A method for the preparation of anti-caking 2-aminoethanol bisulfite prisms

By optimizing the preparation process of 2-aminoethanol hydrogen sulfate, adding spherical additives and anti-caking agents, and controlling the crystallization process, the problems of easy agglomeration and high energy consumption in the existing technology were solved, and the preparation of 2-aminoethanol hydrogen sulfate with large particle size, high sphericity and excellent anti-caking performance was achieved.

CN122145350APending Publication Date: 2026-06-05ZHEJIANG JINKE CHEM

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
ZHEJIANG JINKE CHEM
Filing Date
2026-01-30
Publication Date
2026-06-05

AI Technical Summary

Technical Problem

Existing 2-aminoethanol hydrogen sulfate products have small particle size and are prone to agglomeration. They are also prone to moisture absorption during storage and transportation, resulting in poor flowability, which affects the filtration and separation process. Furthermore, the preparation process poses safety risks and high energy consumption.

Method used

By preparing seed slurry, dehydrating and esterifying, and crystallizing and growing crystals, adding spherical additives and anti-caking agents, controlling the crystallization process, and optimizing temperature and stirring rate, 2-aminoethanol hydrogen sulfate crystals with large particle size and high sphericity are prepared.

Benefits of technology

2-Aminoethanol hydrogen sulfate with large and uniform particle size, high sphericity, and excellent anti-caking properties was obtained, which improved crystallization efficiency, reduced production energy consumption, and avoided product agglomeration and bridging.

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Abstract

The application provides a preparation method of anti-caking 2-aminoethanol hydrogen sulfate spherulites. By optimizing the preparation of a seed slurry, a dehydration rate, a reaction endpoint temperature, and the subsequent cooling process, the crystallization growth process of 2-aminoethanol hydrogen sulfate is controlled, and the 2-aminoethanol hydrogen sulfate with an average particle size greater than 600 mu m is prepared through drying, so that the product has high yield and high purity.
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