Three-stage nano oxygen injection system for oxygen-carrying nano bubble water and preparation method of oxygen-carrying nano bubble water

Abstract

The invention discloses a three-stage nano oxygen injection system for oxygen-carrying nano bubble water and a preparation method of the three-stage nano oxygen injection system. The three-stage nano oxygen injection system comprises a water source input unit, a pretreatment module, a Venturi oxygen injection device, a high-pressure homogenization module, an ultrasonic nanocrystallization module, a bubble stabilizing tank, a quality detection module and a filling output module. According to the three-stage nano oxygen injection system and the preparation method thereof, through an innovative multi-stage bubble dissolving technology, the solubility and stability of oxygen in water are greatly improved, and the problems of low dissolving efficiency, unstable bubbles and the like in a traditional oxygen water technology are solved. By simplifying the production process and reducing the production cost, the method can be applied to production of healthy drinks on a large scale, meets the requirements of consumers for efficient oxygen supplement and health functions, and has wide market prospects and good commercial values.

Description

Technical Field

[0001] The present invention relates to the technical field of water oxygenation, and more particularly to a three-stage nano-oxygen injection system for oxygen-carrying nano-bubble water and a preparation method thereof. Background Art

[0002] With the increasing demand for healthy drinking water, functional sports water, medical and health care, and beauty products, oxygen-carrying nanobubble water has attracted widespread attention due to its microparticle size, stable oxygen dissolution, and high bioavailability. However, existing preparation technologies suffer from numerous challenges, including difficulty controlling bubble size, which cannot be consistently maintained within the nanoscale range; low oxygen injection efficiency and insufficient oxygen utilization; poor system stability, high equipment complexity, and unstable operation; and a lack of integrated control over the process chain, resulting in a low level of production line automation.

[0003] Therefore, there is an urgent need for an oxygen-carrying nanobubble water preparation system with scientific structure, high process integration and strong intelligent control capability to improve product quality and industrial feasibility. Summary of the Invention

[0004] The main purpose of this invention is to provide a three-stage nano-oxygen injection system for oxygen-carrying nanobubble water and its preparation method, which are used for the production of oxygen-carrying nanobubble water. This system utilizes multi-stage nanobubble generation and injection technology to effectively increase the solubility of oxygen in water and ensure the stability and sustained release of dissolved oxygen, thus meeting the demand for efficient dissolved oxygen in various fields.

[0005] To achieve the above objectives, the present invention provides a three-stage nano-oxygen injection system for oxygen-carrying nano-bubble water, comprising:

[0006] Water source input unit, providing initial pure water and connecting to the pretreatment system;

[0007] The pretreatment module filters, dechlorinates, and adjusts the temperature of the water to ensure that the water entering the system meets the quality standards;

[0008] The Venturi oxygen injection device uses the Venturi effect to introduce high-purity oxygen into the flowing water, completing the first-stage mixing and coarse oxygen injection;

[0009] The high-pressure homogenization module refines the gas-liquid mixture to micron level through high-pressure shearing, achieving secondary crushing and homogenization;

[0010] The ultrasonic nano-crystallization module performs three-level ultrasonic oscillation treatment in the frequency range of 20 to 100 kHz to further nano-crystallize the bubbles;

[0011] The bubble stabilization tank uses the principles of static pressure and slow flow to maintain bubble suspension and uniform distribution;

[0012] The quality detection module is equipped with dissolved oxygen concentration analyzer, particle size detector and other equipment to achieve online quality monitoring;

[0013] The filling output module packages the qualified sparkling water into finished product containers in a quantitative manner.

[0014] Preferably, the system is also provided with an integrated intelligent control center, which is connected to multiple sets of sensors and performs closed-loop adjustment on core parameters such as Venturi oxygen injection rate, homogenization pressure, and ultrasonic frequency through an automatic feedback adjustment algorithm, thereby achieving precise control and stable operation of the entire process.

[0015] Preferably, the sensors include a temperature sensor, a pressure sensor, an oxygen content sensor, and a gas-liquid ratio sensor.

