Efficient homogenizing valve group, homogenizer and homogenizing method

Abstract

The invention relates to the technical field of micro-nano homogenizing and emulsifying equipment, and discloses a high-efficiency homogenizing valve group, a homogenizer and a homogenizing method.The high-efficiency homogenizing valve group comprises a valve body provided with a homogenizing channel, and the homogenizing channel is provided with a turbulent flow ring protruding in the radial direction; the homogenizing assembly is arranged in the homogenizing channel; the homogenizing assembly comprises a first valve element and a second valve element, the second valve element is provided with a homogenizing groove, the first valve element covers the second valve element, and the end wall of the first valve element and the homogenizing groove form a homogenizing cavity; the first valve element is provided with a feeding hole, the feeding hole is communicated with the homogenizing cavity and the inlet end of the homogenizing channel, the second valve element is provided with a discharging hole, and the discharging hole is communicated with the homogenizing cavity and the outlet end of the homogenizing channel; wherein the homogenizing groove comprises a confluence channel and a collision channel, the collision channel is communicated with the confluence channel, and the discharging hole is formed in the confluence channel; the width of the collision channel is larger than the depth of the collision channel, and the depth of the collision channel is smaller than 1 mm. According to the homogenizing valve group, the dispersing and crushing effects on fibrous raw materials can be improved.

Description

Technical Field

[0001] The present invention relates to the technical field of micro-nano homogenization emulsification equipment, and particularly relates to an efficient homogenization valve group, a homogenizer and a homogenization method. Background Art

[0002] Homogenizers are mainly used in industries such as biology, medicine, food, and chemical engineering for operations such as cell disruption, beverages, fine chemicals, and the preparation of liposomes, fat emulsions, nano-suspensions, microemulsions, lipid microspheres, emulsions, dairy products, large infusions, dyes, etc. Under the reciprocating motion of the plunger pump, the homogenizer sucks the fluid material into the high-pressure chamber and then pressurizes and transports the material to a homogenization valve group with a small gap. When the fluid passes through the small gap, the flow is blocked and a high pressure is formed, causing various substances in the fluid to undergo strong shearing, impact, cavitation explosion, turbulence and other effects, so that the fluid material after passing through the homogenization valve group is ultra-finely refined and evenly dispersed; however, at present, when the homogenizer is used for fibrous raw materials such as multi-walled carbon nanotubes, single-walled carbon nanotubes, bio-based nanofibrillated cellulose, cotton and linen fibers, viscose fibers, ceramic or glass inorganic fibers, and difficult-to-disperse raw materials such as graphene, there are still problems with poor dispersion and fragmentation effects. Summary of the Invention

[0003] The present invention aims to solve at least one of the technical problems existing in the prior art. For this reason, the present invention provides an efficient homogenization valve group that can improve the dispersion and fragmentation effects on fibrous raw materials.

[0004] The present invention also provides a homogenizer with the above-mentioned efficient homogenization valve group.

[0005] The efficient homogenization valve group according to the first aspect embodiment of the present invention includes: A valve body provided with a homogenization channel, and the homogenization channel is provided with a radially protruding turbulence ring; A homogenization component disposed in the homogenization channel; the homogenization component includes a first valve core and a second valve core. The second valve core is provided with a homogenization groove. The first valve core covers the second valve core, and the end wall of the first valve core and the homogenization groove form a homogenization chamber. The first valve core is provided with a feed hole, and the feed hole communicates the homogenization chamber and the inlet end of the homogenization channel. The second valve core is provided with a discharge hole, and the discharge hole communicates the homogenization chamber and the outlet end of the homogenization channel; Wherein, the homogenization groove includes a confluence channel and a collision channel. The collision channel communicates with the confluence channel, and the discharge hole is disposed in the confluence channel; the width of the collision channel is greater than the depth of the collision channel, and the depth of the collision channel is less than 1 mm.

