Movable chemical analysis experiment device

Abstract

The invention discloses a movable chemical analysis experiment device, and relates to the technical field of nuclear power plant chemistry. Comprising a box body, a first section and a second section which are arranged in the box body, and a transition section arranged between the first section and the second section; the sample separation unit comprises a sample separation machine body and a sample receiver, the sample separation machine body and the sample receiver are arranged in a first interval, the sample bottle is arranged below the sample separation machine body, and the cleaning bottle is arranged on one side of the sample bottle; the second section comprises a sample treatment table, a fixed seat and a water tank arranged in the first section and the second section. The device can be used as a mobile on-site laboratory, does not occupy extra rooms, and ensures chemical analysis requirements during installation and debugging of engineering construction, the fixed seat can limit a large-scale instrument, the large-scale instrument is prevented from inclining or collapsing when the box body moves, and the working efficiency is improved by arranging the sample splitting machine body.

Description

Technical Field

[0001] The present invention relates to the technical field of nuclear power plant chemistry, in particular to a mobile chemical analysis experimental device. Background Art

[0002] During the construction of a nuclear power plant, due to the heavy pressure on the main construction schedule on site, the construction of various auxiliary systems has been delayed to varying degrees. In order to meet the chemical analysis needs during the installation and commissioning of the units, it is necessary to outsource chemical analysis or purchase and configure instruments and equipment to establish a temporary laboratory to quickly complete the analysis tasks and ensure the smooth progress of installation and commissioning.

[0003] For on-site flushing, debugging, and other tasks, the timeliness of chemical analysis is extremely important. Outsourced chemical analysis requires samples to be sent to external units for testing, which takes a long time and is only suitable for testing a small number of samples with ample time. The timeliness of outsourced analysis cannot be guaranteed. However, there are problems with building temporary laboratories: temporary laboratory sites are difficult to equip, and each room in the on-site construction has its specific purpose. Establishing a laboratory requires occupying the room, affecting the realization of the room's original function; establishing a temporary laboratory requires purchasing and configuring chemical analysis instruments, which increases investment and risks exceeding the budget; during the construction period, water, electricity, gas, and HVAC around the on-site rooms are all part of the later construction content, and the water, electricity, and gas of the temporary laboratory cannot be guaranteed, affecting the realization of the laboratory's function; continuous construction around the temporary laboratory allows dust to easily enter the laboratory, causing damage to laboratory instruments and equipment. Summary of the Invention

[0004] In view of the above problems existing in the existing mobile chemical analysis experimental device, the present invention is proposed.

[0005] Therefore, the present invention provides a mobile chemical analysis experimental device, the purpose of which is to solve the problem that temporary laboratory sites are difficult to equip.

[0006] In order to solve the above technical problems, the present invention provides the following technical solutions: a mobile chemical analysis experimental device, comprising an installation unit, including a box body, a first section and a second section arranged in the box body, and a transition section arranged between the first section and the second section; a sample separation unit, comprising a sample separation body and a sample receiver, the sample separation body and the sample receiver are arranged in the first section, a sample bottle is arranged below the sample separation body, and a cleaning bottle is arranged on one side of the sample bottle.

[0007] As a preferred solution of the mobile chemical analysis experimental device described in the present invention, the second section includes a sample processing table and a fixed seat, and a water tank arranged in the first section and the second section; the fixed seat, the sample separation body and the sample receiver are arranged on the sample processing table.

[0008] As a preferred solution of the mobile chemical analysis experimental device described in the present invention, the fixed seat includes a slider and a screw, a slide rail arranged on the upper surface of the fixed seat, a slider slidably connected in the slide rail, a screw passing through the upper center axis position of the slider, and a limit plate arranged on the external thread connection of the screw.

[0009] As a preferred solution of the mobile chemical analysis experimental device of the present invention, a plurality of fixing holes are distributed in an array on the bottom of the inner wall of the slide rail, and the lower end of the screw is spherical and movably connected in the fixing hole.

[0010] As a preferred solution of the mobile chemical analysis experimental device described in the present invention, the transition area includes an emergency material cabinet, a spirit level, a waste liquid collection box, two groups of desalted water pipes arranged on the waste liquid collection box, and the other ends of the two groups of desalted water pipes are respectively connected to the water tanks in the first area and the second area.