[0016] Also included is a method for preparing a three-stage nano-oxygen injection system for oxygen-carrying nano-bubble water, comprising the following steps:

[0017] (1) Purify the water source and adjust the temperature to the set range;

[0018] (2) The water source introduces pure oxygen into the Venturi device to achieve first-level oxygen injection and mixing;

[0019] (3) After the first stage of oxygen injection and mixing, it enters the high-pressure homogenizer and undergoes secondary nano-shearing at 40-120 MPa;

[0020] (4) After the secondary nano-shearing, it enters the ultrasonic module and completes the tertiary nano-bubble generation at a frequency of 20-100 kHz;

[0021] (5) After the third-level nanobubbles are generated, they are introduced into a bubble stabilization tank for static absorption to improve bubble stability;

[0022] (6) After completion, online detection of oxygen content and bubble size;

[0023] (7) Filling and output are carried out after meeting the standards.

[0024] Compared with the prior art, the present invention has the following advantages:

[0025] 1. Multi-stage oxygen injection structure design: The three-stage nano-oxygen injection method (Venturi oxygen injection, high-pressure homogenization, and ultrasonic nano-injection) works synergistically to make the dispersed particle size of oxygen in water smaller and the distribution more uniform, significantly improving the bubble stability and dissolved oxygen retention capacity.

[0026] 2. Controllable bubble size: The bubble size generated is stably controlled between 10 and 100 nanometers, effectively extending the suspension time of bubbles in water, enhancing the bioavailability of water and the freshness of taste.

[0027] 3. Significantly improved oxygen content: Through system coordination and closed-loop control, the dissolved oxygen content of the produced sparkling water can reach 30-65 mg / L, which is more than three times higher than all traditional methods, meeting the requirements of high-end functional drinking water and medical and health care markets.

[0028] 4. Intelligent and precise control: Equipped with a sensor cluster and control algorithm, it can monitor key parameters such as temperature, pressure, oxygen content, and gas-liquid ratio in real time, achieve dynamic adjustment and automatic operation, and improve system stability and production consistency.

[0029] 5. High process integration: The system has a compact structure and a high degree of modularity, which facilitates equipment integration, maintenance and process upgrades, and has good prospects for industrialization and market application.

[0030] 6. Wide range of applications: The system is suitable for oxygen-carrying drinking water, functional beverages, high-dissolved oxygen water for aquaculture, medical oxygen water flushing fluid and other fields, and has broad commercial application potential. BRIEF DESCRIPTION OF THE DRAWINGS

[0031] Figure 1 The accompanying drawing is a flow chart of the present invention. DETAILED DESCRIPTION

[0032] The present invention discloses a three-stage nano-oxygen injection system for oxygen-carrying nano-bubble water, comprising:

[0033] Water source input unit, providing initial pure water and connecting to the pretreatment system;

[0034] The pretreatment module filters, dechlorinates, and adjusts the temperature of the water to ensure that the water entering the system meets the quality standards;

[0035] The Venturi oxygen injection device uses the Venturi effect to introduce high-purity oxygen into the flowing water, completing the first-stage mixing and coarse oxygen injection;

[0036] The high-pressure homogenization module refines the gas-liquid mixture to micron level through high-pressure shearing, achieving secondary crushing and homogenization;

[0037] The ultrasonic nano-crystallization module performs three-level ultrasonic oscillation treatment in the frequency range of 20 to 100 kHz to further nano-crystallize the bubbles;

[0038] The bubble stabilization tank uses the principles of static pressure and slow flow to maintain bubble suspension and uniform distribution;

[0039] The quality detection module is equipped with dissolved oxygen concentration analyzer, particle size detector and other equipment to achieve online quality monitoring;

[0040] The filling output module packages the qualified sparkling water into finished product containers in a quantitative manner.

[0041] The system also features an integrated intelligent control center connected to multiple sensors, including temperature, pressure, oxygen content, and gas-to-liquid ratio sensors. An automatic feedback control algorithm provides closed-loop regulation of key parameters such as the Venturi oxygen injection rate, homogenization pressure, and ultrasonic frequency, enabling precise control and stable operation throughout the entire process.

[0042] This application is the first to connect three oxygen injection and nano-processing technologies, namely Venturi oxygen injection, high-pressure homogenization, and ultrasonic nano-processing, into a unified system to achieve layered nano-processing, significantly improving bubble stability and oxygen dissolution efficiency.

[0043] The system can stably control the bubble particle size within the range of 10 to 100 nm. Through the synergistic effect of triple processing technology, it has industry-leading bubble particle size uniformity and long-term suspension performance.