[0006] The efficient homogenization valve group according to the embodiment of the present invention has at least the following beneficial effects: When the fluid solution flows forward through the homogeneous channel, a reverse backflow will be formed at the turbulence ring. The backflow solution impacts the forward-flowing solution to form turbulence, thereby achieving the preliminary shearing of the fluid solution. After the fluid solution enters the homogeneous chamber through the feed hole, the fluid solution undergoes a high-speed collision in the collision channel, thereby achieving the secondary high-speed shearing of the fluid solution, thereby enhancing the dispersion and fragmentation effects of the fibrous raw materials in the fluid solution. The depth of the collision channel is less than 1 mm, and the width of the collision channel is greater than the depth, which is convenient for the fibrous raw materials to collide at high speed in an unfolded posture, further enhancing the dispersion and fragmentation effects of the fibrous raw materials.

[0007] According to some embodiments of the present invention, the width W of the collision channel and the depth D of the collision channel satisfy: W≥3D.

[0008] According to some embodiments of the present invention, a plurality of the collision channels are provided, and the plurality of collision channels are arranged at intervals along the extending direction of the confluence channel; the extending direction of the confluence channel is perpendicular to the extending direction of the collision channel, and the plurality of collision channels are all communicated with the confluence channel.

[0009] According to some embodiments of the present invention, the homogeneous tank includes a collision area, and the collision area is provided with partition bars, and the partition bars divide the collision area into a plurality of the collision channels; The confluence channel penetrates through the middle of the collision area, the first valve core is provided with a plurality of feed holes, and the plurality of feed holes are all communicated with the collision area, and the plurality of feed holes are symmetrically arranged with respect to the confluence channel.

[0010] According to some embodiments of the present invention, the collision area includes a first edge and a second edge that are symmetrically arranged, and the first edge and the second edge are symmetrically arranged with respect to the confluence channel.

[0011] According to some embodiments of the present invention, the inner side wall of the turbulence ring is an arc surface.

[0012] According to some embodiments of the present invention, a homogenization module is further installed in the homogeneous channel. The homogenization module includes a through hole that penetrates through the homogenization module. The through hole includes a first flared section, a straight section, and a second flared section, and the straight section communicates the first flared section and the second flared section; Along the radial direction of the homogenization module, the inner diameters of the first flared section and the second flared section gradually increase outward along the straight section, and the first flared section and the second flared section cooperate to form the turbulence ring.

[0013] According to some embodiments of the present invention, along the direction of the material flow channel in the homogeneous channel, a plurality of the turbulence rings are arranged in parallel in the homogeneous channel, and the inner diameters of the plurality of turbulence rings increase in sequence.

[0014] The homogenizer according to the second aspect embodiment of the present invention includes a separation device and the above-mentioned homogenizing valve group. The separation device is used to receive the fluid solution discharged by the high-efficiency homogenizing valve group and separate the homogenizing raw materials in the fluid solution. Since the homogenizer includes the above-mentioned homogenizing valve group, it has at least all the beneficial effects of the homogenizing valve group.

[0015] The homogenizing method according to the third aspect embodiment of the present invention is applicable to the above-mentioned homogenizer. The homogenizing method includes the following steps: Input a fluid solution to the high-efficiency homogenizing valve group for homogenizing operation and cycle a set number of times; The high-efficiency homogenizing valve group outputs the fluid solution to the separation device for separation operation; Among them, the fluid solution is mixed by raw materials, a liquid solvent and a supercritical carbon dioxide solvent, and the raw materials and the supercritical carbon dioxide solvent account for 0.1% to 99.9% of the total volume of the fluid solution; In terms of specific surface area ratio, in the fluid solution, the ratio of the specific surface area of the supercritical carbon dioxide solvent to the specific surface area of the raw materials is 0.1 to 30; In terms of volume ratio, in the fluid solution, the ratio of the volume of the supercritical carbon dioxide solvent to the volume of the raw materials is 0.1 to 50.

[0016] The additional aspects and advantages of the present invention will be partially given in the following description, partially become obvious from the following description, or be understood through the practice of the present invention. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] The following further describes the present invention with reference to the drawings and embodiments, where: Figure 1 is a schematic structural diagram of the homogenizing valve group according to the first aspect embodiment of the present invention; Figure 2 is Figure 1 a cross-sectional view of the homogenizing component in Figure 3 is Figure 2 a front view of the first valve core of the homogenizing component in Figure 4 is Figure 2 a front view of the second valve core of the homogenizing component in Figure 5 is Figure 1 a cross-sectional view of the first embodiment of the homogenizing module in Figure 6 is Figure 1 a cross-sectional view of the second embodiment of the homogenizing module in