[0011] As a preferred solution of the mobile chemical analysis experimental device described in the present invention, the sample dividing body includes a rotating arm and a sample dividing needle, the rotating arm is provided with several groups, the array is distributed to form a rectangular structure, and is evenly distributed on the sample dividing body, the sample dividing needle is rotatably connected to the lower end of the rotating arm, and a storage cavity is provided at the lower end of the sample dividing needle.

[0012] As a preferred solution of the mobile chemical analysis experimental device described in the present invention, the storage chamber includes a sealing piston, the sealing piston is arranged in the storage chamber, and its outer wall is tightly fitted with the inner wall of the storage chamber, a power rod is arranged on the sealing piston, a driving spring is arranged on the power rod, and an electric push rod is arranged on the driving spring.

[0013] As a preferred solution of the mobile chemical analysis experimental device of the present invention, the power rod is in the shape of an "I" character, with upper and lower ends in the shape of discs, and its diameter is equal to that of the sample dividing needle.

[0014] As a preferred solution of the mobile chemical analysis experimental device of the present invention, the needle head arranged at the lower end of the sample dividing needle is conical in shape, and the maximum diameter of the upper part thereof is smaller than the diameter of the sealing piston.

[0015] As a preferred solution of the mobile chemical analysis experimental device of the present invention, the cleaning bottle includes cleaning water and dry air, the cleaning water is arranged in the cleaning bottle, and the dry air is arranged at the cleaning bottle mouth.

[0016] The beneficial effects of the present invention are as follows: it can be used as a mobile on-site laboratory without occupying additional rooms, ensuring the chemical analysis needs during engineering construction, installation and commissioning, and the fixed seat can limit the position of large instruments, so that when the box is moved, it will not tilt or collapse, and by configuring a sample separation body, the work efficiency is improved. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following briefly introduces the drawings required for use in the description of the embodiments. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work.

[0018] Figure 1 It is a schematic diagram of the overall structure of the mobile chemical analysis experimental device of the present invention.

[0019] Figure 2 It is a structural schematic diagram of the fixing seat in the mobile chemical analysis experimental device of the present invention.

[0020] Figure 3 It is a structural schematic diagram of the fixing seat in the mobile chemical analysis experimental device of the present invention.

[0021] Figure 4 This is a schematic structural diagram of the sample separation unit in the mobile chemical analysis experimental device of the present invention.

[0022] Figure 5 The figure is a schematic diagram of the structure of the sample separation unit in the mobile chemical analysis experimental device of the present invention.

[0023] Figure 6 The figure is a schematic diagram of the structure of the sample separation unit in the mobile chemical analysis experimental device of the present invention.

[0024] Figure 7 The figure is a schematic diagram of the structure of the sample separation unit in the mobile chemical analysis experimental device of the present invention. DETAILED DESCRIPTION

[0025] In order to make the above-mentioned objects, features and advantages of the present invention more obvious and easy to understand, the specific embodiments of the present invention are described in detail below with reference to the accompanying drawings.

[0026] In the following description, many specific details are set forth to facilitate a full understanding of the present invention. However, the present invention may also be implemented in other ways different from those described herein. Those skilled in the art may make similar generalizations without violating the connotation of the present invention. Therefore, the present invention is not limited to the specific embodiments disclosed below.

[0027] Secondly, the term "one embodiment" or "embodiment" herein refers to a specific feature, structure, or characteristic that may be included in at least one implementation of the present invention. The phrase "in one embodiment" appearing in various places throughout this specification does not necessarily refer to the same embodiment, nor does it individually or selectively refer to an embodiment that is mutually exclusive of other embodiments.

[0028] Furthermore, the present invention is described in detail with reference to schematic diagrams. For ease of illustration, when describing the embodiments of the present invention, cross-sectional views illustrating device structures may be partially enlarged and not to scale. Furthermore, the schematic diagrams are merely illustrative and should not limit the scope of protection of the present invention. Furthermore, in actual production, the three-dimensional dimensions of length, width, and depth should be included.