[0044] Through a three-stage coordinated oxygen injection and stabilization mechanism, the system can consistently produce highly oxygenated water at concentrations of 30 to 65 mg / L, far exceeding the standard for ordinary sparkling water. Utilizing multi-parameter online sensing (temperature, pressure, gas-liquid ratio, particle size, and oxygen content) coupled with built-in algorithms, the system enables real-time control, adaptive adjustment, and remote intelligent management of the entire process. Its clear structural layout and integrated system as standard modules make it suitable for industrial mass production, rapid deployment, and customized applications.

[0045] Also included is a method for preparing a three-stage nano-oxygen injection system for oxygen-carrying nano-bubble water, comprising the following steps:

[0046] (1) Purify the water source and adjust the temperature to the set range;

[0047] (2) The water source introduces pure oxygen into the Venturi device to achieve first-level oxygen injection and mixing;

[0048] (3) After the first stage of oxygen injection and mixing, it enters the high-pressure homogenizer and undergoes secondary nano-shearing at 40-120 MPa;

[0049] (4) After the secondary nano-shearing, it enters the ultrasonic module and completes the tertiary nano-bubble generation at a frequency of 20-100 kHz;

[0050] (5) After the third-level nanobubbles are generated, they are introduced into a bubble stabilization tank for static absorption to improve bubble stability;

[0051] (6) After completion, online detection of oxygen content and bubble size;

[0052] (7) Filling and output are carried out after meeting the standards.

[0053] Example 1

[0054] The preparation of oxygen-carrying nano bubble water adopts the three-stage nano oxygen injection system of the present invention, and the specific steps are as follows:

[0055] The water source input unit provides initial pure water, which is connected to the pretreatment module to filter and dechlorinate the water and adjust the temperature to 25°C.

[0056] The Venturi oxygen injection device uses the Venturi effect to introduce high-purity oxygen into flowing water, controls the Venturi oxygen injection rate, and completes primary mixing and coarse oxygen injection.

[0057] The gas-liquid mixture enters the high-pressure homogenization module and undergoes high-pressure shearing at a pressure of 80MPa, which refines the gas-liquid mixture to the micron level, achieving secondary crushing and homogenization.

[0058] Entering the ultrasonic nano-crystallization module, three-level ultrasonic oscillation treatment is performed at a frequency of 60kHz to further nano-crystallize the bubbles.

[0059] The nano-sized bubble water is introduced into the bubble stabilization tank, and the static pressure and slow flow principles are used to maintain the suspension and uniform distribution of bubbles. It is then left to absorb for 30 minutes.

[0060] The quality detection module is equipped with a dissolved oxygen concentration analyzer, a particle size detector and other equipment to achieve online quality monitoring. The dissolved oxygen content is detected to be 45 mg / L and the bubble particle size is within the range of 10 to 100 nm.

[0061] After meeting the standards, the qualified sparkling water is quantitatively packaged into finished product containers through the filling output module.

[0062] Example 2

[0063] The preparation of oxygen-carrying nano bubble water adopts the three-stage nano oxygen injection system of the present invention, and the specific steps are as follows:

[0064] The water source input unit provides initial pure water, which is connected to the pretreatment module to filter and dechlorinate the water and adjust the temperature to 20°C.

[0065] The Venturi oxygen injection device uses the Venturi effect to introduce high-purity oxygen into flowing water, controls the Venturi oxygen injection rate, and completes primary mixing and coarse oxygen injection.

[0066] The gas-liquid mixture enters the high-pressure homogenization module and undergoes high-pressure shearing at a pressure of 100 MPa, which refines the gas-liquid mixture to the micron level, achieving secondary crushing and homogenization.

[0067] Entering the ultrasonic nano-crystallization module, three-level ultrasonic oscillation treatment is performed at a frequency of 80kHz to further nano-crystallize the bubbles.

[0068] The nano-sized bubble water is introduced into the bubble stabilization tank, and the static pressure and slow flow principles are used to maintain the suspension and uniform distribution of bubbles. It is then left to absorb for 25 minutes.

[0069] The quality detection module is equipped with a dissolved oxygen concentration analyzer, a particle size detector and other equipment to achieve online quality monitoring. The dissolved oxygen content is detected to be 55 mg / L and the bubble particle size is within the range of 10 to 100 nm.

[0070] After meeting the standards, the qualified sparkling water is quantitatively packaged into finished product containers through the filling output module.

