Intermittent rectification reaction device

Abstract

The utility model discloses an intermittent rectification reaction device and relates to the technical field of rectification reaction. The device comprises a spacing mechanism and a feeding pipe, a cleaning mechanism is arranged at the bottom of the spacing mechanism, a rotating shaft is rotationally connected to the interior of the feeding pipe, a rotating drum is fixedly connected to the outer surface of the rotating shaft, and a storage hole is formed in the rotating drum. By arranging the spacing disc, the motor is started to drive the rotary disc to rotate, the rotary disc rotates to drive the push rod to rotate, when the push rod rotates to the spacing disc, the rotary disc rotates to enable the push rod to enter the sliding groove of the spacing disc, then the push rod rotates to drive the spacing disc to rotate, and the spacing disc rotates to drive the rotary drum to rotate. When the rotary drum rotates, redundant materials are scraped off through the scraping plate, only the materials in the material storage holes are reserved, and after the material storage holes with the materials rotate to the bottom, the materials fall into the semicircular disc through gravity to be discharged, quantitative feeding of the reaction raw materials is ensured, and then the purpose of intermittent quantitative discharging is achieved.

Description

Technical Field

[0001] The utility model belongs to the technical field of distillation reaction, in particular to an intermittent distillation reaction device. Background Art

[0002] Distillation reaction is a separation and purification method commonly used in chemical engineering, which combines chemical reaction and distillation process. The main purpose of this process is to separate the components in the mixture by distillation and produce new compounds in the reaction;

[0003] In the process of feeding, the existing distillation reaction device feeds the next material after the internal raw materials have reacted. Problems arising in the reaction process are uncontrollable, and the amount of material fed cannot be accurately controlled. The device sets a spacer plate, and when the spacer plate rotates, it drives the drum to rotate, and then feeds through the storage hole opened inside the drum to ensure the quantitative feeding and accuracy of the reaction raw materials. For this purpose, we provide an intermittent distillation reaction device. Utility Model Content

[0004] The utility model aims to provide an intermittent distillation reaction device, which feeds materials through a storage hole opened inside a rotating drum to ensure the quantitative feeding and accuracy of the reaction raw materials, and solves the problem that the next feeding is carried out after the internal raw materials have reacted, the problems arising in the reaction process cannot be controlled, and the amount of feeding cannot be accurately controlled.

[0005] In order to solve the above technical problems, the utility model is realized by the following technical solutions:

[0006] The utility model discloses an intermittent distillation reaction device, comprising a spacer mechanism and a feed pipe, wherein a cleaning mechanism is arranged at the bottom of the spacer mechanism, a rotating shaft is rotatably connected inside the feed pipe, a rotating drum is fixedly connected to the outer surface of the rotating shaft, a material storage hole is opened inside the rotating drum, the right side of the rotating shaft penetrates the feed pipe and extends to the outside, a spacer disk is fixedly connected to the right side of the rotating shaft, the back side of the spacer disk contacts the rotating disk, and a push rod is fixedly connected to the back side of the rotating disk;

[0007] A motor is fixedly connected to the right side of the turntable, and the right side of the turntable is fixedly connected to the output end of the motor. A base is fixedly connected to the bottom of the motor. A scraper is fixedly connected to the inside of the feed pipe. The inner side of the scraper contacts the outer surface of the drum. The storage hole is rotated to the bottom by the rotation of the drum and then falls into the semi-circular disk by gravity for discharge, thereby ensuring the quantitative delivery of the reaction raw materials.

[0008] Furthermore, a rotating shaft is rotatably connected inside the feed pipe, the left side of the rotating shaft passes through the feed pipe and extends to the outside, and a knob is fixedly connected to the left outer surface of the rotating shaft. The baffle is opened by turning the knob so that the material on the top of the baffle can enter the storage hole.

[0009] Furthermore, a gear 1 is fixedly connected to the outer surface of the rotating shaft, a rack is meshedly connected to the top and bottom of the gear 1, a gear 2 is meshedly connected to the inner side of the rack, a center rod is fixedly connected to the inside of the gear 2, the right side of the center rod passes through the feed pipe and extends to the inside, a baffle is fixedly connected to the outer surface of the center rod, the outer surface of the baffle is matched with the inner wall of the feed pipe, and the amount of feed is controlled by the baffle to prevent blockage.