[0018] Reference numerals in the drawings: Valve body 100, homogeneous channel 110, turbulence ring 111; Homogeneous component 200, first valve core 210, feed hole 211, second valve core 220, discharge hole 221, homogeneous groove 222, collision channel 2221, confluence channel 2222, collision area 230, first edge 231, second edge 232, partition strip 240; Homogeneous module 300, through hole 310, first flared section 311, straight section 312, second flared section 313. Specific embodiments

[0019] The embodiments of the present invention will be described in detail below. The examples of the embodiments are shown in the drawings, where the same or similar reference numerals denote the same or similar elements or elements with the same or similar functions throughout. The embodiments described below with reference to the drawings are exemplary and are only used to explain the present invention and should not be construed as a limitation of the present invention.

[0020] In the description of the present invention, it should be understood that the orientation or positional relationship indicated by terms such as up and down is based on the orientation or positional relationship shown in the drawings. It is only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus should not be construed as a limitation of the present invention.

[0021] In the description of the present invention, "a plurality of" means more than two. If the first and second are described, it is only for the purpose of distinguishing technical features and should not be construed as indicating or implying relative importance or implicitly indicating the quantity of the indicated technical features or implicitly indicating the sequence relationship of the indicated technical features.

[0022] In the description of the present invention, unless otherwise clearly defined, words such as "set", "installed", and "connected" should be understood in a broad sense. Those skilled in the art can reasonably determine the specific meanings of the above words in the present invention in combination with the specific content of the technical solution.

[0023] Refer to Figures 1 to 6, the high-efficiency homogenization valve group according to the embodiment of the first aspect of the present invention includes a valve body 100 and a homogenization component 200. The valve body 100 is provided with a homogenization channel 110, and the homogenization channel 110 is provided with a turbulator ring 111 protruding radially; the homogenization component 200 is arranged in the homogenization channel 110; the homogenization component 200 includes a first valve core 210 and a second valve core 220. The second valve core 220 is provided with a homogenization groove 222, the first valve core 210 covers the second valve core 220, and the end wall of the first valve core 210 and the homogenization groove 222 form a homogenization cavity; the first valve core 210 is provided with a feed hole 211, the feed hole 211 communicates the homogenization cavity and the inlet end of the homogenization channel 110, and the second valve core 220 is provided with a discharge hole 221, the discharge hole 221 communicates the homogenization cavity and the outlet end of the homogenization channel 110; wherein, the homogenization groove 222 includes a confluence channel 2222 and a collision channel 2221, the collision channel 2221 is communicated with the confluence channel 2222, and the discharge hole 221 is arranged in the confluence channel 2222. When the fluid solution flows forward through the homogenization channel 110, a reverse backflow will be formed at the turbulator ring 111, and the backflow solution collides with the forward-flowing solution to form turbulence, thereby realizing the preliminary shearing of the fluid solution; after the fluid solution enters the homogenization cavity through the feed hole 211, the fluid solution undergoes high-speed collision in the collision channel 2221, thereby realizing the secondary high-speed shearing of the fluid solution, thereby improving the dispersion and fragmentation effects of the fibrous raw materials in the fluid solution. The above-mentioned forward flow of the fluid solution through the homogenization channel 110 means that the fluid solution flows from the inlet end to the outlet end of the homogenization channel 110, and the reverse backflow refers to Figure 1 as shown.

[0024] Further, in this embodiment, the depth of the collision channel 2221 is preferably less than 1 mm, and the width of the collision channel 2221 is greater than the depth, which is convenient for the fibrous raw materials or graphite raw materials to collide at high speed in an unfolded state, improving the dispersion and fragmentation effects of the raw materials. The depth of the collision channel 2221 can be specifically set according to the ratio of the length of the raw material to be homogenized to the pipe diameter. For example, if the raw material to be homogenized is graphite powder and graphene is obtained through the homogenization valve group of this embodiment, the depth of the collision channel 2221 can be preferably set to a set multiple of the particle size of the graphite particles, for example, set to 3 to 10 times the particle size depth of the graphite particles. The width W of the collision channel 2221 and the depth D of the collision channel 2221 preferably satisfy: W≥3D. The depth D of the collision channel 2221 refers to Figure 2 as shown, and the width W of the collision channel 2221 refers to Figure 4 as shown. By setting the width W of the collision channel 2221 to be significantly greater than the depth D, during the collision, it is difficult for the fibrous raw materials to stack in the depth direction of the collision channel 2221, and it is convenient for the fibrous raw materials to unfold, so that the fibrous raw materials or graphite raw materials can more achieve "head-on" collisions, improving the dispersion and fragmentation effects of the fibrous raw materials and graphite raw materials.