[0071] This invention aims to produce oxygen-carrying nanobubble water with high stability, high oxygen content, and controllable particle size. The currently proposed "three-stage nano-oxygen injection system" solution is the optimal integrated approach. However, in theory, there are several alternative technical solutions, which differ from the present invention in terms of effectiveness, stability, and cost controllability:

[0072] Two-stage oxygen injection system (excluding ultrasonic module): This system uses only two-stage oxygen injection technology (Venturi + high-pressure homogenization), which can improve bubble refinement to a certain extent. However, due to the lack of the third stage of particle size reduction (ultrasonic shearing), the particle size distribution is unstable and difficult to effectively control at the nanometer level. This makes bubble agglomeration and oxygen escape more likely. While the equipment is relatively low in cost, the bubble size is mostly 0.3 to 5 microns, and the upper limit of oxygen solubility is limited (approximately 10 to 15 mg / L), making it unsuitable for high-end product scenarios.

[0073] Plasma bubble activation: Low-temperature plasma is used to activate oxygen and water, forming microbubble clusters and promoting the formation of free radical structures. This method theoretically improves solubility and bubble encapsulation. However, due to potential free radical side reactions, high safety control costs, and complex electric field structures, it has only been explored in small quantities in laboratories or medical applications. High costs, complex equipment, and difficult process control make it difficult to achieve stable, large-scale continuous production, posing food contact safety risks.

[0074] Chemical oxygen carrier solution method (such as hydrogen peroxide additives): This method increases oxygen levels by adding a small amount of chemical oxygen carriers, such as diluted H2O2 or magnesium oxide, to drinking water. While this method is effective in increasing oxygen concentration quickly, it does not conform to the concept of "purely physical preparation" for healthy drinking water and may not be approved for food-grade drinking or for the consumer market due to chemical residue issues. High oxygen concentrations and the risk of additive residues make it unsuitable for long-term drinking or the high-end drinking water market.

[0075] Mechanical gas-liquid agitation or cyclone mixing: Oxygen is introduced into the water through strong agitation or a cyclone injector. This method has a simple structure and is suitable for industrial cooling water and fishery oxygenation. However, it cannot effectively refine bubbles to the nanometer level and has low oxygen utilization efficiency, making it unsuitable for producing food-grade sparkling water. Low cost, large particle size, and low oxygen retention rate result in failure to meet industry standards for oxygen-carrying water.

[0076] While several alternative solutions exist, none can match the "three-stage nano-oxygen injection system" proposed in this invention in achieving nanoparticle size control, high dissolved oxygen concentration, food-grade safety, and continuous production capabilities. Therefore, the technical solution of this invention possesses innovative advantages and represents the most optimized integrated solution available.

[0077] This invention improves oxygen solubility and dissolution efficiency. Existing oxygen water technologies often use high-pressure or bubble injection, but these methods have limited efficiency and stability in dissolving oxygen. This invention utilizes a three-stage nano-oxygen injection system and a step-by-step dissolution technique. Each stage of the equipment refines the bubbles in a different way, maximizing oxygen solubility. This three-stage dissolution process significantly increases the oxygen dissolution efficiency of the product compared to traditional methods, ensuring that oxygen is fully dissolved in the water.

[0078] The present invention ensures stable oxygen dissolution and sustained release. Traditional oxygen dissolution in water is often affected by the size and stability of bubbles, resulting in a short period of stability in water. The present invention's three-stage nano-oxygen injection system precisely controls the size and distribution of bubbles, ensuring a long-term, stable oxygen presence in water. Nanobubble technology improves bubble stability and ensures sustained oxygen release in water, ensuring a continuous oxygen supply after consumption and preventing oxygen escape.

[0079] This invention simplifies the production process and reduces production costs. Traditional oxygen water production typically requires complex, high-pressure equipment, which is costly and unsuitable for large-scale production. The three-stage nano-oxygen injection system of this invention optimizes bubble generation technology and employs a multi-stage dissolution process, eliminating the need for high-pressure equipment and simplifying the production process. This system not only significantly reduces production costs but also improves production efficiency, making it suitable for large-scale industrial production.

[0080] This invention enhances the product's health benefits and market competitiveness. The oxygen-carrying nanobubble water not only provides efficient oxygen dissolution but also helps promote exercise recovery, boost immunity, and enhance antioxidant function. Through its three-stage nano-oxygen injection system, the product provides consumers with more efficient oxygen supplementation and possesses significant health benefits, meeting the needs of athletes, fitness enthusiasts, the elderly, and others for healthy drinks. This will enhance the product's market competitiveness and enable it to gain a foothold in the functional beverage market.