[0029] Example 1, with reference to Figure 1 - Figure 3 This is the first embodiment of the present invention, which provides a mobile chemical analysis laboratory device, including a housing 101 measuring 6000×3000×2800mm. Housing 101 is divided into a first compartment 102 on the left and right, a second compartment 103, and a transition compartment 104 in the middle. These three areas are connected by an access door. The second compartment 103 is the anion analysis area, primarily conducting anion liquid chromatography analysis. The first compartment 102 is the cation analysis area, primarily conducting atomic absorption cation analysis. The transition compartment 104 is a preparatory area for entering the first and second compartments 102 and 103, primarily used for changing clothes, configuring auxiliary equipment, and shielding from external influences. Each experimental area is equipped with a sample processing table 102a. The laboratory cabinet is 900mm high and 600mm wide. All experimental instruments are placed on the sample processing table 102a. The lower portion of the cabinet is equipped with a cabinet and a drawer for storing laboratory reagents, consumables, and other supplies.

[0030] The experimental area is equipped with a large analytical instrument fixing seat 102b, which is made of iron and has a heavy weight. Its main function is to provide stability and prevent the fixing seat 102b from sliding on the sample processing table 102a. Its weight and material help to keep the fixing seat 102b stable when the large instrument is placed or used. A track is provided on the fixing seat 102b. The slider 102b-1 is slidably connected in the track, so that the slider 102b-1 can move along the fixing seat 102b. In this way, the position of the slider 102b-1 can be adjusted to adapt to instruments of different sizes. There is a circular hole on the slider 102b-1, and a screw 102b-2 is movably connected in the circular hole. There are several fixing holes 102b-5 distributed in an array at the bottom of the inner wall of the track. The screw 102b-2 passes through the slider 102b-1 and is movably connected in the fixing hole 102b-5, and the screw 1 The bottom of 02b-2 is spherical, and the spherical shape helps the screw 102b-2 to automatically align with the fixing hole 102b-5, because the distance from any point of the sphere to the center of the sphere is equal, which makes it easier for the screw 102b-2 to find the center of the fixing hole 102b-5 when inserted. A limit plate 102b-4 is threadedly connected to the outside of the screw 102b-2 above the slider 102b-1. By rotating the limit plate 102b-4, its height can be adjusted to support large instruments. The design of the limit plate 102b-4 allows the user to adjust the support height as needed to accommodate instruments of different heights. The provision of multiple fixing seats 102b can provide all-round protection for large instruments and is used to fix large analytical instruments such as ion chromatographs to prevent large analytical instruments from sliding during transportation and use.

[0031] The experimental area is equipped with a demineralized water pipe 104d and a tap water pipe, with a water tank 102c located below. Below this tank 102c is a temporary water tank and water purifier, which can serve as a temporary water source to meet analytical water needs when external water is unavailable. The experimental area is also equipped with constant temperature and humidity air conditioning and dust-proof windows to ensure that the laboratory temperature and humidity range is 20% to 70%.

[0032] The transition area is provided with a box 101 door as a personnel entrance and exit passage, and an emergency material cabinet 104a is provided to store emergency materials for experiments. At the same time, a waste liquid collection box 104c is provided at the bottom of the cabinet. The water tank size is 1500×20×2000mm to collect waste water during the experiment. A liquid level gauge for the waste liquid collection box 104c is also provided in the transition area to monitor the waste liquid collection situation in real time.

[0033] Example 2, reference Figure 4 - Figure 7, which is the second embodiment of the present invention. This embodiment is different from the first embodiment in that: the sample separation unit 200 includes a sample separation body 201 and a sample receiver 202, the sample separation body 201 and the sample receiver 202 are arranged in the first section 102, a sample bottle 203 is arranged below the sample separation body, and a cleaning bottle 204 is arranged on one side of the sample bottle 203.

[0034] Furthermore, the rotating arms 201a are provided with several groups arranged in a rectangular array and evenly distributed on the sample divider body 201. This allows the sample divider body 201 to process multiple samples simultaneously, improving experimental efficiency and processing capacity. The sample divider needle 201b is rotatably connected to the lower end of the rotating arm 201a, and is used to directly contact the sample and perform the sample division operation to precisely control the distribution of the sample.