[0025] Currently, most of the homogenizing equipment on the market adopts a cylindrical collision channel 2221. In order to increase the crushing effect on the fibrous raw materials and graphite raw materials and make the fibrous raw materials and graphite raw materials achieve a "tit-for-tat" collision, it is necessary to reduce the inner diameter of the collision channel 2221 as much as possible. However, the reduction in the inner diameter of the collision channel 2221 can easily lead to blockage of the collision channel 2221, affecting the crushing efficiency and crushing effect. The flat collision channel 2221 in this embodiment is not easy to be blocked, and can achieve a good crushing effect on the fibrous raw materials and graphite raw materials, greatly improving the crushing efficiency.

[0026] Reference Figure 4 As shown, in the embodiment of the present invention, there are multiple collision channels 2221, and the multiple collision channels 2221 are arranged at intervals along the extension direction of the confluence channel 2222. The extension direction of the confluence channel 2222 is perpendicular to the extension direction of the collision channel 2221. The confluence channel 2222 passes through the multiple collision channels 2221, and the multiple collision channels 2221 are all connected to the confluence channel 2222. Specifically, the homogenizing tank 222 includes a collision area 230, and the collision area 230 is provided with a dividing bar 240. The dividing bar 240 is used to separate the collision area 230 into multiple collision channels 2221. The multiple collision channels 2221 can improve the collision efficiency of the raw materials, thereby reducing the number of times the raw materials circulate in the homogenizing component 200. There are multiple discharge holes 221 to facilitate the rapid discharge of the fluid solution. The specific positions of the multiple discharge holes 221 can be specifically set according to actual conditions. Exemplarily, refer to Figure 4 As shown, there are two discharge holes 221 which are respectively arranged at the two ends of the converging channel 2222, so that the raw materials can flow out after sufficient collision.

[0027] Further, the first valve core 210 is provided with a plurality of feed holes 211, and the plurality of feed holes 211 are all connected to the collision area 230, and the plurality of feed holes 211 are symmetrically arranged about the confluence channel 2222. Figure 3 As shown, there are two feed holes 211, which are respectively connected to the collision area 230 and are preferably as far away from the collision channel 2221 as possible, so as to facilitate the uniform distribution of the fluid solution into the multiple collision channels 2221; the multiple feed holes 211 are symmetrically arranged about the confluence channel 2222, so as to facilitate the uniform distribution of the fluid solution into the collision channels 2221 on both sides of the confluence channel 2222, thereby improving the dispersion and crushing effects of the fluid solution.

[0028] In the embodiment of the present invention, the collision area 230 includes a first edge 231 and a second edge 232 symmetrically arranged, the first edge 231 and the second edge 232 are symmetrically arranged about the confluence channel 2222, the confluence channel 2222 is arranged in the middle of the collision area 230, and both ends of the confluence channel 2222 extend out of the collision area 230.Figure 4 As shown, after the homogeneous valve group of this embodiment is installed, the two feed holes 211 of the first valve core 210 respectively correspond to the middle positions of the first edge 231 and the second edge 232. Preferably, both the first edge 231 and the second edge 232 are arc-shaped edges, and both ends of the first edge 231 and the second edge 232 extend towards the direction close to the confluence channel 2222, so as to facilitate the rapid flow of the fluid solution towards the collision channels 2221 near both ends of the confluence channel 2222, and can make the amount distribution of the fluid solution in the multiple collision channels 2221 uniform.