[0081] The present invention offers the flexibility to adapt to diverse application scenarios. The three-stage nano-oxygen injection system is highly adaptable and flexible, enabling customized production based on diverse needs. In diverse application scenarios (such as sports recovery, anti-aging, and daily health management), the system can be adjusted based on bubble dissolution requirements, ensuring optimal results for each application scenario.

[0082] This invention promotes environmental protection and sustainable development. The production process does not rely on complex chemical additives or high-pressure equipment, reducing energy consumption and equipment investment. By optimizing the bubble generation and dissolution processes, the system is more environmentally friendly and meets modern society's requirements for green environmental protection and sustainable development.

[0083] In summary, the three-stage nano-oxygen injection system and its preparation method utilize innovative multi-stage bubble dissolution technology to significantly improve the solubility and stability of oxygen in water, resolving issues such as low dissolution efficiency and unstable bubbles in traditional oxygen water technologies. By simplifying the production process and reducing production costs, this invention can be widely applied in the production of healthy beverages, meeting consumer demand for efficient oxygen supplementation and health benefits, and possesses broad market prospects and excellent commercial value.

[0084] Note that the above are only preferred embodiments of the present invention and the technical principles used. Those skilled in the art will understand that the present invention is not limited to the specific embodiments described herein, and that various obvious changes, readjustments, and substitutions can be made by those skilled in the art without departing from the scope of protection of the present invention. Therefore, although the present invention has been described in more detail through the above embodiments, the present invention is not limited to the above embodiments, and may include more other equivalent embodiments without departing from the concept of the present invention, and the scope of the present invention is determined by the scope of the appended claims.

Claims

1. A three-stage nano-oxygen injection system for oxygen-carrying nano-bubble water, characterized in that: include: Water source input unit, providing initial pure water and connecting to the pretreatment system; The pretreatment module filters, dechlorinates, and adjusts the temperature of the water to ensure that the water entering the system meets the quality standards; The Venturi oxygen injection device uses the Venturi effect to introduce high-purity oxygen into the flowing water, completing the first-stage mixing and coarse oxygen injection; The high-pressure homogenization module refines the gas-liquid mixture to micron level through high-pressure shearing, achieving secondary crushing and homogenization; The ultrasonic nano-crystallization module performs three-level ultrasonic oscillation treatment in the frequency range of 20 to 100 kHz to further nano-crystallize the bubbles; The bubble stabilization tank uses the principles of static pressure and slow flow to maintain bubble suspension and uniform distribution; The quality detection module is equipped with dissolved oxygen concentration analyzer, particle size detector and other equipment to achieve online quality monitoring; The filling output module packages the qualified sparkling water into finished product containers in a quantitative manner.

2. The three-stage nano-oxygen injection system for oxygen-carrying nano bubble water according to claim 1, characterized in that: The system also has an integrated intelligent control center that connects multiple sets of sensors and uses automatic feedback adjustment algorithms to perform closed-loop adjustment on core parameters such as Venturi oxygen injection rate, homogenization pressure, and ultrasonic frequency, thereby achieving precise control and stable operation of the entire process.

3. The three-stage nano-oxygen injection system for oxygen-carrying nano-bubble water according to claim 2, characterized in that: The sensors include a temperature sensor, a pressure sensor, an oxygen content sensor, and a gas-liquid ratio sensor.

4. The method for preparing the three-stage nano-oxygen injection system for oxygen-carrying nano bubble water according to claim 1, characterized in that: The following steps are involved: (1) Purify the water source and adjust the temperature to the set range; (2) The water source introduces pure oxygen into the Venturi device to achieve first-level oxygen injection and mixing; (3) After the first stage of oxygen injection and mixing, it enters the high-pressure homogenizer and undergoes secondary nano-shearing at 40-120 MPa; (4) After the secondary nano-shearing, it enters the ultrasonic module and completes the tertiary nano-bubble generation at a frequency of 20-100 kHz; (5) After the third-level nanobubbles are generated, they are introduced into a bubble stabilization tank for static absorption to improve bubble stability; (6) After completion, online detection of oxygen content and bubble size; (7) Filling and output are carried out after meeting the standards.

Images