[0010] Furthermore, the cleaning mechanism includes a main body fixedly connected to the bottom of the feed pipe, the top of the main body is fixedly connected to the bottom of the base, a motor is fixedly connected to the center of the bottom of the main body, a rotating shaft is fixedly connected to the output end of the motor, a semi-circular disk is fixedly connected to the bottom of the main body, a diverter table is fixedly connected to the center of the inner part of the semi-circular disk, and a discharge buckle is provided at the bottom of the semi-circular disk, so that materials are dispersed and put into the diverter table to prevent them from being put into one place, causing the bottom material to be incompletely reacted.

[0011] Furthermore, a connector is fixedly connected to an outer surface of the rotating shaft, a connecting rod is fixedly connected to an outer surface of the connector, two connecting rods are provided, and a cleaning plate is fixedly connected to the other end of the connecting rod on the left side, and the inside of the main body is cleaned by the cleaning plate.

[0012] Furthermore, the left side of the cleaning plate is in contact with the interior of the main body, the other end of the connecting rod on the right side is fixedly connected to the vertical plate, the interior of the vertical plate is fixedly connected to a fixing rod, the outer surface of the fixing rod is rotatably connected to a cleaning sponge, the front and back sides of the cleaning sponge are in contact with squeezing rods, and the dirty water inside the cleaning sponge is cleaned by the squeezing rods.

[0013] Furthermore, the top and bottom of the extrusion rod are fixedly connected to the top and bottom of the inner wall of the vertical plate respectively, a discharge pipe is fixedly connected to the right side of the main body, a handle is rotatably connected inside the discharge pipe, a baffle plate 1 is fixedly connected inside the discharge pipe, a rotating plate is in contact with the left side of the baffle plate 1, and the left side of the rotating plate is fixedly connected to the right side of the handle, and the discharge pipe is opened by rotating the rotating plate to discharge the material.

[0014] The utility model has the following beneficial effects:

[0015] 1. The utility model sets a spacing disk, and the motor starts to drive the turntable to rotate, and the rotation of the turntable drives the push rod to rotate. When the push rod rotates to the spacing disk, the turntable rotates to make the push rod enter the slide groove of the spacing disk, and then the push rod rotates to drive the spacing disk to rotate, and the rotation of the spacing disk drives the rotating drum to rotate. When the rotating drum rotates, the scraper scrapes off the excess material and only keeps the material in the storage hole. After the storage hole with material rotates to the bottom, it falls into the semicircular disk by gravity for unloading, ensuring the quantitative delivery of the reaction raw materials, thereby achieving the purpose of intermittent quantitative unloading.

[0016] 2. The utility model arranges a cleaning sponge. When the motor is started, the rotating shaft is driven to rotate, and then the connector is driven to rotate through the rotating shaft, and the connecting rod is driven to rotate through the connector. Then, the cleaning plate and the cleaning sponge are driven by the connecting rod to clean the inside of the main body. The inner wall is first scraped by the cleaning plate, and when the cleaning sponge is cleaned, the cleaning sponge is squeezed by the squeezing rod to squeeze out the dirty water inside, thereby ensuring the cleanliness of the inner wall of the main body and preventing the crystals produced by the reaction from interfering with the reaction process.

[0017] Of course, any product implementing the present invention does not necessarily need to achieve all of the advantages described above at the same time. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] In order to more clearly illustrate the technical solutions of the embodiments of the utility model, the drawings required for describing the embodiments are briefly introduced below. Obviously, the drawings described below are only some embodiments of the utility model. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work.

[0019] Figure 1 It is a schematic diagram of the overall structure of the utility model;

[0020] Figure 2 This is a schematic diagram of the structure of the right side of the feed pipe of the utility model;

[0021] Figure 3 This is a schematic diagram of the front cross-sectional structure of the main body of the utility model;

[0022] Figure 4 This is a front cross-sectional structural diagram of the feed pipe of the utility model;

[0023] Figure 5 For this utility model Figure 4 A is a schematic diagram of the enlarged structure of the middle part;

[0024] Figure 6 This is a schematic diagram of the internal cross-sectional structure of the discharge pipe of the utility model;

[0025] Figure 7The utility model is a schematic diagram of the internal cross-sectional structure of the cleaning sponge.