[0029] Refer to Figure 1 As shown, there are multiple turbulence rings 111 in the embodiment of the present invention. The multiple turbulence rings 111 are arranged at intervals along the material flow path direction of the homogeneous channel 110, and the multiple turbulence rings 111 can enhance the turbulence effect on the fluid solution in the homogeneous channel 110. The cross-sectional shape of the turbulence ring 111 can be set according to the actual situation. For example, it can be set as an arc or a rectangle, that is, the inner side wall of the turbulence ring 111 can be set as an arc surface or a plane. Preferably, the inner side wall of the turbulence ring 111 is set as an arc surface to reduce the loss of dynamic potential energy caused by turbulence, reduce the damage to the inner side wall of the turbulence ring 111 caused by turbulence, and at the same time increase the reverse flow rate and speed caused by the turbulence ring 111.

[0030] Furthermore, the inner diameters of the multiple turbulence rings 111 in this embodiment can be set to be equal or unequal. For example, along the material flow path direction of the homogeneous channel 110, the inner diameters of the multiple turbulence rings 111 can increase in sequence, or the inner diameters of the multiple turbulence rings 111 can decrease in sequence, or the inner diameter of the middle turbulence ring 111 is larger than the inner diameters of the turbulence rings 111 at both ends, or the inner diameter of the middle turbulence ring 111 is smaller than the inner diameters of the turbulence rings 111 at both ends, etc. Through experiments, in order to further enhance the turbulence effect caused by the turbulence ring 111, preferably along the material flow path direction of the homogeneous channel 110, the inner diameters of the multiple turbulence rings 111 increase in sequence.

[0031] It can be conceived that along the material flow path direction of the homogeneous channel 110, the turbulence ring 111 can be arranged at the front end or the rear end of the homogeneous component 200 as shown in Figure 1 . That is, the fluid solution can first flow through the turbulence ring 111 and then enter the homogeneous component 200, or it can first flow through the homogeneous component 200 and then enter the turbulence ring 111, which is not limited in this embodiment.

[0032] In the embodiment of the present invention, the turbulence ring 111 can be arranged on the inner side wall of the homogeneous channel 110, or can be formed by a detachable homogeneous module 300, so as to facilitate changing the inner diameter of the turbulence ring 111 according to different raw materials to be broken. Refer to Figure 5 、 Figure 6As shown, the homogenization module 300 includes a through-hole 310 passing through the homogenization module 300. The through-hole 310 includes a first flared section 311, a straight section 312, and a second flared section 313. The straight section 312 connects the first flared section 311 and the second flared section 313. Along the radial direction of the homogenization module 300, the inner diameters of the first flared section 311 and the second flared section 313 gradually increase outward along the straight section 312. The first flared section 311 and the second flared section 313 cooperate to form a turbulence ring 111. By changing the shapes and sizes of the first flared section 311 and the second flared section 313, different types of turbulence rings 111 can be formed. For example, the cross-sections of the first flared section 311 and the second flared section 313 can be set as Figure 5 the arc shown or Figure 6 the straight line shown, Figure 5 the inner side walls of the first flared section 311 and the second flared section 313 shown in can also be concave or convex, which is not limited in this embodiment.

[0033] Furthermore, the inner diameter of the straight section 312 of the through-hole 310 can be set to be equal to or unequal to the inner diameter of the homogenization channel 110. For example, the inner diameter of the straight section 312 can be set to be greater than or less than or equal to the inner diameter of the homogenization channel 110, which is not limited in this embodiment.

[0034] In the embodiment of the present invention, the number of the homogenization modules 300 can be set according to the actual situation, and the installation position of the homogenization modules 300 can also be set according to the actual situation. For example, along the material flow path direction of the homogenization channel 110, multiple homogenization modules 300 can be arranged in parallel at the front end of the homogenization assembly 200, or multiple homogenization modules 300 can be arranged in parallel at the rear end of the homogenization assembly 200, or homogenization modules 300 are provided at both the front and rear ends of the homogenization assembly 200.

[0035] The homogenizer according to the second aspect embodiment of the present invention includes a separation device and the above-mentioned homogenization valve group. The separation device is used to receive the fluid solution discharged by the high-efficiency homogenization valve group and separate the homogenized raw materials in the fluid solution. The separation device includes a separation and extraction tank. The inside of the separation and extraction tank is at normal pressure or low pressure. After the fluid solution after high-efficiency homogenization enters the separation and extraction tank, it will become a micro-nano aerosol state. The supercritical carbon dioxide liquid returns to the gaseous state after returning to normal pressure or low pressure. The carbon dioxide gas enters the recovery, compression and recycling device after filtration, and the remaining materials become finished products through hierarchical recovery. Since the homogenizer includes the above-mentioned homogenization valve group, it has at least all the beneficial effects of the homogenization valve group, which will not be elaborated here.

