to the interior of the filtering and separating box 101 and is provided with a lower exhaust port 304 located at the bottom of the industrial filter cloth 601. The output ends of the lower exhaust port 304 and the upper exhaust port 305 both correspond to the discharge port 106.

[0060] The use process of the separation device for purifying silymarin proposed in this embodiment is as follows: when the device is in use, the silymarin stock solution is transported to the interior of the filtering and separating box 101 through the solution transport pipe 501, and the power of the flow of the silymarin stock solution drives the water flow impeller 403 to rotate to generate mechanical power. Through the guiding effect of the arc-shaped guide plate 502, the silymarin stock solution unidirectionally impacts one side of the water flow impeller 403, thereby driving the water flow impeller 403 to rotate;

[0061] The rotation of the water impeller 403 drives the support shaft 404 to rotate, thereby driving the airflow impeller 405 to rotate and disturb the airflow to flow upward, thereby generating wind force. At the same time, the rotation of the support shaft 404 drives the transmission unit 402 to rotate, thereby driving the central shaft 200 to rotate accordingly.

[0062] The silymarin stock solution transported to the inside of the filtration and separation box 101 through the solution transport pipe 501 is blocked by the baffle 104 and falls to the top of the industrial filter cloth 601 by its own gravity, so as to be filtered through the industrial filter cloth 601, so that the solid and liquid in the silymarin stock solution are separated. After the liquid containing silymarin is filtered through the industrial filter cloth 601, it is concentrated in the inside of the liquid collecting bucket 102 and directed out, while the solid particles such as the broken leaves and seeds of silymarin are retained on the top of the industrial filter cloth 601;

[0063] The rotation of the central shaft 200 drives the support collar 701 and the mounting ring 605 to rotate respectively, and the rotation of the mounting ring 605 drives the support frame 606, the support block 604, and the industrial filter cloth 601 to rotate accordingly, and the support block 604 drives the rolling slider 602 to roll and displace inside the slide 105. At the same time, as the industrial filter cloth 601 rotates, when the industrial filter cloth 601 with the solid particles such as broken leaves and seeds of milk thistle on the top rotates to the position of the clamping discharge port 106, the industrial filter cloth 601 is concave downward by the stretching and guiding action of the rolling slider 602 and the support block 604, thereby forming a concave structure obliquely downward, so that the solid particles such as broken leaves and seeds of milk thistle on the top of the industrial filter cloth 601 automatically slide to the position of the discharge port 106 for discharge;

[0064] When the industrial filter cloth 601 forms a concave structure downward, the industrial filter cloth 601 is stretched because the concave area is larger than the flat area, and thus the industrial filter cloth 601 is in a stretched state, and the synchronous adaptability of the synchronous connection section 603 is stretched at the same time;

[0065] As the support ring 701 rotates, the guide groove 702 rotates. The two groups of limit protrusions 711 are displaced up and down inside the guide groove 702, and the first slider 709 and the second slider 712 are moved back and forth alternately up and down. The first slider 709 and the second slider 712 are moved back and forth up and down, and the rack 708 is moved back and forth up and down by the first slider 709 and the second slider 712. Then, the two groups of meshing incomplete gears 710 are respectively driven to rotate by the two groups of racks 708, and the two groups of corresponding first hammers 704 and second hammers are respectively driven by the rotation of the incomplete gears 710. 705 alternately and reciprocally hammers the top of the industrial filter cloth 601. During the process of hammering the top of the industrial filter cloth 601, since the industrial filter cloth 601 is in a stretched state, the filter gap thereof is enlarged. The fluff burrs stuck in the filter gap are separated out by the inertia of the hammering. The fluff burrs stuck in the filter gap are kept in the upper position due to the inertia, and the industrial filter cloth 601 is displaced downward by the instantaneous hammering, thereby generating separation. Through the effect of the hammering, the separation function of the fluff burrs of the silymarin leaves contained in the silymarin stock solution during the filtration process of the industrial filter cloth 601 is realized;

[0066] Furthermore, the airflow generated by the disturbance of the airflow impeller 405 is transported to the positions of the lower exhaust port 304 and the upper exhaust port 305 through the first air delivery pipe 301, the main air delivery pipe 302, and the second air delivery pipe 303, and is located at the top position of the industrial filter cloth 601 through the upper exhaust port 305, so that the broken leaves and seeds of the milk thistle on the top of the industrial filter cloth 601 are blown by the airflow to the position of the discharge port 106 for discharge;

[0067] At the same time, the silybum leaf fluff separated from the industrial filter cloth 601 is affected by the airflow and discharged toward the position of the discharge port 106;

[0068] The airflow output from the upper exhaust port 305 blows upward from the bottom of the industrial filter cloth 601, and then cooperates with the first hammer 704 and the second hammer 705 to make the silymarin leaf hairs stuck in the filter gap of the industrial filter cloth 601 separate and move upward, so as to prevent the hairs from moving downward and merging into the silymarin liquid due to the increase of the filter gap.