[0026] In the accompanying drawings, the components represented by the reference numerals are listed as follows:

[0027] 1. Spacing mechanism; 101. Feeding pipe; 102. Spacing plate; 103. Rotating plate; 104. Push rod; 105. Base; 106. Motor; 107. Knob; 108. Rotating shaft; 109. Storage hole; 110. Rotating shaft; 111. Semicircular plate; 112. Diverter; 113. Discharging buckle; 114. Baffle; 115. Rotating drum; 116. Scraper; 117. Gear 1; 11 8. Rack; 119. Center rod; 120. Gear 2; 2. Cleaning mechanism; 201. Main body; 202. Motor 1; 203. Connector; 204. Rotating shaft 1; 205. Connecting rod; 206. Cleaning plate; 207. Vertical plate; 208. Cleaning sponge; 209. Fixed rod; 210. Extrusion rod; 211. Discharge pipe; 212. Handle; 213. Baffle 1; 214. Rotating plate. DETAILED DESCRIPTION

[0028] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments of the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0029] See also Figure 1-7 As shown, the utility model is an intermittent distillation reaction device, comprising a spacing mechanism 1 and a feed pipe 101, a cleaning mechanism 2 is arranged at the bottom of the spacing mechanism 1, a rotating shaft 110 is rotatably connected inside the feed pipe 101, a rotating drum 115 is fixedly connected to the outer surface of the rotating shaft 110, a material storage hole 109 is opened inside the rotating drum 115, the right side of the rotating shaft 110 penetrates the feed pipe 101 and extends to the outside, a spacing disk 102 is fixedly connected to the right side of the rotating shaft 110, the back side of the spacing disk 102 contacts the rotating disk 103, and the back side of the rotating disk 103 is fixedly connected to a push rod 104;

[0030] The right side of the turntable 103 is fixedly connected to a motor 106, the right side of the turntable 103 is fixedly connected to the output end of the motor 106, the bottom of the motor 106 is fixedly connected to a base 105, the inside of the feed pipe 101 is fixedly connected to a scraper 116, the inner side of the scraper 116 is in contact with the outer surface of the drum 115, the motor 106 is started to drive the turntable 103 to rotate, and the push rod 104 is driven to rotate by the rotation of the turntable 103. When the push rod 104 rotates to the spacer disc 102, the turntable 103 rotates to drive the push rod 104 enters into the slide groove of the spacing disk 102, and then the push rod 104 rotates to drive the spacing disk 102 to rotate, and the spacing disk 102 rotates to drive the rotating drum 115 to rotate. When the rotating drum 115 rotates, the scraper 116 is used to scrape off the excess material to retain the storage hole 109. After the storage hole 109 with material rotates to the bottom, it falls into the semi-circular disk 111 by gravity for unloading, ensuring the quantitative delivery of the reaction raw materials, thereby achieving the purpose of intermittent quantitative unloading.

[0031] A rotating shaft 108 is rotatably connected inside the feed pipe 101 . The left side of the rotating shaft 108 penetrates the feed pipe 101 and extends to the outside. A knob 107 is fixedly connected to the outer surface of the left side of the rotating shaft 108 .

[0032] A gear 117 is fixedly connected to the outer surface of the rotating shaft 108, and a rack 118 is respectively meshed with the top and bottom of the gear 117, and a gear 2 120 is meshed with the inner side of the rack 118. A center rod 119 is fixedly connected to the inside of the gear 2 120, and the right side of the center rod 119 passes through the feed pipe 101 and extends to the inside, and a baffle 114 is fixedly connected to the outer surface of the center rod 119, and the outer surface of the baffle 114 is adapted to the inner wall of the feed pipe 101.

[0033] The cleaning mechanism 2 includes a main body 201 fixedly connected to the bottom of the feed pipe 101, the top of the main body 201 is fixedly connected to the bottom of the base 105, a motor 202 is fixedly connected at the center of the bottom of the main body 201, a rotating shaft 204 is fixedly connected to the output end of the motor 202, a semi-circular disk 111 is fixedly connected to the bottom of the main body 201, a diverter table 112 is fixedly connected at the center of the inner part of the semi-circular disk 111, and a discharge buckle 113 is provided at the bottom of the semi-circular disk 111.

[0034] A connector 203 is fixedly connected to the outer surface of the rotating shaft 1 204 , and a connecting rod 205 is fixedly connected to the outer surface of the connector 203 . There are two connecting rods 205 in total, and a cleaning plate 206 is fixedly connected to the other end of the connecting rod 205 on the left side.