[0036] The homogenization method according to the third aspect embodiment of the present invention is applicable to the above-mentioned homogenizer. The homogenization method includes the following steps: Input a fluid solution into the high-efficiency homogenization valve group for homogenization operation and cycle for a set number of times; The high-efficiency homogeneous valve group outputs a fluid solution to a separation device for separation and extraction operations; Among them, the fluid solution is composed of raw materials, liquid solvents, dispersants, and supercritical carbon dioxide solvents. For example, for the production of graphene, the raw material can be graphite powder; the liquid solvent can be one or more of inorganic solvents such as water, organic solvents such as alcohols and toluenes, and can also include materials that prevent the raw materials from agglomerating again after dispersion, such as polyvinylpyrrolidone, carboxymethyl cellulose, polyvinylidene fluoride, polystyrene butadiene, etc. The appropriate liquid solvent can be selected according to different raw materials. Preferably, the particle size of the liquid solvent used is close to that of the raw material, so as to facilitate the impact on the raw material and enable the raw material to obtain better intercalation, dispersion, and fragmentation effects. Currently, for the dispersion and fragmentation of fibrous raw materials and difficult-to-disperse raw materials such as graphene, usually only supercritical carbon dioxide solvent is mixed with the raw materials. For example, in a patent application for a method for preparing graphene by supercritical fluid explosion method with the application number CN201510994548.7, only supercritical carbon dioxide and graphite powder are mixed as the fluid solution. In this application, by adding a liquid solvent to the fluid solution, according to the calculation of specific surface area and volume ratio, under the condition of meeting the dosage for good dispersion of the raw materials, the addition amount of the supercritical carbon dioxide solvent can be reduced, thereby reducing the preparation cost, reducing the investment in the recovery system, and improving the separation and extraction efficiency of the raw materials; the liquid solvent is difficult to be compressed, and using a liquid solvent with a particle size close to that of the raw material can significantly improve the dispersion and fragmentation effects on the raw materials. In the fluid solution, preferably, the raw materials and the supercritical carbon dioxide solvent account for 0.1% to 99.9% of the total volume of the fluid solution; if in terms of specific surface area ratio, in the fluid solution, preferably, the ratio of the specific surface area of the supercritical carbon dioxide solvent to the specific surface area of the raw materials is 0.1 to 30; if in terms of volume ratio, in the fluid solution, preferably, the ratio of the volume of the supercritical carbon dioxide solvent to the volume of the raw materials is 0.1 to 50.

[0037] Furthermore, by adding a liquid solvent to the fluid solution, the use of the supercritical carbon dioxide solvent can be reduced. The supercritical carbon dioxide solvent will be converted into a gas in the separation and extraction tank to facilitate the separation of the raw materials, and when the supercritical carbon dioxide is converted into a gas, a huge expansion will occur. Therefore, higher requirements are imposed on the structural strength of the separation device, and a larger container is required to store the gaseous carbon dioxide, resulting in higher manufacturing costs and maintenance costs of the equipment; in this embodiment, through a scientific formula, the use of supercritical carbon dioxide is minimized, the structural strength of the separation device can be appropriately reduced, and the volume of the container for storing the gaseous carbon dioxide can be reduced, thereby reducing the manufacturing costs and maintenance costs of the equipment.

[0038] In the description of this specification, the descriptions referring to terms such as "one embodiment", "some embodiments", "example", "specific example", or "some examples" mean that the specific features, structures, materials, or characteristics described in connection with the embodiment or example are included in at least one embodiment or example of the present invention. In this specification, the schematic representations of the above terms do not necessarily refer to the same embodiment or example. Moreover, the specific features, structures, materials, or characteristics described can be combined in a suitable manner in any one or more embodiments or examples. In addition, those skilled in the art can combine and combine the different embodiments or examples described in this specification.