[0069] At the same time, the airflow output from the upper exhaust port 305 cooperates with the airflow output from the lower exhaust port 304 to further promote the discharge of waste from the top of the industrial filter cloth 601;

[0070] During the up-and-down displacement of the first slider 709 and the second slider 712 , the stability of the up-and-down displacement structure of the first slider 709 and the second slider 712 is maintained by the support slide bar 707 .

[0071] Example 2

[0072] like Figure 1 , Figure 2 , Figure 6 , Fig.10 As shown, a separation process for purifying silymarin, the process steps are as follows:

[0073] Step 1: First, the infusion assembly 500 is connected to the external silymarin stock solution pipeline, and the silymarin stock solution is transported to the interior of the separation box assembly 100 for filtration;

[0074] Step 2: Then, the flow force of the silymarin stock solution drives the water flow impeller 403 to generate mechanical power, and simultaneously drives the air flow impeller 405 to rotate to generate wind power;

[0075] Step 3: The industrial filter cloth 601 is driven to rotate by mechanical power to transport the filtered milk thistle residue to the output end of the separation box assembly 100 for discharge;

[0076] Step 4: Using mechanical power to drive the first hammer 704 and the second hammer 705 to hammer the surface of the industrial filter cloth 601 to separate the spicules of the milk thistle leaves;

[0077] Step 5: The wind generated by the rotation of the airflow impeller 405 blows the discharge of the silymarin residue, thereby completing the separation and purification process of silymarin.

[0078] The above describes the specific implementation methods of the embodiments of the present invention, but the embodiments of the present invention are not limited to the above-mentioned specific implementation methods. The above-mentioned specific implementation methods are merely illustrative and not restrictive. Ordinary technicians in this field can also make many forms under the guidance of the embodiments of the present invention, all of which are protected by the embodiments of the present invention.

Claims

1. A separation device for purifying silymarin, characterized in that: The invention comprises a separation box assembly (100), wherein the input end of the separation box assembly (100) is connected to an infusion assembly (500), the infusion assembly (500) is connected to an external silymarin stock solution pipeline, and an air-generating mechanism (400) is arranged on the outside of the infusion assembly (500), wherein the air-generating mechanism (400) comprises a water flow impeller (403) and an air flow impeller (405), wherein the silymarin stock solution flows inside the infusion assembly (500) and drives the water flow impeller (403) to rotate to generate mechanical power, and drives the air flow impeller (405) to rotate through the water flow impeller (403) to generate wind power; A central axis (200) is disposed in the middle of the separation box assembly (100), and a filtering mechanism (600) is disposed outside the central axis (200). The filtering mechanism (600) comprises an industrial filter cloth (601), and the industrial filter cloth (601) is used to filter the silymarin stock solution; A striking mechanism (700) is provided at a position outside the central axis (200) near the top of the filtering mechanism (600), the striking mechanism (700) comprising a first hammer (704) and a second hammer (705), the mechanical power generated by the water flow impeller (403) drives the first hammer (704) and the second hammer (705) to alternately and reciprocally strike the top of the industrial filter cloth (601); An airflow cleaning mechanism (300) is provided on the top of the separation box assembly (100) and is interconnected with the pneumatic generating mechanism (400). The wind force generated by the airflow impeller (405) drives the airflow to flow through the airflow cleaning mechanism (300) and is transported to the interior of the separation box assembly (100), thereby performing airflow cleaning on the upper and lower end surfaces of the industrial filter cloth (601).

2. A separation device for purifying silymarin according to claim 1, characterized in that: The separation box assembly (100) comprises a filtering and separating box body (101), a liquid collecting hopper (102) is arranged at the bottom of the filtering and separating box body (101), a top plate (103) is arranged at the top of the filtering and separating box body (101), the central axis (200) penetrates from the middle of the top of the top plate (103) to the inside of the filtering and separating box body (101), the central axis (200) is connected to the bearing seat of the top plate (103), a slide groove (105) is arranged on the inner wall of the filtering and separating box body (101), and a discharge port (106) is arranged on the outer side of the filtering and separating box body (101), the slide groove (105) is an annular structure, and the slide groove (105) is stretched downward at a position close to the discharge port (106).

3. A separation device for purifying silymarin according to claim 2, characterized in that: The infusion assembly (500) comprises a solution delivery tube (501) and an arc-shaped guide plate (502); the arc-shaped guide plate (502) is arranged on one side of the inner wall of the solution delivery tube (501); the output end of the solution delivery tube (501) is connected to the input end of the filtration and separation box (101); a baffle (104) corresponding to the output end of the solution delivery tube (501) is arranged on the inner wall of the filtration and separation box (101); the baffle (104) is used to limit and block the silymarin stock solution delivered by the solution delivery tube (501) to the inside of the filtration and separation box (101).