[0035] The left side of the cleaning plate 206 contacts with the inside of the main body 201, and the other end of the connecting rod 205 on the right is fixedly connected to a vertical plate 207, and a fixing rod 209 is fixedly connected to the inside of the vertical plate 207. The outer surface of the fixing rod 209 is rotatably connected to a cleaning sponge 208, and the front and back sides of the cleaning sponge 208 are in contact with an extrusion rod 210. The motor 1 202 is started to drive the rotating shaft 1 204 to rotate, and then the connector 203 is driven to rotate through the rotating shaft 1 204, and the connecting rod 205 is driven to rotate through the connector 203, and then the cleaning plate 206 and the cleaning sponge 208 are driven by the connecting rod 205 to clean the inside of the main body 201. The inner wall is first scraped off by the cleaning plate 206, and when the cleaning sponge 208 is cleaned, the cleaning sponge 208 is squeezed by the extrusion rod 210 to squeeze out the dirty water inside, thereby ensuring the cleanliness of the inner wall of the main body 201 and preventing the crystals produced by the reaction from interfering with the reaction process.

[0036] The top and bottom of the extrusion rod 210 are fixedly connected to the top and bottom of the inner wall of the vertical plate 207 respectively, and a discharge pipe 211 is fixedly connected to the right side of the main body 201, and a handle 212 is rotatably connected inside the discharge pipe 211. A baffle 213 is fixedly connected inside the discharge pipe 211, and the left side of the baffle 213 contacts a rotating plate 214, and the left side of the rotating plate 214 is fixedly connected to the right side of the handle 212.

[0037] A specific application of this embodiment is that the staff pours the reaction material into the feed pipe 101, and then rotates the rotating shaft 108, the rotating shaft 108 drives the gear 1 117 to rotate, and then the rotating shaft 108 is driven to move inward by the rotation of the gear 1 117, and then the rotating shaft 108 drives another gear 2 120 to rotate, and the gear 2 120 rotates to drive the center rod 119 to rotate, and the center rod 119 rotates to drive the baffle 114 to move inward to open the feed pipe 101. The material is opened, and then the material falls onto the rotating drum 115, and a part of it enters the storage hole 109, and the motor 106 is started. The motor 106 starts to drive the rotating disk 103 to rotate, and the rotation of the rotating disk 103 drives the push rod 104 to rotate. When the push rod 104 rotates to the spacing disk 102, the rotation of the rotating disk 103 causes the push rod 104 to enter the chute of the spacing disk 102, and then the push rod 104 rotates to drive the spacing disk 102 to rotate, and the rotation of the spacing disk 102 drives the rotating drum 115 to rotate. The drum 115 rotates to scrape off the excess material through the scraper 116, leaving only the material in the storage hole 109. After the storage hole 109 with material rotates to the bottom, it falls into the semi-circular disk 111 by gravity, and then slides to the bottom through the semi-circular disk 111, and is dispersed through the diverter 112 to prevent the material from falling into the main body 201 and accumulating, causing incomplete reaction. When cleaning is needed, the motor 202 is started, and the motor 202 starts to drive the rotating shaft 204 to rotate. , and then the connector 203 is driven to rotate through the rotating shaft 204, and the connecting rod 205 is driven to rotate through the connector 203, and then the cleaning plate 206 and the cleaning sponge 208 are driven by the connecting rod 205 to clean the inside of the main body 201. The inner wall is first scraped by the cleaning plate 206, and then when the cleaning sponge 208 is cleaned, the cleaning sponge 208 will be squeezed by the squeezing rod 210 to squeeze out the dirty water inside, thereby ensuring the cleanliness of the inner wall of the main body 201.

[0038] In the description of this specification, the description with reference to the terms "one embodiment", "example", "specific example", etc. means that the specific features, structures, materials or characteristics described in conjunction with the embodiment or example are included in at least one embodiment or example of the utility model. In this specification, the schematic representation of the above terms does not necessarily refer to the same embodiment or example. Moreover, the specific features, structures, materials or characteristics described can be combined in any one or more embodiments or examples in a suitable manner.