[0035] Storage chamber 201c includes a sealing piston 201c-1, a power rod 201c-2, a drive spring 201c-3, and an electric push rod 201c-4. These components work together to control the storage and release of samples. Sealing piston 201c-1 is positioned within storage chamber 201c, with its outer wall tightly fitting the inner wall. It controls the intake and discharge of samples by moving up and down within storage chamber 201c. When the piston moves upward, it expels air or sample from storage chamber 201c; when it moves downward, it draws in sample. Power rod 201c-2, the component that transmits power, has its lower end fixedly connected to sealing piston 201c-1. Power rod 201c-2 is shaped like an I, with disc-shaped upper and lower ends, and its diameter equal to that of sample dividing needle 201b. This allows the power rod 201c-2 to be tightly coupled with the sample needle 201b, ensuring efficient power transmission. The "I"-shaped structure also provides additional stability and support. The electric push rod 201c-4 is the power source for the entire system. Driven by a motor, it converts electrical energy into linear motion, thereby pushing the power rod 201c-2. A drive spring 201c-3 is provided between the electric push rod 201c-4 and the power rod 201c-2. This acts as a buffer and reset when the electric push rod 201c-4 pushes the power rod 201c-2. The drive spring 201c-3 absorbs some of the impact force and helps the power rod 201c-2 return to its initial position when the electric push rod 201c-4 stops working.

[0036] After the electric push rod 201c-4 receives the control signal, the motor starts working, pushing the power rod 201c-2 forward or backward. The movement of the power rod 201c-2 drives the sealing piston 201c-1 to move in the storage chamber 201c, thereby controlling the storage and release of the sample. When the sample needs to be released, the electric push rod 201c-4 pushes the power rod 201c-2 to make the sealing piston 201c-1 drop, and the sample is released through the needle 201c-5 of the sample dividing needle 201b. When the sample release needs to be stopped, the electric push rod 201c-4 stops working, and the driving spring 201c-3 helps the power rod 201c-2 and the sealing piston 201c-1 return to their initial positions.

[0037] Furthermore, the cleaning bottle 204 includes cleaning water 204a and dry air 204b, which are used to clean and dry the sample dividing needle 201b during the experiment to prevent cross contamination and ensure the purity of the sample.

[0038] During use, the electric push rod 201c-4 and the drive spring 201c-3 are used to move the sealing piston 201c-1 to the bottom of the storage chamber 201c so as to load the sample. The sample is injected into the storage chamber 201c until the sample fills the storage chamber 201c. The electric push rod 201c-4 is operated to make the sealing piston 201c-1 rise, close the opening of the storage chamber 201c, and ensure the sealing of the sample. The rotating arm 201a is rotated to move the sample needle 201b to the position where the sample needs to be distributed. The electric push rod 201c-4 is controlled to make the sealing piston 201c-1 descend, thereby pushing the sample through the needle 201c-5 of the sample needle 201b. When the needle 201c-5 of the sample needle 201b contacts the target container The device continues to control the sealing piston 201c-1 to descend, releases an appropriate amount of sample, and transfers the sample from the storage chamber 201c to the target position by precisely controlling the movement of the electric push rod 201c-4 and the sealing piston 201c-1. After the sampling operation is completed, immerse the sampling needle 201b in the cleaning water 204a in the cleaning bottle 204 for cleaning. Then, use the dry air 204b at the mouth of the cleaning bottle 204 to dry the sampling needle 201b to remove moisture and residue. Repeat the operation. If multiple samples need to be sampled, repeat the steps until all samples are correctly distributed. After completing all sampling operations, clean and dry the sampling needle 201b and the storage chamber 201c, and then store them in an appropriate location for next use.

[0039] The remaining structures are the same as those of Example 1.

[0040] It is important to note that the construction and arrangement of the present application shown in a number of different exemplary embodiments are merely illustrative. Although only a few embodiments are described in detail in this disclosure, it should be readily understood by those who refer to this disclosure that many modifications are possible (e.g., the size, scale, structure, shape, and proportion of various elements, as well as parameter values (e.g., temperature, pressure, etc.), mounting arrangements, use of materials, color, changes in orientation, etc.) without departing substantially from the novel teachings and advantages of the subject matter described in this application. For example, an element shown as integrally formed may be composed of multiple parts or elements, the position of the element may be inverted or otherwise changed, and the nature, number, or position of the discrete elements may be altered or changed. Therefore, all such modifications are intended to be included within the scope of the present invention. The order or sequence of any process or method steps may be changed or reordered according to alternative embodiments. In the claims, any "means plus function" clause is intended to cover the structure described herein that performs the function, and is not only structurally equivalent but also equivalent structures. Other replacements, modifications, changes, and omissions may be made in the design, operating conditions, and arrangement of the exemplary embodiments without departing from the scope of the present invention. Therefore, the invention is not limited to the specific embodiments, but extends to various modifications that still fall within the scope of the appended claims.