4. A separation device for purifying silymarin according to claim 3, characterized in that: The pneumatic generating mechanism (400) further comprises a gas collecting cylinder (401) which is fastened to the top of the solution delivery pipe (501); the bottom diameter of the gas collecting cylinder (401) is larger than the width of the solution delivery pipe (501); a support shaft (404) which penetrates into the solution delivery pipe (501) is arranged in the middle of the gas collecting cylinder (401); a water flow impeller (403) is arranged on the outside of the support shaft (404) which is located inside the solution delivery pipe (501); one side of the water flow impeller (403) corresponds to the arc-shaped guide plate (502); an air flow impeller (405) is arranged on the top of the support shaft (404); and a transmission unit (402) which is transmission-connected to the central shaft (200) is arranged on the outside of the support shaft (404).

5. A separation device for purifying silymarin according to claim 4, characterized in that: The airflow cleaning mechanism (300) comprises a main air supply pipe (302) interconnected with the air collecting cylinder (401); the output end of the main air supply pipe (302) is respectively provided with a first air supply pipe (301) and a second air supply pipe (303); the output end of the first air supply pipe (301) extends to the interior of the filtering and separation box (101) and is provided with an upper exhaust port (305) located at the top of the industrial filter cloth (601); the output end of the second air supply pipe (303) extends to the interior of the filtering and separation box (101) and is provided with a lower exhaust port (304) located at the bottom of the industrial filter cloth (601); the output ends of the lower exhaust port (304) and the upper exhaust port (305) both correspond to the discharge port (106).

6. The separation device for purifying silymarin according to claim 2, characterized in that: The filtering mechanism (600) further comprises a mounting ring (605) sleeved on the outside of the central axis (200); the outside of the mounting ring (605) is uniformly connected to a support frame (606) by a universal joint; one end of the support frame (606) away from the mounting ring (605) is universally connected to a support block (604); two adjacent groups of the support blocks (604) are connected by a synchronous connection joint (603); the synchronous connection joint (603) is ductile; and the support block (604) is provided with a position close to the inside of the filtering and separation box (101). A rolling slider (602) rolls and displaces inside the slide groove (105), and the support frame (606) and the top of the support block (604) jointly support an industrial filter cloth (601), and the inner side of the industrial filter cloth (601) is sealed and connected to the outer side of the mounting ring (605), and the industrial filter cloth (601) is elastic, and the industrial filter cloth (601) at a position close to the discharge port (106) is guided by the rolling slider (602) to be stretched downward to form a concave structure inclined downward, and the output end of the concave structure corresponds to the discharge port (106).

7. A separation device for purifying silymarin according to claim 6, characterized in that: The striking mechanism (700) further comprises a supporting collar (701) sleeved on the outside of the central shaft (200), a guiding groove (702) being provided on the outside of the supporting collar (701), and the guiding groove (702) being a continuous wavy groove structure fitting the outer wall of the supporting collar (701).

8. The separation device for purifying silymarin according to claim 2, characterized in that: Two groups of support slide bars (707) are symmetrically arranged at the bottom of the top plate (103) near the outer side of the support ring (701), and the outer sides of the two groups of support slide bars (707) are respectively sleeved with a first slide bar (709) and a second slide bar (712) of symmetrical structure, and the first slide bar (709) and the second slide bar (712) are provided with a limiting protrusion (711) adapted to the guide groove (702) on the side close to the support ring (701), and the limiting protrusion (711) drives the first slide bar (709) and the second slide bar (712) to be in an up-and-down dislocation distribution state, and the first slide bar (709) and the second slide bar (712) are both provided with a rack (708) on the side away from the support ring (701).

9. A separation device for purifying silymarin according to claim 8, characterized in that: A support frame (703) is provided at the bottom of the top plate (103) near the first slider (709) and the second slider (712), a mounting shaft (706) is provided at the bottom of the support frame (703), two groups of symmetrically distributed first hammers (704) and second hammers (705) are provided on the outer side of the mounting shaft (706), and the first hammers (704) and the second hammers (705) are respectively provided with incomplete gears (710) at positions near the second slider (712) and the first slider (709), and the incomplete gears (710) are meshed with the rack (708).

10. A separation process for purifying silymarin, using the separation device for purifying silymarin as claimed in claim 1, wherein the process steps are as follows: Step 1: First, the infusion assembly (500) is connected to an external silymarin stock solution pipeline, and the silymarin stock solution is transported to the interior of the separation box assembly (100) for filtration; Step 2: Then, the flow force of the silymarin stock solution drives the water flow impeller (403) to generate mechanical power, and simultaneously drives the air flow impeller (405) to rotate to generate wind power; Step 3: The industrial filter cloth (601) is driven to rotate by mechanical power to transport the filtered milk thistle residue to the output end of the separation box assembly (100) for discharge; Step 4: Using mechanical power to drive the first hammer (704) and the second hammer (705) to hammer the surface of the industrial filter cloth (601) to achieve the function of separating the pubescent thorns of the milk thistle leaves; Step 5: The wind generated by the rotation of the airflow impeller (405) blows the discharge of the silymarin residue, thereby completing the separation and purification process of silymarin.

Citation Information

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