[0039] The preferred embodiments of the utility model disclosed above are only used to help explain the utility model. The preferred embodiments do not describe all the details in detail, nor do they limit the utility model to the specific implementation methods described. Obviously, many modifications and changes can be made according to the content of this specification. This specification selects and specifically describes these embodiments in order to better explain the principles and practical applications of the utility model, so that technicians in the relevant technical field can well understand and use the utility model. The utility model is limited only by the claims and their full scope and equivalents.

Claims

1. A batch distillation reaction device, comprising a partition mechanism (1) and a feed pipe (101), wherein a cleaning mechanism (2) is arranged at the bottom of the partition mechanism (1), and a rotating shaft (110) is rotatably connected inside the feed pipe (101). Features: The outer surface of the rotating shaft (110) is fixedly connected to a rotating drum (115), a material storage hole (109) is provided inside the rotating drum (115), the right side of the rotating shaft (110) passes through the feeding pipe (101) and extends to the outside, the right side of the rotating shaft (110) is fixedly connected to a spacer disk (102), the back side of the spacer disk (102) contacts a rotating disk (103), and the back side of the rotating disk (103) is fixedly connected to a push rod (104); The right side of the rotating disk (103) is fixedly connected to a motor (106), the right side of the rotating disk (103) is fixedly connected to the output end of the motor (106), the bottom of the motor (106) is fixedly connected to a base (105), the inside of the feeding pipe (101) is fixedly connected to a scraper (116), and the inner side of the scraper (116) is in contact with the outer surface of the rotating drum (115).

2. A batch distillation reaction device according to claim 1, It is characterized in that A rotating shaft (108) is rotatably connected inside the feed pipe (101), the left side of the rotating shaft (108) passes through the feed pipe (101) and extends to the outside, and a knob (107) is fixedly connected to the left outer surface of the rotating shaft (108).

3. A batch distillation reaction device according to claim 2, It is characterized in that The outer surface of the rotating shaft (108) is fixedly connected to a gear 1 (117), the top and bottom of the gear 1 (117) are respectively meshed with racks (118), the inner side of the rack (118) is meshed with a gear 2 (120), the inner side of the gear 2 (120) is fixedly connected to a center rod (119), the right side of the center rod (119) passes through the feed pipe (101) and extends to the inside, the outer surface of the center rod (119) is fixedly connected to a baffle (114), and the outer surface of the baffle (114) is adapted to the inner wall of the feed pipe (101).

4. A batch distillation reaction device according to claim 1, It is characterized in that The cleaning mechanism (2) comprises a main body (201) fixedly connected to the bottom of the feed pipe (101), the top of the main body (201) is fixedly connected to the bottom of the base (105), a motor 1 (202) is fixedly connected at the center of the bottom of the main body (201), a rotating shaft 1 (204) is fixedly connected to the output end of the motor 1 (202), a semicircular disk (111) is fixedly connected to the bottom of the main body (201), a diverter table (112) is fixedly connected at the center of the interior of the semicircular disk (111), and a discharge buckle (113) is provided at the bottom of the semicircular disk (111).

5. A batch distillation reaction device according to claim 4, It is characterized in that The outer surface of the rotating shaft 1 (204) is fixedly connected to a connector (203), and the outer surface of the connector (203) is fixedly connected to a connecting rod (205). There are two connecting rods (205) in total, and the other end of the connecting rod (205) on the left is fixedly connected to a cleaning plate (206).

6. A batch distillation reaction device according to claim 5, It is characterized in that The left side of the cleaning plate (206) is in contact with the inside of the main body (201); the other end of the connecting rod (205) on the right side is fixedly connected to a vertical plate (207); a fixing rod (209) is fixedly connected to the inside of the vertical plate (207); a cleaning sponge (208) is rotatably connected to the outer surface of the fixing rod (209); and the front and back sides of the cleaning sponge (208) are in contact with squeezing rods (210).

7. A batch distillation reaction device according to claim 6, It is characterized in that The top and bottom of the extrusion rod (210) are respectively fixedly connected to the top and bottom of the inner wall of the vertical plate (207); a discharge pipe (211) is fixedly connected to the right side of the main body (201); a handle (212) is rotatably connected inside the discharge pipe (211); a baffle plate 1 (213) is fixedly connected inside the discharge pipe (211); a rotating plate (214) is in contact with the left side of the baffle plate 1 (213); and the left side of the rotating plate (214) is fixedly connected to the right side of the handle (212).

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