[0041] Additionally, in order to provide a concise description of exemplary embodiments, all features of an actual embodiment (i.e., those features that are not relevant to the best mode presently contemplated for carrying out the invention or those that are not relevant to implementing the invention) may not be described.

[0042] It should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention and are not intended to limit the present invention. Although the present invention has been described in detail with reference to the preferred embodiments, those skilled in the art should understand that the technical solutions of the present invention may be modified or replaced by equivalents without departing from the spirit and scope of the technical solutions of the present invention, which should all be included in the scope of the claims of the present invention.

Claims

1. A mobile chemical analysis experimental device, characterized in that: include, The installation unit (100) comprises a box (101), a first section (102) and a second section (103) disposed in the box (101), and a transition section (104) disposed between the first section (102) and the second section (103); The sample separation unit (200) comprises a sample separation body (201) and a sample receiver (202), the sample separation body (201) and the sample receiver (202) being arranged in a first section (102), a sample bottle (203) being arranged below the sample separation body (201), and a cleaning bottle (204) being arranged on one side of the sample bottle (203).

2. The mobile chemical analysis experimental device according to claim 1, characterized in that: The second section (103) includes a sample processing station (102a) and a fixing seat (102b), and a water tank (102c) arranged in the first section (102) and the second section (103); The fixing seat (102b), the sample separation body (201) and the sample receiver (202) are arranged on the sample processing platform (102a).

3. The mobile chemical analysis experimental device according to claim 2, characterized in that: The fixing seat (102b) comprises a slider (102b-1) and a screw rod (102b-2), a slide rail (102b-3) arranged on the upper surface of the fixing seat (102b), a limiting disk (102b-4) arranged on the slider (102b-1) and slidably connected to the slide rail (102b-3), a screw rod (102b-2) passing through the upper middle axis position of the slider (102b-1), and an external threaded connection of the screw rod (102b-2).

4. The mobile chemical analysis experimental device according to claim 3, characterized in that: A plurality of fixing holes (102b-5) are distributed in an array on the bottom of the inner wall of the slide rail (102b-3); the lower end of the screw rod (102b-2) is spherical and movably connected in the fixing hole (102b-5).

5. The mobile chemical analysis experimental device according to claim 4, characterized in that: The transition zone (104) includes an emergency supply cabinet (104a), a level meter (104b), a waste liquid collection box (104c), two groups of desalted water pipes (104d) arranged on the waste liquid collection box (104c), and the other ends of the two groups of desalted water pipes (104d) are respectively connected to the water tanks (102c) in the first zone (102) and the second zone (103).

6. The mobile chemical analysis experimental device according to claim 5, characterized in that: The sample dividing body (201) comprises a rotating arm (201a) and a sample dividing needle (201b); the rotating arm (201a) is provided with a plurality of groups, which are arranged in an array to form a rectangular structure and are evenly distributed on the sample dividing body (201); the sample dividing needle (201b) is rotatably connected to the lower end of the rotating arm (201a); and a storage cavity (201c) is provided at the lower end of the sample dividing needle (201b).

7. The mobile chemical analysis experimental device according to claim 6, characterized in that: The storage chamber (201c) comprises a sealing piston (201c-1), the sealing piston (201c-1) is arranged in the storage chamber (201c), and its outer wall is tightly fitted with the inner wall of the storage chamber (201c), a power rod (201c-2) arranged on the sealing piston (201c-1), a driving spring (201c-3) arranged on the power rod (201c-2), and an electric push rod (201c-4) arranged on the driving spring (201c-3).

8. The mobile chemical analysis experimental device according to claim 7, characterized in that: The power rod (201c-2) is in the shape of an "I" character, with the upper and lower ends being disc-shaped, and its diameter is equal to that of the sample dividing needle (201b).

9. The mobile chemical analysis experimental device according to claim 8, characterized in that: The needle (201c-5) is arranged at the lower end of the sample dividing needle (201b), and the needle (201c-5) is conical in shape, and the maximum diameter of the upper part thereof is smaller than the diameter of the sealing piston (201c-1).

10. The mobile chemical analysis experimental device according to claim 9, characterized in that: The cleaning bottle (204) comprises cleaning water (204a) and dry air (204b), wherein the cleaning water (204a) is arranged in the cleaning bottle (204), and the dry air (204b) is arranged at the mouth of the cleaning bottle (204).

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