[0039] The embodiments of the present invention have been described in detail above in conjunction with the accompanying drawings. However, the present invention is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present invention within the scope of knowledge possessed by those of ordinary skill in the art.

Claims

1. An efficient homogenization valve group, characterized in that, Including: A valve body is provided with a homogenization channel, and the homogenization channel is provided with a radially protruding turbulence ring; A homogenization assembly is arranged in the homogenization channel; the homogenization assembly includes a first valve core and a second valve core. The second valve core is provided with a homogenization groove. The first valve core covers the second valve core, and a homogenization cavity is formed between the end wall of the first valve core and the homogenization groove. The first valve core is provided with a feed hole, the feed hole communicates the homogenization cavity and the inlet end of the homogenization channel, the second valve core is provided with a discharge hole, and the discharge hole communicates the homogenization cavity and the outlet end of the homogenization channel; Wherein, the homogenization groove includes a confluence channel and a collision channel, the collision channel is communicated with the confluence channel, and the discharge hole is arranged in the confluence channel; the width of the collision channel is greater than the depth of the collision channel, and the depth of the collision channel is less than 1 mm.

2. The high-efficiency homogenizing valve group according to claim 1, characterized in that: The width W of the collision channel and the depth D of the collision channel satisfy: W≥3D.

3. The high-efficiency homogenizing valve group according to claim 1, characterized in that: A plurality of the collision channels are provided, and the plurality of collision channels are arranged at intervals along the extending direction of the confluence channel; the extending direction of the confluence channel is perpendicular to the extending direction of the collision channel, and the plurality of collision channels are all communicated with the confluence channel.

4. The high-efficiency homogenizing valve group according to claim 3, wherein: The homogenization groove includes a collision area, and the collision area is provided with a partition strip, and the partition strip divides the collision area into a plurality of the collision channels; The confluence channel penetrates through the middle of the collision area, the first valve core is provided with a plurality of feed holes, and the plurality of feed holes are all communicated with the collision area, and the plurality of feed holes are symmetrically arranged with respect to the confluence channel.

5. The high-efficiency homogenizing valve group according to claim 4, characterized in that: The collision area includes a first edge and a second edge which are symmetrically arranged, and the first edge and the second edge are symmetrically arranged with respect to the confluence channel.

6. The high-efficiency homogenization valve group according to claim 1, wherein: The inner side wall of the turbulence ring is an arc surface.

7. The high-efficiency homogenizing valve group according to claim 1, wherein: A homogenization module is further installed in the homogenization channel. The homogenization module includes a through hole penetrating through the homogenization module. The through hole includes a first flared section, a straight section and a second flared section, and the straight section communicates the first flared section and the second flared section; Along the radial direction of the homogenization module, the inner diameters of the first flared section and the second flared section gradually increase outward along the straight section, and the first flared section and the second flared section cooperate to form the turbulence ring.

8. The high-efficiency homogenizing valve group according to claim 1, wherein: Along the material flow path direction in the homogenization channel, a plurality of the turbulence rings are arranged in parallel in the homogenization channel, and the inner diameters of the plurality of turbulence rings increase in sequence.

9. A homogenizer, characterized in that: Including a separation device and the high-efficiency homogenization valve group according to any one of claims 1 to 8, wherein the separation device is used to receive the fluid solution discharged by the high-efficiency homogenization valve group and separate the homogenization raw material in the fluid solution.

10. A homogenization method applicable to the homogenizer according to claim 9, characterized in that, Including the following steps: Inputting a fluid solution into the high-efficiency homogenization valve group for homogenization operation and circulating for a set number of times; The high-efficiency homogenization valve group outputs the fluid solution to the separation device for separation and extraction operation; Wherein, the fluid solution is composed of a raw material, a liquid solvent and a supercritical carbon dioxide solvent, and the raw material and the supercritical carbon dioxide solvent account for 0.1% to 99.9% of the total volume of the fluid solution; In terms of specific surface area ratio, in the fluid solution, the ratio of the specific surface area of the supercritical carbon dioxide solvent to the specific surface area of the raw material is 0.1 to 30; Alternatively, in terms of volume ratio, in the fluid solution, the ratio of the volume of the supercritical carbon dioxide solvent to the volume of the raw material is 0.1 to 50.

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